High temperature materials for reusable spacecraft characterized under extreme conditions Project Summary Ceramics and ceramic composites provide highly sought-after capabilities that have the potential to withstand extreme temperatures and heat fluxes, severe oxidation and high mechanical stresses associated with next generation re-entry environments. The complexity of these extreme operational conditions demands stringent tolerances on failure initiation and consequently an extension of the boundaries of current characterization capabilities. Proposed here is a real-time approach to elucidating the evolution of mechanical and structural properties of these materials under load at ultrahigh temperatures that will pave the way to much-needed significant advances in thermomechanical performance for reusable spacecraft. Breakthroughs achieved by the PI in the i) initiation of in situ techniques coupling thermo-mechanical testing with high resolution synchrotron x-rays as well as the ii) advent of new techniques for data capture and analysis of complex geometries, will be leveraged to determine real-time strain evolution and material degradation under extreme environments. The outcome of the novel studies will unravel fundamental mechanisms leading to failure under applied loads at high temperature through real-time experimental investigations. In particular it is expected that the proposed approach will provide high spatial resolution, real-time strain for the design of advanced materials with superior performance in extreme environments.