GENERAL CHEMISTRY 1114 LAB Instructor: Jerry Fong 305 Physical & Health Science Bldg 587-3692 fongjd@alfredstate.edu Lab Texts: 1) Laboratory Manual for Chemistry, Amman 2013 (hot pink version) Materials: Bring the following to the lab each week: 1)safety glasses/goggles/side shields 2)calculator 4)permanent felt pen (`Sharpies’) 5)ruler 3)permanent ink pen 6)Mead Composition book=lab note book) Assignments: You are required to read each assigned experiment (see reverse side) prior to coming to the laboratory. Pre-lab quizzes will be administered throughout the term composed of 3 simple questions starting the second week of labs (9/1-9/5) There are two kinds of lab assignments 1) Minor labs will be graded in lab and returned to you the next day. They will be written entirely in your lab notebook and contain the following: a) a statement of the experiment’s Purpose (*) b) a brief description of the Procedure (*) you will use to achieve it.. (Avoid a Done entirely step-by-step procedural description. A single paragraph is preferred.) in the lab c) a legible and well-labeled tabulation of Observations & Data d) an example of critical Calculations e) statement of Results & Conclusions 2) Major labs are composed of your lab book entries described above for a minor lab, as well as a separate, type-written formal report which contains a description of the Theory underlying the procedure . Rubrics and examples will be provided. As with minor labs, your lab book entries will be graded before you leave the lab for the day. The Theory piece will be turned in two or three days from when you did the lab and graded separately from the lab book. You will also be required to read and sign a Laboratory Safety Rules Agreement. Notebook Format: We will follow typical industry practice in annotating lab notebooks. Include the following: o lab book titled with name, course number lab section and meeting time o current table of contents on first 2-3 pages o each page is numbered, initialed and dated. Experiment title at top of each page. o all information recorded with permanent ink with sections (Purpose, Procedure Observations/Data, Calculations, Results/Conclusions) clearly labeled. o corrections made with a single line drawn through the error with initial & date (No white out, erasing or destruction of any entry.) Use a to fill in any half-empty pages left after you complete notebook entries English Requirement: Both your lab notebook and major report must be in clear, error-free English. I will not grade them until the written English meets the standards described in “The Brief New Century Handbook,” 2nd edition by Hult and Huckin, the text used in Comp 1403/1503. To underscore my seriousness on this issue, you will be assumed to have a zero (0) for the lab until I am satisfied regarding its written English. I expect complete sentences with correct spelling and sensible punctuation. Grading: Minor Labs 15 points each Major Labs 50 points each If you miss or fail two labs you fail the course. !!! Safety: All students are required to wear safety or prescription eyeglasses with side shields during the entire lab. NO CONTACT LENSES are allowed. Open-toed shoes or sandals are forbidden. Leather shoes, sneakers or other footwear with complete foot coverage are ok, No eating, drinking or smoking in lab. Avoid dangling jewelry and shorts. A lab apron or lab coat is strongly advised. Do not wear your `Sunday best’ to lab. It’s a dirty place and clothes are rapidly ruined. You must be familiar with use of the following safety devices: a)fire extinguisher b)fire blanket c)shower d)eye wash Report all accidents to your instructor immediately. SYLLABUS: Laboratory Schedule for General Chemistry 1114 Fall Semester 2014 EXPERIMENT Laboratory Regulations & Safety Procedures; The Lab Book Lab check-in Naming Inorganic Compounds WEEK DATE 1 8/25-8/29 2 9/1-9/5 * 3 9/8-9/12 REFERENCE Lab manual pp. 5-6 Lab manual pp. 1-4 Instructor Handouts* individual lab instructors use their own lessons for this Naming rules are found on inside flap of Lab manual and in the lecture text, pp. 52-61 Nuts and Bolts Lab Manual pp. 23-24 4 9/15-9/19 Determination of a Chemical Formula Lab Manual pp 49-56 5 9/22-9/26 Reaction Stoichiometry of Iron with Copper(II) Sulfate Lab Manual pp. 181-183 6 9/29-10/3 Reactions in Aqueous Solution-Developing Solubility Rules Lab Manual pp. 155-158 *************************************************************************************** 7 10/6-10/10 10/6-10/10 October mini-break (no labs in week 7) *************************************************************************************** 8 10/13-10/17 Solutions, Dilutions and Acidimetry Lab Manual pp. 57-63 9 10/20-10/24 Preparation of Copper Chloride (I) with Pre-Lab Lab Manual pp. 101-105 10 10/27-10/31 Verification of the Ideal Gas Law Lab Manual pp. 119-122 10 11/3-11/7 Introduction to Spectrophotometry Lab Manual pp. 85-90 Assign Modeling Atomic Dimensions Lab Manual pp. 21-22 12 11/10-11/14 Student Presentations on Modeling Atomic Dimensions 13 11/17-11/21 Distillation ala’ Vino Lab Manual pg 169 ************************************************************************************** 14 11/24-11/28 Thanksgiving break. No labs scheduled ************************************************************************************** 15 12/1-12/5 The Geometric Structure of Molecules Lab Manual pp. 91-100 Lab Check-out