Chapter 4 Resonator Measurement and Characterization In this chapter, the experimental methods used to characterize the Draper resonator prototype devices and their measurement results are presented. It begins with a summary of the measurement of packaged resonators manufactured by TFR Technologies, Inc. (63140 Britta St. C-106, Bend OR 97701), which was performed to validate the testing and analysis procedures before using them on new experimental devices. 4.1 S-parameter Measurements S-parameters are usually the measurement variables of choice when characterizing multiport devices at RF frequencies. At these high frequencies, not only do the lumped element approximations of circuit elements break down, true opens and shorts become infeasible to implement, which precludes direct impedance measurement. Through calibration and mathematical manipulations, impedance data may be acquired from sparameters. Once this data was obtained for each device, it was matched to a circuit model and equivalent parameters were extracted. 4.1.1 Materials and Setup The TFR devices were FBAR-type resonators packaged in alumina with two external ground-signal-ground (GSG) probing pads. The total packaged dimensions were about 31 Network Analyzer Ground Signal Resonator Ground Wafer probes Figure 4.1: Schematic view of a single Draper resonator test structure showing placement of testing probe tips. The background gray represents the substrate silicon. Nickel was used for the top electrode metal and is shown in black. The bottom electrode metal, Molybdenum, is shown in white, and as shown is only accessible from above through one set of probe pads. 3.8mm x 2.6mm x 0.8mm. The expected resonant frequency was about 2.1 GHz. The Draper resonators were fabricated onto a wafer and measured directly from it. Many devices with a variety of bar dimensions and tether lengths were placed onto one wafer. Each device was connected to a pair of GSG probe pads for measurement (Figure 4.1). All s-parameter measurements were performed in air at room temperature. Both the TFR and Draper devices were designed to be tested in a two-port configuration. When measuring the TFR devices, a Hewlett-Packard 8510C Network Analyzer, Cascade Microtech probe station, 1000 m pitch GSG probe tips from GGB Industries, Inc., and a 6 GHz GGB calibration substrate were used. For the Draper devices, measurements were taken with a Hewlett Packard 8753E Network Analyzer and 150 m pitch GSG probe tips on the same probe station, with a smaller calibration substrate from the same company. 32 4.1.2 Data Collection Procedure Before measurements can be taken, the testing apparatus needs to be calibrated on open, load, short, and through structures with known parameters. The calibration substrates provide these structures and the necessary parameter values, which are loaded into the network analyzer before calibration. During calibration, the network analyzer is swept through a given frequency range on each test structure multiple times. The data for each structure are averaged, and with the preloaded parameter values the analyzer calculates calibration coefficients that remove the effects of the probe tips, transmission cables linking the probe tips to the analyzer, and the analyzer measurement channels. Each calibration is only good for a short period of time as environmental variables such as temperature affect the test apparatus. For these setups it was found that calibrating once per working day was sufficient for a given frequency range. For each set of devices, data were initially taken in a wide frequency band to locate the resonance of interest, and then a very high resolution measurement was taken about the resonant frequency. Sparameters were measured on several consecutive sweeps then averaged and saved to disk as complex values, to be later imported into MATLAB for analysis. 4.2 Data Analysis The goal of the data analysis was to produce parameters characterizing the resonators and closely associated parasitics that would be useful when employing these resonators for a given application, like a filter. The analysis proceeded as follows: first, the s-parameters were transformed to z-parameters. Then, a discrete element two-port network model was applied, and the z-parameters were transformed to discrete impedance values for these elements. Finally, this data was fitted to a lumped element circuit model for each impedance element, and circuit element parameters were extracted. From equivalent circuit parameters, a resonator may be implemented easily into most filter designs using established techniques. 33 4.2.1 Data Transformation Four S-parameters were measured for each TFR device: S11, S12, S21, S22. Sij is measured by inputting an electrical wave at port j and measuring the output at port i while setting the inputs at all other ports to zero and terminating them with matched loads to cancel reflections. Sij is the ratio of the complex amplitudes of the output wave at port i and the input at port j [20] (Figure 4.2): Vk 0, k j + V1 - 2-port Port 2 network V2- V2+ Figure 4.2: Incident and reflected waves of a two-port system S12 Data 1 Magnitude (unitless) V1 Vi V j Port 1 S ij 0.8 0.6 0.4 0.2 0 0.5 Phase (radians) (4.1) 0 -0.5 -1 -1.5 1.5 2 2.5 Frequency (GHz) Figure 4.3: Typical S-parameter data 34 3 In theory, any network of passive elements should be reciprocal with S12 = S21, and inspection of the data confirmed that these values differed by less than 1% for all devices, so they were averaged into a composite parameter S12 (Figure 4.3). A two-port network can also be fully described by four z-parameters, defined as in Eqns. 4.2 and 4.3 and Figure 4.4: (4.2) V1 Z11I1 Z12 I 2 (4.3) V2 Z21I1 Z22 I 2 Once again, for a passive network the cross parameters should be equal, so Z12 is set equal to Z21. Z-parameters may be transformed from s-parameters using the following equations, assuming a reciprocal network where S12 = S21 and Z12 = Z21 [20]: (4.4) Z11 Z 0 2 (1 S11 )(1 - S 22 ) S12 2 (1 S11 )(1 - S 22 ) - S12 (4.5) Z12 Z 0 2S12 2 (1 S11 )(1 - S22 ) - S12 (4.6) Z 22 2 (1 S11 )(1 S 22 ) S12 Z0 2 (1 S11 )(1 - S 22 ) - S12 I1 V1 - 2-port network Port 2 + Port 1 For all measurements, the line impedance Z0 was 50. + V2 - Figure 4.4: Port voltage and current conventions for a two-port system 35 I2 4.2.2 Network Impedance Model Zb Za Zc Figure 4.5: Two-port impedance -model A two-port “” network was used to model each device as a collection of discrete impedances (Figure 4.5). Applying Kirchoff’s Laws to this model and combining with Eqns. 4.2 and 4.3 results in the following expressions for each impedance: (4.7) Z11 Z a Z b Z c Za Z b Zc (4.8) Z12 Za Zc Za Zb Zc (4.9) Z 22 Z c Z a Z b Za Z b Zc This model is over-simplified; its advantage is that the fitting procedure is greatly facilitated since this model only has as many independent impedance values as the number of independent two-port S-parameter values. However, its use can only be justified if the resulting error is not too significant. The fitting with this model proved acceptable for the TFR devices, and should be sufficiently accurate for the Draper devices as well because test structures will be included on-wafer to allow direct measurement of the major unmodeled parasitic elements. Now, the equations giving the port characteristics in terms of the internal impedances can be inverted to yield explicit expressions for each impedance, where |Z| ≡ Z11Z22-Z122: (4.10) Z a (4.11) Z b Z Z 22 - Z12 Z Z12 36 (4.12) Z c Z Z11 - Z12 4.2.3 Parameter Extraction The transformations described in the previous section were performed on the measured data for each device to give Za, Zb, and Zc as a function of frequency. Zb, which models the resonator block, was compared to the equivalent impedance generated by the Butterworth Van-Dyke model (Section 3.3) for a set of circuit element values, which were varied by the MATLAB routine lsqcurvefit to get the best fit. The initial values for the fit routine were calculated as follows: the maximum and minimum impedance magnitudes (“|Zp|” and “|Zs|”) and the frequencies at which they occur (“fp” and “fs”) were extracted from the data for Zb. From analysis of the BVD transfer function, the following relations are obtained [19]: (4.13) ws 2πf s 1 LC (4.14) w p 2πf p ws 1 C C0 (4.15) Z s R R 1 jws RC 0 (4.16) Z p 1 - jw p RC 0 2 p w RC 2 0 1 w RC 02 2 p Using these equations, a very good approximation for the desired parameters R, L, C, and C0 is obtained from |Zp|, |Zs|, fp, and fs. When fitting to the sharp resonance peak, an accurate initial guess was necessary to obtain a good final fit, and these approximations proved sufficient. 37 4.3 Measurement Results 4.3.1 TFR Devices Measurement and analysis of ten TFR devices was carried out while awaiting fabrication of the Draper resonator prototypes. Figure 4.6 plots Zb for one measured device alongside the equivalent BVD impedance calculated from fitted parameters. The matching is excellent, with an average per-point error less than 2% for frequencies near or below the resonance. The error is about 15% for higher frequencies as the lines begin to deviate, partly due to unmodeled parasitics whose effects grow more pronounced at higher frequencies, and partly because the BVD model only contains one resonance while the actual resonators exhibit higher-order modes. The dominating behavior expected of the shunt impedances Za and Zc is of a capacitor, from consideration of the physical makeup of these devices. They were fit to a series RLC circuit instead of only one capacitor to allow for a slightly different slope in magnitude, and to account for the real component of impedance present in the data. Zb Magnitude and Phase Impedance Phase (radians) Impedance Magnitude (dB) 60 50 40 30 20 data model 10 0 2 1 0 -1 -2 1.5 2 2.5 Frequency (GHz) Figure 4.6: Measured and modeled Zb. Simulation parameters: R = 2.76 , L = 91.6 nH, C = 0.061 pF, C0 = 1.54 pF 38 3 Impedance Magnitude (dB) Za Magnitude and Phase 50 45 40 35 data model 30 Impedance Phase (radians) 25 -1 -1.5 -2 -2.5 1.5 2 2.5 3 Frequency (GHz) Zc Magnitude and Phase Impedance Phase (radians) Impedance Magnitude (dB) 50 45 40 35 data model 30 25 1 0 -1 -2 -3 1.5 2 2.5 3 Frequency (GHz) Figure 4.7: Measured and modeled impedance data for Za and Zc Pictured in Figure 4.7 are the measured impedances Za and Zb for the same device as in Figure 4.6, plotted with their fitted RLC impedances. There is some coupling to the resonance evident, which is due to unmodeled factors. Nine of the ten identical devices measured had similarly-shaped data: the tenth matched remarkably well with a single 39 uncoupled capacitance. The fitting routine proceeded very smoothly for all ten sets of data, due to strong matching with the model. 4.3.2 Draper Resonator Measurements Fabrication of the first Draper resonators was delayed due to difficulty in obtaining high quality Aluminum Nitride (AlN) films. Since the goal of the first fabrication run was to assess basic device functionality and frequency scaling behavior, two fabrication steps were identified that could be postponed till later runs. Their removal had a significant impact on the frequency response of these initial resonators, so the nature of the imperfections will be briefly explained before presenting the results. Impact of Incomplete Fabrication The major fabrication steps are described by Figure 4.8. The steps skipped were d and e in the figure. Their purpose is to reduce the extra capacitance that would otherwise be placed in parallel with the resonator, which is a very significant amount as the probe pad is on the order of 1000 times the area of the resonator bar. As it turns out, an additional parallel capacitance of this magnitude mostly overwhelms any resonant peaks, even with Q as high as 104, according to simulation (Figure 4.9). Exacerbating this difficulty, the Q of these initial resonators is not expected to be over 1000 as the processing has yet to be optimized. Thus, the resistance at resonance is competing with a very small impedance shorting out the resonator due to this large capacitance. The shunting is more severe at higher frequencies because the capacitor impedance is inversely proportional to frequency, and for the majority of the devices on the wafer no resonance could be detected at the expected frequency. Fortunately, a few bars made with extra-large dimensions had resonant frequencies low enough to be detectable over the capacitor shunting. Also, the increased bar cross-sectional area meant reduced impedance level overall, which also helped these larger resonators to have detectable resonances. 40 (a) (b) (c) (d) (e) Figure 4.8: Overview of Draper resonator test structure fabrication. The material depicted in white is Molybdenum, gray is AlN, hatched is Nickel, and black is a conductive weld. (a) Overhead view of resonator with ground probe strips. (b) Sideview of initial stack as deposited on silicon substrate. This stack pattern represents all three GSG strips. (c) Ni and AlN layers are removed from the left probe pads of all three strips to allow contact with the bottom electrode. (d) The tethers on the resonator strip only have their electrodes selectively etched to reduce capacitance. (e) All three strips have the top and bottom electrodes shorted together to eliminate stray capacitance. 41 0 S21 (dB) -20 Cthru=2pF Cthru=0 -40 -60 -80 -100 -120 780 790 800 810 820 830 (a) -15 S21 (dB) -16 -17 -18 -19 -20 188 190 192 194 196 Frequency (MHz) 198 200 (b) Figure 4.9: Shunting effect of a large parallel capacitance “Cthru” on resonator response. (a) 6 m bar length, f0 = 800 MHz, Q = 104 (b) 25 m bar length, f0 = 193 MHz, Q = 1000 Measurement and Analysis of Longitudinal Mode Resonances Longitudinal-mode resonances were detected for devices of two bar lengths: 25 m and 30 m. Typical S21 data for both lengths are plotted in Figure 4.10. Note that on this scale, the resonant peaks are hardly discernible. However it is clear that the wideband characteristics are very similar, although quite a bit different than that of a single capacitor. High resolution data was taken for four devices around their resonances, two of each length. Figures 4.11 and 4.12 show Zb for all these devices after data transformation. The average series resonant frequencies of 148.3 MHz and 125.3 MHz for each bar length are about as expected when electrode loading is taken into account (which was 42 -5 S21 (dB) -10 -15 -20 -25 -5 S21 (dB) -10 -15 -20 -25 100 150 200 250 300 350 400 Frequency (MHz) 450 500 550 600 Figure 4.10: S21 magnitude data for 25 m (top) and 30 m (bottom) long devices. Longitudinal length mode resonances are circled. Magnitude () 595 580 590 585 570 580 575 560 570 565 Phase (degrees) 550 -81 -83 -82 -84 -83 -85 -84 -86 -85 146 -87 147 148 149 Frequency (MHz) 148 148.5 149 Frequency (MHz) Figure 4.11: Transformed impedance Zb for two 25 m long resonators. 43 149.5 Magnitude () 900 960 880 940 860 920 900 840 880 Phase (degrees) 820 -71 -72 -73 -74 -75 121.5 122 122.5 123 123.5 124 Frequency (MHz) -76.5 -77 -77.5 -78 -78.5 -79 -79.5 -80 121.5 122 122.5 123 123.5 Frequency (MHz) 124 Figure 4.12: Transformed impedance Zb for two 30 m long resonators. ignored in the prior derivation for the resonant frequency). Inspection of the plots shows a discrepancy between the data and the ideal BVD impedance, most evidently in the phase behavior. A BVD resonator has an almost entirely imaginary impedance offresonance, so its impedance phase should be about 90 degrees plus some multiple of 180. The deviation from one of these values indicates an additional unmodeled component in the through impedance of these devices which adds a real component to the impedance, possibly additional parasitic resistance in series with Zb. In the case of the 30 m bars, there is clearly a more complex unmodeled behavior affecting the data as the phase shows a significant slope as well. The net result of these deviations is that algorithmic fitting of the BVD model to this data is nearly impossible, and could only be attempted with a model modified to better fit this data. Since these prototypes were fabricated with a large masking parasitic that hindered measurement, which should be removed from future runs, it was decided premature to develop a more complex model at this point. Instead, parameters were fitted by hand to the BVD model for the prototype devices. The results and equivalent BVD parameters are shown in Figure 4.13. The additional 44 590 simulated data Magnitude () 580 570 560 550 -80 simulated data Phase (degrees) -82 -84 -86 -88 -90 145.5 146 146.5 147 147.5 148 148.5 149 149.5 150 Frequency (MHz) Figure 4.13: Fitted and measured Zb impedance of a 25 m resonator. R = 11500 W, L = 6.7 mH, C = 0.1718 fF, C0 = 1.89 pF capacitance basically replaces the C0 of the resonator, since parallel capacitances add and the parasitic capacitance is about 1000 times the natural value of C0. The fitted value for this capacitance is about what was expected from the area of the probe pads. The value of Q estimated from these values (which is not affected by C0 except through the difficulty in measurement and fitting presented by the shunting effect) is 542, once again approximately what was expected from this first round of fabricated devices. The Q values for future devices should be much improved as various aspects of the fabrication process are optimized. As mentioned above, the primary goal of the prototype fabrication round was to confirm resonator functionality. By finding longitudinal resonances that varied as expected with length, proper function of these devices was verified. 45 Probe Pad Parasitics The transformed data for the probe pad parasitic impedances Za and Zc exhibited some Impedance Magnitude () 15000 10000 5000 0 100 150 200 250 300 350 400 Frequency (MHz) 450 500 550 600 450 500 550 600 (a) 1600 Impedance Magnitude () 1400 1200 1000 800 600 400 100 150 200 250 300 350 400 Frequency (MHz) (a) Figure 4.14: Transformed impedances Za (a) and Zc (b). 46 interesting behavior. One representative set of data is shown in Figure 4.14. The first important detail is that the port impedances are not symmetric, which makes sense since the pads themselves are not symmetric: on one side the probe touched down on a single layer of metal on the substrate, while on the other side the probe touched down on top of the three-layer stack. Unfortunately, the pad orientation of the measurement ports was not recorded, so it is not certain which probe pad corresponds to which port impedance. Some general observations about the impedance data can still be made. First, the origin of the impedance should primarily be due to fringe capacitance between the probe signal pads and the two neighboring ground pads in each G-S-G probe pad set. One impedance looks very much like a capacitor while the other looks like a much smaller capacitive response with a good deal of complex behavior added in. A possible explanation for this is that the fringe capacitance for one side is much higher than the other, so the stronger capacitance dominates its modeled impedance response while the weaker capacitance on the other side allows more subtle, complex behaviors to become noticeable. The presence of the piezoelectric stack on only one set of probe pads could change the effective dielectric constant of the fringe capacitance and explain the different capacitance values. 47 48