RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Doc. Class 1 /Cat: 2 RAS MARKAZ CRUDE OIL PARK GAS TESTING PROCEDURE B1 21 Apr 21 33 Issue for Approval Huang Xing Jude O Xing Hang A1 02 Sep 20 32 Issue for Review / Comments Huang X Jude O. Xing Hang REV DATE PAGES DESCRIPTION PP /CHK /APP Page 1 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Doc. Class 1 /Cat: 2 Table of Contents 1 GENERAL ..................................................................................................................................................... 4 2 PURPOSE..................................................................................................................................................... 5 3 SCOPE .......................................................................................................................................................... 5 4 CHANGES TO THE DOCUMENT ............................................................................................................... 5 5 ALARP ......................................................................................................................................................... 6 6 DEFINITIONS AND ABBREVIATIONS ..................................................................................................... 6 7 REFERENCE DOCUMENTS ........................................................................................................................ 7 8 ROLES AND RESPONSIBILITIES ............................................................................................................... 8 9 GAS TESTING ............................................................................................................................................11 9.1 9.2 9.3 9.4 9.5 9.6 9.7 9.8 9.9 9.10 SCOPE .......................................................................................................................................................... 11 POTENTIAL HAZARDS .................................................................................................................................... 11 GAS TEST REQUIREMENTS.............................................................................................................................. 12 TESTING INSTRUMENTS.................................................................................................................................. 14 COMBUSTIBLE GASES..................................................................................................................................... 15 TOXIC AND SUFFOCATING GASES ................................................................................................................... 17 OXYGEN DEFICIENCY ..................................................................................................................................... 18 GAS TESTER .................................................................................................................................................. 18 PRE-USER CHECKS ........................................................................................................................................ 18 GAS TESTING PROCESS .................................................................................................................................. 20 APPENDIX 1 – ATMOSPHERIC TESTING .......................................................................................................22 APPENDIX 2 – OXYGEN CONTENT TESTING ...............................................................................................23 APPENDIX 3 – FLAMMABLE GAS TESTING ..................................................................................................25 APPENDIX 4 - TOXIC GAS TESTING ..............................................................................................................27 APPENDIX 5 – HYDROCARBON VAPOUR NARCOTIC EFFECT ..................................................................29 APPENDIX 6 – DENSITY OF DIFFERENT GASES ...........................................................................................30 APPENDIX 7 – GAS TESTING CHECKLIST .....................................................................................................31 APPENDIX 8 – EXPLOSIVE RANGE AND GAS BEHAVIOUR ........................................................................32 A1 APPENDIX 9-CONFINEDSPACE CERTIFICATE………………………………………………………………………34 Page 2 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Doc. Class 1 /Cat: 2 REVISION CONTROL SHEET REV. NO. A1 DATE 02 Sep 20 PAGE NO. All Pages DESCRIPTION OF CHANGES First Issue B1 20 Apr 21 All Pages Second Issue Revised as per Company Comments This page records the revision status of this document NOTES: Revisions after first issue are denoted as follows: a) By a vertical line in the right-hand margin against the revised text and, b) By a triangle symbol for graphics, the revision number being denoted within the symbol. Revision symbols are positioned adjacent to the revision. Page 3 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 1 Rev. B1 Doc. Class 1 /Cat: 2 GENERAL Oman Tank Terminal Company (OTTCO) plans to build a new grassroots Crude Oil Storage Terminal at Ras Markaz, on the eastern Arabian Sea coast of the Sultanate of Oman. The proposed coastal site is located approximately 70 km south of DUQM. The site is approximately 130m above the sea level and terminates at a cliff edge with little or no coastal beach area at sea level. The size of the area available for terminal development is roughly 13 km2. The terminal is to be designed to provide a total gross storage capacity of up to 200 Million Barrels of crude oil (MMbbl). The Project will involve the design, construction and operation of offshore tanker loading / offloading facilities, onshore storage facilities and associated infrastructure, pipelines and roads. The facility is to be designed to handle the loading and offloading of crude oil from and to the following vessels: Suezmax; Very Large Crude Oil Carriers (VLCC); Ultra Large Crude Oil Carriers (ULCC). The principal modes of terminal operation will be: Tanker unloading into the Storage Facilities Page 4 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Tanker loading from the Storage Facilities Inter-tank transfers within the Storage Facilities Crude oil import by pipeline from Nahada Crude oil export by pipeline to Duqm Refinery Tank Crude Oil Blending Doc. Class 1 /Cat: 2 PURPOSE 2 A1 3 Rev. B1 The purpose of this procedure is to present the significance of the high level requirements for gas testing and define the key hazards and methods of testing. Gas testing is mandatory prior to work especially hot work, during purging operations, to investigate gas alarms, during entry into confined spaces, etc. being undertaken in a process or hydrocarbon area that carries a risk to personnel or equipment from exposure to explosive, flammable, toxic or life threatening vapours. Gas testing shall also be required in any other area where the above risks are considered to exist which are covered by EPC Contractor Permit to Work system. SCOPE This procedure applies to all personnel during pre-commissioning, commissioning, start-up, servicing and performing maintenance on machine, equipment and systems associated with the process line in which an unexpected ignition could occur if there is any heat source electrostatic discharge. This procedure specifies minimum requirements for the prevention of ignition from gases or hydrocarbon cloud. It is applicable for protecting all employees in EPC Contractor, Subcontractors and Vendors undertaking the projects from the hazards of gases, fumes, vapors and where Hydrocarbons, oil and gas are produced or treated and where presence of Toxic and combustible gases and Oxygen deficiency / enrichment possibility has been proven by the safe method of gas testing. 4 CHANGES TO THE DOCUMENT Responsibility for the upkeep of the Document shall be with EPC Contractor HSE Manager, the Custodian. Changes to this document shall only be authorised and approved by the Owner. Users of the Document who identify inaccuracy or ambiguity can notify the Custodian or his/her delegate and request changes be initiated. The Requests shall be forwarded to the Custodian. The Document Custodian should ensure review and re-verification of this procedure every 2 years. Page 5 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 5 Rev. B1 Doc. Class 1 /Cat: 2 ALARP ALARP is the acronym for ‘As Low As Reasonably Practicable’ which simplified means, ‘reducing the risk to a level at which the cost and effort (time and trouble) of further risk reduction are grossly disproportionate to the risk reduction achieved’. Full Compliance to EPC Contractor Standards and Procedures is a key element in achieving ALARP. 6 DEFINITIONS AND ABBREVIATIONS AGT : Authorized Gas Tester ALARP : As Low As Reasonably Practicable Authorized Employee : Is a person who uses the energy control procedure. Affected Employee Is a person who works in an area in which the energy control procedure has been implemented. Company : Oman Tank Terminal Company L.L.C. (OTTCO) Contract : The EPC Contract between Company and EPC Contractor Consultant (PMC) : Worley Parsons Engineering Pty Ltd (WP) Dangerous goods : Articles, chemicals, materials, or substances that are capable of posing a significant risk to health, safety, or property when transported by air EPC Contractor : China Petroleum Pipeline Engineering Co., Ltd. (CPP) Energize : Connected to an energy source or containing residual or stored energy Energy Isolating Device : Is a mechanical device that physically prevents the transmission or Energy Source : Entry Permit : IDHL : IPMT : Company Project Management Team comprising OTTCO and Consultant personnel. Energy Source : Any source of electrical, mechanical, hydraulic, pneumatic, chemical, thermal, or other energy HRA : release of energy. An energy source is any electrical, mechanical, hydraulic, pneumatic, gravitational, chemical, nuclear, thermal, or other energy source that could cause injury A written document provided by the worker that specifies the conditions of entry into a hazardous confined space Immediately Dangerous to Life or Health Health Risk Assessment Page 6 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 A1 7 Rev. B1 Doc. Class 1 /Cat: 2 JHA : Job Hazard Analysis LEL : Lower Explosive Limit MSDS : Material Safety Data Sheet NORM : Naturally Occurring Radioactive Material O&M : Operation and Maintenance Oxygen Deficiency : An atmosphere containing oxygen at a concentration of less than 19.5% by volume as measured by an oxygen measuring device. PPE : Personal Protective Equipment PPM : Parts Per Million PTW : Permit To Work SCBA : Self-Contained Breathing Apparatus SHOC : Safe Handling of Chemicals STEL : Short Term Exposure Limit Sub-contractor : Means any person or persons, firms, companies to whom any part of the work has been subcontracted (directly or indirectly) by EPC Contractor and the legal successors in title to each of these parties Shall : Indicates Mandatory requirement Should : Indicates that the requirement is strongly recommended to be adhered to TLV : Threshold Limit Value TRIC : Toolbox Risk Identification Card Vendor : Means a supplier of Goods and/or Equipment for the Facility and/or the Works including related documentation and services, where necessary, in connection with the installation, testing, commissioning and start up support of any such Goods or Equipment. UEL : Upper Explosive Limit REFERENCE DOCUMENTS RD 114/2001 : Law for the Conservation of the Environment and Prevention of Pollution RD 35/2003 : Oman Labour Law MD 286-2008 : The regulation of Occupational Safety and Health for the Establishments Page 7 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Doc. Class 1 /Cat: 2 5440-8710-SP-000-0002 : HSE Instruction to Contractor 9686-6160-PR-000-0001 : Project HSSE Plan 9686-6160-PR-000-0002 : Construction Environmental Management Plan 9686-6160-PR-000-0003 : Health Management Plan 9686-6160-PR-000-0004 : Security Management Plan 9686-6160-PR-000-0005 : Emergency Preparedness and Response Plan 9686-8130-PR-000-0001 : Commissioning Procedure 9686-6160-PR-000-0005 : Commissioning HSE Plan 9686-6160-PR-000-0006 : Incident Reporting & Investigation Procedure 9686-6160-PR-000-0008 : Permit To Work Procedure 9686-6160-PR-000-0008 : Risk Assessment and Management Procedure 9686-6160-PR-000-0017 : Environmental Monitoring Plan 9686-6160-PR-000-0012 : Audit and Inspection Procedure 9686-6160-PR-000-0013 : Fire Prevention Procedure OHSAS 18001/45001 : Occupational Requirements OHSAS 18002 : Guidelines for the implementation of OHSAS 18001 ILO Convention : Convention concerning Safety and Health in Construction Health & Safety Management System, Environmental Management System, Requirements ISO 14001 ILO Convention : Convention concerning Safety and Health in Construction ROLES AND RESPONSIBILITIES 8 A1 All affected personnel must be familiar with this procedure and Trained . If they do not understand something within the procedure they shall ask their line supervisor or Operations Team /Operations head to explain it. It is the line Supervisor’s Responsibility to ensure that all his subordinates have been adequately instructed and understood this procedure. Role The Deputy Project Manager Responsibility Ensure that the work is carried out as per this present document, where necessary. Ensure that a system is in place to train and to evaluate the competency of the designated gas testers. Page 8 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 HSE Manager A1 Commissioning Manager Permit Applicant Rev. B1 Doc. Class 1 /Cat: 2 Provide sufficient signs, barriers and flashing lights as appropriate to the area covered. Provide instruction with regard to the hazards and arrangements in place. To provide sufficient numbers of compatible and approved gas detection equipment on site. Planning the work, as far as practicable, to include contingency plans and arrangements. Adequate calibration and test equipment, with spare parts that can be fitted on site. Ensure sufficient numbers of Rescue equipment as required by the numbers of persons who may be exposed. Monitor the safety of all working practices. Custody of portable gas detection equipment and the training of the site designated gas testers. Ensure adequate and appropriate emergency plans and equipment are in place should an incident occur. Ensure all necessary tests are carried out as required by the Work site condition and as stated by the permit to work system upon completion of a specific risk assessment. Ensure supervision and Subcontractor management are familiar with this procedure and that all persons concerned are trained as well. Ensuring all the necessary gas checks have been identified and carried out prior to the issue of relevant Work Permits. Monitor site conditions and ensuring that persons who may be affected by this procedure are aware of the hazards and precautions to be taken. Arrange for the necessary training of personnel for testing, calibration and maintenance of records. Update this procedure as necessary. Ensure that routine calibration checks of all portable gas detectors are carried out in accordance with the manufacturers’ instructions. Ensuring that all persons working are aware of, and comply with the relevant points from this Safety Procedure. Communicate all activities with the HSE department and participate in SIMOPS activities. Define the gas testing requirements for the work Prepare the Job Safety Plan and indicate the frequency of gas testing Page 9 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Area Authority A1 Issuing Authority A1 Authorised Gas Tester Rev. B1 Doc. Class 1 /Cat: 2 Ensure a gas free test certificate / Confined Space Entry Certificate where scheduled tests readings are logged is attached to the work related PTW & JSA Complete the appropriate section for gas testing on the PTW Indicate the special gas detection equipment is required e.g. hydrocarbons in inert Tick the gases to be tested for on PTW. Verify that a gas free test certificate / Confined Space Entry Certificate where scheduled tests readings are logged is attached to the work related PTW & JSA. Indicate how often the test shall be repeated on PTW. State if continuous monitoring for gas is required during the work. Gives possible advise for safety assurance Agree requirements of gas testing with the Permit Applicant Agree the Job Safety Analysis. Ensure an authorised gas tester handles the activity Ensure all technicians under his supervision read and understand the procedures Comply with EPC Contractor Permit to Work System regarding gas testing requirements and frequencies Performs all Gas testing activities Complete a gas free test certificate / Confined Space Entry Certificate attached to the work related PTW & JSA - where scheduled tests readings are logged. Carryout ‘ad-hoc’ gas testing when required Enter gas test results and frequency of further tests on PTW and Confined Space Entry Certificate / Additional Gas Test sheet (if applicable), A1 NOTE: Authorised Gas tester to agree test results with area authority and enter into PTW. Permit Holder HSSE Supervisor Include gas testing requirements in the TRIC Agree gas test results Ensure compliance to gas testing requirements is adhered to Ensure correct type of gas detector is used for the gas testing activity Monitor the safety of all working practices. Ensuring that all necessary gas tests are carried out by AGT as required by the Work Permit System Page 10 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Maintenance/ Operations Staff 9 9.1 Rev. B1 Doc. Class 1 /Cat: 2 Ensure that work area is free of any dangerous gas. Ensure details of the area gas testing records are kept Ensure all PPE needed to carry out the job is used Ensure the emergency preparedness plan is in place and everyone knows what to do Comply with this procedure Ensure the procedures are read and understood Report every anomaly to the HSE department GAS TESTING Scope The scope of this procedure shall cover; - the hazards which gas testing shall address; - the requirements for gas testing; - typical testing instruments used; - the gas tester and; - pre-user checks The procedure shall make reference where appropriate to material located in other documents and provide links to those documents where necessary. 9.2 Potential Hazards Generally the potential hazards addressed by gas testing are; - Oxygen enriched atmosphere - Oxygen depleted atmosphere - Flammable or explosive atmosphere - Toxic atmosphere - Hydrocarbon enriched atmosphere (narcotic effect) Each of the above shall be addressed with a more detailed description in the Appendix. 9.2.1 Oxygen Enriched Atmosphere Atmospheres containing more than 21.5 % vol. oxygen shall be treated as oxygen enriched. Generally oxygen enrichment does not occur often as the source of the extra oxygen shall have to be introduced. Oxygen enriched atmospheres when mixed with hydrocarbons can result in explosive mixtures quicker than would be the case with normal air (20.8%). Page 11 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 9.2.2 Rev. B1 Doc. Class 1 /Cat: 2 Oxygen Depleted Atmosphere Atmospheres containing less that 20% vol. oxygen shall be treated as oxygen depleted. Such atmospheres can occur when gas freeing of purging has been carried out to remove hydrocarbons / toxics or air. The oxygen in the atmosphere shall have been normally replaced / diluted with an inert gas i.e. nitrogen. 9.2.3 Flammable Atmosphere Flammable or explosive atmospheres are those that contain mixtures when exposed to an ignition source will or may ignite and burn. Such atmospheres can be created when opening pipework or equipment that contains or has contained hydrocarbons. 9.2.4 Toxic Atmosphere Toxic atmospheres are those that contain concentrations of vapours that shall cause injury or death to humans. Such atmospheres may have sufficient oxygen to support life and insufficient flammable concentrations to cause explosions or fire, but may contain sufficient concentrations of the toxic to harm personnel. An example would be H2S or mercury. 9.2.5 Hydrocarbon Enriched Atmosphere Hydrocarbon enriched atmospheres are those where the concentrations of hydrocarbon vapours are sufficient to induce a narcotic effect on personnel inside the atmosphere. 9.3 A1 Gas Test Requirements The Confined space certificate shall be referenced to determine the frequency of gas testing and the specific work it is required for and it will be confirmed and validated by Area Authority. In general gas testing is required for the following types of work; Breaking containment Hot work in a process or hydrocarbon area Gas freeing and purging Confined space entry / work within a confined space Checking for suspected gas leaks Providing clearance for work activities A1 Use of diesel engines in a process / hydrocarbon area( Petrol Vehicles are not allowed in a process facility/Hydrocarbon area) Vehicle entry to a process / hydrocarbon area Page 12 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Doc. Class 1 /Cat: 2 Possible areas of frequent hydrocarbon drift 9.3.1 Breaking Containment Gas testing shall be required when containment is broken on any system containing hydrocarbon or toxic liquids / solids / vapours. Appropriate PPE and safety equipment i.e. SCBA, masks, face visors etc, shall be worn as necessary. The type of gas tested for shall be indicated on the PTW by the Area Authority in addition to the frequency of testing. Types of gas can include one or all of the following; Hydrocarbons H2S Mercury NORM 9.3.2 Hot Work in a Process or Hydrocarbon Area Hot work carried out in an area where hydrocarbons are present or can be present must be preceded by a gas test of the work site and adjacent areas to address the risk of fire and explosion caused by concentrations within the Lower Explosive Limits. The gas test shall be primarily for hydrocarbons and carried out in accordance with the specification of the Permit to Work. 9.3.3 Gas Freeing or Purging Gas freeing of pipework and equipment shall be carried out prior to work being undertaken on hydrocarbon or toxic system. The normal medium for gas freeing is an inert, nitrogen or water. During gas freeing processes using nitrogen the gas testing shall be to detect hydrocarbons in an inert atmosphere and requires the appropriate testing equipment to be used. 9.3.4 Confined Space Entry/Work within a confined space Spaces or vessels requiring entry by personnel to inspect or carryout work shall require to be tested prior to and during the work. Confined space gas testing shall be to determine whether the atmosphere within the space can safely support life. Tests shall be for oxygen content and hydrocarbons / toxics. 9.3.5 Checking for Suspected Gas Leak Small gas leaks in and around pipework and equipment may be detected using portable gas testing equipment. Page 13 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 9.3.6 Rev. B1 Doc. Class 1 /Cat: 2 Providing Clearance for Work Activities Work activities in hazardous area shall require that the atmosphere at the work site and in the surrounding areas is safe before permission is given to carry-out the work activity. 9.3.7 Use of Diesel Engines in a Process / Hydrocarbon Area The use of internal combustion engines (diesel driven) within a process or hydrocarbon area shall be subject to authorization and require gas testing in accordance with EPC Contractor permit to work system Diesel driven plant i.e. mobile cranes, air compressors etc, shall be subject to continuous gas monitoring while in use. The units shall also be subject to a gas test prior to starting. The gas test shall primarily be to check for hydrocarbons. 9.3.8 Vehicle Entry to a Process / Hydrocarbon Area Vehicles shall only be allowed into a process area if covered by a PTW. A PTW is not required for a hazardous area but gas testing is mandatory for both. Vehicles shall be subject to continuous gas monitoring while inside the area. The gas test shall be to check for an explosive or flammable atmosphere 9.4 Testing Instruments Gas testing shall only be carried out by authorized ‘gas testing’ personnel who have completed the 3rd Party training. The details of these personnel shall be registered with EPC Contractor. A1 Testing must be carried out using approved instruments. The following types will be in use by EPC Contractor: Multigas monitors (indication usually in %LEL or %Vol or ppm dependant on the gas being monitored) Explosimeters (indication usually in %LEL) Detector tubes (indication usually in ppm or volume) NOTE: When testing for mercury, NORM or hydrocarbons in an inert atmosphere specialist meters are required and the user shall be trained in its use. Page 14 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 9.4.1 Rev. B1 Doc. Class 1 /Cat: 2 Multi Gas Monitors Multigas monitors are capable of measuring a number of gases simultaneously. The gases monitored and displayed can include Flammable, Oxygen, Carbon Monoxide, Hydrogen Sulphide, Sulphur Dioxide, Chlorine, Nitrogen Dioxide, Ammonia, and Carbon Dioxide. The results are displayed continuously. The multigas meter is provided with a sample pump allowing for deep penetration testing of confined spaces and well cellars from a safe location. Audible and visual alarm is provided making the monitors suitable for deployment in the confined space or as perimeter guard for protection and warning. 9.4.2 A1 9.4.3 Explosimeter Monitors Explosimeter are provided to measure only ‘flammable’ gases. The monitor will provide a measurement of the immediate area from which the sample is taken, which can be remote if sample lines and probes are used. The reading is displayed on a meter by needle deflection. The sensitivity of the instrument is set by the control ‘knob’. The instrument shall only be used by personnel who have undertaken the appropriate 3rd Party Training. Detector Tubes Detector tubes are single ‘spot’ check devices for detection of gases in the direct vicinity of where the sample is taken. Different detector tubes are provided for different gases, the selection of the detection tube being dependent on the gas being detected. A ‘fixed volume1’ sample is drawn through the detector tube by a hand pump. The detector tubes are calibrated and the change in colour observed will indicate the concentration of the gas present. 9.5 Combustible Gases 9.5.1 Maximum Permissible Concentration The explosive, or flammability limits of gases and vapors, are normally expressed as a volume percentage range between Lower Explosive Limits (LEL) and Upper Explosive Limits (UEL). These levels vary for different compounds and it is the Lower Explosive Limit (LEL) that is used as a basis for the combustible gas test. The table below lists the LEL and UEL of some relevant gases: GAS LEL % UEL % Methane 5.30 13.30 Ethane 3.00 15.50 Butane 1.86 8.41 Page 15 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Pentane 1.30 7.80 Propane 2.10 9.30 Hydrogen 4.00 74.20 hydrogen sulfide 4.30 46.00 Acetylene 2.50 82.00 Ammonia 15.00 28.00 Doc. Class 1 /Cat: 2 For example, in an atmosphere containing Methane, a reading of 10 % LEL on the explosimeter dial indicates that the actual concentration in the air is 10 % of 5.3 = 0.53 % by volume. (See Figure 1 of this procedure.) Note that an explosimeter needs sufficient range of oxygen to give a true reading (more than 15% Volume).Unless otherwise stated in manufactures’ manual; Explosimeter to measure the % of LEL do not work correctly when the atmosphere contains less than 15% Oxygen. Before opening a vessel or pipe work to the atmosphere always ensure it is free from gases and hydrocarbon content. In case of O2 deficiency (less than 15%) such as gas freeing activities, gas testing shall be performed by Infra Red (IR) combustible gas detectors. Before gas testing of any pipeline, vessel or equipment , it is required to know about the fluid of that pipeline or equipment then to know about density of the specified gas which needs to be checked by gas testing. 9.5.2 Combustible Gas Detectors Combustible gas tests must be carried out using only gas detectors suitably calibrated for use with hydrogen and/or hydrocarbon gas mixtures. Meter readings are given as a percentage of the LEL of the combustible gas and it is the result which must be specified in the appropriate space of the Work Permit. Sludge or scale, within a vessel, gives off vapor when disturbed and/or heated, this fact must be borne in mind when testing for gas in a confined space to determine the suitability for entry. Before and after each series of tests, or up to a maximum of two-hours continuous use, the meter must be checked for minimum response, following the procedure in the instruction manual. Information and results from detectors must be reported to the Safety supervisor /Safety Engineer. Oils heavier than kerosene do not give off sufficient vapor at ambient temperature to be detected. Work places must, therefore always be visually inspected for the presence of such oils, and if present, they must be removed, or blanketed, to the satisfaction of Production/Site Superintendent and the Safety Authority. Information and results from detectors and any gas chromatography analysis must be reported to the person in charge of the installation and the Safety Authority for assessment. Water, or liquid hydrocarbons, must not be allowed to enter the instrument. When testing sumps or equipment where liquid could be present, a liquid trap must be fitted to the sample line. Warning: The calibration gas used should be as closed as possible from the potentially explosive atmosphere monitored. Particularly the reading of the explosimeter when sampling condensates vapors Page 16 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Doc. Class 1 /Cat: 2 might be over optimistic if methane is used as calibration gas (which is generally the case in gas processing plant). 9.5.3 Continuous Monitors There are various instruments available for the continuous monitoring of combustible gas atmosphere. Some instruments are designed as free-standing, self-powered units fitted with a portable diffusion head and flammable gas and vapor detectors. They are used with an alarm system. Gas concentrations up to 100 % LEL are indicated on a meter and the alarm is a penetrating audio signal, coupled with a flashing lamp. The level at which the alarm operates can be pre-set by internal adjustment. The monitor can be used for spot sampling with the addition of an aspirator. By the addition of an aspirator the monitor can be used for spot sampling. Warning: Combustible gas detectors are designated to detect gas in AIR. It is not possible for the instrument to give an accurate LEL reading in a steam, inert or oxygen deficient / enriched atmosphere. Special equipment ("Tank safe" monitor) or chemical detector tubes shall be used in such cases. 9.6 Toxic and Suffocating Gases 9.6.1 Maximum Permissible Concentration The toxic gases most likely to be encountered are Hydrogen Sulfide (H2S) and Carbon Monoxide (CO). The maximum concentrations of these toxic gases for entry are as follows: MAXIMUM CONCENTRATIONS OF TOXIC GAS (PPM) FOR ENTRY Gas Entry without Breathing Apparatus Hydrogen Sulfide (H2S) < 1 ppm 1 to 20 ppm > 20 ppm < 1 ppm 1 to 250 ppm > 250 ppm Carbon Monoxide (CO) Entry With Suitable Breathing Apparatus No Entry Purge and Retest There are two methods used for the detection of toxic gases: Portable Detectors, used for continuous monitoring. Detector Tubes, used to measure the concentration in a spot test. H2S is heavier than air so may concentrate in lower areas; it is resolvable in water or sludge, so it is essential to empty the vessels and containers before any entry to, or hot work activities Page 17 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 9.6.2 Rev. B1 Doc. Class 1 /Cat: 2 Portable Detectors (Continuous Monitoring) Some types of portable detectors allow the monitoring of hydrogen, carbon monoxide or sulfur dioxide content in the range 0 - 200 ppm by means of interchangeable sensor heads. The instrument gives audible and visual alarms, which are adjustable throughout the measuring range. There are two levels of alarm that produce different tones and visual LED indication for the Long Term Exposure Limit (LTEL) and Short Term Exposure Limit (STEL) values of the toxic gas being measured. The concentration is displayed on a meter in ppm. 9.7 Oxygen Deficiency Before entering a vessel or enclosed space, tests of the oxygen content of the atmosphere must be made. Tests must also be carried out whenever there is any doubt as to purity of the air within a vessel. Internal rusting of the metal in a closed empty tank, which has been unused for some time, may cause oxygen deficiency. Oxygen deficiency tests are carried out by: Oxygen Monitors - continuous checking. Multi-gas Detectors - spot checks. Clearance to enter a vessel or confined space without wearing breathing apparatus is only given when the concentration of oxygen in the atmosphere is in an acceptable level. Acceptable level of an atmospheric oxygen concentration is 20.9 percent. Although the OSHA recommended Oxygen level for entry is between %20 to %23 but we must note that the reduction or enhancement of oxygen may be reason for presence of toxic gas or other chemical reaction. 9.8 Gas Tester An Authorised Gas Tester (AGT) is a person who has passed the 3rd Party Gas Testing Course and holds a current Gas Testers Card, and has passed either a Permit to Work Signatories or Holders Course. 9.9 Pre-User Checks Before using a portable gas detector (with exception of detector tubes) the following shall be observed: Ensure that the gas detector ‘test’ is in date. Do not use a gas detector that is ‘out of test’ Check the gas detector for signs of damage. If damaged record and report the nature of the damage and exchange the gas detector for one that is undamaged (if possible) Before using the gas detector ensure the ‘battery’ is fully charged After switching on purge the gas detector with uncontaminated air Allow the gas detector to complete the ‘start-up sequence’ (if applicable) before use If the gas detector uses a calibration gas check that the reading is correct to the calibration gas Page 18 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Doc. Class 1 /Cat: 2 Follow all manufacturers safety instructions for use NOTE: If in doubt reference the Manufacturers O&M manual In both cases, the Authorised Gas Tester must: Gas test at the frequency stated on the Permit or Confined Space Entry Certificate. Fill in the result of the gas test on the Gas Test Record and Sign it. When a test result indicates that it is NOT safe to work, the Authorised Gas Tester must: Tell the Permit Holder to stop any current work. Tell the Permit Holder and Area Authority that it is not safe to work, and why, so that the problem can be dealt with. Page 19 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 A1 9.10 Rev. B1 Doc. Class 1 /Cat: 2 Gas Testing Process Permit Applicant Area authority Issuing Authority Identifies the gas Permit Holder Inspect the location testing requirements for the work Authorised Gas Tester with PA and Informs the Review And AA in case of any Agrees the additional requirements requirement Enter the requirements on the Permit to work Validate the PTW Authorizes the daily after inspecting PTW the work location, monitor of gas testing by AGT Ensure the Permit holder is informed of gas testing requirements Conduct daily TBT Enter the type of gases to be and Ensure all the tested and frequency of testing workers are trained on PTW (Commissioning& and safe to work Hydro carbon area)/CSC certificate PTWH HOT Work COLD Work Carries out Initial gas test each day in accordance with requirements using correct device Agree Gas test results with AA and AGT Carries out Initial gas test each day and IA will monitor the activity Carries out Subsequent gas test in accordance with requirements using correct device Maintain gas test Log Page 20 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Doc. Class 1 /Cat: 2 The process, as described below, shall be typical of the normal gas testing carried out EPC Contractor in accordance with the Permit to Work system. 1. The Permit Applicant shall identify the gas testing requirements for the work to be undertaken. The gas testing requirements shall be entered on the PTW 2. A1 The Area Authority shall review the gas testing requirements and agree or amend as required. For HOT Work permits a site visit is mandatory but for Cold work permits, it is recommended. Area Authority shall identify the gases to be tested for and the frequency of the gas testing after the initial test. The Area Authority shall authorise the PTW 3. The Permit Applicant shall ensure that gas testing requirements are clearly explained to the Permit Holder. These shall be included in the TRIC 4 The Area Authority /Issuing Authority shall enter the gases to be tested for and the frequency of testing on the PTW before validation (see 2 above) 5. Is the PTW a Hot work or a Cold work? The class of the permit shall dictate who undertakes the initial gas test for the work covered For Hot Work permits(Commissioning & Hydro carbon area) Authority/Issuing Authority will conduct the first gas test of each day. the Area NOTE: This ruling can be changed to allow the Authorised Gas Tester (if not an Area Authority) to conduct this test and requires the Area Authority authorisation and approval For Hot work and Cold work (Commissioning & Hydro carbon) permits an Authorised Gas Tester can conduct all gas tests 6. The Permit Holder shall witness the initial gas test and agree the result. 7. The Area Authority / Authorised Gas tester shall conduct all subsequent gas tests required by the PTW 8. The Authorised Gas tester shall maintain the gas testing log Page 21 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Doc. Class 1 /Cat: 2 Appendix 1 – Atmospheric Testing Atmospheric testing is required to evaluate the hazards of the permit space and for verification that acceptable entry conditions for entry into that space exist. Similarly where ‘hot work’ is to be undertaken which is adjacent to live plant Continuous gas testing shall be undertaken to evaluate the risk of hydrocarbon or toxic gas (throughout the life of HOT work activity). A1 Evaluation Testing The atmosphere of the permit space should be analysed using test equipment for the specific gases expected to be present to identify and evaluate any hazardous atmospheres that may exist or arise, so that appropriate procedures can be developed to conduct the required work safely. Evaluation and interpretation of the gas measurement data, and development of the procedure, should be done by, or reviewed by technically qualified personnel based on a Risk Assessment. Verification Testing The atmosphere of a permit space which may contain a hazardous atmosphere shall be tested, using the appropriate gas test equipment to evaluate conditions are safe, at the time of analysis, to commence the required work. Results of testing (i.e., actual concentration, etc.) shall be recorded on the Permit to Work (PTW). Measurement is by volume of the total atmosphere. Duration of Testing Measurement of values for each atmospheric parameter should be made for at least the minimum response time of the test instrument specified by the manufacturer. Testing Stratified Atmospheres When monitoring for entries involving a descent into atmospheres that may be stratified, the atmospheric envelope shall be tested a distance of approximately 4 feet (1.22 m) in the direction of travel and to each side. If a sampling probe is used, the entrant's rate of progress should be slowed to accommodate the sampling speed and detector response. Order of Testing A test for oxygen is performed first because most combustible gas meters are oxygen dependent and will not provide reliable readings in an oxygen deficient atmosphere. Combustible gases are tested for next because the threat of fire or explosion is both more immediate and more life threatening, in most cases, than exposure to toxic gases and vapours. If tests for toxic gases and vapours are necessary, they are performed last. Page 22 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Doc. Class 1 /Cat: 2 Appendix 2 – Oxygen Content Testing Oxygen content shall be determined by gas testing when considering the entry of personnel into a ‘permit required confined space’. The tests shall generally include the following Oxygen Deficiency At atmospheric level the normal atmospheric concentration of oxygen is 20.8% vol. Atmospheres containing less than 20% vol. oxygen are considered to be oxygen-deficient or hypoxic. NOTE: The oxygen content of air reduces as altitude increases, therefore locations at more than 1000 metres above sea level appropriate corrections should be made and appropriate precautions taken. Oxygen deficiency in an atmosphere can result in asphyxiation. A relatively small reduction in the oxygen level can lead to impaired mental ability and can provoke a feeling of euphoria or well being leading to an overoptimistic judgment of the situation. The effects generally occur without alerting the senses. Loss of consciousness can occur without warning. This can happen even in circumstances where only a person’s head is inside a confined space. Very low oxygen concentrations, below 10%, can lead to unconsciousness and death. Inhaling an atmosphere with no oxygen results in instant death. There is no panic or discomfort; death is swift and silent. Oxygen deficiency can result from: Displacement of air from low points in a confined space by heavier gases such as hydrocarbons or carbon dioxide; Purging of the confined space with an inert gas to remove flammable or toxic gases, fumes, vapours or aerosols; Naturally occurring biological processes that consume oxygen, which can occur in sewers, storage tanks, wells etc.; Leaving a vessel completely closed for some time, since the process of rust2 formation on the inside surface consumes oxygen; Increased levels of carbon dioxide evolving from limestone chippings associated with drainage operations; Burning and welding, which consume oxygen; Displacement of air during pipe freezing with liquid nitrogen; Gradual depletion of oxygen as workers breathe in confined spaces and where provision of replacement air is inadequate. Page 23 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Doc. Class 1 /Cat: 2 Any reduction in the oxygen level from the atmospheric concentration shall be accounted for or investigated, the risks assessed and appropriate measures taken. Entry into confined spaces containing 16 to 20% by volume oxygen shall not be allowed unless a Risk Assessment has been completed and approval has been obtained from the appropriate authority. Note: Newly fabricated or shot blasted carbon steel vessels are especially vulnerable to rusting CAUTION: This shall only be by exception, when the source of oxygen deficiency is understood and it is not practical to ventilate the confined space to atmospheric oxygen level. Atmospheres containing less than 16% vol. oxygen shall be treated in the same way as toxic atmospheres that are Immediately Dangerous to Life and Health (IDLH). Oxygen Enrichment At atmospheric level the normal atmospheric concentration of oxygen is 20.8% vol. Atmospheres containing more than 21.5 % vol. oxygen should be treated as oxygen enriched or hyperoxic. Oxygen enrichment will significantly increase flammability of clothing, grease and other combustible materials. Oxygen enrichment can result from: Leaks from oxygen containing equipment such as gas cylinders, valves, hoses and welding torches; Inadvertent use of oxygen instead of air for ventilation or breathing air; Deliberate addition of oxygen to increase the level of an oxygen deficient atmosphere. Any increase in the oxygen level above normal during confined space entry activities shall be investigated, a Risk Assessment completed and appropriate measures taken. The most common oxygen containing equipment is that used in gas cutting operations. Cylinders, gas hoses, valves and welding torches shall be handled with care and should be daily inspected for damage. Gas cylinders shall not be taken into confined spaces unless the risks have been assessed and appropriate authorisation is obtained from the Responsible Supervisor. If allowed into the confined space all such equipment shall be removed during breaks and at the end of the working day. Page 24 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Doc. Class 1 /Cat: 2 Appendix 3 – Flammable Gas Testing Flammable gas testing shall be carried out to detect accumulations of flammable vapours, fumes or dust which could ignite in the presence of a source of ignition. Flammable vapours or fumes typically result from: Materials previously processed or stored in the vessel or tank; Electrostatic build up resulting from the interaction of incompatible fluids. A1 Sludge or other deposits disturbed during cleaning; Material left under scale, even after cleaning; Material leaking through the tank floors; Material leaking from behind vessel linings (lagging, refractory etc.) or from vessel fittings such as tank floating roof pontoons and legs, instrument connections or pipes; Materials leaking from flanges or vents on process pipes running through the confined space, e.g. process tubes in a furnace combustion chamber; Vapour entering the confined space from nearby process plant that has not been effectively isolated or from nearby work that is not well controlled; Solvents brought into the space for cleaning, painting, dye penetration tests or in adhesives; Gases brought into the space / area for welding or gas cutting, including leakage from cylinders, valves and hoses; Contaminated firewater / process water used to wash the confined space and introduced by hoses; Vapour or fumes that build up in sewers, manholes, contaminated ground or excavations. A source of ignition can be any heat source having enough energy to ignite a flammable vapour air mixture, or to raise the temperature above the auto-ignition temperature. Possible ignition sources include: Open flames and sparks resulting from welding, gas cutting and grinding; Sparks or arcs produced by electrical equipment, lightning and electrostatic charges; Hot pipes or exhausts that can raise the flammable mixture above the auto-ignition temperature; Heat of friction during drilling, sawing or other cutting activities; Pyrophoric materials, e.g. iron sulphide in scale; Page 25 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Doc. Class 1 /Cat: 2 Thermite reactions from aluminium or other alloy tools striking against rusted iron or steel; Any highly reactive material capable of producing sufficient heat for combustion, for example: - Strong oxidising substances, such as hydrogen peroxide used in waste treatment facilities; - Chemicals that undergo self-accelerating exothermic reactions when a critical temperature is reached, such as ethylene oxide. The recommended approach to controlling flammable vapours in confined spaces or where ‘hot work’ is being undertaken is to eliminate all flammable materials from area before the work is undertaken. The objective should be no detectable flammable vapour, i.e. an explosimeter reading less than 1% LEL. WARNING: Confined space entry shall not be allowed into spaces where the flammable concentration is greater than 10% LFL. Page 26 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Doc. Class 1 /Cat: 2 Appendix 4 - Toxic Gas Testing Toxic gas testing shall be carried out to identify and detect toxic substances either in or adjacent to the confined spaces or other places of work. Substances can be solids, liquids or gases. Toxic vapours can cause injury, acute or long-latency illness, or death, depending on the characteristics of the substances, the concentration and the duration of exposure. For example, prolonged exposure to benzene can cause kidney damage or even leukaemia. Toxic hazards in confined spaces can result from the same sources as the flammable hazards. Common toxic substances in the oil and gas industry are: Acute toxic gases such as hydrogen sulphide, carbon monoxide, hydrogen fluoride, ammonia and chlorine; Hazardous liquids such as benzene, polycyclic aromatics, lead/anti-knock compounds, hydrazine and biocides; Narcotic gases and vapours such as butane, pentane, hexane, gasoline and gas condensate; Catalyst dusts, such as nickel, platinum, and molybdenum. Toxicity data for specific substances, e.g. Material Safety Data Sheets (MSDS) or Safe Handling Of Chemical Cards (SHOC), shall be required from the supplier of materials or from government authorities, and shall be made available on site. If these are not available, then a competent industrial hygienist shall assess the toxicity of the intermediates and products. Crude oil and refinery process streams are mixtures of many hydrocarbons that individually have significant toxic or narcotic effects. The Health Risk Assessment (HRA), as input to the Job Hazard Analysis (JHA), shall assess the hazards of the mixture in the situation / areas where persons could be exposed. Specifically, the HRA should make a recommendation on whether flammability measurements are sufficient to detect harmful levels of the potentially toxic substance. Different criteria may be needed for: Confirming that the atmosphere in the confined space is safe for entry, for planned work, and Requiring persons to leave the space in case of an increased level during the work Substances that are harmful by inhalation normally have an assigned Occupational Exposure Limit (OEL). An Action Limit of 50% of the published OEL shall be applied as the trigger for implementing specific measures for controlling exposure to the toxic substance during the confined space work, but the target should be to reduce the airborne concentration to ALARP. OEL data may not be available for some toxic dusts, sludge and other substances, in which case specialist occupational hygiene advice should be sought. Entry into confined spaces containing a concentration of toxic vapour, fume or dust between the OEL and the IDLH value shall be allowed only by exception when and it is not practical to ventilate the confined space or otherwise remove the hazard to reduce the toxic concentration. In this case it shall Page 27 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Doc. Class 1 /Cat: 2 only be allowed when the source, nature and concentration of the toxic hazard is understood and exposure is adequately controlled by other means. Entry into confined spaces containing a concentration of toxic vapour, fume or dust above the IDLH value shall not be allowed. The most notable toxic gas to be encountered in EPC Contractor activities during commissioning and startup is hydrogen sulphide (H2S). Allowable concentrations are related to the Threshold Limit Value (TLV) which represents the concentration to which a worker may be exposed without suffering adverse health effects. For the H2S the TLV is 10 ppm, for an 8-hour period. The short-term exposure level (STEL) for H2S is 15 ppm and is the concentration of H2S gas in air above which protective equipment must be used. Page 28 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Doc. Class 1 /Cat: 2 Appendix 5 – Hydrocarbon Vapour Narcotic Effect Testing for hydrocarbon vapour shall be carried out prior to / and during Confined Space Entry and at any time that hydrocarbon vapours are suspected of being present in or around a space, vessel or tank where personnel are working. Detection of hydrocarbon vapour is by the use of Drager Detection Tubes. Page 29 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Doc. Class 1 /Cat: 2 Appendix 6 – Density of Different Gases GAS Density (Air = 1) Ammonia Butane Carbon Dioxide Carbon Monoxide Ethane Ether (diethyl) Ethylene Ethylene Oxide Formaldehyde Hydrazine Hydrogen Hydrogen Cyanide (poison) Hydrogen Sulphide (poison) Methane Mathanol Methylamine Nitric Oxide Oxigen Propane 0.6 2.1 1.5 0.97 1.05 2.5 0.97 1.5 1.07 1.1 0.07 0.93 1.18 0.54 1.1 1.08 1.04 1.1 1.55 Page 30 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Doc. Class 1 /Cat: 2 Appendix 7 – Gas Testing Checklist No. Descriptio n 1 Are personnel trained in the use of gas detector equipment? 2 Are explosimeters only used when the level of oxygen is sufficient i.e. > 15 %? 3 Yes No N/A Comments Are personnel aware of where to take sample readings? 4 Are oxygen monitors with alarms worn by personnel who enter enclosed spaces? 5 Is a gas test performed before any hot work? 6 Is there a permanent gas detector (with alarms set at 25% LEL) when any hot work is performed within a vessel or an enclosed space? 7 Has the correct permit been issued? 8 Are oxygen levels checked sufficiently often for work in an enclosed space? 9 Are personnel aware of the dangers of oxygen enrichment? 10 Is there any possibility of the presence of H2S or CO? If so, is it being tested for? Page 31 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Doc. Class 1 /Cat: 2 Appendix 8 – Explosive Range and Gas Behaviour Gas Behaviour Page 32 of 33 RAS MARKAZ CRUDE OIL PARK PROJECT (PHASE1) GAS TESTING PROCEDURE Doc No: 9686-6160-PR-000-0040 Rev. B1 Doc. Class 1 /Cat: 2 Appendix 9 – Confined space certificate A1 Certificate No. Confined Space Certificate Work Permit No. 1. Details of Confined Space Site / Location: Equipment / Space to be Entered Sub -Contractor: Reason for Confined Space Entry: ………….............................................................................................................................................. …………………………………………………………………………………………………………………………………………………………………………………………………………… 2. Worksite Preparation and Control Measures (Items to be checked by Area Authority/Issuing Authority before Confined space entry can proceed and confirmed by signature in box 4&5) Control Measures Equipment/Vessel to be removed from service and isolated from all source of dangerous liquid, gases. Equipment / Vessel to be isolated from all source of energy Conduct Gas Testing for the confined space atmosphere Provide adequate access / Escape routes are provided Provide adequate ventilation Provide safe temporary lighting Specific HSE Requirement A rescue plan to be formulated and briefed to work team Safety harness and lifeline to be provided Provide warning sign for CSE Breathing Apparatus Air Moving equipment installed & Operational Lifelines & resuscitation equipment available Standby personnel Name: ……………………………………………………………………. Equipment Surrounding area checked and safe from hazards raising from other work/operations Isolation Certificates are attached Electrical Certificate No. Mechanical Certificate No. 3. Gas Testing GAS Oxygen Hydrocarbon LIMIT RESULTS 20 – 21% Vol. 0% LEL for Hot work, 4% LEL for Cold Work without BA, 10 LEL for Cold work with BA % % GAS H2S Carbon Monoxide LIMIT RESULTS 10PPM 50PPM PPM PPM Others AGT Name: …………………………………………… Sign: …………………………… Auth. No. .………………….. Date: ……………………… Time: …………………… Gas Test to be repeated at the intervals of ……….Hrs / Continuous Gas monitoring Required during the Execution of work Yes No Breathing Apparatus need to be worn 4. Authorization to Enter Confined Space by Area Authority (AA) I certify that the above results indicate that the Confined space covered by this certificate is safer to enter ,Gas Test to be repeated at the intervals specified as above 5. Issuing Authority (IA) 6. Permit Holder 7. Worksite Endorsement by Issuing Authority (IA) – Required every shift / Work Period Date Initial Date Initial (To be signed by the off going permit holder whenever work is suspended) Issuing Authority (IA) Permit Holder Issuing Authority (IA) Permit Holder Issuing Authority Permit Holder Issuing Authority Permit Holder Issuing Authority Permit Holder Issuing Authority Permit Holder Issuing Authority Permit Holder (IA) (IA) (IA) (IA) (IA) Certificate Closure 8. Closed and Permit Returned Permit holder Name: ……………………………………………………………… Signature: ………………………………………………………………………………. Date: ……………………………………………………………………………………… Area Authority (AA) Name: …………………………………………………… Signature: ………………………………………………………………………………. Date: ……………………………………………………………………………………… Page 33 of 33