KOYA UNIVERSITY PETROLEUM ENGINEERING DEPARTMENT THIRD STAGE PRODUCTION TECHNOLOGY II , S6 CHAPTER FOUR OIL AND GAS SEPARATION @DPTE 2025 Dr. Sarhad Ahmed Farkha Sarhad.ahmed@koyauniversity.org PhD Petroleum Engineering – Production Engineering – Koya University – October 2024 MSc Petroleum Engineering- Teesside Uni. United Kingdom October 2013 BSc Petroleum Engineering – Koya University July 2010 Member of Society of Petroleum Engineer (SPE), Onepetro access Separation Design 30 Separators Design @KOU 2024-2025 DPTE Separation Design 31 Separators Design General Separator Design Consideration: Factors Affecting Separation: The following factors must be determined before separator design: • Gas and liquid flow rates (minimum, average, and peak) • Operating and design pressures and temperatures • Surging or slugging tendencies of the feed streams • Physical properties of the fluids such as density and compressibility • Designed degree of separation (e.g., removing 100% of particles greater than 10 microns) • Presence of impurities (paraffin, sand, scale, etc.) • Foaming tendencies of the crude oil • Corrosive tendencies of the liquids or gas @KOU 2024-2025 DPTE Separation Design 32 Separators Design General Separator Design Consideration: Design Considerations: The following must be considered in designing a separator vessel: • The volumes of the dished heads • The length/diameter (L/D) • acceptable when it is between about 3/1 and 8/1 • For a vertical separator, the gas flows through the entire cross section of the upper part of the vessel. • For a horizontal separator, the interface does not have to be at the centerline of the vessel. @KOU 2024-2025 DPTE Separation Design 33 Separators Design • The basic factors that effect on separators design are: 1. Working pressure 2. Working temperature 3. Fluid component • Separator design consisting as follows: 1. Calculate gas section capacity. 2. Calculate oil section capacity. @KOU 2024-2025 DPTE Separation Design 34 A- Vertical Separator Design @KOU 2024-2025 DPTE Separation Design 35 A- Capacity of vertical Separators: 1. Gas Capacity: • Suppose there is a liquid drop in the gravity settling section, the liquid drops will settle at a velocity determined by equation the gravity force (๐ญ๐ ), on the drop with the drag force (๐ญ๐ ) caused by its motion relative to the gas continuous phase. ๐ ๐ ๐ ๐ ๐ ๐๐ ๐๐ (๐. ๐) ๐ ๐ ๐ซ๐๐๐๐๐๐ ๐๐๐๐๐ , ๐ญ๐ = ๐ ๐๐ (๐๐ −๐๐ ) ๐ (๐. ๐) ๐ • If ๐ญ๐ = ๐ญ๐ ; Then the droplet will remain suspended and gas velocity call suspended velocity. ๐ ๐ ๐ ๐ ๐ ๐ ๐๐ ๐๐ = ๐ ๐๐ (๐๐ −๐๐ ) ๐ (๐. ๐) ๐ ๐ ๐.๐ ๐ ๐ ๐ ๐ (๐๐ −๐๐ ) ๐= เต๐๐ ๐ (๐. ๐) ๐ ๐ผ๐๐๐๐๐ ๐๐๐๐๐ , ๐ญ๐ = @KOU 2024-2025 DPTE Separation Design 36 A- Capacity of vertical Separators: 1. Gas Capacity: • If ๐๐ , ๐ & ๐ remain constant, then; ๐.๐ (๐๐ −๐๐ ) เต๐ ๐= ๐ ๐ ๐ ๐ ๐๐ = ๐ ๐ ๐ ๐.๐ ๐ ๐ (๐๐ −๐๐ ) เต๐ ๐๐ = ๐ ๐ ๐ ๐ • (๐. ๐) (๐. ๐) (๐. ๐) Where: ๐๐ฉ = ๐๐ซ๐จ๐ฉ๐ฅ๐๐ญ ๐๐ข๐๐ฆ๐๐ญ๐๐ซ ๐๐ = ๐ ๐๐ฌ ๐๐๐ง๐ฌ๐ข๐ญ๐ฒ , ๐๐/๐๐ญ ๐ ๐ฎ = ๐๐๐๐๐๐๐ ๐๐๐ ๐ ๐๐ฌ ๐ฏ๐๐ฅ๐จ๐๐ข๐ญ๐ฒ ๐ = ๐๐๐๐๐ ๐ ๐ ๐๐๐๐๐๐๐ ๐๐ ๐๐๐๐๐๐๐๐๐ ๐ค = ๐๐ฆ๐ฉ๐ซ๐ข๐๐๐ฅ ๐๐จ๐ง๐ฌ๐ญ๐๐ง๐ญ ๐๐จ = ๐จ๐ข๐ฅ ๐๐๐ง๐ฌ๐ข๐ญ๐ฒ , ๐๐/๐๐ญ ๐ ๐ = ๐๐๐๐๐ฅ๐๐ซ๐๐ญ๐ข๐จ๐ง ๐๐ฎ๐ ๐ญ๐จ ๐ ๐ซ๐๐ฏ๐ข๐ญ๐ฒ. ๐= ๐.๐ ๐๐เต = ๐๐๐๐๐๐๐๐ ๐๐๐๐๐๐๐๐ ๐๐ ๐๐ = gas flow rate, scf/day @KOU 2024-2025 DPTE Separation Design 37 A- Capacity of vertical Separators: 1. Gas Capacity: Apply Material balance equation on gas under separator and standard condition ๐๐ ๐๐ = ๐๐ ๐.๐ ๐๐ ๐.๐ (๐. ๐) Where: • ๐๐ ๐ .๐ = ๐๐๐ ๐๐๐๐ค ๐๐๐ก๐ ๐๐ก ๐. ๐ถ. ๐ ๐๐/๐๐๐ฆ • ๐๐ ๐ .๐ = ๐๐๐๐ ๐๐ก๐ฆ ๐๐ ๐๐๐ ๐๐ก ๐. ๐ถ. ๐ผ๐/๐๐ก 3 • ๐๐ = ๐๐๐ ๐๐ ๐ ๐๐ ๐ ๐๐ ๐๐ ๐ ๐ = ๐๐ ๐ ๐ ๐๐ ๐ • ๐พ๐ = • ๐๐ = ๐๐๐๐๐๐๐๐ก ๐๐๐๐ข๐๐๐ข๐๐ ๐ค๐๐๐โ๐ก • • ๐ = ๐ข๐๐๐ฃ๐๐๐ ๐๐ ๐๐๐ ๐๐๐๐ ๐ก๐๐๐ก , 10.73 ๐พ๐ = ๐๐๐ ๐๐๐๐ฃ๐๐ก๐ฆ • • • ๐ = ๐๐๐ ๐๐๐ฃ๐๐๐ก๐๐๐ ๐๐๐๐ก๐๐ ๐ = ๐ก๐๐๐๐๐๐ก๐ข๐๐ , ห๐ @KOU 2024-2025 DPTE ๐๐ ๐๐ = ๐ ๐๐๐ 29 Separation Design 38 A- Capacity of vertical Separators: 1. Gas Capacity: • Substituting all above into equation (4.8): ๐.๐ ๐ ๐ (๐๐ −๐๐ )เต ๐ท๐ด๐ ๐ ๐ ๐ ๐ ๐ ๐๐น๐ป ๐๐ ๐๐ = ๐ท๐๐ ๐ด๐ ๐๐๐ ๐น๐ป๐๐ • In field unit; 0.5 ๐๐ − ๐๐ ๐ ๐๐ ๐ ๐๐ ๐๐ = 67824 × 10−6 ๐ 2 ๐ ๐๐ ๐ ๐ ๐๐ ๐ ๐.๐ ๐ท (๐๐ −๐๐ ) เต๐ ๐๐ ๐๐ = ๐. ๐ ๐ ๐ ๐ ๐๐ป ๐ • Where: @KOU 2024-2025 DPTE ๐๐ ๐ .๐ = ๐๐๐ ๐๐๐๐ค ๐๐๐ก๐ ๐๐ก ๐. ๐ถ. ๐ ๐๐/๐๐๐ฆ ๐ = ๐๐๐ ๐๐๐ ๐๐๐๐๐๐ก๐๐ ๐๐ ๐ ๐๐๐๐๐๐ก๐๐ , ๐๐ ๐๐ ๐ = ๐ ๐ก๐๐๐๐๐๐ ๐ก๐๐๐. 60 โ (๐. ๐) (๐. ๐๐) (๐. ๐๐) ๐ = ๐ ๐๐๐๐๐๐ก๐๐ ๐๐๐๐๐๐ก๐๐๐ ๐๐๐๐ ๐ ๐ข๐๐, ๐๐ ๐ ๐๐ ๐ = ๐ ๐ก๐๐๐๐๐๐ ๐๐๐๐ ๐ ๐ข๐๐, 14.7 ๐๐ ๐ ๐ = ๐ ๐๐๐๐๐๐ก๐๐ ๐๐๐๐๐๐ก๐๐๐ ๐ก๐๐๐. , ห๐ Separation Design 39 A- Capacity of vertical Separators: 2. Oil Capacity: • Oil capacity design depend on retention time; therefore, the time should be enough to give solution gas in oil the change to be freely. • For most application retention times are between 30 second to 3 minutes have been found to be sufficient. Where foaming crude is present retention time up to four times this amount may be needed. ๐ ๐๐ = ๐ 2 โ๐ 4 ๐๐ ๐๐ ๐๐๐ก๐ข๐๐ = ๐ก ๐ 2 ๐ โ๐เต 4 ๐๐ ๐๐๐ก๐ข๐๐ = ๐ก × @KOU 2024-2025 DPTE 4.12 4.13 1440 5.615 4.14 Separation Design 40 A- Capacity of vertical Separators: 2. Oil Capacity: ๐ 2 โ๐เต ๐๐ ๐๐๐ก๐ข๐๐ = 201.4 ๐ก 4.15 • And , for rated oil capacity under separator condition , bbl/day: ๐๐ ๐ = 1Τ2 ๐๐ ๐๐๐ก๐ข๐๐ ๐ 2 โ๐เต ๐๐ ๐ = 100.7 ๐ก • Where: • • ๐๐ = ๐ฃ๐๐๐ข๐๐ ๐๐ ๐๐๐ ๐ ๐๐๐ก๐๐๐, ๐๐ก 3 ๐ = ๐๐๐๐๐ ๐ ๐ ๐๐๐๐๐๐๐ ๐๐ ๐๐๐๐๐๐๐๐๐ • โ๐ = โ๐๐๐โ๐ก ๐๐ ๐๐๐ ๐ ๐๐๐ก๐๐๐ , ๐๐ก • • ๐๐ ๐๐๐ก๐ข๐๐ = ๐๐๐ข๐ก๐๐ ๐๐๐ ๐๐๐๐๐๐๐ก๐ฆ, ๐๐๐/๐๐๐ฆ ๐๐ ๐ = rated oil capacity under separator condition , bbl/day • @KOU 2024-2025 DPTE ๐ก = ๐๐๐ก๐๐๐ก๐๐๐ ๐ก๐๐๐, ๐๐๐๐ข๐ก๐ 4.16 Separation Design 41 A- Capacity of vertical Separators: • For oil and gas capacities calculations can determine inside diameter of separator. Height of gas section ( gas section volume), height of oil section (oil section volume), and them separator volume ( gas section + oil section). • The volume ( Size, d) of vertical separator can be estimated approximately (ignore temperature, gas density and some factors effects), if the following data are known: 1. Operating pressure. 2. Oil gravity (API). 3. Gas capacity ( daily gas production MMcf/day) and By figure below determine diameter (d). @KOU 2024-2025 DPTE Separation Design 42 A- Capacity of vertical Separators: 2. Oil Capacity: @KOU 2024-2025 DPTE Estimate diameter of vertical separator Separation Design 43 A- Capacity of vertical Separators: • Note: • ๐ถ๐๐๐๐๐๐ก๐ฆ ๐๐ ๐ฃ๐๐๐ก๐๐๐๐ ๐ ๐๐๐๐๐๐ก๐๐ = 9.7 × 10−4 ๐2 , ๐๐๐๐๐๐ก๐๐ ๐๐ ๐๐๐โ. • ๐บ๐๐๐๐๐๐๐๐ฆ โ๐๐๐โ๐ก ๐๐ ๐๐๐ ๐ ๐๐๐ก๐๐๐ = โ๐ = 2 ๐ • ๐ธ๐ ๐ก๐๐๐๐ก๐๐๐ โ๐๐๐โ๐ก ๐๐ ๐๐๐ ๐ ๐๐๐ก๐๐๐ = โ๐ • Volume of oil section ๐๐ = ๐๐๐ ๐๐๐๐๐ข๐๐ก๐๐๐ ๐๐๐ก๐ × ๐๐๐ก๐๐๐ก๐๐๐ ๐ก๐๐๐ • โ๐๐๐โ๐ก ๐๐ ๐๐๐ ๐ ๐๐๐ก๐๐๐ = โ๐ = ๐๐ , ๐๐๐Τ๐๐๐๐๐๐๐ก๐๐ ๐๐๐๐๐๐๐ก๐ฆ ๐๐๐/๐๐ก • Height of vertical separator = ๐ป = โ๐ + โ๐ @KOU 2024-2025 DPTE Separation Design 44 A- Capacity of vertical Separators: Example 4.1: Calculate gas and oil rated capacity for vertical separator, use the following data: @KOU 2024-2025 DPTE ๐ณ = ๐๐ ๐๐ ๐จ๐ท๐ฐ = ๐๐° ๐๐ = ๐, ๐๐ ๐๐ ๐ท = ๐๐๐ ๐๐๐ ๐ = ๐๐ ๐๐ ๐ป = ๐๐ โ ๐ธ๐ = ๐. ๐ ๐ = ๐. ๐๐๐ ๐=๐ ๐ = ๐ ๐๐๐๐๐๐ Separation Design 45 A- Capacity of vertical Separators: Example 4.1: Solution: 1- Gas Capacity: ๐๐ ๐๐ = 67824 × 10 −6 2 ๐ ๐ ๐๐ − ๐๐ 0.5 ๐ ๐๐ ๐ ๐๐ ๐ ๐ ๐๐ ๐ 141.5 3 − 131.5 โซ ๐พ = 0.8017 โซ ๐ = 0.8017 × 62.4 = 50.02 ๐ผ๐/๐๐ก ๐ ๐ ๐พ๐ ๐๐๐ค๐ก ๐ ๐๐๐๐๐ ๐พ๐ 400 ×0.8×29 3 ๐ด๐๐ผ = ๐๐ = ๐๐ ๐ = ๐๐ ๐ = 1×10.73×520 = 1.66 ๐ผ๐/ ๐๐ก 50.02 − 1.66 −6 2 ๐๐ ๐๐ = 67824 × 10 (24/12) 0.167 1.66 ๐๐ ๐๐ =6.66 MMSCF/Day 1- Oil Capacity: ๐ 2 โ๐เต ๐๐ ๐ = 100.7 ๐ก (2)2 3.25เต ๐๐ ๐ = 100.7 1 = 1309 ๐๐๐/๐๐๐ฆ @KOU 2024-2025 DPTE 0.5 400 × 520 1 × 520 × 14.7 Separation Design 46 A- Capacity of vertical Separators: Example 4.2: Vertical separator has gas capacity = 100 MMcf/day, oil capacity = 7200 bbl/day, and operation pressure = 400 psi, API = 70°, t = 0.5 minute. What is the separator design (i.e. L &d)? @KOU 2024-2025 DPTE Separation Design 47 A- Capacity of vertical Separators: Example 4.2: Solution: 1- Use figure before to determine d, by P = 400 psi, API = 70°, Qg = 100 MMcf/day ๐ = 72 ๐๐๐โ โซโซ โ๐ = 2๐ = 2 × 72Τ12 = 12 ๐๐ก 2- Use equ. 4.16 to calculate โ๐ : ๐ 2 โ๐เต ๐๐ ๐๐๐ก๐ข๐๐ = 201.4 ๐ก 7200 = 201.4 (72Τ12)2 โ๐เต 0.5 โซโซ โ๐ = 0.5 ft ๐ณ = โ๐ + โ๐ @KOU 2024-2025 DPTE ๐ณ = 0.5 + 12 = 12.5 ๐๐ก Separation Design 48 A- Capacity of vertical Separators: Example 4.2: Solution: @KOU 2024-2025 DPTE Separation Design 49 B- Horizontal Separators Design: @KOU 2024-2025 DPTE Separation Design 50 B- Capacity of Horizontal Separators: 1. Gas Capacity: • Total section area: ๐ด๐ก = ๐ 4 ๐2 4.17 • Area of gas section = 1/2 total area ๐ด๐ = ๐ 2 ๐ 2 ๐ → ๐ด๐ = ๐ 8 4 ๐ 4.18 • From equation 4.18. : ๐ ๐ = ๐. ๐ ๐ • From equation (4.10): ๐๐ − ๐๐ ๐๐ ๐๐ = 67824 × 10−6 ๐๐2 ๐ ๐๐ 0.5 ๐ ๐๐ ๐ ๐ฟ 0.56 ๐ ๐ ๐๐ ๐ 10 4.19 • Where d = separator diameter @KOU 2024-2025 DPTE de = equivalent diameter L = height of separator, ft Separation Design 51 B- Capacity of Horizontal Separators: 2. Oil Capacity: a) Mono – Tube: ๐๐ 1440 ๐๐ ๐๐๐ก๐ข๐๐ = × ๐ก 5.615 ๐ ๐ฟ 2 ๐๐ = ๐ 4 2 4.20 4.21 • Substitute eq. (4.21) in (4.20) ๐ฟ ๐2 ๐๐๐๐๐ก๐ข๐๐ = 100.7 ๐ก • And: ๐๐ ๐ = 50.35 ๐ฟ ๐2 ๐ก 4.22 4.23 • Where: d = inside diameter of separator, ft qo = oil capacity bbl/day t = retention time, minute L = height of separator, ft , qor = rated oil capacity under separator condition bbl/day @KOU 2024-2025 DPTE Separation Design 52 B- Capacity of Horizontal Separators: 2. Oil Capacity: b) Dual – Tube: ๐๐ = ๐ ๐ฟ ๐2 4 4.24 ๐ฟ ๐2 ๐๐๐๐๐ก๐ข๐๐ = 201.4 ๐ก And: ๐๐ ๐ = 100.7 ๐ฟ ๐2 ๐ก 4.25 4.26 • Graphically the volume (size, d) of a horizontal separator can be estimated approximately, if the following data are known: 1. Operating pressure (psia) 2. Oil gravity (API) 3. Gas capacity (daily gas production, MMcf/day) 4. Liquid residence volume, bbl @KOU 2024-2025 DPTE And by figures below determine (d) Separation Design 53 B- Capacity of Horizontal Separators: 2. Oil Capacity: Estimate gas capacity of horizontal separator @KOU 2024-2025 DPTE Separation Design 54 B- Capacity of Horizontal Separators: 2. Oil Capacity: Estimate diameter of horizontal separator @KOU 2024-2025 DPTE Separation Design 55 B- Capacity of Horizontal Separators: Example 4.3: A mono tube horizontal separator has; ๐ณ = ๐๐ ๐๐ ๐จ๐ท๐ฐ = ๐๐° ๐ = ๐๐ ๐๐ ๐ท = ๐๐๐ ๐๐๐ ๐ธ๐ = ๐. ๐ ๐ป = ๐๐ โ ๐ = ๐. ๐๐๐ ๐ = ๐. ๐๐๐ ๐ = ๐. ๐ ๐๐๐๐๐๐ Calculate: 1. ๐๐ ๐ when t = 1 minute. 2. de for-gas section if 3. ๐๐ ๐๐ @KOU 2024-2025 DPTE Ag = 0.5 At. Separation Design 56 B- Capacity of Horizontal Separators: Example 4.3: Solution: 1. Oil Capacity: use equation 4.23: ๐ฟ ๐2 ๐๐ ๐ = 50.35 ๐ก (24/12)2 10เต ๐๐ ๐ = 50.35 1 = 2014 ๐๐๐/๐๐๐ฆ 2- use equation 4.18: ๐ ๐ด๐ก = (24/12)2 = 3.142 ๐๐ก 2 4 ๐ด๐ = 0.5 ๐ด๐ก ๐ด๐ = 1.571 ๐๐ก 2 ๐ 2 ๐ด๐ = ๐ >โซโซ ๐๐ = 1.414 ๐๐ก 4 ๐ @KOU 2024-2025 DPTE Separation Design 57 B- Capacity of Horizontal Separators: Example 4.3: Solution: 3. Use equation 4.19 to calculate gas capacity: ๐๐ − ๐๐ ๐๐ ๐๐ = 67824 × 10−6 ๐๐ 2 ๐ ๐๐ ๐ด๐๐ผ = ๐๐ = 0.5 ๐ ๐๐ ๐ ๐ฟ 0.56 ๐ ๐ ๐๐ ๐ 10 141.5 3 − 131.5 โซ ๐พ = 0.85 โซ ๐ = 0.85 × 62.4 = 53.03 ๐ผ๐/๐๐ก ๐ ๐ ๐พ๐ ๐๐๐ค๐ก ๐ ๐๐ ๐ = ๐๐๐๐๐ ๐พ๐ ๐๐ ๐ = 400 ×0.7×29 0.909×10.73×520 53.03 − 1.6 −6 2 ๐๐ ๐๐ = 67824 × 10 (1.414) 0.382 1.6 ๐๐ ๐๐ =8.49 MMSCF/Day @KOU 2024-2025 DPTE = 1.6 ๐ผ๐/ ๐๐ก 3 0.5 400 × 520 10 0.56 0.909 × 520 × 14.7 10 Separation Design 58 B- Capacity of Horizontal Separators: Example 4.4: Horizontal separator has Qg = 50 MMCF/day, Qo = 4320 bbl/day, P = 800 psi, API = 70°, and t = 1 minute. What is the separator design (i.e. L & d)? @KOU 2024-2025 DPTE Separation Design 59 B- Capacity of Horizontal Separators: Example 4.4: Solution: 1. Use figure ( before) to determine Ag, by P = 800 psi, API = 70° , Qg = 50 MMCF/day. Ag = 5 ft² 1. Use figure ( before) to determine d, by Ag = 5 ft², and Vo = qo * t = (4320*1)/1440 Vo = 3 bbl. d = 35 in , and L = 4d = 4*35 = 140 inch. @KOU 2024-2025 DPTE Separation Design 60 B- Capacity of Horizontal Separators: Example 4.4: Solution: @KOU 2024-2025 DPTE Separation Design 61 B- Capacity of Horizontal Separators: Example 4.4: Solution: @KOU 2024-2025 DPTE Separation Design 62 C- Spherical Separator Design No need @KOU 2024-2025 DPTE Separation 63 End of Lecture @KOU 2024-2025 DPTE
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