2600
8.43
8.41
8.30
8.28
8.02
8.00
7.72
7.70
7.68
7.58
7.56
7.54
2.50
2.50 DMSO-d6
dkurs-20191002-a1.ss.10.fid
2400
2200
2000
1800
1600
1400
1200
1000
800
600
400
200
2.00
2.02
2.01
1.08
2.03
0
16
15
14
13
12
11
10
9
8
-200
7
6
f1 (ppm)
5
4
3
2
1
0
-1
-2
-3
2600
7.58
7.56
7.54
7.72
7.70
7.68
8.02
8.00
8.30
8.28
8.43
8.41
dkurs-20191002-a1.ss.10.fid
2400
2200
2000
1800
1600
1400
1200
1000
800
600
400
200
8.7
8.6
8.5
8.4
8.3
8.2
8.1
8.0
f1 (ppm)
2.03
1.08
2.01
2.02
2.00
0
7.9
7.8
7.7
7.6
-200
7.5
7.4
7.3
9.5
8.5
8.0
7.5
1.99
1.00
1.99
9.0
2.00
1.99
8.6
8.5
8.4
8.3
7.0
8.2
6.5
8.1
6.0
5.5
8.0
5.0
4.5
7.9
4.0
3.5
7.8
3.0
7.7
2.5
2.0
7.6
1.5
1.0
ppm
1g
0.5
ppm
S58
7.726
7.724
7.721
7.705
7.701
7.689
7.686
7.684
7.586
7.582
7.566
7.551
7.547
8.030
8.025
8.020
8.008
8.004
7.998
8.315
8.309
8.307
8.293
8.289
8.286
8.448
8.443
8.438
8.426
8.421
8.416
70000
8.52
8.50
7.96
7.94
2.50
2.50 DMSO-d6
dkurs-20191002-B1.ls.10.fid
65000
60000
55000
50000
45000
40000
35000
30000
25000
20000
15000
10000
5000
16
15
14
13
12
11
10
9
4.03
4.00
0
8
-5000
7
6
f1 (ppm)
5
4
3
2
1
0
-1
-2
-3
7.96
7.94
8.52
8.50
dkurs-20191002-B1.ls.10.fid
1200
1100
1000
900
800
700
600
500
400
300
200
100
8.80
8.70
8.60
8.50
4.03
4.00
0
8.40
8.30
8.20
f1 (ppm)
8.10
8.00
-100
7.90
7.80
7.70
7.60
S50
7.960
7.939
8.518
8.498
-
BF4
I
400 MHz
DMSO-d6
F3C
8.5
8.4
8.3
8.2
8.1
10
9
8.0
7.9
ppm
4.051
8.6
4.000
8.7
3u
CF3
8
7
6
5
4
3
2
1
ppm