Annex to ISO/IEC 17025:2005 declaration of accreditation for registration number: L 059 of TLR Technisch Laboratorium Rotterdam B.V. Rotterdam This annex is valid from: 08-05-2014 to 01-02-2016 No. Material or product Replaces annex dated: 23-04-2014 Type of activity Internal reference number Raw materials for animal feeding stuffs and animal feeding stuffs: Physical / Chemical parameters 1 2 3 4 5 6 7 Animal feeding stuffs Determination of moisture (4 hours drying at 103°C); gravimetric method TL312.01A Raw materials for animal feeding stuffs Determination of moisture (4 hours drying at 103°C); gravimetric method TL312.01A Cereals, flours, groats and meal Determination of moisture (2 hours drying at 130°C); gravimetric method TL312.01C Other raw materials for animal Determination of moisture (2 hours drying at feeding stuffs and animal 130°C); gravimetric method feeding stuffs TL312.01C Compound feeding stuffs containing more than 4 % of sucrose or lactose and compound feeding stuffs containing more than 25 % of mineral salts including water of crystallisation TL312.01D TL312.01B Determination of moisture (at 80°C in a vacuum oven); gravimetric method own method in accordance with EC 152/2009 Annex III-A in accordance with VDLUFA III (3.1) own method in accordance with EC 152/2009 Annex III-A in accordance with VDLUFA III (3.1) Other raw materials for animal Determination of moisture (at 80°C in a feeding stuffs and animal vacuum oven); gravimetric method feeding stuffs Single animal feed of plant origin in accordance with EC 152/2009 Annex III-A in accordance with VDLUFA III (3.1) TL312.01D TL312.01B own method Determination of crude fat (direct extraction); TL312.02A gravimetric method (Soxtherm) equivalent to EC 152/2009 Annex III-H, method A in accordance with VDLUFA III (5.1.1), procedure A This annex has been approved by: Ir. J.C. van der Poel Chief Executive Dutch Accreditation Council RvA Page 1 of 16 Annex to ISO/IEC 17025:2005 declaration of accreditation for registration number: L 059 of TLR Technisch Laboratorium Rotterdam B.V. Rotterdam This annex is valid from: 08-05-2014 to 01-02-2016 Replaces annex dated: 23-04-2014 No. Material or product 8 Other raw material for animal feeding stuffs and animal feeding stuffs Determination of crude fat (direct extraction); TL312.02A gravimetric method own method 9 Single animal feed of animal origin, all composed feeding stuffs and products of which the fat content cannot be obtained without acid hydrolysis Determination of fat (acid hydrolysis); gravimetric method TL312.02B Other raw material for animal feeding stuffs and animal feeding stuffs Determination of fat (acid hydrolysis); gravimetric method TL312.02B Animal feeding stuffs Determination of crude protein; titrimetric method TL312.03A Raw materials for animal feeding stuffs Determination of crude protein; titrimetric method TL312.03A Soybeans and soybean products Determination of Protein Dispersibility Index (PDI); titrimetric method TL312.03B Raw materials for animal feeding stuffs and animal feeding stuffs Determination of crude fibre content; gravimetrical method TL312.04A Determination of crude fibre content according to GAFTA; gravimetrical method TL312.04B Determination of crude ash; gravimetric method TL312.05 Other raw materials for animal Determination of crude ash; gravimetric feeding stuffs method TL312.05 10 11 12 13 14 15 16 17 Animal feeding stuffs Dutch Accreditation Council RvA Type of activity Internal reference number in accordance with EC 152/2009 Annex III-H, method B in accordance with VDLUFA III (5.1.1), procedure B own method equivalent to EC 152/2009 Annex III-C equivalent to VDLUFA III (4.1.1) own method in accordance with AOCS Official method Ba 10-65 in accordance with NEN-EN-ISO 6865 equivalent to EC 152/2009 Annex III-I equivalent to VDLUFA III (6.1.1) equivalent to GAFTA 9:0 in accordance with EC 152/2009 Annex III-M in accordance with VDLUFA III (8.1) own method Page 2 of 16 Annex to ISO/IEC 17025:2005 declaration of accreditation for registration number: L 059 of TLR Technisch Laboratorium Rotterdam B.V. Rotterdam This annex is valid from: 08-05-2014 to 01-02-2016 No. 18 Material or product Animal feeding stuffs Replaces annex dated: 23-04-2014 Type of activity Internal reference number Determination of starch; polarimetric method TL312.06A equivalent to EC 152/2009 Annex III-L equivalent to VDLUFA III (7.2.1) 19 Other raw materials for animal Determination of starch; polarimetric method TL312.06A feeding stuffs own method 20 Animal feeding stuffs Determination of sugar; titrimetric method TL312.07 in accordance with EC 152/2009 Annex III-J, in accordance with VDLUFA III (7.1.1) 21 22 23 24 Other raw materials for animal Determination of sugar; titrimetric method feeding stuffs TL312.07 Animal feeding stuffs Determination of ash insoluble in hydrochloric acid (sand/silica); gravimetric method TL312.05 Other raw materials for animal Determination of ash insoluble in feeding stuffs hydrochloric acid (sand/silica); gravimetric method TL312.05 Animal and vegetable fats and Determination of acid value and acidity oils (FFA); titration TL382.10 25 26 27 own method in accordance with EC 152/2009 Annex III-N own method in accordance with ISO 660 in accordance with NEN-EN 14104 Determination of moisture and volatile matter content; gravimetric method TL382.10 Determination of iodine value; titrimetric method TL382.14 Determination of saponification value In accordance with NEN-EN-ISO 662 in accordance with ISO 3961 in accordance with NEN-EN 14111 TL382.28 in accordance with NEN-EN-ISO 3657 28 29 Soybean products Determination of urease activity; titrimetric method Other raw materials for animal Determination of urease activity; titrimetric feeding stuffs and animal method feeding stuffs Dutch Accreditation Council RvA TL312.22 in accordance with EC 71/250 TL312.22 own method Page 3 of 16 Annex to ISO/IEC 17025:2005 declaration of accreditation for registration number: L 059 of TLR Technisch Laboratorium Rotterdam B.V. Rotterdam This annex is valid from: 08-05-2014 to 01-02-2016 No. 30 31 32 33 34 35 36 37 38 Material or product Animal feeding stuffs Replaces annex dated: 23-04-2014 Type of activity Determination of lactose content; titrimetric method TL312.08 Other raw materials for animal Determination of lactose content; titrimetric feeding stuffs method TL312.08 Vegetables and vegetable products Determination of nitrate; ion-exchange chromatographic (IC) method TL412.11 Fruits Determination of nitrate; ion-exchange chromatographic (IC) method TL412.11 Cereals, wheat, rye and their flours Determination of the falling number (Hagberg-Perten) TL312-09 Animal feeding stuffs Determination of cyanide/hydrocyanic acid; titrimetric method TL412.06 Other raw materials for animal Determination of cyanide/hydrocyanic acid; feeding stuffs titrimetric method TL412.06 Foodstuffs: seaweed Foodstuffs Determination of inorganic arsenic; hydride generation atomic absorption spectrometry (HGAAS) after acid extraction Determination of various metals; after digestion (HNO3) and ICP-MS Cd, Pb, As 39 Determination of various metals; after digestion (HNO3) and ICP-MS V, Co, Ni 40 Internal reference number Raw materials for animal feeding stuffs and animal feeding stuffs 41 Dutch Accreditation Council RvA Determination of various metals; after digestion (HNO3) and ICP-MS Cd, Pb, As, V, Co, Ni Determination of fluoride (F) and chloride (Cl); ion chromatographic IC method in accordance with EC 152/2009 Annex III-K own method in accordance with NEN-EN 12014-2 own method (analysis in accordance with NEN-EN 12014-2) in accordance with NEN-EN-ISO 3093 in accordance with EC 71/250 own method TL412.01B in accordance with NEN EN 15517 TL412.12 digestion: in accordance with NEN-EN 13805 analysis: in accordance with NEN-EN 15763 TL412.12 digestion: in accordance with NEN-EN 13805 analysis: own method TL412.12 digestion: own method analysis: own method TL412.14 own method Page 4 of 16 Annex to ISO/IEC 17025:2005 declaration of accreditation for registration number: L 059 of TLR Technisch Laboratorium Rotterdam B.V. Rotterdam This annex is valid from: 08-05-2014 to 01-02-2016 No. 42 43 44 45 46 47 Material or product Replaces annex dated: 23-04-2014 Type of activity Internal reference number Cereals, fruits and vegetables Determination of inorganic bromide (Br); liquid ion chromatographic IC method TL412.14 Food, animal feeding stuffs and raw materials for animal feeding stuffs Determination of sodium (Na), potassium (K), magnesium (Mg), zinc (Zn), calcium (Ca), phosphorus (P), manganese (Mn), aluminium (Al), iron (Fe), copper (Cu), chromium (Cr); ICP-MS TL412.16 Animal feeding stuffs and raw materials for animal feeding stuffs Determination of mercury (Hg); mercury analyser TL412.17 Food Determination of mercury (Hg); mercury analyser TL412.17 Determination of fluoride content after hydrochloric acid treatment; ionsensitive electrode method (ISE) TL412.18 Animal feeding stuffs Oleaginous seeds Determination of pesticide content; LCMS/MS method own method (analysis in accordance with EN 10304-1) equivalent to NEN-EN 13191-2 own method equivalent to NEN EN 16277 equivalent to NEN EN 15763 in accordance with NEN-EN 16279 TL512.06 own method Bupirimaat Indoxacarb Carbaryl Linuron Carbendazim Metalaxyl Carbofuran Methomyl Carboxin Monocrotophos Cyprodinil Omethoaat Dimefuron Prochloraz Imazalil Thiabendazol Acrinathrin Flufenoxuron Chlorfluazuron Hexaflumuron Diflubenzuron Lufenuron Fipronil Noviflumuron Fluazinam Teflunezuron Flucloxuron (E+Z)Triflumuron Fludioxinil Dutch Accreditation Council RvA Page 5 of 16 Annex to ISO/IEC 17025:2005 declaration of accreditation for registration number: L 059 of TLR Technisch Laboratorium Rotterdam B.V. Rotterdam This annex is valid from: 08-05-2014 to 01-02-2016 No. 48 Material or product Oleaginous seeds Type of activity Internal reference number Determination of pesticide content; GPC-LC- TL512.02 LVI-GCMS own method: a-Endosulfan Dutch Accreditation Council RvA Replaces annex dated: 23-04-2014 Dieldrin a-HCH Dimethoate Alachlor Diphenylamine Aldrin Disulfoton Anthrachinon Endosulfansulfaat Atrazine Endrin Azinphos-ethyl EPN Azinphos-methyl Esfenvaleraat b-Endosulfan Ethion b-HCH Ethoprophos Bifenox Etrimphos Bifenthrin Fenarimol Bromacil Fenitrothion Bromophos-ethyl Fenpropathrin Bromophos-methyl Fenthion Broompropylaat g-HCH Buprofezin Heptachloor Chloorbenzilaat Heptachloor(endo)epoxide Chloorbufam Heptenophos Chloorfenvinphos Hexachloorbenzeen Chloormephos Hexazinon Chloorpropham Isodrin Chloorpyriphos-ethyl Malathion Chloorpyriphos-methyl Metazachloor Chloorthalonil Methoxychloor Chloridazon Metolachloor Chloroneb Mevinphos Cis-Chloordaan Nonachloor-cis Cyanazine Nonachoor-trans Cyanophenphos o,p-DDD Cyfluthrin o,p-DDE Cyhalothrin o,p-DDT Cypermethrin p,p-DDD d-HCH p,p-DDE Diallate p,p-DDT Diazinon Parathion-ethyl Dichlofluanide Parathion-methyl Dichlorvos Permethrin Phosalone Pyrifenox Phosphamidon Simazine Piperonyl-butoxide Sulfoteb Pirimiphos-ethyl Tecnazeen Pirimiphos-methyl Terbutryn (extraction: in accordance with NEN EN 12393-2, clean up: own method, analysis: in accordance with NEN EN 12393-3) Page 6 of 16 Annex to ISO/IEC 17025:2005 declaration of accreditation for registration number: L 059 of TLR Technisch Laboratorium Rotterdam B.V. Rotterdam This annex is valid from: 08-05-2014 to 01-02-2016 No. 49 50 51 52 Material or product Animal feeding stuffs, non1 fatty crops , oleaginous seeds, fats and oils 1 Crops (excluding fresh vegetables), animal feeding stuffs, raw materials for animal feeding stuffs and premixes Apples and apple products Spices and spice extracts Type of activity Internal reference number Determination of the content of PAH’s and PCB’s; GPC-LC-LVI-GCMS TL512.04 own method Naphtalene PCB 28 Phenantrene PCB 52 Antracene PCB 101 Fluoranthene PCB 118 Chrysene PCB 153 Acenaphtene PCB 138 Acenaphthylene PCB 180 Fluorene Sum of benzo(k)- and benzo(b)fluoranthene Benzo(a)pyrene Benzo(ghi)perylene Benzo(a)anthracene Indeno(1,2,3-cd)pyrene Pyrene Dibenzo(a,h)antracene Determination of mycotoxins; HPLC MS/MS TL512.03 own method Deoxynivalenol (DON) / Vomitoxine α-Zearalenol 3-acetyl-DON β-Zearalenol Fumonisin B1 Diacetoxyscripenol Fumonisin B2 Zearalenon (ZEA) Aflatoxine B1 Ochratoxine A (OTA) Aflatoxine B2 Sterigmatocystin Aflatoxine G1 HT-2 Toxine Aflatoxine G2 T-2-Toxine DAS) Determination of patulin content; HPLCMS/MS TL512.07 Determination of dyes; HPLC-MS/MS TL512.08 Rhodamine B Dutch Accreditation Council RvA Replaces annex dated: 23-04-2014 CAS 81-88-9 Butter yellow CAS 60-11-7 Fast Garnet GBC CAS 97-56-3 Para Red CAS 6410-10-2 Toludine Red CAS 2425-85-6 Sudan Red G CAS 1229-55-6 Sudan Red7B CAS 6368-72-5 Sudan I CAS 842-07-9 Sudan II CAS 3118-97-6 Sudan III CAS 85-86-9 Sudan IV CAS 85-83-6 own method own method Page 7 of 16 Annex to ISO/IEC 17025:2005 declaration of accreditation for registration number: L 059 of TLR Technisch Laboratorium Rotterdam B.V. Rotterdam This annex is valid from: 08-05-2014 to 01-02-2016 No. 53 54 Material or product Replaces annex dated: 23-04-2014 Type of activity Internal reference number Animal feeding stuffs, raw materials for feeding stuffs and milk powder Determination of melamine and cyanuric acid; HPLC-MS/MS TL512.09 Raw materials for animal feeding stuffs and animal feeding stuffs Determination of dioxins (PCDD’s), dibenzufurans (PCDF’s), non-ortho-PCB’s and mono-ortho PCB’s: GC-HRMS TL512.10B Dibenzo-p-dioxins (PCDD's): Non-ortho-PCB's 2,3,7,8-TCDD PCB 77 1,2,3,7,8-PeCDD PCB 81 1,2,3,4,7,8-HxCDD PCB 126 1,2,3,6,7,8-HxCDD PCB 169 own method in accordance with NEN-EN 16215, in accordance with EC 278/2012 1,2,3,7,8,9-HxCDD 1,2,3,4,6,7,8 HpCDD Mono-ortho-PCB's OCDD PCB 105 PCB 114 Dibenzofurans (PCDF's) PCB 118 2,3,7,8-TCDF PCB 123 1,2,3,7,8-PeCDF PCB 156 2,3,4,7,8-PeCDF PCB 157 1,2,3,4,7,8-HxCDF PCB 167 1,2,3,6,7,8-HxCDF PCB 189 1,2,3,7,8,9-HxCDF 2,3,4,6,7,8-HxCDF 1,2,3,4,6,7,8-HpCDF 1,2,3,4,7,8,9-HpCDF OCDF Dutch Accreditation Council RvA Page 8 of 16 Annex to ISO/IEC 17025:2005 declaration of accreditation for registration number: L 059 of TLR Technisch Laboratorium Rotterdam B.V. Rotterdam This annex is valid from: 08-05-2014 to 01-02-2016 No. 55 Material or product Oils and fats from plant animal origin and eggs Replaces annex dated: 23-04-2014 Type of activity Determination of dioxins (PCDD’s), dibenzufurans (PCDF’s), non-ortho-PCB’s and mono-ortho PCB’s: GC-HRMS Dibenzo-p-dioxins (PCDD's): Non-ortho-PCB's 2,3,7,8-TCDD PCB 77 1,2,3,7,8-PeCDD PCB 81 1,2,3,4,7,8-HxCDD PCB 126 1,2,3,6,7,8-HxCDD PCB 169 Internal reference number TL512.10B own method (analysis in accordance with NEN-EN 16215 and in accordance with EC 252/2012) 1,2,3,7,8,9-HxCDD 1,2,3,4,6,7,8 HpCDD Mono-ortho-PCB's OCDD PCB 105 PCB 114 Dibenzofurans (PCDF's) PCB 118 2,3,7,8-TCDF PCB 123 1,2,3,7,8-PeCDF PCB 156 2,3,4,7,8-PeCDF PCB 157 1,2,3,4,7,8-HxCDF PCB 167 1,2,3,6,7,8-HxCDF PCB 189 1,2,3,7,8,9-HxCDF 2,3,4,6,7,8-HxCDF 1,2,3,4,6,7,8-HpCDF 1,2,3,4,7,8,9-HpCDF OCDF 56 57 58 59 Oils and fats from plant origin Oils and fats from plant origin Raw materials for animal feeding stuffs Non-fatty crops 1 Determination of mineral oil (C10-C40); GC-FID TL512.17 Determination of mineral oil (C10-C25); GC-FID TL512.17 Determination of mineral oil (C10-C40); GC-FID TL512.17 Determination of dithiocarbamate and thiuramdisulfide residues (as CS2); gaschromatographic method (GC-MS) TL512.19 equivalent to VVR-bundle feed part II OSP 15 own method (analysis: equivalent to VVR-bundle feed part II OSP 15) own method (analysis: equivalent to VVR-bundle feed part II OSP 15) in accordance with NEN-EN 123962 60 Non-fatty food of plant origin Determination of chlormequat and mepiquat; TL512.12 in accordance with NEN-EN 15055 HPLC-MS/MS 61 Raw materials for animal feeding stuffs and animal feeding stuffs Determination of chlormequat and mepiquat; TL512.12 own method (analysis: in HPLC-MS/MS Dutch Accreditation Council RvA accordance with NEN-EN 15055) Page 9 of 16 Annex to ISO/IEC 17025:2005 declaration of accreditation for registration number: L 059 of TLR Technisch Laboratorium Rotterdam B.V. Rotterdam This annex is valid from: 08-05-2014 to 01-02-2016 No. Material or product Replaces annex dated: 23-04-2014 Type of activity Internal reference number Microbiology 62 63 Animal feeding stuffs and food Enumeration of Bacillus cereus at 30°C; products plate count method TL752.05 in accordance with NEN-EN-ISO 7932 Animal feeding stuffs and food Enumeration of β-glucuronidase-positive TL752.06 products Escherichia coli at 44°C; plate count method in accordance with NEN-ISO 16649-2 64 Detection of Salmonella; presence/absence TL752.01A in accordance with NEN-EN-ISO 6579 65 Detection of Salmonella (presence/absence); Salmonella Rapid Test Oxoid 66 Detection of Salmonella (presence/absence); ® Assurance GDS Salmonella, BioControl 67 Enumeration of micro-organisms (Aerobic plate count) at 30°C; plate count method 68 TL752.01B equivalent to NEN-EN-ISO 6579: (AFNOR UNI 03/01-05/91) TL752.01D equivalent to NEN-EN-ISO 6579: (AFNOR TRA 02/12-01/09) TL752.04 in accordance with NEN-EN-ISO 4833 Enumeration of Enterobacteriaceae at 37°C; TL752.02 plate count method in accordance with NEN ISO 21528-2 Enumeration of Enterobacteriaceae at 37°C; TL752.02B equivalent to NEN ISO 21528-2: Petrifilm, plate count method 69 (AFNOR 3M 01/6-09/97) 70 Food and animal feeding stuffs Enumeration of yeasts and moulds at 25°C; plate count method TL752.03C in accordance with NEN ISO 215271 (product with a water activity > 0,95) 71 Animal feeding stuffs and food Enumeration of yeasts and moulds at 25°C; products plate count method, culture medium DG-18 agar 72 Dutch Accreditation Council RvA Enumeration of Staphylococcus aureus at 37°C; plate count method TL752.03B in accordance with NEN ISO 215272 (product with a water activity ≤ 0,95) TL752.09 in accordance with NEN-EN-ISO 6888-2 Page 10 of 16 Annex to ISO/IEC 17025:2005 declaration of accreditation for registration number: L 059 of TLR Technisch Laboratorium Rotterdam B.V. Rotterdam This annex is valid from: 08-05-2014 to 01-02-2016 No. 73 Material or product 76 77 78 79 80 81 82 83 Type of activity Animal feeding stuffs and food Enumeration of Clostridium perfringens at products 37°C; plate count method Internal reference number TL752.10 in accordance with NEN-EN-ISO 7937 Enumeration of mesophilic lactic acid bacteria at 30°C; plate count method TL752.11 Food products, except dairy products and raw shellfish Enumeration of micro-organisms (Aerobic plate count) at 30°C, reading after 48 hours; Petrifilm, plate count method TL752.04B Food stuffs Enumeration of β-glucuronidase-positive Escherichia coli at 42°C; Petrifilm, plate count method TL752.06B Enumeration of Coliforms at 37°C; Petrifilm, plate count method TL752.15 74 75 Replaces annex dated: 23-04-2014 Food products, except raw shellfish in accordance with ISO 15214 equivalent to NEN-EN-ISO 4833: (AFNOR 3M 01/1-09/89) equivalent to NEN-ISO 16649-2: (AFNOR 3M 01/08-06/01) equivalent to NEN-EN-ISO 4832: (AFNOR 3M 01/2-09/89A) Animal feeding stuffs and food Enumeration of Staphylococcus aureus at products 37°C; Petrifilm, plate count method TL752.09B Meat and meat products, Detection of Shigatoxin producing Shigella potatoes, vegetables and and/or E. coli (STEC/EHEC) bacteria; fruits, seeds and beans qualitative real time PCR technique (except garlic and citrus fruits) TL752.34 Food products and environmental samples Detection of Listeria monocytogenes; quick detection method (chromogenic media) TL752.20A Animal feeding stuffs and raw materials for feeding stuffs Detection of Listeria monocytogenes; quick detection method (chromogenic media) TL752.20A Food products and environmental samples Enumeration of Listeria monocytogenes; chromogenic agar plate method TL752.20B Animal feeding stuffs and raw materials for feeding stuffs Enumeration of Listeria monocytogenes; chromogenic plate method TL752.20B Dutch Accreditation Council RvA equivalent to NEN-EN-ISO 6888-2 (AFNOR 3M 01/09-04/03B) own method equivalent to ISO 11290-1 (AFNOR BRD 07/16-01/09) own method (AFNOR BRD 07/1601/09) equivalent to ISO 11290-2 (AFNOR BRD 07/17-01/09) own method (AFNOR BRD 07/1701/09) Page 11 of 16 Annex to ISO/IEC 17025:2005 declaration of accreditation for registration number: L 059 of TLR Technisch Laboratorium Rotterdam B.V. Rotterdam This annex is valid from: 08-05-2014 to 01-02-2016 No. Material or product Replaces annex dated: 23-04-2014 Type of activity Internal reference number Allergens in food 84 85 Raw materials, spices and processed products Quantitative determination of gluten (gliadin x2); ELISA TL762.19 Food Determination of casein (presence/absence); ELISA TL762.16 equivalent to AOAC-method 2012.01 own method Genetically Modified Food / Feeding stuffs 86 87 Singular and pure raw Screening for Genetically Modified Crops materials (soybean products, (GMO); lightcycler instrument (PCR) maize products, rice products, sugar beet products, flax seed products, rapeseed products, potato products and cotton) TL752.07B Soybean products TL752.08 Quantitative analysis of Roundup Ready Soya (GGO/GMO); lightcycler instrument (PCR) own method own method Microscopy 88 Raw materials for animal feeding stuffs and animal feeding stuffs 89 Determination of Datura species content; gravimetric method 90 91 92 93 Determination of stone shell content in palm- TL612.01 and coconut products; gravimetric method own method TL612.03 own method Determination of product-specific admixture; TL612.02 gravimetric method own method Raw materials for animal feeding stuffs and animal feeding stuffs Determination the content of Castor seed husks; gravimetric method TL612.04 Animal feeding stuffs Determination of animal meal; microscopic method TL612.06 Other raw materials for animal Determination of animal meal; microscopic feeding stuffs method TL612.06 Dutch Accreditation Council RvA in accordance with ISO 5061 in accordance with EG 152/2009, Annex VI own method (analysis in accordance with EG 152/2009, ANNEX VI) Page 12 of 16 Annex to ISO/IEC 17025:2005 declaration of accreditation for registration number: L 059 of TLR Technisch Laboratorium Rotterdam B.V. Rotterdam This annex is valid from: 08-05-2014 to 01-02-2016 No. Material or product Replaces annex dated: 23-04-2014 Type of activity Internal reference number Solid mineral fuels: Physical / chemical parameters 94 Coal 95 TL422.01B Determination of the crude swelling number (FSI) TL422.08 in accordance with NEN-ISO 589, Method B1 in accordance with NEN- ISO 501 Determination of hardgrove grindability index TL422.07 in accordance with ISO 5074 (HGI); gravimetric method 96 97 Determination of total moisture content; gravimetric method Solid mineral fuels Determination of ash; gravimetric method TL422.03 In accordance with NEN- ISO 1171 98 99 Coal and cokes Solid mineral fuels 100 101 102 103 104 Determination of volatile matter content; gravimetric method TL422.02 Determination of carbon (C), hydrogen (H) with the element analyser TL422.05 Determination of nitrogen (N) with the element analyser TL422.05 Determination of sulphur (S) with the element analyser TL422.05 Determination of moisture in the analysis test sample; gravimetric method TL422.01A Determination of gross caloric value by bomb caloric method and calculation of net caloric value TL422.04 Sample preparation of solid mineral fuels in accordance with NEN-ISO 562 in accordance with ASTM D 5373 in accordance with NEN-ISO 29541 in accordance with NEN-ISO 29541 own method in accordance with NEN-ISO 11722 in accordance with NEN-ISO 1928 TL222.02 in accordance to NEN-ISO 18283, in accordance with NEN-ISO 13909-4 105 106 Biomass (wood, residues from Sample preparation of biomass food and tobacco industry for generating energy, solid biofuels and solid secondary biofuels TL272.01 Coal and cokes TL432.01 Determination of fusibility of ash in accordance with NEN EN 14780 in accordance with NEN EN 15443 in accordance with NEN-ISO 540 Dutch Accreditation Council RvA Page 13 of 16 Annex to ISO/IEC 17025:2005 declaration of accreditation for registration number: L 059 of TLR Technisch Laboratorium Rotterdam B.V. Rotterdam This annex is valid from: 08-05-2014 to 01-02-2016 No. 107 Material or product Other solid mineral fuels Replaces annex dated: 23-04-2014 Type of activity Determination of fusibility of ash Internal reference number TL432.01 own method 108 109 110 Solid fuels Determination of fluoride (F) and chloride (Cl); Ion-exchange chromatographic (IC) method 112 113 114 own method Solid biofuels and solid secondary biofuels, coal, cokes and fly ash Determination of ash content; after ashing at TL432.02 o 815 C, total digestion and ICP-MS; own method Solid biofuels and solid secondary biofuels Determination of various metals; after digestion and ICP-MS Na, Mg, Al, Si, P, K, Ca, S, Ti, Fe, Mn Cd, Pb, As, V, Co, Ni 111 TL412.13 TL412.12 digestion and analysis: equivalent to NEN-EN 15297 Solid biofuels and solid secondary biofuels Determination of mercury (Hg); mercury analyser TL412.17 Solid biofuels Determination of mercury (Hg); mercury analyser TL412.17 Biomass (wood, residues from Determination of total moisture; gravimetric food and tobacco industry for method generating energy), solid biofuels and solid secondary biofuels Determination of moisture in the analysis test sample; gravimetric method 115 Determination of ash, gravimetric method equivalent to NEN EN 15297 in accordance with ASTM D6722-01 equivalent to ISO 15237 TL422.01C in accordance with NTA 8200 (2002), NEN-EN 14774-1, NEN-EN 15414-1 TL422.01A in accordance with NTA 8200 (2002), NEN-EN 14774-3, draft NEN-EN 15414-3 TL422.03 in accordance with NTA 8200 (2002), NEN-EN 14775, NEN-EN 15403 116 117 Dutch Accreditation Council RvA Determination of volatile matter content; gravimetric method TL422.02 Determination of carbon (C), nitrogen (N), hydrogen (H) with the element analyser TL422.05 in accordance with NTA 8200 (2002), NEN- EN 15148, NEN-EN 15402 in accordance with NTA 8200 (2002), NEN-EN 15104, NEN-EN 15407 Page 14 of 16 Annex to ISO/IEC 17025:2005 declaration of accreditation for registration number: L 059 of TLR Technisch Laboratorium Rotterdam B.V. Rotterdam This annex is valid from: 08-05-2014 to 01-02-2016 No. Material or product 118 Biomass (wood, residues from food and tobacco industry for generating energy), solid biofuels and solid secondary biofuels 119 120 121 Fly ash Replaces annex dated: 23-04-2014 Type of activity Internal reference number Determination of fluoride (F) and chloride (Cl); IC method TL412.13 Determination of sulphur (S) with the element analyser TL422.05 Determination of gross caloric value by bomb caloric method and calculation of net caloric value TL422.04 Determination of pH, potentiometric method in accordance with NTA 8200 (2002) own method in accordance with NTA 8200 (2002), NEN-EN 14918, NEN-EN 15400 TL432.07 own method 122 Determination of the fineness by wet sieving TL432.08 own method 123 124 125 126 127 Solid biofuels and solid secondary biofuels 128 129 Dutch Accreditation Council RvA Determination of the L*a*b* colour space; colorimetric method TL432.09 Determination of filler aggregate in bituminous mixtures: bitumen number; penetrometric method TL432.10 Determination of free calcium oxide content; titrimetric method TL432.11 Determination of the loss by combustion without correction for the oxidation of sulphides; gravimetric method TL432.12 Determination of minor elements copper (Cu), manganese (Mn), zinc (Zn), chromium (Cr), molybdenum (Mo), antimony (Sb), selenium (Se); ICP-MS TL412.12 Determination of minor elements barium (Ba) and iron (Fe); ICP-MS TL412.12 Determination of total content of sulphur (S) and chlorine (Cl); tube furnace and ion chromatographic method TL412.13 in accordance with NEN-ISO 11664-4 in accordance with NEN-EN 13179-2 in accordance with NEN-EN 451-1 in accordance with EN 196-2 equivalent to NEN-EN 15297 own method (analysis: equivalent to NEN-EN 15297) in accordance with NEN-EN 15289 Page 15 of 16 Annex to ISO/IEC 17025:2005 declaration of accreditation for registration number: L 059 of TLR Technisch Laboratorium Rotterdam B.V. Rotterdam This annex is valid from: 08-05-2014 to 01-02-2016 No. 130 Material or product Solid biofuels and solid secondary biofuels 131 132 133 134 Replaces annex dated: 23-04-2014 Type of activity Internal reference number Determination of ash melting behaviour; characteristic temperatures method TL432.01B Determination of mechanical durability of pellets and briquettes; pellets tester TL272.03 Determination of bulk density; standard measuring container TL272.04 Determination of particle size distribution; Vibrating screen method using sieve apertures of 3,15 mm and below TL272.05A in accordance with NPR CEN/TS 15370-1 in accordance with NEN-EN 15210-1 Part1 in accordance with NEN-EN 15103 in accordance with NEN-EN 15149-2 Determination of particle size distribution of TL272.05B disintegrated pellets; disintegration in hot in accordance with NEN-EN water sieve apertures of 3,15 mm and below 15149-2 in accordance with NEN-EN 16126 135 136 All other pellets Determination of length and diameter of pellets TL612.07 Determination of length and diameter of pellets TL612.07 in accordance with NEN-EN 16127 own method (analysis: in accordance with NEN-EN 16127) Flexible scope 137 138 Crops Crops 1 1 Determination of pesticide content; LCMS/MS method Determination of pesticide content; LVI-GCMS/MS method TL512.27 own method TL512.26 own method (clean-up: own method extraction and analysis: in accordance with NEN EN 15662) 1: By crops is meant: food stuffs and feeding stuffs of plant origin. 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