Summer Undergraduate Laboratory Internship (SULI) Richard Houanche SLAC Joe Frisch 8/30/12 1 Abstract Phase Lock Loop circuit board is made to amplify and match a 476 MHz frequency input from Stanford Synchrotron Radiation Lightsource (SSRL). The SSRL sends 10ps X-Ray pulses at a spin valve sample, so that pictures can be made of the precession of spin waves within it. The PLL board directs the spin waves to oscillate at the correct frequency and phase needed to aim them in front of the X-rays. Knowledge of how spin waves behave at the nanoscale is a fundamental one for understanding how to build efficient spintronic devices. Introduction To learn about spin waves an electrical circuit that can keep synchronization to a signal between five to ten GHz needs to be engineered. Spin waves are a collective excitation of atoms that are believed to propagate in a wave function. Magnetic spin waves in thin film materials will give us the potential to make advancements in flash memory. Phase Lock Loop (PLL) is electronic system that has a modifiable frequency oscillator, which can independently stay synchronized to a signal. The PLL is constructed of many components, amplifiers, mixers, frequency multipliers, frequency synthesizer, and the main component is a PID (proportional–integral–derivative) Controller. Our PLL will be able to take the frequency from Stanford Synchrotron Radiation Lightsource (SSRL), which is 476 MHz and multiply by an integer number n (varying from 12 to 20), than shifting it by 476 MHz / m, where m is any integer from 2 to 17. The PID is the locking system that attaches the frequency synthesizer to the wave and permits the tracking of 2 the moving wave. All of the other parts in the system permit the ability for the PLL to have the correct parameters set for in which we want the frequency, timing, and power to be passing throughout the system. Spin waves that we are looking at are within the ferromagnetic material in spin valve technology. The PLL will direct the spin waves to be oscillating at the correct frequency and phase needed. As we excite the spin waves we can track the amplitude in spatial and time domain. And then using pictures taken by the X-rays of the SSRL at 10ps picoseconds time resolution, we can make a video of how these spin waves move because we control the period in which they move. Knowledge of how spin waves move throughout the thin film layers of the spin valve is the first step to eventually being able to control the spin waves, efficiently. Materials Spectrum Analyzer Amplifiers Signal Generator/ Frequency synthesizer Multipliers Power Supply Divider Power meter Filters Digital Phosphor Oscilloscope Splitters PID (proportional–integral–derivative) controller Mixers Attenuators Comb Generator 3 Background Stanford Synchrotron Radiation Lightsource (SSRL) is a machine that gives off X-rays that are produced by electrons circulating in a storage ring at close to the speed of light. These extremely bright X-rays can be used to investigate materials at the nanoscale. With the SSRL and other technology we will contribute to the enhancement of a thin film structure, called spin valve. Spin valves interpret minimal adjustments in applied magnetic field to a great change in resistance, which is very useful in storing memory with hard drives today. The spin valves are made up of two ferromagnetic layers, with a non magnetic layer in between. When magnetic fields are applied and in the ferromagnetic layers there is a precession of electrons as they interact with each other and that propagation is called spin waves. By taking soft X-rays done at the SSRL of spin valves we will be able to see the spin waves precession within a ferromagnetic material, such as iron. To enhance spin valve technology there has to be a better understanding of how spin waves behave. In the thin film structure, we are analyzing a 5 nm thick layer of nickel-iron, 250 nm of silicon nitride, and on a centrally etched potassium hydroxide substrate. At beam line 131, we use a STXM (Scanning Transmission X-ray Microscopy) with the SSRL this allows us to take images of the spin waves at about 70 picoseconds time resolution, or even down to 10 ps with a special operation mode of SSRL. Our resolution timing is quick but unfortunately the separation between pulses take about 2.1 nanoseconds. Since the process of taking pictures is relatively slow we need to know the precession these spin waves in phase. From using the frequency given by the synchrotron’s x-rays we are able to build a machine that will apply the magnetic field needed to have the sample in the precise place. And with the correct magnetic 4 field being put onto the spin waves the goal of being able to create a video of their travelling precession is possible. The spin waves are mainly excited by the magnetic field, which allows us to direct the motion in a way that will let us see the precession. As we excite the spin waves we can track the amplitude in spatial and time domain. Knowing how spin waves move through this system is the first step to eventually control the spin waves and work on the spin valve technology. For example, spintronic devices exploit both the spin and charge of its electrons, which allows them to be smaller and more energy efficient than conventional electronic circuits. Methods Being able to examine the way spin valves rotate will not be possible without the PLL circuit. The PLL will have an output frequency ranging from about 5700-9600 GHz. It is necessary for frequency levels to be very high because that is the range in which we have predicted the spin waves oscillate at due to many factors, mainly the magnetic field. To be able to increase the frequency in the system we need a series of frequency multipliers and amplifiers. The frequency multipliers increase the signals by factor of 2, 3, or 5 in our circuit and are arranged in a specific manner. In between those multipliers are amplifiers that can handle the correct frequencies along with bringing the power up to the correct power level that the next frequency multiplier can handle. Throughout this multiplier chain we also added attenuators an electronic device that reduces the amplitude of an electronic signal, when needed. We also will needed to have the multiplier chains set up with labels should anyone need to change the configurations, it will be fairly simple to adjust. 5 Table 1. Multiplier chain loses and gains in power Config1 2x attenuator 2x attenuator 3x last 17.2 14.2 17.2 14.2 13.7 17.8 Power before connecting to the Multipliers in (dBM) Config 2 Config 3 Config 4 5x 17 2x 17.2 2x 3x 9.4 attenuator 14.2 attenuator last 14.9 2x 17.2 3x attenuator 14.2 attenuator 2x 13.6 3x 2x 11.9 last last 17.2 Config 5 5x 2x 2x last 17.2 14.2 17.2 14.2 10.5 16 17 9.2 9.6 15.7 (last) is the output power of the last amplifier in the chain, the amplifiers are assumed Diagram 1. Multiplier Chain Diagram to the left represents the multiplier chain. The all of the amplifiers are in blue squares and are labeled with an “A”. The multipliers are in the circles and are labeled 1-8. The adjustable cables are the arrows, if the arrows come from the same amplifier or splitter than they are the same cable. Table 2. Multiplier Chain Speed Sheet Cables A B Cables stay connected to the Amps C D Synthesizer Freq 5791.333 7222.333 7695.333 8647.333 9599.333 Multipliers 1 to E Result Freq (MHz) 5712 A 7143 A 7616 A 8568 A 9520 A 2 1 2 2 1 B C B B C 4 C D D 5 E 4 D 3 C D 7 E 6 D 6 8 8 E 5 E 8 E The table above is the directions needed to change to different configurations of the system. 6 The prospected power that is going to be given from the synchrotron to our system is about zero dBm. That initial power is amplified to about 21 which will go into a splitter, one signal will go to our multiplier chain and, the other will go into our divider. The divider will divide the signal by six and the multiplier chain will increase it to a signal of five to ten GHz and then combine with a mixer after. In doing this process we will then have a high multiple of 476 MHz only of set by on sixth 476 MHz, this is a very important part of the process because it allows for the phase to be slightly offset with the spin waves. If signals of the spin waves and the synthesizer were precisely in phase than the experiment would have the same picture being made constantly, instead different pictures being made at different points in the phase. After the frequency is set to our intended values then it enters the loop of the PID controller and the frequency synthesizer. The frequency initially hits the PID controller which takes that signal and locks it to the signal of the synthesizer which we have set to be the configuration’s predicted output. When everything is set up correctly the PID controller proportional and integral need only be adjusted and the phase lock loop should be operating. The phase lock loop signal will then go to the RF output which will be driving the microwave field. Results An accurate measurement of jitter is necessary for ensuring the reliability of the PLL system. Jitter is the variation of a signal with respect to its ideal position in time. It causes an increase in system noise, uncertainty in the actual phase of the sample, and inter-symbol interference. The lower the jitter the more accurate PLL circuit works. Equations use to calculate Jitter 7 π(π‘) = π΄ sin(ωt) or ππ ππ‘ π(π‘) = π΄ sin(π) = π΄π cos(ππ‘) (1) (2) π = 2πf (3) π = 2πππ‘ (4) π‘= π (5) 2ππ sinβ‘(π1 π‘) π ππ(π€2 π‘ + π) = sin π(π‘ ± Δπ‘) π(π‘) = π΄π ππ(ππ‘ + π) Δπ‘ = (6) (7) Δπ (8) πππ΄ Table 3. List of the PID parameters needed for locking the PLL to the synchrotron Configuration Freq (Hz) Gain P(gain) I=1/T Voltage (V) Amplitude (A) Jitter (s) PID controller parameters 223 53 2222 1 2 3 5.79E+09 7.22E+09 7.70E+09 5 5 5 0.1 0.1 0.1 20 20 50 3.30E-03 4.30E-03 1.50E-03 0.245 0.7 0.36 7.40E-13 2.71E-13 1.72E-13 233 4 8.65E+09 5 0.1 5 3.03E-03 0.17 6.56E-13 522 5 9.60E+09 5 0.1 20 1.30E-03 0.18 2.39E-13 Figure 1. Representation of Jitter, Ideal and Exaggerated Jitter is the timing variation from start to finish. If this was a before and after the distance in between the red dashed lines in the out of phase image would represent the jitter. 8 Discussion 740 fs is the biggest amount jitter in the five configurations; this is remarkable because we were expecting it to be in the picoseconds range. The smallest amount of jitter is 172 fs which came from the third configuration; this may be due to the fact that this multiplier chain had only X2 multipliers. As shown by Table 3 the configurations that started with a X5 multiplier also had considerably low jitter time frames which may be caused two of the X3 multipliers may not be used at their appropriate power levels. A useful attachment that was not integrated into the circuit board was the comb generator. A comb generator is a signal generator that produces multiple harmonics of its input signal, ranging from times 2-25. The entire multiplier chain could be replaced with that single part, with some draw backs. The multiplier chain is less accurate but more convenient pertaining to design and switching frequencies. The main reason that it was not put into the circuit was waiting to receive it in the mail took long than building the entire circuit board. The difference in drift between comb generator and the multiplier chain which is about 4 ps over a 14 hour measurement. This is a great because it verifies that the PLL circuit board will not have a drift that effects our measurements. The measurements have a can only be taken at the speed of the pulses given by the synchrotron, which is about 10 ps. This proves that using the comb generator or the multiplier chain our PLL will control the lock so that it stays within a domain where the phase is continuous trough out the 10 hour long experiments. 9 Summary The Phase Lock Loop circuit board works better than expected. It was used for the spin valve experiment once during the program, and was working fine but unfortunately there was something else wrong with the experiment. The samples that were being used in the experiment were all bad, which did not allow for any pictures to be taken of the spin waves. Knowledge of how spin waves behave at the nano-scale is a fundamental one for understanding how magnetism works at the nano-scale, and hence it allows for the possibility of building efficient spintronic devices. Future work- To create a control loop feedback mechanism so that the scientist running the experiment would not have to borrow the labs PID controller. It would also enhance my understanding of control theory, and how it is works. Also it would be great to continue with the spin valve experiment, interpreting the pictures of the spin waves. 10 http://people.ccmr.cornell.edu/~buhrman/theses/FAlbert.pdf THE FABRICATION AND MEASUREMENT OF CURRENT PERPENDICULAR TO THE PLANE MAGNETIC NANOSTRUCTURES FOR THE STUDY OF THE SPIN TRANSFER EFFECT A Dissertation Presented to the Faculty of the Graduate School of Cornell University in Partial Fulfillment of the Requirements for the Degree of Doctor of Philosophy by Frank Joseph Albert January 2003 http://marcuslab.harvard.edu/theses/DOUWESthesis.pdf This thesis was carried out at the Information Storage Technology Group, MESA Research Institute, University of Twente, P.O. Box 217, 7500AE Enschede Title: The Spin-valve Transistor Author: Douwe Johannes Monsma 11