KONIK`S HPLC Applications Book

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KONIK HPLC APPLICATION BOOK
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Contents
ENVIRONMENTAL APPLICATIONS
FOOD APPLICATIONS
PHARMACEUTICAL APPLICATIONS
CHIRAL APPLICATIONS
CHIRAL APPLICATIONS
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Environmental Applications
1-Determination of multiple Additives in cosmetics
2-Determination of Aldehydes and Ketones as DNPH derivates
3-Ion pair chromatography of Alkyl Sulphates and Alkyl Sulphosuccinates
4-Anion determination according to U.S. EPA Method 300.0 / 317.0 and 326.0.
5-Determination of Anions with Ion pair chromatography and indirect UV detection
6-Determination of Carbamate Insecticides by HPLC with post-column derivatization .
7-Determination of monovalent Cations .
8-Determination of divalent Cations.
9-Separation of Explosives.
10-Biomonitoring of Hydroxypyrene .
11-Determination of Ketones as DNPH Derivates .
12-Analysis of Nitro Polycyclic Aromatic Hydrocarbons.
13-Separation of ortho-, nitro- para Nitroaniline.
14-Fast Determination of PAH .
15-Fast Separation of PAHs on a 2 mm ID column.
16-Separation of Parabens .
17-Chromatographic determination of Pesticides.
18-Determination of Phenoxy acid herbicides .
19-Determination of Priority Pollutant Phenols .
20-Determination of non-ionic Surfactants using HPLC.
21-Analysis of Surfactants in toothpastes by HPLC .
22-Determination of aromatic Hydrocarbon types in middle distillates acc. to prE
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Food Applications
1-Separation of Additives in soft drinks .
2-Determination of Aflatoxins by HPLC with post column derivatization
3-Simultaneous determination of Alcohols, Carbohydrates and Organic Acids .
4-Determination of Alcohols, Carbohydrates and Organic Acids II .
5-Separation of Amines in wine with precolumn derivatization (DANSYL) .
6-HPLC determination of Amines in wine with precolumn derivatization (OPA) .
7-Determination of Amino Acids in beer with precolumn derivatization (OPA) .
8-Inorganic and Organic Anions in beer .
9-Anthocyanins in red and rose wine .
10-Determination of Biogenic Amines in food products by HPLC in combination
with ninhydrin derivatization .
11-Separation of β-Carotene isomers .
12-Determination of Diketopiperazine in soft drinks .
13-Determination of Fatty acids .
14-Analysis of Flavonoids in fruit juice .
15-Stilbene and Flavonoids in red wine samples .
16-Analysis of Flavonoid Glycosides .
17-Separation of Methylfurfural and Hydroxyfurfural in beer .
18-Determination of Mono- and Disaccharides .
19-Determination of Deoxynivalenol (DON) .
20-Determination of Nivalenol (NIV) and Deoxynivalenol (DON) with postcolumn
derivatisation .
21-Analysis of Fusarium Mycotoxines .
22-Ion chromatography for determination of NO2- and NO3- in beverages .
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23-Determination of Organic Acids .
24-Determination of Organic Acids II .
25-Determination of Patulin in apple juice .
26-Separation of Preservatives .
27-Determination of various Sterols .
28-Separation of water soluble Vitamins .
29-Separation of Tocopherols and Vitamin D2 .
30-Separation of fat soluble Vitamins .
31-Fat soluble Vitamins by HPLC with electrochemical detection.
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Pharmaceutical Applications
1-Quality control mixture of Acetyl Cystein .
2-Separation and determination of Opium Alkaloids .
3-HPLC method for the determination of Amineptine and its main Metabolite in
human plasma .
4-Determination of Amino Acids with OPA .
5-Separation of Aniline derivatives with electrochemical detection 64
6-Separation of Anilines and Sulfonamides by HPLC with electrochemical detection .
7-Separation of Trimethoprim and Sulfamethoxazol .
8-Determination of Anticonvulsant drugs and Methyl Xanthine derivatives in serum .
9-Separation of Antiepileptics in serum .
10-Separation of Antirheumatic drugs .
11-Separation of Catecholamines .
12-Determination of Catecholamines II .
13-Clinical analysis of Chloramphenicol .
14-Determination of Citrate and Oxalate in human urine .
15-Determination of Guaifenesin, Codein and Pseudoefedrin in cough syrup .
16-Isocratic separation of the Digoxin and Digitoxin series of Glycosides 75
Separation of Narcotics .
17-Analysis of β-Lactam Antibiotic (Moxalactam) .
18-Analysis of Bisphosphonate Pamidronate Disodium by precolumn derivatization
and fluorescence detection .
19-Determination of Paracetamol and by-products .
20-Separation of Penicillin Antibiotics .
21-Separation of Peptides .
22-Fast separation of Proteins .
22-Separation of Sedative .
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23-Separation of Steroids .
24-Separation of Steroids II .
25-Separation of Sulfa drugs .
26-Separation of Sulfa drugs II .
27-Separation of Tricyclic Antidepressant drugs .
28-Separation of D,L-Tryptophan and Aromatic Acids.
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Chiral Applications
(HPLC)
1-Chiral separation of Abscisic Acid (4-Oxo-2-Cyclohexen-1-yl)-3-Methyl2,4-Pentanedienoic Acid)
2-Chiral separation of 3-Amino-2(2-Naphtyl)-1-Phenyl-Propanol .
3-Chiral separation of Atenolol (2-[4-[2-Hydroxy-3 (1-)Propoxy]Phenyl]Ethanamid).
4-Chiral separation of Atropine (rac-Hyoscyamin) .
5-Chiral separation of 1-Aza[6]Helicene .
6-Chiral separation of 1-Benzene-2-Naphthene-3-Amino Propan(1)ol .
7-Chiral separation of Benzoin (α-Hydroxy-α-Phenylacetophenon) .
8-Chiral separation of Benzyl-Mandelate (Benzyl-2-Hydroxy-3-Phenylpropionate) .
9-Chiral separation of Benzyl-Mandelate (Benzyl-2-Hydroxy-3-Phenylpropionate)
10-Chiral separation of 2,2´Bis(Diphenylphosphinoxid)3,3´Bibenzo[b]Thiophene .
11-Chiral separation of BITIANP
12- 2,2´Bis(Diphenylphosphino)3,3´Bibenzo[b]Thiophene .
13-Chiral separation of 4-Bromphenyl-Glycinamid (2-(4-Bromphenyl)-2-Amino
Acetamid) .
14-Chiral separation of Carbinoxamine (2-[(4-Chlorophenyl)-Pyridin-2-yl-Methoxy]N,N-Dimethyl-Ethanamine) .
15-Chiral separation of Citalopram (1-(3-Dimethylaminopropyl)-1-(4-Fluorphenyl)3H-2-Benzofuran-5-Carbonitrile).
16-Chiral separation of Dilactid .
17-Chiral separation of 1,2-Diphenyl-2-(Tosylamino)Ethanone .
18-Chiral separation of Ethyl-Mandelate .
19-Chiral separation of Etozolin (Ethyl(3-Methyl-4-Oxo-5-Piperidinothiazolidin91
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2-ylidene)Acetate) .
20-Chiral separation of Flavanone (2-Phenyl-1,4-Benzopyrone) .
21-Chiral separation of Hexahydro-6,6-Dimethyl-2-Tosylpyrrolo
[1,2-e]Imidazol-3-one .
22-Chiral separation of Hydroxyzine .
23-Chiral separation of Lactic Acid .
24-Chiral separation of n-Methylephedrin (2-Dimethylamino-1-Phenyl-Propanol) .
25-Chiral separation of Methyl phenyl sulfoxide .
26-Chiral separation of Methyl phenyl sulfoxide II .
27-Chiral separation of Metoprolol (1-(Isoppropylamino)-3-[4-(2Methoxyethyl)Phenoxy]Propan-2-ol) .
28-Chiral separation of 1-(Naphthalene-6-yl)Ethane-1,2-diol .
29-Chiral separation of Naproxen (6-Methoxy-α-Methyl-2-Naphthylessigsäure) .
30-Chiral separation of 1-Phenylethylenglycol (1-Phenylethane-1,2-diol) .
31-Chiral separation of 1-Phenylpropane-1,2-diol .
32-Chiral separation of Pindolol (1-(1H-Indol-4-yloxy)-Propan-2-ol) .
33-Chiral separation of Pindolol (1-(1H-Indol-4-yloxy)-3-(1- Propan-2-ol)
34-Chiral separation of Propranolol (1-Isopropylamino-3-(1-Naphthyloxy)2-Propanol) .
35-Chiral separation of Propranolol (1-Isopropylamino-3-(1-Naphthyloxy)2-Propanol) .
36-Chiral separation of Warfarin (4-Hydroxy-3-(3-Oxo-1-Phenyl-Butyl)-Cumarin) .
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Chiral Applications
(SFC)
1-Chiral separation of Benzyl-Mandelate (Benzyl-2-Hydroxy-3-Phenylpropionate)
2-Chiral separation of 1,1´-Bi-2-Naphthol (BINOL)
3-Chiral separation of Ethyl-Mandelate .
4-Chiral separation of Hydrobenzoin (1,2-Diphenylethane-1,2-diol) .
5-Chiral separation of trans Stilbene Oxide .
6-Chiral separation of Warfarin (4-Hydroxy-3-(3-Oxo-1-Phenyl-Butyl)-Cumarin) .
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