Licensed Copy: Mr. David Williams, National Weights and Measures, 20/03/2009 09:10, Uncontrolled Copy, (c) BSI BS 604:1982 ISO 4788:1980 BRITISH STANDARD CONFIRMED MARCH 1988 Specification for Graduated glass measuring cylinders [ISO title: Laboratory glassware — Graduated measuring cylinders] UDC 681.121.1:666.17 Licensed Copy: Mr. David Williams, National Weights and Measures, 20/03/2009 09:10, Uncontrolled Copy, (c) BSI BS 604:1982 Cooperating organizations The Laboratory Apparatus Standards Committee, under whose direction this British Standard was prepared, consists of representatives from the following: Agricultural Research Council Association for Science Education British Educational Equipment Association British Laboratory Ware Association* British Lampblown Scientific Glassware Manufacturers’ Association Ltd.* British Pharmacopoeia Commission Chemical Industries Association Department of Health and Social Security* Department of Industry (Laboratory of the Government Chemist)* Institute of Petroleum Ministry of Defence* Pharmaceutical Society of Great Britain Royal Society of Chemistry Scientific Instrument Manufacturers’ Association Society of Chemical Industry* Society of Glass Technology Standardization of Tar Products Tests Committee The organizations marked with an asterisk in the above list, together with the following, were directly represented on the Technical Committee entrusted with the preparation of this British Standard: Association of Clinical Biochemists Glass Manufacturers Federation Institute of Medical Laboratory Sciences Individual expert This British Standard, having been prepared under the direction of the Laboratory Apparatus Standards Committee, was published under the authority of the Board of BSI and comes into effect on 26 February 1982 © BSI 07-1999 First published April 1952 First revision February 1982 The following BSI references relate to the work on this standard: Committee reference LBC/27 Draft for comment 78/57109 DC ISBN 0 580 12515 7 Amendments issued since publication Amd. No. Date of issue Comments Licensed Copy: Mr. David Williams, National Weights and Measures, 20/03/2009 09:10, Uncontrolled Copy, (c) BSI BS 604:1982 Contents Page Cooperating organizations Inside front cover National foreword ii 1 Scope and field of application 1 2 References 1 3 Basis of adjustment 1 4 Class of accuracy 1 5 Types 1 6 Series of capacities 1 7 Definition of capacity 1 8 Accuracy 1 9 Construction 1 10 Graduation and figuring 2 11 Inscriptions 3 12 Visibility of graduation lines, figures and inscriptions 3 Figure 1 — General appearance of spouted measuring cylinder shown with integral base of hexagonal form 4 Figure 2 — General appearance of stoppered measuring cylinder shown with integral base of circular form 4 Figure 3 — Scales of measuring cylinders of capacity 5 to 100 ml 5 Figure 4 — Scales of measuring cylinders of capacity 250 to 2 000 ml 6 Table 1 — Series of capacities, divisions and tolerances 1 Table 2 — Dimensions 2 Publications referred to Inside back cover © BSI 07-1999 i Licensed Copy: Mr. David Williams, National Weights and Measures, 20/03/2009 09:10, Uncontrolled Copy, (c) BSI BS 604:1982 National foreword This British Standard, which has been prepared under the direction of the Laboratory Apparatus Standards Committee, is identical with ISO 4788 “Laboratory, glassware — Graduated measuring cylinders”, published in 1980 by the International Organization for Standardization (ISO) and supersedes the first edition published in 1952 which is now withdrawn. The principal differences between this edition and that of 1952 include the deletion of specified scale length, the recommendations on overall height being made mandatory, and an improvement in the stability on an inclined surface. Terminology and conventions. The text of the international standard has been approved as suitable for publication as a British Standard without deviation. Some terminology and certain conventions are not identical with those in British Standards; attention is especially drawn to the following. The comma has been used throughout as a decimal marker. In British Standards it is current practice to use a full point on the baseline as the decimal marker. Wherever the words “International Standard” appear, referring to this standard, they should be read as “British Standard”. Cross-references International standard Corresponding British Standard ISO 383:1976 BS 572:1960 Interchangeable conical ground glass joints (Technically equivalent) ISO 384:1978 BS 5898:1980 Specification for principles of design and construction of volumetric glassware for laboratory use (Identical) ISO 4794, referred to in 12.3, is in course of preparation. Since the reference is non-mandatory it does not affect the validity of this British Standard. A related standard to ISO 4794 is BS 3996:1978 “Specification for colour coding for one-mark and graduated pipettes (including requirements for the service performance of the colour coding enamels)”. A British Standard does not purport to include all the necessary provisions of a contract. Users of British Standards are responsible for their correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. Summary of pages This document comprises a front cover, an inside front cover, pages i and ii, pages 1 to 6, an inside back cover and a back cover. This standard has been updated (see copyright date) and may have had amendments incorporated. This will be indicated in the amendment table on the inside front cover. ii © BSI 07-1999 Licensed Copy: Mr. David Williams, National Weights and Measures, 20/03/2009 09:10, Uncontrolled Copy, (c) BSI BS 604:1982 1 Scope and field of application This International Standard specifies requirements for an internationally acceptable series of cylinders, with a graduated scale and either a pouring spout or a stopper, adequate for general laboratory purposes. The details specified are in conformity with ISO 384. 2 References Table 1 — Series of capacities, divisions and tolerances Nominal capacity Smallest scale division Maximum permitted error Maximum capacity corresponding to lowest graduation line ml ml ml ml 0,1 0,2 0,5 1 1 2 5 10 20 ± 0,1 ± 0,2 ± 0,5 ± 1 ± 1 ± 2 ± 5 ± 10 ± 20 0,5 1 2,5 5 10 20 50 100 200 ISO 383, Laboratory glassware — Interchangeable conical ground joints. ISO 384, Laboratory glassware — Principles of design and construction of volumetric glassware. ISO 4794, Laboratory glassware — Pipettes — Methods for assessing the chemical resistance of enamels used for colour coding. 5 10 25 50 100 250 500 1 000 2 000 3 Basis of adjustment 7 Definition of capacity 3.1 Unit of volume The capacity corresponding to any graduation line shall be defined as the volume of water at 20 °C, expressed in millilitres, contained by the cylinder at 20 °C when filled to that graduation line. The unit of volume shall be the cubic centimetre (cm3), for which the name millilitre (ml) may be used. NOTE The term millilitre (ml) is commonly used as a special name for cubic centimetre (cm3), in accordance with the International System of Units (SI). 3.2 Reference temperature The standard reference temperature, i.e. the temperature at which the cylinder is intended to contain its nominal volume (nominal capacity), shall be 20 °C. NOTE If the cylinder is required for use in a country which has adopted a standard reference temperature of 27 °C (the alternative recommended in ISO 384 for tropical use), this value shall be substituted for 20 °C. 4 Class of accuracy One class of accuracy only is specified, the accuracy being lower than that associated with items of volumetric glassware intended for analytical use. NOTE If, exceptionally, the reference temperature is 27 °C, this value shall be substituted for 20 °C. When checking the capacity of a cylinder, the meniscus shall be set so that the plane of the upper edge of the graduation line is horizontally tangential to the lowest point of the meniscus, the line of sight being in the same plane. 8 Accuracy Errors in capacity shall not exceed the maximum permitted errors shown in Table 1. These errors represent the maximum permissible error at any point and also the maximum permissible difference between the errors at any two points. 9 Construction 5 Types 9.1 Material Cylinders shall be provided either with a pouring spout (see Figure 1), or with a ground neck (see Figure 2) and a suitably fitting stopper. The cylinders shall be constructed of glass of suitable chemical and thermal properties, shall be as free as possible from visible defects and shall be reasonably free from internal stress. 6 Series of capacities The series of capacities of graduated measuring cylinders shall be as shown in Table 1. NOTE If capacities of cylinders other than those listed in Table 1 are required, it is recommended that they conform to the essential requirements of this International Standard. © BSI 07-1999 9.2 Wall thickness The cylinders shall be sufficiently robust in construction to withstand normal usage and the wall thickness shall show no gross departure from uniformity. 1 Licensed Copy: Mr. David Williams, National Weights and Measures, 20/03/2009 09:10, Uncontrolled Copy, (c) BSI BS 604:1982 9.3 Stability 10 Graduation and figuring The cylinders shall stand vertically without rocking or spinning when placed on a level surface. They shall not topple when placed empty (without stopper, if provided) on a surface inclined at an angle of 15° to the horizontal. 10.1 Graduation lines 9.4 Base The base shall be of glass, or a suitable plastics material, and may be either circular or of other suitable form provided the cylinder satisfies the requirements of 9.3. 9.5 Rim and spout 9.5.1 The rim of the cylinder shall be fire-polished and shall lie in a plane at right angles to the axis of the cylinder. 9.5.2 The spout of a spouted cylinder shall be so formed as to enable the contents of the cylinder to be poured out in a narrow stream without spilling or running down the outside of the cylinder. 9.6 Neck and stopper On a stoppered cylinder, the neck shall be ground to a suitable socket size preferably selected from ISO 383. A well fitting stopper of glass or suitable inert plastics material shall be supplied. 9.7 Dimensions The cylinders shall comply with the dimensional requirements shown in Table 2. Table 2 — Dimensions Capacity Internal height to highest graduation line min. Overall heighta max. Distance from highest graduation line to top of cylinder or base of neck min. ml mm mm mm 5 10 25 50 100 250 500 1 000 2 000 55 65 85 110 145 200 250 310 380 115 140 170 200 260 335 390 470 570 20 20 25 30 35 40 45 50 50 a In the case of a stoppered cylinder, the “overall height” shall be considered to be height to the base of the neck (see Figure 2). 2 10.1.1 Graduation lines shall be clean, permanent uniform lines of thickness not exceeding: 0,3 mm for cylinders of nominal capacity 5 and 10 ml; 0,4 mm for cylinders of nominal capacity 25, 50, 100 and 250 ml; 0,5 mm for cylinders of nominal capacity 500, 1 000 and 2 000 ml. 10.1.2 All graduation lines shall lie in planes at right angles to the longitudinal axis of the cylinder. 10.1.3 Graduation lines may be omitted from the bottom portion of the cylinder, but the ungraduated capacity shall not exceed the maximum value specified in Table 1. 10.2 Spacing of graduation lines There shall be no evident irregularity in the spacing of the graduation lines. 10.3 Length of graduation lines 10.3.1 The length of the short lines shall be not less than 10 % and not more than 20 % of the circumference. 10.3.2 The length of the medium lines shall be approximately 1,5 times the length of the short lines and they shall extend symmetrically at each end beyond the ends of the short lines. 10.3.3 The length of the long lines shall be not less than twice the length of the short lines and they shall either extend symmetrically at each end beyond the ends of the short lines or, if they extend almost completely round the circumference of the cylinder, they shall be so disposed that the gaps in them are situated vertically above one another and at one side of the cylinder when it is viewed from the front in the position of normal use. 10.4 Sequence of graduation lines 10.4.1 On cylinders of capacities 5 ml, 50 ml, 100 ml and 1 000 ml: a) every tenth graduation line shall be a long line, reading the scale from the top; b) there shall be a medium line midway between two consecutive long lines; c) there should be four short lines between consecutive medium and long lines. 10.4.2 On cylinders of capacities 10 ml, 250 ml and 2 000 ml: a) every fifth graduation line shall be a long line, reading the scale from the top; b) there shall be four short lines between two consecutive long lines. © BSI 07-1999 Licensed Copy: Mr. David Williams, National Weights and Measures, 20/03/2009 09:10, Uncontrolled Copy, (c) BSI BS 604:1982 10.4.3 On cylinders of capacities 25 ml and 500 ml: a) every tenth graduation line shall be a long line, reading the scale from the top; b) there shall be four medium lines equally spaced between two consecutive long lines; c) there shall be one short line between two consecutive medium lines and between consecutive medium and long lines. 10.5 Position of graduation lines The graduation lines shall form a vertical scale on the cylinder. On a spouted cylinder the spout shall be to the left when the cylinder is positioned with the scale facing the viewer, as shown in Figure 1. 10.6 Figuring of graduation lines Graduation lines shall be figured as illustrated in Figure 3 and Figure 4 and in accordance with the following principles. 10.6.1 On a cylinder of 250 ml capacity, alternate long lines shall be figured from 20 to 240 with an additional figure 250; alternatively, alternate long lines shall be figured from 30 to 250 ml. On cylinders of 10 ml and 2 000 ml capacity, alternate long lines shall be figured. 10.6.2 On all cylinders except those of 10 ml, 250 ml and 2 000 ml capacity, every long line shall be figured. 10.6.3 The scheme of figuring shall be such that the figure representing the nominal capacity refers to the highest graduation line. 10.6.4 Figures shall be placed immediately above the long lines to which they refer and slightly to the right of the adjacent shorter lines. The figures shall alternatively be placed slightly to the right of the end of the line to which they refer in such a way that an extension of the line would bisect them. © BSI 07-1999 11 Inscriptions The following inscription shall be permanently marked on all cylinders: a) the symbol “cm3” or the symbol “ml” to indicate the unit of volume (see note to 3.1); b) the inscription “20 °C” to indicate the standard reference temperature; NOTE If, exceptionally, the reference temperature is 27 °C, this value shall be substituted for 20 °C. c) the letters “In” to indicate that the cylinder has been adjusted to contain its indicated capacity; d) the maker’s and/or vendor’s name or mark; e) in the case of a cylinder with a standard interchangeable stopper, the size number of the joint, marked on both the cylinder and the stopper. It is recommended that, in the case of cylinders with non-interchangeable stoppers, an identification number should be marked on both the cylinder and the stopper. 12 Visibility of graduation lines, figures and inscriptions 12.1 All figures and inscriptions shall be of such size and form as to be clearly legible under normal conditions of use. 12.2 All graduation lines, figures and inscriptions shall be clearly visible and permanent. 12.3 The durability of graduation lines and inscriptions should be tested by the methods described in ISO 4794. 3 Licensed Copy: Mr. David Williams, National Weights and Measures, 20/03/2009 09:10, Uncontrolled Copy, (c) BSI BS 604:1982 Figure 1 — General appearance of spouted measuring cylinder shown with integral base of hexagonal form 4 Figure 2 — General appearance of stoppered measuring cylinder shown with integral base of circular form © BSI 07-1999 Licensed Copy: Mr. David Williams, National Weights and Measures, 20/03/2009 09:10, Uncontrolled Copy, (c) BSI BS 604:1982 Figure 3 — Scales of measuring cylinders of capacity 5 to 100 ml © BSI 07-1999 5 Licensed Copy: Mr. David Williams, National Weights and Measures, 20/03/2009 09:10, Uncontrolled Copy, (c) BSI BS 604:1982 Figure 4 — Scales of measuring cylinders of capacity 250 to 2 000 ml 6 © BSI 07-1999 Licensed Copy: Mr. David Williams, National Weights and Measures, 20/03/2009 09:10, Uncontrolled Copy, (c) BSI BS 604:1982 Publications referred to See national foreword. © BSI 07-1999 Licensed Copy: Mr. David Williams, National Weights and Measures, 20/03/2009 09:10, Uncontrolled Copy, (c) BSI BS 604:1982 ISO 4788:1980 BSI — British Standards Institution BSI is the independent national body responsible for preparing British Standards. 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