Design and development of sensors, measurement systems, and measurement methods in the NDE 4.0 framework. More info about this article: https://www.ndt.net/?id=29302 Alessandro Sardellitti1 1 Department of Electrical and Information Engineering, University of Cassino and South- ern Lazio, Cassino, Italy E-mail: alessandro.sardellitti@unicas.it Abstract The concept of Industry 4.0 has revolutionized the manufacturing sector by integrating advanced technologies, real-time monitoring and data analysis to improve production processes. This thesis highlights the critical role of quality control in Industry 4.0, employing IoT sensors, artificial intelligence and data analytics for early defect detection. The focus is on continuous and comprehensive inspection using Non-Destructive Testing and Evaluation (NDT&E) methods. This thesis addresses the challenge of developing methodologies aligned to NDE 4.0, employing low-cost sensors for on-line and real-time measurements. In particular, the study explores eddy current methods for thickness estimation overcoming limitations through optimization techniques. Furthermore, the application of dimensional analysis is introduced to reduce the complexity of NDT&E problems. The research contributes valuable insights and methodologies for efficient quality control in the context of Industry 4.0. Keywords: NDT&E, NDE 4.0, Eddy Current Techniques, Dimensional analysis, Methods Development. 1 Introduction In recent years, production processes have developed increasingly stringent quality standards and there is a growing need to carry out not just spot inspections, but continuous and comprehensive checks on the produced samples. Quality control methods ensure that the products meets the specified parameters, minimizing variations and defects. The real strength lies in the early detection of defects; indeed, using IoT sensors, artificial intelligence and data analysis, deviations from design or project parameters can be quickly identified, preventing problems from arising and reducing waste [1]. Sensors and data analysis work together to predict maintenance and production needs, avoiding unplanned downtime that could interrupt production and compromise quality [2]. In the framework of quality control, Non-Destructive Testing and Evaluation (NDT&E) methods play a key role. The importance of NDT&E lies in its ability to detect defects, imperfections or irregularities that could compromise the performance of products or systems without altering the physical and chemical characteristics of the product being analyzed [3, 4]. Through the application of these methods, the integrity, safety and reliability of materials, components and structures is ensured. © 2024 The Authors. Published by NDT.net under License CC-BY-4.0 https://creativecommons.org/licenses/by/4.0/ https://doi.org/10.58286/29302 Many parameters can be analyzed using these methods. For example, geometrical parameters of the sample (e.g. thickness parameter) are indicative of how the mechanical forming process is performing (such as pressing processes, rolling etc.) and determines the structural characteristics of the produced sample [5,6]. Another application is the analysis of the chemical characteristics of the sample. For instance, the electrical conductivity determines the quality of the part in the molding (in the case of metallic materials) and curing (in the case of composite materials) processes [7, 8]. In addition, parameters that indicate the degradation of the sample are crucial; an example is the loss of material that occurs in the case of corrosion processes [9]. All these parameters determine the quality and remaining lifetime of the sample under analysis. These issues have been studied within the NDE community for a long time and there are now many technologies and methodologies that provide good accuracy. The challenge that this research project aims to solve is to identify methodologies that are in line with the context of NDE 4.0. This context is made of low-cost sensors, easily integrated into automated measurement systems and optimized measurement time and processing [10, 11]. The challenge of the research activity has been to develop sensors, measurement systems, and methodologies that have the purpose of applicability in the NDE 4.0 context. In Section 2 the study of the geometric parameters of greatest interest in the industrial and research area has been realized. In this context, the thickness of metallic samples was observed to be an important parameter in the context of industrial quality control. Two different methods based on Eddy Current Techniques (ECT) have been developed in order to apply this techniques in industrial environment with low measurement time and good accuracies. Finally, in Section 3 the application of the dimensional analysis on NDT&E framework has been described. This methodology can systematically reduce the analysis complexity of the problems by decreasing the number of variables involved. For instance, the reduction of the number of variables has a major impact when a physical problem is modelled either via a numerical approach or via a machine learning approach. 2 Eddy Current methods for thickness estimation of metallic plates: proposed optimizations Thickness measurements have a key role in many industrial applications related to metallic plates because they provide information about the quality of both the manufacturing process and the realized product in term of structural strength and elasticity. These aspects are fundamental in all those application fields, such as in automotive and aerospace, where the integrity of the metallic plates components has a direct impact on the safety of human beings. In the industrial practice, some metrological checks are carried out by using touch-trigger probes, laser-based measurement methods, ultrasound methods [12]. These measurement methods are characterized by high measurement times, high cost of the instrumentation and nonintegrability within automated measurement systems. Several research groups are investigating the possibility offered by ECT, which typically assure low costs, simple probes, and easy integration to online, real-time, and automated measurement systems. Inside the broad field of the ECT proposed in the literature, there are several methods that allow the estimation of thickness by means of a multi-frequency analysis or pulsed eddy current analysis [5, 13, 14]. In particular, in [5,13], Yin et al. proposed and optimized measurement probes and processing algorithms suitably developed for non-magnetic materials able to give accuracy compatible with industrial quality standards and a good robustness to lift-off variations. In detail, using different combinations of coils to perform the generation and detection of the excitation and reaction magnetic flux respectively, Yin et al. compared measurements performed both in air and on the sample under test to estimate the thickness of planar samples. Although the methods proposed [5] appear to be promising, they have some limitations in terms of applicability in the aforementioned context of real-time, in-line measurements with good, constant measurement accuracy over the entire range of thicknesses analyzed. Firstly, the method proposed in [5] relies on the constancy of a certain parameter (α0 ). Unfortunately, this parameter is highly dependent on the thickness of the sample, and it can be maintained constantly only asymptotically for thicknesses much smaller than the size of the probe (see Eq. 1 and Figure 1). This makes the method impractical for thick samples or in the presence of curved surfaces. For instance, in the latter case, there are two conflicting constraints: (i) the probe has to be much larger than the thickness of the sample and (ii) the probe has to be much smaller than the curvature of the sample, so as to approximate the surface of the sample by means of its tangent plane, in a neighborhood of the probe itself. α(∆) = σ µ0 ωmin ∆ . 2 (1) ( ) [1/m] 1000 800 600 400 200 0 0 5 10 [mm] 15 20 25 Figure 1: Complete behaviour of α(∆) for a defined probe (blue line), together with its constant approximation (α0 = 126.28 m−1 ) valid for small ∆/D (black line) [6]. Secondly, in [5, 13], the key feature for estimating the thickness of plates is the value of the frequency where a proper quantity achieves its minimum value (∆R/ω). To get proper accuracy in measuring the thickness of the sample under test, this minimum needs to be located in an accurate manner. In turn, this requires several measurements at different frequencies with high frequency resolution which makes the approach time-consuming and not suitable for almost real-time applications. In order to solve the first limitation, in [6] was provided a deep, complete, and more general theoretical framework for the method proposed in [5], allowing it to be extended to a broader class of thickness measurements. From the technical perspective, it was proved that the critical constant parameter α0 has to be replaced by a new function α = α(∆) , which depends on the thickness (∆). With this “minimal ”modification, the method’s range of applicability was extended while identifying its underlying physical limit. Two algorithms were developed to make the optimal use of the identified variable α = α(∆). The first algorithm is iterative and is conceived for applications where the unknown thickness ranges from 0 up to the theoretical limit of the method (see Figure 2). The second algorithm is based on a polynomial approximation of α(∆) and provides the thickness as the solution of an algebraic equation of the same degree as the approximating polynomial (see Figure 3). Figure 2: Schematic representation of the developed iterative algorithm and the respective graphic representation [6]. Figure 3: Schematic representation of the developed algebraic algorithm [6]. For the second limitation, in [15] was proposed a strategy with a multi-tone and interpolation combination. In particular, a multisine excitation signal approach was applied to collect the data onto a proper set of frequencies then appropiate techniques were applied in order to interpolate the data at all the frequencies required to locate accurately the minimum of the response (see Figure 4). The combination of the multisine signal to allocate efficiently the measurement frequencies with the data interpolation results in a reduction of the number of required measurements and, in the ultimate analysis, of the overall measurement time. Figure 4: Graphic representation of the developed strategy with a multi-tone and interpolation combination [15]. A suitable experimental set-up was realized to allow the excitation and acquisition of the signal of interest and to show experimentally the performance obtained with the proposed methods [6,15]. In Figure 5 is represented the block diagram experimental set-up (more information are available in [6]). Tests were carried out on samples with different conductivities and thicknesses as shown in Table 1. Figure 5: Schematic block diagram of the experimental set-up [7]. Table 1: Characteristics of the considered case studies [6]. Name code Metal alloy #a #b #c #d #e #f EN AW-1050A EN AW-1050A EN AW-1050A EN AW-1050A EN AW-1050A 2024T3 Nominal thickness [mm] 0.469 1.035 1.969 2.912 3.994 2.003 Electrical conductivity [MS/m] 35.4 35.3 35.0 35.3 34.5 18.8 Plate dimensions [cm x cm] 13 x 18 25 x 25 25 x 50 25 x 25 25 x 25 20 x 20 Thickness estimation performance has been compared in terms of the Relative Thickness Error (RTE), defined as: ∆e − ∆a RT E = · 100 (2) ∆a where ∆a is the actual thickness of the sample and ∆e is the estimated thickness. Figure 6 (a) summarizes the obtained experimental results for the configurations of Table 1 applying the iterative and the algebraic algorithms. As expected, the smallest RTEs were observed by adopting the best α value related to the considered nominal thickness, with RTEs lower than 1% except for the sample #a, for which an RTE of 1.35% was found. For the original approach of [5], the RTE significantly worsened, rising to 14%. The smallest error (2.68%) is obtained for a thickness equal to 1 mm. On the other hand, the new approaches yield an excellent performance. Indeed, the RTEs are always lower than 2.5% and, in several cases, are comparable with the “ideal” values obtained by using the a priori knowledge of α(∆), i.e. the thought experiment. About the experimental performance obtained applying the developed strategy with a multitone and interpolation combination, different kind of interpolating polynomial have been analyzed. In particular were analyzed classic interpolating polynomial and piecewise interpolating polynomial: Fourth Order Interpolating Polynomial (FOIP), Fourth Order Chebyshev Interpolating Polynomial (FOCIP),Modified Akima Interpolator Polynomial (MAIP) and Piecewise Cubic Hermite Interpolator Polynomial (PCHIP). Figure 6: Obtained experimental results applying (a) the developed iterative and the algebraic algorithms and (b) the developed strategy with a multi-tone and interpolation combination. From the results shown in Figure 6 (b), it is possible to note how the maximum RTE is about 4% (accuracies in line with the reference methods). In the other hand, the measurement time for a typical situation was reduced from 13 to 2.66 seconds with a similar level of accuracy to that represented in [5]. 3 Introduction of dimensional analysis in Nondestructive Testing and Evaluation Problems related to NDT&E typically involve several variables. As a matter of fact, the result of an NDT&E test depends on (i) the probe’s parameters (geometry, materials, ...), (ii) the geometrical and the physical characteristics of the sample under testing (e.g. thickness, electrical conductivity, magnetic permeability etc.) and (iii) the parameters describing the geometrical relationship between the probe and the sample under testing (e.g. lift-off, tilt angle etc.). From the experience gathered in this context [6, 15], the number of variables involved and the correlated nature of these variables (e.g., excitation frequency or electrical conductivity and thickness of the sample) make an NDT&E problem difficult to handle. In this context, dimensional analysis is a mathematical tool for analyzing problems involving physical quantities [16]. Dimensional analysis can be used to simplify complex equations by highlighting the fundamental quantities that describe a problem. Among the various tools available, the Buckingham’s π theorem represents a widely used tool in the literature [17, 18]. It states that a certain physical relation of n variables can be rewritten in terms of p dimensionless parameters, defined as π groups, where p = n − k, with k number of physical dimensions involved [19]. This research activity brought the application of the Buckingham π theorem to the NDT&E community for the first time [7, 20]. In particular, application of the ECT for the estimation of the thickness and the electrical conductivity has been analyzed. This specific application was chosen because the thickness estimation methods usually presented in the literature require a priori knowledge of the electrical conductivity of the metallic sample [5], which is not always known. In addition, the electrical conductivity of metallic material is a good feature to estimate the mechanical characteristics. In particular, the research activity has given to the NDT&E community these major contributions: (i) a proper relationship in terms of dimensionless groups among the measured quantity Figure 7: Eddy Current Probe placed on a conductive plate with its geometrical characteristics [7]. and the physical variables affecting it, in a frequency domain ECT experiment. It was assumed that the measured quantity is the self or mutual impedance of the probe. This assumption is not restrictive of the generality of the method; (ii) a method together with its algorithm counterpart for the simultaneous estimation of the thickness and electrical conductivity by using dimensionless groups. 3.1 Buckingham’s π theorem in the Eddy Current framework In literature, it is possible to find various kinds of Eddy Current Probe (ECP) which differ in shape and materials as well as different kind of operations, i.e. single frequency or multimodal measurements. In order to show the effectiveness of the proposed method we focus on a specific case, but all the reasoning below can be applied with few irrelevant changes to other cases. Specifically, for a double-coil ECP with a non-magnetic core, the measured quantity is ∆Ż = Żm,plate − Żm,air , i.e. the difference between the mutual-impedance of the coil when it is placed on the plate and when it is in air. The measured quantity, for a prescribed angular frequency ω, depends on several physical parameters ∆Ż = f (ω, σ , ν0 , ∆h, D, t, L0 , θ ) , N1 N2 (3) where σ is the electrical conductivity of the plate, ν0 the magnetic reluctance of the vacuum, ∆h the thickness of the plate, D a reference length for the probe, l0 the lift-off,θ the tilting of the probe w.r.t to the normal to the plate and N1 -N2 the number of turns of the excitation and receiver coil respectively. Furthermore, in the dimensionless vector t = (r1 /D, h/D) all the normalized geometrical parameters of the ECP are grouped, see Figure 7. The normalization length D is chosen equal to the external radius r2 of the probe. The Buckingham’s π theorem allows us to reduce the number of variables required to characterize the measured quantity. Applying this theorem, can be stated that there exist p = n − k dimensionless groups π1 , π2 , . . . , π p such that the original scalar equation can be cast in the form π1 = F (π2 , . . . , π p ) . (4) For the case of interest, all the variables can be expressed in terms of k = 3 fundamental dimensions that are: length, time and resistance. For this reason, Equation (3) can be recast in terms of p = 6 π groups, that are listed in Table 2. Since the aim is to retrieve the electrical conductivity and the thickness of the sample under test, given the probe, i.e. given θ , l0 and t, π4 , π5 and π6 are assumed to be known and we focus on π1 , π2 and π3 . Specifically, the relationship between dimensionless groups is r ∆Żν0 ωσ ∆h =F D , . N1 N2 ωD 2ν0 D (5) For given θ , l0 and t, Equation (3) becomes ∆Ż = f˜ (ω, σ , ν0 , ∆h, D) , N1 N2 (6) where f˜ is equal to f but with prescribed θ , l0 and t. Comparing Equation (5) and (6) it is possible to appreciate the impact of Buckingham’s π theorem. In fact, starting from a complex function of five real-valued parameters, we obtain a relationship involving only two real-valued parameters. In other words, function F can be easily characterized numerically or experimentally while the same task requires much more effort with respect to the function f . Furthermore, the function F can be represented in the plane (π2 , π3 ) and the inverse problem of interest is traced back to an analysis in this plane. This is the fundamental point leading to the inversion method presented in the next section. Assuming the functional form in (5), retrieving the electrical conductivity and the thickness of the plate means to solve the following equation F(π2 , π3 ) = π̄1 , (7) where π̄1 is the measured quantity at a prescribed angular frequency ω. Since the measured quantity (∆Ż) and the unknowns (σ , ∆h) are not mixing in the π groups, this task can be easily done by means of level curves of π̄1 . Specifically, it is possible to represent any real-valued function of π̄1 in the plane (π2 , π3 ). For example, we choose as features the real part Re{π̄1 }, the imaginary Im{π̄1 } , the modulus |π̄1 | and the phase π̄1 of π̄1 (see Figure 8). The solution of (7) is evaluated by putting the level curves of at least two features on the same (π2 , π3 ) plane. All the curves intersect in one point (π2∗ , π3∗ ). Hence, it is trivial to compute the unknowns as 2ν0 π2∗ 2 σ= , ∆h = Dπ3∗ . (8) ω D The method has been presented from the underlying concept to a successful experimental validation carried out on metallic plates with different thicknesses (from 1 to 4 mm) and electrical conductivities (from 17 to 58 MS/m) shown in Table 3 adopting the experimental set-up represented in Figure 5. The obtained experimental set-up are shown in Figure 9. From the results, it can be note that the maximum relative error in thickness estimantion is about 4% while in electrical conductivity estimation is about 2.5% The method can be applied to either single or multi-frequency data and its negligible computational cost makes it suitable for industrial in-line inspections. Table 2: Dimensionless groups, arising from Buckingham’s π theorem, for the case of interest. 0 π̄1 = N1∆NŻν 2 ωD π groups q ωσ π2 = D 2ν0 π3 = ∆h D π4 = lD0 π5 = t π6 = θ Figure 8: Level curves of Re{π̄1 }, Im{π̄1 }, |π̄1 | and π̄1 [20]. Table 3: Analyzed sample. Name code #a #b #c #d #e #f 4 Metal alloy Aluminium (2024-T3) Copper Aluminium (6061-T6) Aluminium (AW-1050A) Aluminium (AW-1050A) Aluminium (AW-1050A) Electrical conductivity [MS/m] 17.66 58.50 28.23 35.27 35.44 35.91 Thickness [mm] 2.03 0.98 1.97 1.03 2.93 3.98 Conclusions The proposed research activities in Non-Destructive Testing, particularly in NDE 4.0, have resulted in solutions for thickness measurements, electrical and magnetic parameters of metallic materials, and corrosion detection using Eddy Current methods. Two solutions for estimating metallic material thickness were proposed. The first optimized existing methods from scientific literature to meet industrial requirements, resulting in three combined methods achieving the needed accuracy (4%) over a broader thickness range (0.5 - 4 mm) and in less than 3 seconds. The second solution introduced dimensional analysis to NDT&E, reducing variables and ensuring excellent measurement performance for thickness and electrical conductivity estimation. Future developments include extending Buckingham’s π theorem to multi-layer structures, unknown liftoff problems, and magnetic materials. Application on anisotropic materials and data fusion strategies for corrosion studies are also considered, along with exploring electrical signatures in artificial intelligence algorithms. 5 Statement The presented work is based on the PhD thesis of Alessandro Sardellitti entitled “Design and development of sensors, measurement systems, and measurement methods in the NDE 4.0 framework. ”, which was submitted at University of Cassino and Southern Lazio in December 2023. Figure 9: Obtained experimental results for (a) thickness and (b) electrical conductivity estimation. References [1] P. Tambare, C. Meshram, C.-C. Lee, R. J. Ramteke, and A. L. 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