WEEKS
1 st
,
Sept.
07-13.
2 nd
,
Sept.
14-20.
GROUPS
1, 3, 4, 5, 7,
10, 12
2, 6, 8, 9, 11,
13-16, 17-20,
21-23, 24-27
1, 3, 4, 5, 7,
10, 12
MEDICAL CHEMISTRY PRACTICUM
1st YEAR OF GENERAL MEDICINE AND DENTISTRY, 2015-2016
“A” PRACTICAL ROOM
Laboratory safety instructions. Fire-regulations.
(Lab. Pract. pp. 4-5.)
Chemical calculations. Concentration of solutions. (Lab. Pract. pp. 10-13.)
Laboratory techniques: laboratory equipments, volumetric apparatus. Filtration. Preparations of solutions. (Lab. Pract. pp. 6-14.)
Chemical analysis of drinking-water.
(Lab. Pract. pp. 15-20.)
Quantitative analysis. Acid-base titrations: strong acid-strong base, weak acid-strong base titrations. (Lab. Pract. pp. 30-45.)
GROUPS
2, 6, 8, 9, 11,
13-16, 17-20,
21-23, 24-27
1, 3, 4, 5, 7,
10, 12
2, 6, 8, 9, 11,
13-16, 17-20,
21-23, 24-27
“B” PRACTICAL ROOM
Laboratory safety instructions. Fire-regulations.
(Lab. Pract. pp. 4-5.)
Chemical calculations. Concentration of solutions. (Lab. Pract. pp. 10-13.)
Laboratory techniques: laboratory equipments, volumetric apparatus. Filtration. Preparations of solutions. (Lab. Pract. pp. 6-14.)
Chemical analysis of drinking-water.
(Lab. Pract. pp. 15-20.)
Chromatography I. Paper chromatography: separation of food dyes and separation of metal ions. (Lab. Pract. pp. 106-113.)
3 rd
,
Sept.
21-27.
4 th
,
Sept. 28-
Oct.
04.
5 th
,
Oct.
05-11.
6 th
,
Oct.
12-18.
7 th
,
Oct.
19-25.
2, 6, 8, 9, 11,
13-16, 17-20,
21-23, 24-27
Quantitative analysis. Acid-base titrations: strong acid-strong base, weak acid-strong base titrations. (Lab. Pract. pp. 30-45.)
1, 3, 4, 5, 7,
10, 12
2, 6, 8, 9, 11,
13-16, 17-20,
21-23, 24-27
Chromatography II. Ion exchange chromatography. (Lab. Pract. pp. 114-120.) Gel filtration. Desalting of egg-white solution. (Lab.
Pract. pp 121-123.)
Chromatography II. Ion exchange chromatography. (Lab. Pract. pp. 114-120.) Gel filtration. Desalting of egg-white solution. (Lab.
Pract. pp 121-123.)
1, 3, 4, 5, 7,
10, 12
Elektrometry. Electrometric pH measurement.
Potentiometric titrations. Determination of buffering capacity. (Lab. Pract. pp. 97-105.)
1, 3, 4, 5, 7,
10, 12
Chromatography I. Paper chromatography: separation of food dyes and separation of metal ions. (Lab. Pract. pp. 106-113.)
2, 6, 8, 9, 11,
13-16, 17-20,
21-23, 24-27
1, 3, 4, 5, 7,
10, 12
2, 6, 8, 9, 11,
13-16, 17-20,
21-23, 24-27
Reactions kinetics. Kinetic study of the saponification reaction of ethylacetate. Kinetic analysis of the oxidation of iodide ion using the
Landolt-method. (Lab. Pract. pp. 124-131.)
Reactions kinetics. Kinetic study of the saponification reaction of ethylacetate. Kinetic analysis of the oxidation of iodide ion using the
Landolt-method. (Lab. Pract. pp. 124-131.)
Spectrophotometry. Photometric determination of inorganic phosphate. Determination of acid labile phosphate in organic compounds. (Lab.
Pract. pp. 67-77.)

12 th
,
Nov.
23-29.
13 th
,
Nov. 30-
Dec.
06.
14 th
,
Dec.
07-13.
8 th
,
Oct. 26–
Nov. 01.
9 th
,
Nov.
02-08.
10 th
,
Nov.
09-15.
11 th
,
Nov.
16-22.
2, 6, 8, 9, 11,
13-16, 17-20,
21-23, 24-27
1, 3, 4, 5, 7,
10, 12
Elektrometry. Electrometric pH measurement.
Potentiometric titrations. Determination of buffering capacity. (Lab. Pract. pp. 97-105.)
Redox titrations. Iodometric titrations.
Titrations with potassium bromate.
(Lab. Pract. pp. 46-57.)
2, 6, 8, 9, 11,
13-16, 17-20,
21-23, 24-27
Redox titrations. Iodometric titrations.
Titrations with potassium bromate.
(Lab. Pract. pp. 46-57.)
1, 3, 4, 5, 7,
10, 12
2, 6, 8, 9, 11,
13-16, 17-20,
21-23, 24-27
1, 3, 4, 5, 7,
10, 12
2, 6, 8, 9, 11
Qualitative analysis of mono- and disaccharides.
(Lab. Pract. pp. 24-29.) Polarimetry.
Polarimetric analysis of carbohydrates. (Lab.
Pract. pp. 91-96.)
Qualitative analysis of mono- and disaccharides.
(Lab. Pract. pp. 24-29.) Polarimetry.
Polarimetric analysis of carbohydrates. (Lab.
Pract. pp. 91-96.)
Analysis of inorganic salts and complexes.
(Lab. Pract. pp. 21-23.)
Complexometric titrations.
(Lab. Pract. pp. 58-66.)
Analysis of inorganic salts and complexes.
(Lab. Pract. pp. 21-23.)
Complexometric titrations.
(Lab. Pract. pp. 58-66.)
1, 3, 4, 5, 7,
10, 12
2, 6, 8, 9, 11,
13-16, 17-20,
21-23, 24-27
Spectrophotometry. Photometric determination of inorganic phosphate. Determination of acid labile phosphate in organic compounds. (Lab.
Pract. pp. 67-77.)
Enzyme kinetics.
Assay of glycogen phosphorylase activity.
(Lab. Pract. pp. 132-140.)
1, 3, 4, 5, 7,
10, 12
2, 6, 8, 9, 11,
13-16, 17-20,
21-23, 24-27
1, 3, 4, 5, 7,
10, 12
2, 6, 8, 9, 11,
13-16, 17-20,
21-23, 24-27
Enzyme kinetics.
Assay of glycogen phosphorylase activity.
(Lab. Pract. pp. 132-140.)
Quantitative protein analysis: Biuret assay.
Bradford assay. (Lab. Pract. pp. 84-87.)
Assay of glucose. Enzymatic determination of glucose in blood serum. (Lab. Pract. pp. 88-90.)
Quantitative protein analysis: Biuret assay.
Bradford assay. (Lab. Pract. pp. 84-87.)
Assay of glucose. Enzymatic determination of glucose in blood serum. (Lab. Pract. pp. 88-90.)
Photometric determination of iron. (Lab. Pract. pp. 78-83.)
Practical exam:
GR. 13-16, 17-20, 20-23, 24-27
1, 3, 4, 5, 7,
10, 12
Photometric determination of iron.
(Lab. Pract. pp. 78-83.)
15 th ,
Dec.
14-18.
1, 3, 4, 5, 7,
10, 12
Practical exam.
2, 6, 8, 9, 11
Practical exam.