Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group Engineered Composite Repairs: End User Good Practice Guide Version 1 A deliverable of the HSE Shared Research Project on Engineered Composite Repairs Authors: David Johnson HSE Science Division Matthew Blackburn HSE Energy Division Report Number: EM/19/53 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group Engineered Composite Repairs: End User Good Practice Guide Version 1 A deliverable of the HSE Shared Research Project on Engineered Composite Repairs Report authorised by: Report approved by: Date of Issue: Authors: End User/Customer: Technical Reviewer: Editorial Reviewer: Project number: Access control marking: Distribution list: Prof Andrew Curran BSc PhD FRSB FCMI Hon FFOM John Allen BSc PhD CChem MRSC 31st August 2020 David Johnson BEng MSc(Eng) MSc CEng MIMMM Matthew Blackburn MA CEng MIMechE SRP: Engineered Composite Repair Sponsor Group Adam Bannister BMet CEng FIMMM Paul McCann BEng CEng MIMechE PH15252 Commercial in Confidence: Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group SRP: Engineered Composite Repair Sponsor Group Disclaimer: This report and the work it describes were co-funded by the Health and Safety Executive (HSE) and the sponsors of the HSE Shared Research Project on Engineered Composite Repairs. Its contents, including any opinions and/or conclusions expressed, are those of the authors alone and do not necessarily reflect HSE policy. © Crown copyright 2020 Page 1 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group ACKNOWLEDGEMENTS This document was produced under the auspices of the HSE Shared Research Project on Engineered Composite Repairs. The project was sponsored by the following organisations. Their support is duly acknowledged: Shell U.K. Ltd Spirit Energy Ltd Sellafield Ltd EDF Energy Ltd TAQA Bratani Ltd Belzona Polymerics Ltd Henkel Ltd Rockrose Energy Plc Centrica Storage Ltd National Grid Plc Chrysaor Ltd TEAM Industrial Services Metalyte Pipeworks Ltd BSEE Page 2 of 56 CNOOC U.K. Ltd Total U.K. Ltd SGN Ltd Apache North Sea Ltd ICR Integrity Ltd Clockspring|NRI Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group CONTENTS ACKNOWLEDGEMENTS ............................................................................................. 2 GLOSSARY, ACRONYMS AND DEFINITIONS ................................................................ 5 1 2 3 4 5 6 INTRODUCTION ................................................................................................. 7 1.1 Background ............................................................................................................................. 7 1.2 Scope ....................................................................................................................................... 7 1.3 Purpose ................................................................................................................................... 7 1.4 Relevant Legal Requirements ................................................................................................. 8 SUMMARY OF KEY CONSIDERATIONS................................................................. 9 2.1 General.................................................................................................................................... 9 2.2 Key Considerations.................................................................................................................. 9 PHASE 1: DECISION MAKING PROCESS ............................................................. 14 3.1 General.................................................................................................................................. 14 3.2 Anomaly Identification and Characterisation ....................................................................... 14 3.3 Corrective Action .................................................................................................................. 14 3.4 Repair .................................................................................................................................... 15 PHASE 2: PRE-INSTALLATION ACTIVITIES .......................................................... 18 4.1 General.................................................................................................................................. 18 4.2 Assigning Roles and Responsibilities for Composite Repair Application .............................. 18 4.3 Supply of Input Data and Review of Repair Design .............................................................. 18 4.4 On-site Preparation and Organisation .................................................................................. 20 PHASE 3: INSTALLATION .................................................................................. 22 5.1 General.................................................................................................................................. 22 5.2 Repair Location Site Preparation .......................................................................................... 22 5.3 Repair Installation ................................................................................................................. 23 5.4 Inspection/Quality Assurance ............................................................................................... 24 5.5 Post Installation Tasks/Requirements .................................................................................. 24 5.6 Repair Completion Documentation ...................................................................................... 28 PHASE 4: ONGOING INTEGRITY MANAGEMENT ................................................ 29 6.1 General.................................................................................................................................. 29 6.2 Records.................................................................................................................................. 29 6.3 In-Service Inspection ............................................................................................................. 31 Page 3 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group 7 6.4 Ongoing Validity of Input Data.............................................................................................. 34 6.5 Life Extension/Life Reduction ............................................................................................... 34 6.6 Decommissioning and Removal ............................................................................................ 36 REFERENCES .................................................................................................... 37 APPENDIX A - ENGINEERED COMPOSITE REPAIRS: KEY CONSIDERATIONS................ 39 A1 General.................................................................................................................................. 39 A2 Surface Preparation .............................................................................................................. 39 A3 Defect / Leak Sealing ............................................................................................................. 44 A4 Cure ....................................................................................................................................... 45 A5 In-service Inspection ............................................................................................................. 46 A6 Training and Competency ..................................................................................................... 47 A7 Applications........................................................................................................................... 48 APPENDIX B – VISUAL INSPECTION CHECKLIST ........................................................ 51 APPENDIX C – NDT TECHNIQUE SELECTION CHART (PART A) ................................... 52 APPENDIX D – NDT TECHNIQUE SELECTION CHART (PART B) ................................... 53 APPENDIX E - NDT TECHNIQUE SELECTION CHART (PART C) .................................... 54 APPENDIX F – HOLD POINTS AND MANUFACTURING CONSIDERATIONS .................. 55 Page 4 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group GLOSSARY, ACRONYMS AND DEFINITIONS KEY TERMS Defined life The actual repair service lifetime. This is defined by the end user and is often informed by the shutdown or maintenance cycle of the repaired system. The defined life is less than or equal to the design life of the repair. Design life Maximum application lifetime of the repair. Job Responsible Coordinator An individual appointed by the operator to oversee the repair process. Pressure testing After repair application, pressure testing may be required. This could be to confirm the integrity of the repair, or, if a shutdown was required, to bring plant back into service. If a pressure test is required after a shutdown, it is paramount that the test pressure is communicated with the repair supplier and the repair is designed for the test pressure. Substrate The surface to which the repair is applied. Interface The bond between the laminate and the substrate. Laminate Part of a repair system that is the composite. Surface preparation Preparation of substrate prior to applying composite repair. Safety Critical Failure(s) that could cause or contribute substantially to a major accident; or a purpose of which is to prevent, or limit the effect of, a major accident. Page 5 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group ACRONYMS DLR Defined life repair DRS Dynamic response spectroscopy HSE Health and Safety Executive JRC Job Responsible Coordinator NDT Non-destructive testing PEC Pulsed eddy current (inspection technique) RBI Risk based inspection MIC Microbially induced corrosion P&ID Piping and instrumentation diagram QR Quick response – as in, QR code. RFID Radio frequency identification Page 6 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group 1 1.1 INTRODUCTION Background Over recent years there has been an increasing trend towards the use of composite repairs on impaired containment equipment. This has brought benefits in terms of improved integrity and reduced downtime. However, the risks associated with the application of such repairs have not always been correctly evaluated. Whilst the majority of repairs have been successful, there have also been failures. These have been attributable to a range of factors including poor installation practices, deficient design, inadequate specification and use in unsuitable applications. In 2017 a Shared Research Project sponsored by HSE, operators and repair suppliers was established to improve the collective knowledge and understanding of composite repairs. The project focussed on a number of key areas, such as: quality assurance and integrity management; inspection; inservice performance; and human factors. A key deliverable of the project was to identify and document agreed good practice to promote improved management of composite repairs throughout their lifecycle. As such, this document incorporates key learnings, insights and lessons learned identified as part of the project. 1.2 Scope There are two recognised standards for the design and installation of engineered composite repairs, ASME PCC-2 [1] and the standard that underpins this guide, BS EN ISO 24817 [2]. The scope of this document is primarily concerned with the external application of composite repairs to impaired pipework used in the petroleum, petrochemical and natural gas industries. However, with appropriate consideration the principles are relevant to a wide range of industries and containment applications. Given their ubiquity, wet laid/hand laminated repairs are the focus, although many of the principles outlined are equally valid for other types of composite repair, such as pre-cured systems. Given its prevalence in plant applications, the repair of carbon steel substrates forms the basis of this guide. However, many of the key principles and considerations are equally valid for other substrates provided they form part of a qualified repair system. 1.3 Purpose BS EN ISO 24817 details the qualification and design, installation, testing and inspection aspects of composite repairs. This document should be used in conjunction with the Standard, and serves as a practical guide for end users. It provides additional information pertinent to the upfront decision making process in selecting a composite repair, factors to be considered in the design and application of the repair, and broader integrity management considerations. The intention is that end users take account of the good practice highlighted by this document in developing their own inhouse procedures. The guide is set out in four separate but inherently linked phases: Phase 1: Decision Making Process; Phase 2: Pre-Installation Activities; Phase 3: Installation; Phase 4: Ongoing Integrity Management. Preceding the section on the decision making process (Phase 1), there is a summary Page 7 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group of key considerations, specific to engineered composite repairs. The purpose of the information in this section is to underpin and inform the decision making process. 1.4 Relevant Legal Requirements Applicable regulations in the United Kingdom (UK) include: 1. The Control of Major Accident Hazards (COMAH) Regulations, 2015 [3] (Onshore only) 2. Health and Safety at Work etc Act, 1974 [4] 3. The Offshore Installations (Offshore Safety Directive) (Safety Case etc) Regulations 2015 (SCR2015) [5] (offshore only) 4. The Pipeline Safety Regulations (PSR), 1996 [6] 5. The Pressure Systems Safety Regulations (PSSR), 2000 [7] (Onshore only) 6. The Offshore Installations (Prevention of Fire & Explosion and Emergency Response) Regulations, 1995 [8] (Offshore only) 7. The Management of Health and Safety at Work Regulations, 1999 [9] 8. The Offshore Installations and Wells (Design and Construction, etc) Regulations, 1996 [10] (Offshore only) 9. The Provision and Use of Work Equipment Regulations (PUWER), 1998 [11] End users should take account of the good practice highlighted by this document with respect to the specific legal and regulatory frameworks pertinent to their industrial sector and operations. Page 8 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group 2 2.1 SUMMARY OF KEY CONSIDERATIONS General The successful specification, installation and through-life management of engineered composite repairs relies on a number of key factors. Fundamental, is a robust and informed decision making process, establishing whether a composite repair is the most appropriate course of action, establishing whether it is technically viable and, particularly for safety critical repairs, whether its integrity can be assured for its entire lifecycle. Thus, for the process to be effective, it needs to be underpinned with an appropriate level of knowledge and a general awareness of the key considerations. This Section summarises key considerations to inform the decision making process outlined in Section 3. It is, in part, an abridged version of Appendix A, which can be consulted for more detailed information1. 2.2 Key Considerations 2.2.1 Causes of Failure The top three critical installation steps associated with the ultimate failure of a composite repair have been identified as: i. Surface Preparation; ii. Curing; iii. Defect/Leak Sealing. It is also noteworthy that a number of repair failures have been attributed to incomplete or inaccurate information being supplied to the repair supplier by the client. This serves to reaffirm the importance of this particular pre-installation task. 2.2.2 Training and Competency All end user personnel involved in the specification, application and management of engineered composite repairs should have had sufficient training and be deemed competent. Some roles/responsibilities for key members of staff are listed below: Technical Authority (or equivalent) i. ii. iii. 1 Review of repair supplier design proposals and verifying that they are fit for purpose. Aware of the general capabilities and limitations of composite repair technology and non-destructive testing (NDT) techniques. This will inform the decision making process as to whether a composite repair is feasible/appropriate. Reviewing repair close out documentation and establishing that the repair reflects what was proposed and is fit for purpose. Appendix A also provides detailed references to underpin the points outlined in this section. Page 9 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group On-site field engineers (or equivalent) i. ii. Aware of the key hold points as well as pre/post installation quality assurance checks. Sign-off following post-installation inspection and reviewing any associated documentation/paperwork. On-site inspection engineers (or equivalent) i. ii. Aware of the key areas to inspect and allowable limits for defects. Reviewing inspection data (visual and/or more sophisticated forms of NDT) and highlighting anomalies for further investigation. End user confirmation at key hold points should be undertaken for all safety critical repairs. 2.2.3 Applications The highest in-service failure rate to date on pipework systems has been on reducers and tees. Vessels require special consideration, with over one in ten repairs applied subsequently failing in service. This failure rate is significantly higher than for all other repair applications. For novel repairs, perhaps infrequently applied, or repairs with specific considerations (e.g. restricted access), consideration should be given to undertaking full-scale feasibility trials. 2.2.4 Defect/Leak Sealing Repairs to defects that have gone through-wall and are leaking are possible but require special consideration. Requires confirmation that any leak sealing device/technology has isolated the leak and will do so for the duration of the repair installation, including curing. The presence of any leak sealing device should be considered at the design stage in defining the defect size and geometry used for the design. Inadequate or ineffective leak sealing measures at the time of repair installation have resulted in several repair failures on safety critical equipment. 2.2.5 Surface Preparation Surface preparation of the substrate is critical to achieving satisfactory adhesion between the repair laminate and repair surface. It is the single most important step for ensuring a successful repair. It is imperative that the surface preparation procedure (and subsequent repair) is managed. Time delays can lead to oxidation (and further contamination) of the prepared surface which affects the initial strength, integrity and, in particular, durability of the adhesive bond. To maximise surface preparation quality, exposure times between process steps should be kept to an absolute minimum. Contaminants can significantly affect bond performance and need to be removed/reduced to acceptable levels. In terms of bond durability: Grit blast cleaning to Sa 2.5 > Hand or Power tool cleaning to St 3 >> Hand or Power tool cleaning to St 22. 2 It should be noted that both cleanliness and roughness are important. As such, the surface preparation method, tool(s) used, preparation grade stipulated etc should also be accompanied by a surface profile requirement. Page 10 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group The surface preparation method leading to the most durable repairs is via abrasive blastcleaning using grit, resulting in an angular surface profile in the range 75-115µm and a preparation grade of Sa 2.5. This should be the default choice for all safety critical repairs3. It has been demonstrated that a specialised rotary bristle tool4 is the most effective power tool; leading to more durable repairs than those made on surfaces prepared using other power tools. Hand or power tool cleaning (to a surface preparation grade of St 2 and St 3) using a wire brush and a rotating abrasive belt have been demonstrated to be ineffective. There is a limited evidence base for medium/long term integrity using current practices. This is particularly relevant to safety critical applications where the repair affords primary containment. 2.2.6 Cure The cure schedule should be managed to give the same level of cure (or glass transition temperature) during the installation of the repair as was qualified and assumed in the design. Where, based on qualification testing, the supplier can demonstrate that the required glass transition temperature is achieved by ambient cure alone, then heat treatment may be omitted. In all other cases the supplier shall provide a heat treatment procedure (temperature profiles and hold times) which has been demonstrated to achieve the required glass transition temperature during qualification. Any heat applied to cure must be controlled and known. Taking credit for heat treatment due to heating from the process fluid is not permitted. Post curing should only be undertaken once the resin has hardened and on equipment that is depressurised and drained. Pressure cannot be brought back to normal operating conditions until an acceptable level of cure has been achieved. Not doing so has been identified as a principal cause of repair failure. Consideration needs to be afforded to the total number of layers that make up the repair laminate, the number of layers that can be cured at one time, and the cumulative time this will take. 2.2.7 In-service Inspection The three candidate areas for inspection are: (1) the repair laminate; (2) the substrate; (3) the bond between the repair laminate and the substrate. When determining the extent and periodicity of inspection, consideration should be given to the degradation mechanism(s) of the substrate, its location (internal or external), as well as consequences of failure. A risk based inspection (RBI) [or suitable equivalent] approach should be adopted. The application of a composite repair prevents subsequent substrate inspection using: standard ultrasonic testing, including phased array; surface NDT methods; visual examination; and magnetic particle inspection. There remains no validated inspection technique to establish the integrity of the bond, emphasising the importance of appropriate surface preparation and adherence to qualified procedures. 3 The inclusion of a silane treatment step in the surface preparation procedure can lead to improved bond durability between the repair laminate and the substrate. 4 See Appendix A for full details. Page 11 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group For non-safety critical applications, it is likely that any inspection schedule will be limited to a periodic visual examination only. (See Appendix B) For safety critical applications, the viability of effectively deploying proposed NDT techniques should be established – this may require practical trials prior to repair application. For safety critical applications, a baseline inspection should be conducted pre and post repair installation. For safety critical applications - in addition to visual inspection, inspections using available NDT equipment should be used to confirm the condition of the substrate throughout the repair lifetime. For safety critical applications: External Defects i. ii. iii. A maintenance strategy should be in place to ensure that the repair laminate remains intact, with no evidence of edge lifting or corrosion at the edges of the repair. Periodicity of any inspection should be such that the integrity of the line remains assured. The potential for internal corrosion must be considered throughout the life of the repair. If internal corrosion is determined as active, then a suitable strategy to mitigate the threat should be determined (e.g. change in process conditions, use of inhibitors or reduced life of repair, etc). Internal Defects or Through-Wall Defects i. Further deterioration or growth of the defect may continue despite application of the repair, unless other measures are taken and are verified to be effective. ii. In addition to the requirements of the external corrosion case, the maintenance strategy should ensure that the internal defect does not grow to a size greater than that assumed in the design or that the repair laminate does not disbond from the substrate. iii. Awareness of limitations of NDT techniques for identifying and characterising pit-like features, particularly microbial induced corrosion (MIC). iv. It is important to be aware of, and take account of, the increased risk profile when a defect is through-wall and the repair is acting as the primary means of containment. This may have been due to an external and/or internal mechanism. The integrity of the repair must be ensured throughout its lifecycle. Appendices C-E provides a summary of the inspection techniques along with their capabilities and limitations. Pulsed eddy current (PEC), radiography and dynamic response spectroscopy (DRS) are the most established techniques for the inspection of composite repairs but still have a range of limitations. DRS, in particular, can be used as a quality assurance tool immediately post repair application. Page 12 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group 2.2.8 Repair Lifetime Design Life The design life is the maximum application lifetime of the repair. It is defined by the owner and used by the repair supplier for the purposes of design. It may transpire that the owner defined design life is not feasible given the defect type and service conditions. It should be agreed between the repair supplier and the client. The minimum design lifetime of the composite repair shall be two years. It is important that the client ensures that any information/data used for the purposes of design by the repair supplier is robust and accurate. Through-life considerations – findings from inspection data/changes in process conditions may mean that the initial inputs are no longer valid. These have implications for repair integrity and safety. Defined Life The defined life is the actual application or intended service lifetime of the repair. It defines the time after which the repair needs to be re-validated or its removal scheduled. The defined life is set by the end-user with due consideration of the risks associated with each repair. For safety critical applications the defined life should be set by the risk assessment on a case by case basis. For safety critical applications, if the repair is intended to provide the primary means of containment (either immediately after application or at any time during the life of the repair) it should be considered for short-term use only5. Special consideration should be afforded to scenarios where there is an active internal degradation mechanism where damage has not yet broken through-wall but could do so during the life of the repair. In this case, the ability of the repair to provide primary containment must be demonstrated for the largest defect that is considered may develop. Initial, successful performance of the repair, shall not be considered to provide any indication of future reliability because of the changes expected in the defect. 5 Consideration should be given to bringing shutdowns forward if the risk profile warrants such action – the integrity of the repair must be ensured throughout its lifecycle. Page 13 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group 3 3.1 PHASE 1: DECISION MAKING PROCESS General During the lifetime of engineering plant and offshore installations it is probable that fixed equipment (such as piping on process and utility systems) will suffer from degradation necessitating the need for remedial action. These anomalies represent a deviation from what is considered standard, normal or expected and a process should be in place that captures each key step from identification right through to successful close-out. The process is likely to include a range of personnel and all roles and responsibilities should be clearly defined. This helps ensure that the process works at a system level with reduced propensity for errors or oversight. This section details the key elements of the decision making process. In particular, it covers repair versus replacement considerations as well as repair selection. 3.2 Anomaly Identification and Characterisation When identified, a survey should be undertaken to fully characterise the anomaly as well as to establish the condition of the surrounding substrate. Documentation should include the following: Location of the anomaly (asset; component Detail of the damage found - degradation mechanism(s) and extent of the defect. type; component or line identification number; physical location; access requirements; P&ID.) Component leaking/not leaking Safety critical/non-safety critical Service Material type Corrosion allowance Component insulated/not insulated Corrosion circuit Nominal wall thickness Piping class Design and operating temperature and pressure The level of detail should permit a comprehensive and robust assessment to be made. Given that an anomaly likely constitutes a failure in the integrity management system, any possible mitigating actions should be identified in order to prevent reoccurrence. 3.3 Corrective Action In the case where an anomalous item means that a component will have limited or no remaining redundancy and cannot tolerate any further deterioration, an engineering assessment should be undertaken for continued service and corrective action. An assessment of the anomaly should be made and remedial options considered. Possible options include: 1. Replacement of the defective item; 2. Isolation and/or removal of the defective item or modification to the system control parameters to limit temperature/pressure exposure, e.g. reduce system trip pressures; 3. Implementation of a routine inspection / monitoring regime; 4. Undertaking a detailed engineering study to identify possible solutions or tolerability, e.g. fitness for service assessment; 5. Defined life repair. Page 14 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group It should be noted that more than one mitigation option may be required – i.e. the application of a defined life repair may also require an interim inspection / monitoring task prior to the repair being installed. Where replacement or repair are the options being considered, guidance for safety critical pipework is provided in HSE Offshore Safety Notice 04/2005 – Weldless Repair of Safety Critical Piping, July 2005 [31]. The philosophy described which is directly transferrable to other industry sectors is6, in order of preference: 1. Replace like for like7; 2. Temporary repair until replacement can be carried out; 3. Permanent repair only where replacement is not practical. Whilst the focus of the Safety Notice relates to safety critical pipework, this philosophy is valid for all containment equipment. Indeed, adopting this approach is in line with the principles of prevention and acts to control risks at source rather than taking palliative measures. To inform the top level repair or replace decision making process, a number of aspects should be considered, including: 3.4 Why repair rather than replace? What additional safety and business risk will this bring if safety critical? How tolerant of the safety/business risks are we/should we be? Corporate view? Can we manage the long-term integrity challenges this will bring? What operational changes could make a repair unsuitable – are these controlled? Lifecycle cost – resource etc. Viability – particularly access and ability to perform processes to required standard, e.g. surface preparation. On-going integrity management considerations, e.g. inspection. Repair 3.4.1 Defined Life Repairs Repairs to safety critical equipment should only be considered when all reasonable measures to enact a replacement in the first instance have proven unsuccessful. Repairs should be assessed with respect to their risk and the conclusion reached that there is no practicable means of replacement in the short term. This may be due to operational constraints, part availability, lead times or hot work constraints. If this is the case, a defined life repair could be considered. These generally take the form of engineered clamps or engineered composite repairs. For safety critical repairs offshore there should be ongoing dialogue with Verification Bodies. 6 The hierarchy of risk control and inherent safety are detailed in COMAH guidance (with respect to Reg 5) and ‘Reducing Risks, Protecting People’ (R2P2). 7 In this context, like for like means replacing the component to the original design basis. It does not preclude improving the component design/specification. Page 15 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group For non-safety critical applications the same philosophy should apply, accepting that the reduced risk posed by the fluid media or service function means that defined life repairs may be tolerated to a greater extent. 3.4.2 Repair Selection The selection of an appropriate repair technique or product can only be made when the cause and extent of the defect, existing design /operating criteria, work site access and operational constraints are established and understood. Each repair technique has its own limitations (service, pressure, temperature, material, geometry, size, specialist vendor requirements, cost and delivery, etc.) and it is critical that the repair selected is fit for purpose taking into account the nature of the defect throughout the lifecycle. All proposed defined life repairs should undergo an engineering assessment to ensure suitability. The engineering assessment should not only establish whether a repair type is technically viable, but also whether it is the correct course of action. Therefore, the level of assessment should be tailored to the defined life repair’s intended service and consequences of failure. For safety critical repairs this essentially takes the form of a risk assessment. In certain cases the suitability of a repair may require a formal management of change procedure to be carried out. Some of the main elements to be considered are: Can the repair be installed whilst the component is operational or what level of isolation/purge is required? Safety considerations – live blasting etc. What is the nature and location of the defect? Estimation of the rate of and extent of any further deterioration that would further compromise the pipe condition or any installed repair. What are the design and operating conditions of the defective component? Is the component subject to any upset conditions? Including start-up/shut down. Is the repair required to be suitable during or after a major incident such as a mechanical impact, jet or pool fire or explosion? Type of component and geometry being repaired (pipe/vessel, simple/complex). What hazards are associated with system service? (Fluid, Pressure, Temperature) What are the previous delivery times for this type of repair? What is the availability of personnel with the competency to apply the repair? Can the required level of surface preparation be achieved safely? Extent and specification. What operational measures, including (if relevant) permits, gas testing and fire protection requirements are required to ensure safety near the repair area? Consideration of the ability to inspect beneath clamps, wraps and connectors once fitted to determine the condition of the pipework. Determining access and suitability for future inspection to monitor further degradation in service. What are the anticipated failure modes of the component? What are the anticipated failure modes of the repair? What is the anticipated life span of the repair? Are any further operational controls required, in addition to the temporary repair, to ensure ongoing integrity? Page 16 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group Remaining life of pipework to which the joint/repair is to be carried out. Determining access, complexity suitability for installation of the repair. Compatibility of the repair clamp/wrap with the internal/external environment. Determining whether additional supports are required to support the repair due to extra loading on the pipework. Does the application of the repair render any equipment inoperable (such as an encapsulated valve)? What are the implications? Is there the potential for a change in process conditions over the lifetime of the repair that could lead to new types of degradation? Cumulative risk – multiple repairs on one line. Is there a risk of any interaction between multiple repairs? Inspection resource requirements. Does the owner have the necessary expertise on site to manage the installation of the repair? Does the site have the necessary expertise to manage through-life? Likelihood of over pressurisation e.g. pressure testing of the repaired system. Can this additional loading be accounted for in the design of the repair? Availability of data to inform design/specification of the repair. Likelihood of success – perhaps based on previous experience or industry good practice. The effect of the operating cycle on the integrity of the repair, effects of load cycling (if this is a feature of plant operation – how can it affect the integrity of the repair?) Will installation of the repair ‘move’ the failure mode to elsewhere? (vibration, pressure, heat etc.) and the Special attention should be afforded to situations where widespread deterioration of a system exists, perhaps multiple repairs on a single line. In these situations the risk assessment must consider the cumulative risk; this may be impaired fire performance, excessive weight, the potential for multiple leak sites etc. Special attention should also be afforded to situations where there is an active internal degradation mechanism. This is particularly the case for microbiologically induced corrosion (MIC). The evaluation should be undertaken by competent persons. It is important to still be mindful of the replacement option when undertaking this exercise. This is especially true where data/information/circumstances may make a repair difficult. The replacement/repair decision may have to be revisited. During the screening exercise the viability of applying an engineered composite repair will have been evaluated. BS EN ISO 24817 calls for a repair feasibility assessment8 to be undertaken by the owner and repair supplier. A curtailed number of factors from Section 3.4.2 are considered. 8 BS EN ISO 24817:2017, Section 7.1 Page 17 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group 4 4.1 PHASE 2: PRE-INSTALLATION ACTIVITIES General If the output of the repair decision making process (Phase 1) is that an engineered composite repair is to be installed then there are a number of key pre-installation activities that need to take place. The repair process should be coordinated by a competent owner representative. This section discusses roles and responsibilities, assessment of the repair design and key on-site preparation and organisation considerations. If a pre-installation baseline inspection has been specified this should be conducted. 4.2 Assigning Roles and Responsibilities for Composite Repair Application An operator representative (herein referred to as a ‘Job Responsible Coordinator’) should be assigned to manage the key elements of the process, engaging with internal and external parties to install a repair within prescribed timescales and to the agreed standard. It is particularly important that the ‘Job Responsible Coordinator’ identifies a focal point at the repair application site (independent of operations) thereby ensuring that the environment/facilities are as agreed with the repair supplier. This ‘on-site field engineer’ (or equivalent) should coordinate the repair installation and ensure that tasks are carried out to the appropriate standard and within specified timescales. The level of supervision and quality assurance should be proportional to the consequences of failure, with greater emphasis placed on repairs to safety critical equipment. In order to facilitate communications, the contact information for the ‘Job Responsible Coordinator’ should be supplied in the assessment. To ensure correct repair installation it is important that all lines of communication are clear, with the ‘Job Responsible Coordinator’ communicating with the repair supplier and, in offshore applications, the operations teams both on and offshore. Depending on the nature and complexity of the repair, application could be undertaken either by the repair supplier or alternatively support personnel including core crew, maintenance and inspection contractor personnel. In the case of non-repair supplier personnel, they shall have undertaken formal training via the product vendor and have been deemed competent. This guide assumes the former (i.e. repair supplier applied) but the key principles are common. Repairs to safety critical equipment should only be installed by the vendor or a vendor approved supplier. 4.3 Supply of Input Data and Review of Repair Design The ‘Job Responsible Coordinator’ will ensure that the repair supplier has all information required to appropriately design the repair. An overview of the information required is provided in BS EN ISO 24817, Annex A9. Each repair supplier may have their own internal forms and requirements; Annex A should be used as the minimum level of detail in these cases. The data inputs include: pipe details; repair class and lifetime; loading; defect and projected size; anticipated conditions during installation of the repair; facilities to be provided by the client and details of the defect area. The detail level to which these requirements are fulfilled will have been determined by the output of the repair feasibility assessment (Section 3.4.2). In practice, all data may have been supplied to the 9 BS EN ISO 24817:2017, Section 7.4, also provides further information. Page 18 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group repair supplier at the enquiry stage and therefore no further information may need to be provided. Photographs of the defective part to be repaired, along with locational information and drawings will aid the design and installation of the repair, Figure 4.1. Figure 4.1 Photo of the spool to be repaired along with isometrics, plot plans and P&IDs. The repair supplier will provide a number of documents prior to repair application. These include a method statement, risk assessment and a work pack that should provide drawings of the repair along with the design calculations. The proposed design, including calculations, should be subject to an internal review by the ‘Technical Authority’ (or equivalent) to verify their applicability and accuracy. In particular, the inputs used for design purposes should be checked. Where appropriate, Independent Verification Bodies should be consulted. The work pack should also include the repair supplier’s training certifications and relevant details of their competence to complete the repair as designed. Elements that need to be checked/verified include: The repair lifetime/replacement date are as expected. The design risk assessment is sufficient for the repair under consideration, and suitably mitigates all foreseeable incidents. That any preferred system de-pressurisation is acceptable and realistic - or the design, as submitted, shall be re-worked accordingly to The repair system method statement, including details of the surface preparation, the quality of application, the interface Page 19 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group alter and/or eliminate the system depressurisation. between the repair and existing finishes and the repair acceptance criteria. The repair drawing is specific and appropriate to the repair under consideration. Details of the interface protection system (if applicable) between the repair and the existing pipe/plant. The defect size and geometry used in the design calculations are 10 representative/correct. Have any stop gap leak sealing techniques been installed? Have these been considered in the design? Confirm the size of the stopgap used is less than or equal to the size of the defect used in the design. The curing time for the repair, providing limitations on what can and cannot be done to the repair until curing is complete. The design has suitably addressed the required fire performance and has mitigated the potential for cathodic disbondment associated with pipe/plant that is cathodically protected (if appropriate). If deemed required by the design, the pressure testing regime is appropriate and can be undertaken safely. Confirm repair designed for test pressure. That the composite repair supplier’s ‘installers’ are qualified to the requirements of BS EN ISO 24817, Annex I, that their qualifications are within date and the composite repair supplier is registered on the owner’s approved repair supplier list. That the composite repair supplier has provided a declaration that the repair shall be designed, installed and finished in accordance with BS EN ISO 24817. Inspection requirements are included and are achievable in term of technique(s) and periodicity. It is notable that a number of repair failures have been attributed to incomplete or inaccurate information being supplied to the repair supplier by the client [12]. Indeed, this has been identified as one of the principal reasons for repair failure. 4.4 On-site Preparation and Organisation The ‘Job Responsible Coordinator’ should confirm and agree any on-site requirements with the repair supplier and communicate these to the ‘on-site field engineer’, as appropriate. The ‘on-site field engineer’ should be accountable for ensuring that the repair location and any other requirements are in place prior to the arrival of the repair supplier. Requirements are likely to include access to storage and a working area for laying out materials and wetting out the reinforcement fabric. A covered table is normally required for wetting out the fabric and to reduce the risk of contamination. 10 The selection of the generic through-wall defect and size for design, i.e. the selection of the correct dimension, may not simply be the size of the actual defect but rather may be either the dimension of the unprepared surface area neighbouring the defect or if filler is used over the defect, the dimension of the defect is the surface area of filler. Page 20 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group The repair location should be accessible by the repair supplier’s representatives and any other interested parties. It should be noted that in some instances this may require scaffolding to be erected or the use of specialist equipment. In order to create an environment that permits the repair to be installed (within prescribed limits) a habitat may need to be erected. Approval (via permits or equivalent) may be required for any heat sources, lighting and photographic apparatus. If line isolation is required this should be discussed with all parties to establish how this is to be achieved and implemented. Further, if pressure testing is required post repair application this also needs to be organised. Pressure testing is discussed further in Section 5.5.4. Work orders relating to any post-installation requirements such as paint coatings (particularly at the ends of the repair) need to be placed. The repair supplier should be able to advise on the storage requirements for resins, it is important that any recommendations are followed. Generally speaking, all constituent materials should be kept dry and at moderate temperatures as temperature extremes can lead to defective/damaged constituent materials and/or make them difficult to work with. Shelf life of constituents/materials should be monitored/checked. Page 21 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group 5 5.1 PHASE 3: INSTALLATION General Successful installation is directly related to the workmanship of the technicians who undertake the repair. It is an entirely manual process, with often difficult working conditions and time pressures. This section details the hold points during installation of a repair system, quality assurance checks prior to the commencement of the repair, the installation, and post installation inspection and quality assurance considerations. It also details post installation tasks and requirements. 5.2 Repair Location Site Preparation 5.2.1 General As detailed in Section 4.4, the ‘on-site field engineer’ is accountable for ensuring that the repair site and any requirements are as agreed with the repair supplier. A site briefing and risk assessment should be completed prior to the commencement of any work. Given that the risk assessment will have been prepared in advance, its relevance to the actual location/conditions should be verified. The repair supplier should verify that the repair site is that detailed in the repair work pack. 5.2.2 Hold Points During Installation of a Repair System BS EN ISO 2481711 specifies a number of hold points during the installation of a composite repair. These cover: the method statement; environmental conditions; surface preparation; filler profile; stage check on reinforcement fibre or cloth orientation; tests of repair laminate; QA records; pressure testing. For safety critical applications the ‘on-site field engineer’ should witness the process and corroborate information/activities either at these designated hold points or at other times. An overview of a wet lay-up composite manufacturing process and some suggested hold points can be found in Appendix F. 5.2.3 Surface Preparation Surface preparation is most commonly undertaken by an owner nominated representative (e.g. onsite fabric maintenance team) and less frequently by the repair supplier. In the case of the former, it is particularly important that dialogue has taken place between the repair supplier and ‘on-site field engineer’ to ensure that the required equipment and materials are available to enable the qualified surface preparation procedure to be replicated on site. The surface preparation procedure on-site should be the same as that qualified by the repair supplier and used in the design. This includes not only the extent12 of the surface preparation but also the preparation grade, the surface profile, the method and tool(s) used and the time the prepared surface is exposed before repair application. Time between surface preparation steps should be kept to an absolute minimum. Wherever possible the surface should be prepared immediately prior to repair application. For safety critical repairs, non-conformances are a cause for rejection and the (correct) surface preparation procedure should be repeated until the desired specification(s) are achieved. 11 12 BS EN ISO 24817:2017, Section 8, Table 14 Overall extent as well as confirming any surface neighbouring defect has also been prepared, if assumed in the design. Page 22 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group Importantly, if the surface preparation on-site is not to specification and cannot be achieved in practice then a re-design by the repair supplier would be required and could subsequently mean that qualification data is not available and the repair proposed is not suitable and should not be applied. The impact of any change should be evaluated in the context of the original decision making process (Section 3), particularly the risk assessment. 5.2.4 Quality Assurance Checks Prior to Application of the Repair BS EN ISO 2481713 details quality assurance checks for the substrate prior to application of the repair to ensure the condition of the site is as per the design. This includes, as a minimum, the geometry, material and dimensions of the substrate, surface preparation, surface temperature and the location/size/nature of the defect. In addition to the substrate checks described above, if a leak sealing clamp (or other device) is present, it should be confirmed that it is not leaking. For safety critical repairs the ‘on-site field engineer’ (or another person deemed competent) should verify the pre-application checks. The pre-application hold points (Section 5.2.2) and quality checks are deemed particularly important as it has been established that, collectively, non-conformances account for the largest number of repair failures [12]. Specific issues relate to defect size (larger than assumed in the design), incorrect/inferior surface preparation, incorrect surface preparation extent, lack of leaking sealing or leaking clamps during installation, environmental conditions not suitable for repair application. 5.3 Repair Installation The installation of the composite repair should be carried out in accordance with the approved method statement and by the repair supplier’s qualified installers. A photographic record of the key installation steps and hold points should be taken by the repair supplier, and for lower risk repairs it is likely that this record will suffice in preference to witnessing each stage. If the pipe has been isolated/depressurised/undergone pressure reduction in order to apply the repair, the repaired substrate may be returned to service only after the specified cure schedule has been achieved. The required cure time, and cycle, before re-pressurisation of the pipework is specified by the repair supplier and must be followed as accurately as possible. Additional heat sources such as heating blankets may be required. Repair failures attributed to non-conformances at this stage have been as a result of [12]: (1) incorrect type/amount of primer being applied; (2) incorrect number of layers applied; (3) poor cloth wet out; (4) high levels of voidage; (5) poor consolidation due to access restrictions; (6) lack of compression; (7) curing protocol not being fulfilled; (8) insufficient curing time; (9) environmental conditions (too cold). 13 BS EN ISO 24817:2017, Section 9.2, Table 15 Page 23 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group 5.4 Inspection/Quality Assurance 5.4.1 Inspection of the repair after installation Post application, the repair supplier’s technicians shall inspect the repair and compare to the acceptable limits detailed in BS EN ISO 2481714. The inspection will focus on the interface between the pipe and the ends of the repair, the surface resin rich layer and the repair laminate. Dimensional checks of the repair should be completed to confirm the axial extent, taper length and repair thickness are as per the design. Hardness testing should be conducted and cure schedules reviewed to infer degree of cure. When deemed acceptable, the repair supplier's technicians shall ensure that they adequately record the repair by means of photographs, and shall complete and sign all paperwork, certificates and documentation associated with the repair. If the ‘on-site field engineer’ has witnessed the repair process they may wish to undertake a further inspection along with reviewing any documentation and signing off the repair. At this time, if a post-installation baseline inspection (using more sophisticated NDT techniques) has been specified this should now be conducted (or at the earliest opportunity) and documented in a manner that permits comparison with future repeat inspections. 5.5 Post Installation Tasks/Requirements 5.5.1 Corrosion Protection Reinstatement Post repair application there will be prepared metal surfaces at the ends of the repair. For substrates susceptible to corrosion it is important that measures are taken to reinstate the original coating or a suitable alternative as soon as possible. Failure to protect the edges of the repair can lead to localised corrosion of the substrate. Figure 5.1 14 Corrosion at edges of repair due to lack of corrosion protection applied post repair. BS EN ISO 24817:2017, Section 9.2, Table 16 Page 24 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group If this is not remedied within a suitable timeframe, the corrosion can become progressively worse. This can lead to two issues: (1) The corrosion can progress under the tapered regions of the repair, Figure 5.1, leading to wall-thinning and local disbondment; (2) if (1) occurs the interface acts as a repository for moisture which is known to be especially deleterious to adhesive bonds [27]. With appropriate planning and the correct materials this situation can be easily avoided. Painting the bare metal regions should be undertaken after the visual QA inspection of the repair has been completed, Figure 5.2. This should be completed as soon as possible after repair application; preferably at the time of manufacture. Clarifying from the outset who will reinstate the corrosion barrier is important. Usually the corrosion barrier is reinstated by the owner, and requires specific skills and attention. The paint can extend from the substrate over the landing areas or taper regions of the repair15. If a coating is applied over the tapered regions these should be clearly marked to help minimise the risk of damage during maintenance16. If for some reason reinstatement of the corrosion protection cannot take place at the time of repair manufacture the ‘Job Responsible Coordinator’ should ensure that the ongoing inspection and maintenance of the repair is considered until such time as the corrosion barrier can be reinstated. The repair should not be considered as complete from an operator perspective until this task is completed. Figure 5.2 Paint coating to mitigate corrosion of substrate at edges of repair. 5.5.2 Paint Coating In addition to coating the bare metal at the edges of the repair, consideration should be given to extending this coating over the entire repair. Doing so can act to highlight the presence of the repair as well as offering some UV protection, Figure 5.3. 15 Check with the repair supplier that the paint coating is compatible with the composite repair if extending paint onto repair. For carbon repairs a glass layer may be used to isolate the substrate from the carbon reinforcement. This glass layer may extend beyond the taper region of the repair. As such, the axial length of the isolation layer needs to be documented and identified after recoating. 16 Page 25 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group Figure 5.3 Repair painted orange to promote awareness amongst on-site operatives17 However, application of the paint can hinder visual examination of the repair laminate. Accordingly, the propensity for UV damage should be discussed with the repair supplier at the design stage to establish whether it is a realistic proposition based on location and design life. Prior to any paint application, the repair supplier should be consulted to confirm that the paint coating is compatible with the repair. 5.5.3 Additional Precautions It is important to protect the repair from damage in service, perhaps incurred via uncoordinated and ill-informed fabric maintenance activities or accidental damage from dropped objects or chemical exposure. In part this risk can be reduced by having appropriately updated engineering drawings to indicate the presence and criticality of any repairs. In addition, the presence of the composite repair on the pipe on site should be identified with suitable markings. For locations where it is appropriate to do so, a warning sign should also be fitted, Figure 5.4. A high visibility paint coating can aid identification and define the boundaries of the repair (Section 5.5.2). 17 Note prepared section of substrate to right of repair that has not been coated – considerations outlined in Section 5.5.1 apply. Page 26 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group Figure 5.4 (l-r) Tapered region damaged by fabric maintenance activities; warning sign to warn site operatives of presence of composite repair. If through the risk assessment process it was deemed that protective covers were required to protect the repair from impact damage these should now be installed (Figure 5.5). Consideration will need to have been given to the ease with which the cover(s) can be removed to facilitate inspection activities. Figure 5.5 (l-r) Composite repair; with impact protection cover in place. 5.5.4 Pressure Testing Pressure testing can be undertaken once the repair has been applied and has fully cured. This should have been specified by the owner (with due consideration to the risk assessment), if required, or as recommended by the relevant design standard for the substrate. The primary candidate for pressure testing is likely to be a safety critical repair to a through-wall defect. In this case, a pressure test can be used to highlight major installation shortcomings – e.g. insufficient surface preparation. If the line required isolation, or production needed to be stopped during repair application it may become necessary to perform a pressure test when the line is reintroduced to service. If this is the case, the repair must have been designed to accommodate the pressure test conditions. Therefore, if a pressure test is required on the system on start-up then the pressure reached during this test Page 27 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group must be accounted for as part of the design process. Discussions early on in the repair design process will allow for the design to take pressure testing into account; a more substantial repair may be required due to the increased demand of the pressure test. A guidance note [32] is available on the safety requirements for pressure testing. 5.6 Repair Completion Documentation The following documentation shall be provided by the repair supplier to the owner on completion of the repair. Repair details and unique reference. Repair design, comprising details of laminate lay-up. Material records and batch numbers. Repair application. Quality control records. Competency certificates of installer and supervisor. Independent inspection (if carried out), comprising test report. Service inspection, comprising details of service inspection intervals and repair condition. Details of the curing cycle. Details of pressure test (if carried out). Operating and system conditions during manufacture. Any deviations from agreed method or design. Photographic record. Post installation, a closeout report should be prepared by the repair supplier and provided to the client. This acts as a formal record of the repair installation and documents the above information. This information should be retained for future reference, see Section 6.2. Page 28 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group 6 6.1 PHASE 4: ONGOING INTEGRITY MANAGEMENT General The effort afforded to the ongoing integrity management of installed engineered composite repairs should be based on their criticality and the consequences of failure. The focus should be on repairs to safety critical equipment, which will include implementing the in-service inspection strategy defined at the decision making stage. This section covers the important task of updating records, in particular adding the repair to the defined life repair register and updating engineering documentation. It also covers in-service inspection, life extension/reduction and decommissioning. 6.2 Records 6.2.1 Defined Life Repair Register BS EN ISO 2481718 details owner responsibilities which includes setting up a defined life repair register. The defined life repair register (also known as a temporary repair register or composite repair management system) is an essential requirement for managing the lifecycle of the repair. The ‘Job Responsible Coordinator’ should ensure that a close out report is received from the repair supplier and that the repair is added to the register and is subsequently signed off by the ‘Technical Authority’ (or equivalent). The register should include the following items: 18 Unique repair number Date identified / notified Line number P & ID number Piping isometric drawing number Location (module / level) Service Hydrocarbon (Yes / No) Safety critical system (Yes/No) Applicable performance standard Date of repair application Operational conditions at time of repair Repair type Expiry date Inspection plan / Routine number Inspection frequency Planned replacement date Shutdown required for replacement (Yes/No) Repair status (live / closed). Anomaly report / MCDR Repair completion documentation Process conditions before and after repair application Photographs of defect/repair process etc. Inspection technique(s) Defect type – active/inactive Design life and defined life Coating reinstated (substrate at edges of repair) Process fluid BS EN ISO 24817:2017, Annex L Page 29 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group 6.2.2 Identification Each repair should be allocated a unique reference ID from the register. The unique reference number should be stencilled or otherwise permanently marked on the repaired section to facilitate subsequent inspection and reporting, Figure 6.1. The use of quick response (QR) codes and Radiofrequency identification (RFID) can also aid in the identification of repairs.19 Figure 6.1 Identification approaches – defined life repair (DLR) tag; sticker affixed to repair and stencilled ID reference.20 6.2.3 Updating Engineering Documentation Relevant engineering documentation (e.g. P&IDs/Isometrics/Plot Plans) should be updated such that there is no ambiguity as to where the repairs are located and their criticality, Figure 6.2. A photograph of the repair’s location and condition should also be included. 19 When engineered composite repairs are used for underground applications GPS coordinates should be recorded and logged for future reference. 20 Note prepared sections of substrate that have not been coated – considerations outlined in Section 5.5.1 apply. Page 30 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group Figure 6.2 6.3 Updated engineering documentation – photos, Isometrics, plot plans and P&IDs. In-Service Inspection 6.3.1 General An inspection strategy should have been developed with inputs from the repair supplier and specialist inspection companies. An RBI approach is suggested with details documented in the DLR register. A review of in-service failures [13] suggests that the vast majority of repairs that fail do so within a relatively short period (within weeks) post-installation. This is generally attributable to installation related issues and, in particular, sub-standard surface preparation. Whilst this failure data may reflect that in the vast majority of instances composite repairs have been used on a short term basis only (and as such failure data pertaining to medium/long term applications is not available), it does demonstrate that verifying initial integrity should form an important part of the overall inspection strategy. 6.3.2 Inspection Strategy The inspection strategy should have been defined at the decision making stage and will specify the periodicity of the inspection as well as indicating whether the inspection should cover one or more of the following: (1) repair laminate; (2) substrate; (3) bond. Page 31 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group For non-safety critical repairs the inspection will likely take the form of a visual examination of the repair and the adjacent substrate. BS EN ISO 2481721 provides guidance on defects and allowable limits for the resin rich layer, repair laminate and interface between the substrate and repair at the edges. An informed visual examination performed well can not only identify whether the repair has failed, but also some signs of deterioration. To aid the visual examination it is recommended that an inspection template is produced along the same lines as that in Appendix B. It is suggested that photographic records be taken at each inspection to monitor condition over time. It is particularly important to examine the tapered regions of the repair for any evidence of the laminate lifting away from the substrate. Feeler gauges can be helpful in establishing the extent of any lifting in the tapered region. Leaks or weeps often manifest themselves at the edges of the repair but sometimes can also be seen coming through the body of the repair, Figure 6.3. These leaks indicate that the composite repair has failed. Figure 6.3 (l-r) Leak at edge of repair22; through main body of composite repair. Safety critical repairs are likely to be subjected to the same visual examination as non-safety critical repairs, albeit on a more frequent basis. In addition, as detailed in Section 2.2.7, inspection of the substrate should have been considered. For external substrate defects, the periodicity will have been set such that the integrity of the line remains assured. For internal mechanisms, an inspection strategy will have been derived that permits evaluation of the footprint, and/or depth, of any defects to verify that they are within tolerable limits with respect to the repair design. For safety critical gas systems, gas detection equipment should also be considered. A key element at this stage is the verification/validation of the assumptions made at the decision making stage. In other words, establishing whether the inspection strategy defined at the decision making stage provides the required data to ensure integrity. Issues related to coverage and/or resolution may necessitate revisiting the inspection strategy (informed by Appendices C-E) and in some cases may require a re-evaluation as to whether an engineered composite repair is appropriate (Section 3.3). 21 22 BS EN ISO 24817:2017, Section 9.2, Table 16 Note prepared section of substrate that has not been coated – considerations outlined in Section 5.5.1 apply. Page 32 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group 6.3.3 Key Inspection Techniques – Ongoing Integrity Considerations Section 2.2.7 detailed that dynamic response spectroscopy (DRS), pulsed eddy current (PEC)23 and radiographic techniques (or a combination thereof) are the most established techniques for the inspection of composite repairs. If an inspection was conducted directly after repair installation (Section 5.4.1) this can act as a baseline for all future inspection activities. If the inspection strategy was to use solely DRS to detect defects in the laminate, bondline and substrate a review of baseline data would indicate whether this is still an acceptable approach. Using DRS, any flaws in the laminate and/or bondline precludes substrate thickness measurements in those areas. A review of the baseline data would provide an indication of the likely successful coverage for wall thickness measurement and whether a further technique would be required, perhaps using DRS solely to identify/monitor defects in the laminate/bondline. Comparison with baseline inspection data would be particularly useful for detecting new defects in the laminate or bondline, despite the exact (through-thickness) position of the flaw not being indicated. It would not be expected that flaws would develop in the laminate or interface post installation. In such cases the operator should liaise with the repair supplier. If the inspection strategy was to monitor general external corrosion using PEC, a key consideration will be to verify that there is also no threat from any internal corrosion mechanism. If a baseline inspection has been performed this provides an opportunity to monitor for any changes. This can be enhanced by interrogating the inspection data. For a repair applied for general external corrosion any changes in wall thickness measurement are likely to indicate the presence of an internal mechanism. If it is a localised mechanism it is unlikely to be detected. In line with DRS and PEC, for radiographic techniques a baseline inspection provides an opportunity to monitor change. The main focus should be consideration to any future threats and accessibility to enable the number of required exposures and from the appropriate angles. 6.3.4 Key Considerations Section 6.3.2 highlighted the importance of confirming/validating that the inspection strategy defined at the decision making stage yields the required data to ensure integrity. For safety critical repairs this is something that needs to be considered throughout the life of the repair. For repairs to substrates suffering from external corrosion, consideration should be given to any changes to process conditions that may result in the substrate being exposed to a different degradation mechanism than was envisaged when the repair was designed and installed. For any planned changes to process conditions it is expected that an appropriate risk assessment is conducted (See Section 6.4). If the repair is considered to be safety critical, significant corrosion at the edges of the repair (potentially coupled with lifting of the repair laminate) should result in a reassessment of the design requirement and potentially, repair of the original repair or replacement. 23 Substrate only. Page 33 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group 6.3.5 Remedial Action If defects in the interface, resin rich layer, and repair laminate are outwith the limits specified within BS EN ISO 2481724 then there are three options: Removal of the repair (this should be undertaken if the repair has failed). Repair of the repair laminate. Localised repair of the damaged region. Under certain circumstances, if defects are identified in the repair laminate, the repair can be treated as a defect and a new composite repair can be applied over the compromised one. However, careful consideration needs to be given before this approach is employed as it can lead to excessively large repairs25. If inspection of the substrate indicates that the size of the defect is found to be approaching or exceeding that used in the design, advice should be sought from the repair supplier. In the case of the former, this is particularly important where the periodicity of inspections is such that the defect size may exceed that used in the design prior to the next planned inspection. If additional defects in the substrate are identified during inspection that were not accounted for at the design stage, advice should be sought from the repair supplier as part of a broader risk assessment. In particular, it should be established whether an engineered composite repair remains the appropriate corrective action given the additional defects (see Section 3.3). 6.4 Ongoing Validity of Input Data As detailed in Section 2.2.8, the repair design is informed by the input data supplied by the client. These inputs represent only a small part of the broader considerations as to whether the use of an engineered composite repair is the most appropriate course of action (Section 3.3). For safety critical repairs it is important that the accuracy and validity of the original design inputs/assumptions remain valid and that the broader considerations detailed in Section 3.3 are reviewed on a periodic basis. Prior to any planned change it is expected that an appropriate risk assessment is conducted that gives due consideration to features such as the repair. This should include consulting the repair supplier to identify any compatibility issues and broader fitness for service considerations. In the event of an unplanned change in process conditions the owner should seek the advice of the repair supplier. Consideration of the process conditions and the potential effect on the composite repair should be made throughout its lifetime. 6.5 Life Extension/Life Reduction 6.5.1 Extension The decision to extend the repair design life should be documented. All supporting records to underpin any decisions should also be kept for future reference. 24 25 BS EN ISO 24817:2017, Section 9.2, Table 16 This may also impact the efficacy of NDT techniques given additional repair thickness. Page 34 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group For non-safety critical repairs it is suggested that the owner should discuss an extension to the design lifetime with the repair supplier taking into account operating history. The repair shall undergo a visual inspection. Provided it is assessed that failure of the repair would present no significant risk to personnel safety or damage to the environment this close visual inspection will suffice and a life extension may be granted provided the repair remains in good condition with no signs of deterioration. For safety critical repairs the design and installation details must be available (these shall include records of the surface preparation of the substrate and that the design and cure of the repair met the original specifications) and the installation records must be sufficient to demonstrate the repair was installed in full compliance with the repair supplier’s qualified procedures. In particular, the surface preparation achieved (in terms of preparation grade, surface profile, method and tool(s) used) at the time of installation shall be considered with respect to performance, long-term durability and approval of any life extension. In addition, the substrate should be inspected to inform the decision making process. Factors to be considered in determining if the design life of a safety critical repair may be extended include: Inspection for degradation of repair. NDT of repair and substrate, if possible. Substrate degradation (corrosion) mechanism(s) (internal/external). The surface preparation procedure when installed. Additional threats since installed or over additional lifetime (e.g. different/additional degradation mechanism(s)). Review of installation documentation. Service conditions and operational history with respect to repair design conditions. Review of calculations. Limiting factor for design life initially and whether this still stands or can be overcome. Evidence of the system being able to extend beyond its current life. Validity/applicability assessment. Repair is acting or could act as primary means of containment. of original risk Special consideration should be afforded to the design life extension of safety critical repairs where the repair is acting or could act as the primary means of containment. As detailed in Section 2.2.8, such repairs are for short term use only. Re-validation of the repair design lifetime is performed by re-designing the repair based on the required lifetime and the most up to date inspection data on the defect of concern26. 6.5.2 Reduction As detailed in Section 6.3, changes to process conditions and other threats can occur. If the review of the broader considerations detailed in Section 3.3 concludes that an engineered composite repair is still appropriate, the implications of these changes on the original design basis will need to be considered. 26 Note that any redesign may also impact on the efficacy of NDT techniques. Page 35 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group The repair supplier should be approached and requested to re-evaluate the design based on the new information. The outcome of this assessment may be: (1) an engineered composite repair is no longer viable; (2) Remedial action; (3) In the absence of any (possible) remedial action, a reduction in the design life of the repair. The operator should also re-consider the defined life of the repair to establish whether it is still suitable in light of the new information. The defined life repair register and any other appropriate documentation should be revised to reflect any changes. 6.6 Decommissioning and Removal 6.6.1 Decommissioning Adequate systems of work and documentation should be maintained (in particular a repair register) such that it is clearly apparent when the defined lives of repair systems are approaching and action is required. Reference should be made to the original risk assessment prior to decommissioning of a repair system. If necessary, a revised risk assessment should be carried out. 6.6.2 Repair removal The removal of repair material may be achieved by mechanical means (e.g. grit blasting and highpressure water jetting). This activity should be informed by an appropriate risk assessment. Page 36 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group 7 REFERENCES 1. ASME PCC-2, Repair of Pressure Equipment and Piping, 2018 2. BS EN ISO 24817:2017, Petroleum, petrochemical and natural gas industries – Composite repairs for pipework – Qualification and design, installation, testing and inspection (ISO 24817:2017), 2017. 3. Control of Major Accident Hazards (COMAH) Regulations, 2015 4. Health and Safety at Work etc Act, UK Public General Acts, 1974 5. The Offshore Installations (Offshore Safety Directive) (Safety Case etc) Regulations 2015 (SCR2015) 6. The Pipeline Safety Regulations (PSR), UK Statutory Instruments, 1996 7. The Pressure Systems Safety Regulations (PSSR), UK Statutory Instruments, 2000 (Onshore only) 8. The Offshore Installations (Prevention of Fire & Explosion and Emergency Response) Regulations, UK Statutory Instruments, 1995 (Offshore only) 9. The Management of Health and Safety at Work Regulations, UK Statutory Instruments, 1999 10. The Offshore Installations and Wells (Design and Construction, etc) Regulations, UK Statutory Instruments, 1996 (Offshore only) 11. The Provision and Use of Work Equipment Regulations (PUWER), UK Statutory Instruments, 1998 12. Yeomans, E.Y., Human Factors associated with installation of an Engineered Composite Repair – Task and human failure analysis, ERG/18/29, HSE, 2018 13. Harris, W., Review of In-service Failures, ES/2018/33, HSE, 2018 14. BS EN ISO 8501 – Visual assessment of surface cleanliness, Part 1 – Part 4 15. BS EN ISO 8502 – Tests for the assessment of surface cleanliness, Part 2 – Part 12 16. BS EN ISO 8503 – Surface roughness characteristics of blast-cleaned steel substrates, Part 1 – Part 5 17. BS EN ISO 8504 – Surface preparation methods, Part 1 – Part 3 18. Guidance Notes on Composite Repairs of Steel Structures and Piping, American Bureau of Shipping (ABS), September 2019 19. Davis, M., Review of Adhesive Bonding Aspects of BS EN ISO 24817, Adhesion Associates Pty. Ltd., 2019 20. BS EN ISO 8502-5, Preparation of steel substrates before application of paints and related products — Tests for the assessment of surface cleanliness — Part 5: Measurement of chloride on steel surfaces prepared for painting (ion detection tube method), 1998 21. Recommended Practice, DNV-RP-C301, Design, fabrication, operation and qualification of bonded repair of steel structures, July 2015 22. BS EN ISO 8504-1, Preparation of steel substrates before application of paints and related products — Surface preparation methods — Part 1: General principles, 2019 23. BS EN ISO 8504-2, Preparation of steel substrates before application of paints and related products — Surface preparation methods — Part 2: Abrasive blast-cleaning, 2019 24. BS EN ISO 8504-3, Preparation of steel substrates before application of paints and related products — Surface preparation methods — Part 3: Hand- and power-tool cleaning, 2018 Page 37 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group 25. BS EN ISO 8501-1, reparation of steel substrates before application of paints and related products — Visual assessment of surface cleanliness — Part 1: Rust grades and preparation grades of uncoated steel substrates and of steel substrates after overall removal of previous coatings, 2007 26. BS EN ISO 8503-5, Preparation of steel substrates before application of paints and related products — Surface roughness characteristics of blast-cleaned steel substrates — Part 5: Replica tape method for the determination of the surface profile, 2017 27. Broughton, J., 'Wedge Test Benchmarking Trials', A report prepared by Oxford Brookes University for the Health and Safety Executive, Health and Safety Executive, EM/20/19, 2020 28. Bannister, A.C., Nemcova, A., Inspection Techniques for Composite Wrapped Pipes: Lookup Charts for Technique Selection, EM/19/51, HSE, 2019 29. Bannister, A.C., Nemcova, A., Inspection Techniques for Composite Wrapped Pipes: Selection, Capabilities and Limitations, EM/19/47, HSE, 2019 30. Yeomans, E.Y., Engineered Composite Repairs – addressing human factors issues associated with installation – training and qualification, HF/19/17, HSE, 2019 31. HSE Safety Notice 04/2005 – Weldless Repair of Safety Critical Piping, HSE, 2005 32. Safety Requirements for Pressure Testing, Guidance Note GS4 (Fourth Edition), Health and Safety Executive, 2012 Page 38 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group APPENDIX A - ENGINEERED COMPOSITE REPAIRS: KEY CONSIDERATIONS A1 General The successful specification, design, installation and through-life management of engineered composite repairs depends on a number of factors. This section provides an overview of some key considerations. In part, these have been selected based on reviews of in-service failures [12, 13]. The top three [12] critical installation steps associated with the ultimate failure of a composite repair have been identified as: (1) Surface Preparation; (2) Curing; (3) Defect/Leak Sealing. Training and experience was also identified [12] as a key topic where improvement could lead to a greater number of compliant installations with fewer failures. The effect of component type/geometry is also considered [13]. Inspection has been included given its importance for ongoing integrity management, as have design/defined life considerations based on the implications of the above. The intention is that the information in this section should be used to supplement and inform the decision making process outlined in Section 3. A2 Surface Preparation A2.1 General Surface preparation of the substrate is critical to achieving satisfactory adhesion27 between the repair laminate and repair surface. It is the single most important step for ensuring a successful repair. Surface preparation generally involves removing contaminants from the substrate by degreasing, exposing a fresh chemically active surface and in some cases modifying the surface by a chemical process to enhance bond durability. Thus, surface treatment of steel produces a rough surface, free from contamination and enhances the formation of chemical bonds between steel and the adhesive. Effective surface preparation is necessary to achieve initial strength and particularly long-term durability in the service environment. Failure to adequately prepare a bonding surface may result in bond failure and/or corrosion of the bond region. The fact that the results of the bonding process cannot be fully verified by subsequent inspection and testing acts to reaffirm the essential need for good process control and adhering to qualified procedures. The four standards below address the preparation of steel substrates: 1. 2. 3. 4. BS EN ISO 8501 – Visual assessment of surface cleanliness [14] BS EN ISO 8502 – Tests for the assessment of surface cleanliness [15] BS EN ISO 8503 – Surface roughness characteristics of blast-cleaned steel substrates [16] BS EN ISO 8504 – Surface preparation methods [17] 27 In this case it is the adhesion (i.e. the interfacial interactions) that is the consideration - how the environment is attacking the interface and how well the interface resists this is a function of surface preparation. Bulk changes and chemical compatibility are also important and need to be considered. Page 39 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group These standards were originally conceived for the corrosion protection of steel structures by painting, but have since been used for preparing steel surfaces for repair using bonded repair technology. It is important to note that BS EN ISO 24817 is a performance based standard. As such, the surface preparation processes and procedures should be qualified by testing. An overview of the key steps is provided in the following sections. A2.2 On-site Conditions Guidance [18] suggests the steel temperature and air humidity should be monitored for possible condensation on the steel during surface preparation and fabrication/installation. It is stated that the steel temperature should be at least 3°C higher than the air dew point and that the relative humidity should not be greater than 80%. BS EN ISO 24817 states that for installation of the repair the surface of the pipe shall be dry and at a temperature above the dew point or otherwise in compliance with the conditions validated by repair qualification testing28. BS EN ISO 2481729 suggests that repairs should not be applied when the temperature of the surface is less than 3°C above the dew point of the surrounding air or when the relative humidity of the air is greater than 85%, unless local conditions dictate otherwise. Verifying the environmental conditions are acceptable is a key hold point during the installation of a repair system30. A2.3 Removal of Contaminants Contaminants are well known to adversely affect bond performance. Contaminants can include: slag, rust, laminated rust scale, mill scale, oil, grease, salts including chlorides and sulphates, moisture etc. Prior to mechanical abrasion using the selected method (see A2.4), an initial treatment should be performed that removes any surface contaminants. This is often achieved via water/solvent based cleaners. Performing the mechanical abrasion step prior to the removal of contamination will force the contaminants to be embedded in the surface deleteriously affecting bond performance [19]. Where salt contamination is plausible (e.g. coastal locations/offshore), a salt test should be performed. BS EN ISO 8502-5 [20] describes a field test for the measurement of chloride ions. Chloride salts left on a surface before mechanical treatment can have a deleterious effect on performance. Acceptance levels of 80 mg/m2 [21] and 50 mg/m2 [18] are quoted in existing guidance. For severely contaminated surfaces an additional step is required. Heavy, firmly adhering rust and scale should firstly be removed via hand/power tool cleaning or water jetting, as appropriate. The initial treatment should then be conducted prior to the main mechanical abrasion step using the selected method [19]. 28 29 30 BS EN ISO 24817:2017, Section 6 BS EN ISO 24817:2017, Section J3 BS EN ISO 24817: 2017, Section 8.3, Table 14 Page 40 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group A2.4 Surface Cleaning31 (Mechanical Abrasion) BS EN ISO 8504-1 [22] covers surface preparation methods with the most relevant described in BS EN ISO 8504-2 [23] (Abrasive blast cleaning) and BS EN ISO 8504-3 [24] (Hand- and power-tool cleaning). Abrasive blast-cleaning is achieved via the impingement of abrasive onto the surface to be prepared. The abrasive used takes the form of grit which is angular and has fractured faces. Hand-tool cleaning involves preparing the steel substrate by the use of hand tools, without power assistance. This usually takes the form of scrapers, hand wire brushes etc. Power-tool cleaning involves preparing the steel substrate by the use of power-assisted hand tools. It is important to note that this step does not remove oils, grease etc, hence the importance of the stage detailed in Section A2.3. Once complete, all loose material should be removed. At this stage some surface preparation procedures incorporate an additional degreasing step. In all cases, once completed it should be ensured that the surface is dry and all debris has been removed. A2.5 Assessment A2.5.1 General BS EN ISO 24817 details the surface preparation hold points32. These encompass visual assessment of the surface cleanliness, assessment of the surface profile and wettability. A2.5.1 Visual assessment of surface cleanliness BS EN ISO 8501-1:2007 [25] specifies a number of preparation grades33, indicating the method of surface preparation and the degree of cleaning. The most common preparation grades are Sa 2.534, St 2 35 and St 336. It is paramount that the surface preparation grade achieved on-site is the same [including the method/tool(s)/procedures used] as those used to qualify the repair system and for the purposes of design. A2.5.2 Assessment of the roughness of cleaned surfaces BS EN ISO 8503 [16] defines tests for the assessment of the roughness of abrasive blast-cleaned surfaces. BS EN ISO 8503-5 [26] is most relevant, describing a replica tape method for the determination of the surface profile. Existing guidance states that the surface profile should range from 75 to 115µm [18, 21]. 31 The use of the word ‘cleaning’ for this step in standards can lead to confusion. A clean surface is an essential requirement for adhesion. However, a clean surface is not a sufficient condition for adhesion. The surface must also be chemically active to enable reactions to occur at the interface. This step usually involves abrasion to remove existing weak oxide layers, leaving the surface to develop a fresh chemically active and stable surface that is suitable for adhesion. 32 BS EN ISO 24817: 2017, Section 8.3, Table 14 33 Sa, St or FI indicates the type of cleaning method used. The number indicates the degree of cleaning from mill scale, rust and previous coatings. Surface preparation by blast-cleaning is designated by the letters ‘Sa’, surface preparation by hand and power tool cleaning, such as scraping, wire-brushing and grinding is designated by the letters ‘St’, whilst surface preparation by flame cleaning is designated by the letter ‘FI’. 34 Sa 2.5: When viewed without magnification, the surface shall be free from visible oil, grease and dirt, and from mill scale, rust, paint coatings and foreign matter. Any remaining traces of contamination shall show only as slight stains in the form of spots or stripes. 35 St 2: Thorough hand and power tool cleaning: When viewed without magnification, the surface shall be free from visible oil, grease and dirt, and from poorly adhering mill scale, rust, paint coatings and foreign matter. 36 St 3: Very thorough hand and power tool cleaning: As for St 2, but the surface shall be treated much more thoroughly to give a metallic sheen arising from the metallic substrate. Page 41 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group In practice, the replica tape method is often also used on surfaces prepared using other methods in an attempt to establish a minimum surface profile. A2.5.3 Assessment of Surface Wettability Adhesive bonding involves a liquid ‘wetting’ a solid surface. This implies the formation of a thin film of liquid spreading uniformly in contrast to one that readily breaks into bead-like droplets. The formation of bead-like droplets implies that the surface is contaminated. A continuous film indicates good wettability whilst the formation of distinct droplets indicates poor wettability. A stipple test is defined in BS EN ISO 2481737. A2.5.4 Non-conformance If after conducting the assessment stage it transpires that the required grade/specification has not been achieved the surface preparation procedure and any subsequent assessment should be repeated. It should be noted that a surface that was originally deemed to be compliant and to specification may subsequently be deemed to be non-compliant if oxidation occurs. In this case, as above, the surface preparation procedure and any subsequent assessment should be repeated. A2.6 Corrosion Inhibitors and Chemical Treatment A2.6.1 Corrosion Inhibitors Specifically formulated corrosion inhibitors (i.e. not grease) work by delaying the onset of corrosion of the prepared surface. If such corrosion inhibitors are considered to be part of the surface preparation procedure it is essential that their use has been qualified by testing. In particular, any effect on the initial strength, integrity or durability of the bond needs to be established. In the absence of such data, the focus should be to minimise exposure times between process steps and to repeat the surface preparation procedure if oxidation occurs (Section A2.5.4). In some cases corrosion inhibitors may also include coupling agents that take the form of silanes (see Section A2.6.2). If a qualified corrosion inhibitor is applied as part of the surface preparation procedure and there is going to be a subsequent delay in the lamination step, it is important to protect the surface of the pipe from contamination post application of the corrosion inhibitor. A2.6.2 Chemical Treatment BS EN ISO 2481738 states that a chemical treatment may (or may not) be used. A chemical treatment can be applied to a prepared surface to prevent hydration, thereby enhancing bond longevity [19]. One effective method is the use of silanes. Silanes can be used in three ways: (1) As a surface preparation treatment applied directly to the active surface prior to bonding; (2) Incorporated into a primer that must be applied directly to the active surface prior to bonding; (3) Incorporated as an additive in the adhesive/resin system that must be applied directly to the active surface during the bonding process. 37 BS EN ISO 24817:2017, Table 14 BS EN ISO 24817: 2017, Section J.2 38 Page 42 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group Whilst the inclusion of a silane treatment step can lead to improved durability, their effectiveness is dependent on a range of factors including the surface condition of the metal. As such this needs to be well controlled via the use of an effective surface preparation procedure prior to application. If a chemical treatment step is considered to be part of the surface preparation procedure it is essential that their use has been qualified by testing. In particular, any effect on the initial strength, integrity or durability of the bond needs to be established. A2.7 Surface Drying It is important that post application of any primers etc and prior to commencement of the lamination procedure that there is no evidence of any surface liquid remaining. A2.8 Surface Exposure Times BS EN ISO 2481739 states that the time period between completion of the surface preparation stage and the application of the repair laminate should be as short as possible but no longer than four hours. No guidance is provided on the times between actual process steps. It has been demonstrated [27] that a time delay of four hours between surface cleaning (the process described in Section A2.5) and lamination can dramatically reduce bond performance and in-service durability. To maximise surface preparation quality, exposure times between process steps are to be kept to a minimum. All bonding processes must be performed as rapidly as possible, with breaks in the steps kept to an absolute minimum. No foreign matter is to contact the surface. During any breaks in processes, surfaces are to be protected. However, it should be noted that whilst covering the prepared area may prevent further contamination it will not stop weak oxide growth. Given the high potential for contamination during field repairs, the coordination and management of schedules for implementation of repairs should be considered, especially where repair tasks are potentially disrupted by changes of shift teams or where task responsibilities are shared between different contractors [19]. A2.9 In-service Performance and Durability Considerations BS EN ISO 8504-3 [24] states that hand- and power-tool cleaning generally provide a surface cleanliness which is inferior to that achieved by abrasive blast-cleaning. Given this type of abrasion is dependent on repeated contact over the surface, any contaminants can be widely distributed by the process. As detailed in Section A2.5.1, hand- and power-tool cleaning is usually undertaken to achieve a preparation grade of St 2 or St 3. In practice, hand cleaning and power-tool cleaning are often synonymous with preparation grades St 2 and St 3 respectively. Abrasive blast-cleaning is typically undertaken to a preparation grade of Sa 2.5. BS EN ISO 8504-2 [23] considers abrasive blast cleaning to be the most effective method for mechanical surface preparation. Experience in other sectors also suggests that this method is the most effective and has the most reproducible results [19]. It has been demonstrated experimentally [27] that the different cleaning methods lead to contrasting surface topographies and variability in their ability to remove corrosion deposits. Hand 39 BS EN ISO 24817, Section J.2 Page 43 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group cleaning with a wire brush to a preparation grade of St 2 and power-tool cleaning with a rotating abrasive belt to St 3 have been shown to produce inconsistent surface topographies with clear identifiable regions of oxides still visible. In contrast, the use of a specialised rotary bristle tool40 or grit blasting to Sa 2.5 results in considerably more uniform surface topographies, with little to no visible oxides. In terms of durability, it has been demonstrated that grit blasting to a preparation grade of Sa 2.5 leads to superior results compared to a preparation grade of St 3 (achieved using a rotating abrasive belt power tool in [27]) and significantly improved results over a preparation grade of St 2 (achieved manually using a wire brush in [27]). The latter, in particular, led to very poor durability characteristics. It was demonstrated that the specialised rotary bristle tool can lead to results comparable41 to those achieved via grit blasting to Sa 2.5. As such, hand or power tool cleaning (to a surface preparation grade of St 2 and St 3) using a wire brush and a rotating abrasive belt have been demonstrated to be ineffective. The difference in performance between a rotating abrasive belt and the specialised rotary bristle tool highlights the importance of power tool selection. Preparation grade is simply a way of classifying visual surface cleanliness, the broader requirements for adhesion already outlined in Section A2.1 apply. It was found that the addition of a chemical treatment step (silane) to a grit blasted surface to a preparation grade of Sa 2.5 (as per Section A2.6.2) improved durability still further. An overall observation was that despite a clear hierarchy being established, there remains some doubt over current practice and its ability to guarantee optimum durability. Further, it was highlighted that water and therefore water-based fluids are particularly deleterious to adhesive bonds. A number of the above observations are corroborated by a review of in-service failures [13] where it was found that more failures were ultimately attributed to ‘bonding issues’ when a substrate had been prepared to St 2, as compared to St 3 and particularly Sa 2.5. However, overall, the study found that the failure rate was very low. It was also noted that the data suggested that the majority of failures occurred instantaneously. However, in both cases this may be a reflection that in the vast majority of instances composite repairs have been used on a short term basis only – typically to coincide with the expected cycles of shutdowns or maintenance schedule. A3 Defect / Leak Sealing Repairs to defects that have gone through-wall and are leaking are possible but require special consideration. It is particularly important to verify that any leak sealing device/technology has isolated the leak and will do so for the duration of the repair installation, including curing. There have been several repair failures on safety critical equipment where it was established that the 40 In these tests a Monti Bristle Blaster® was used. The Bristle Blaster® is a type of rotary bristle power tool and has the potential to result in a surface cleanliness that exceeds St 3 as per BS EN ISO 8501-1. Visually, without magnification, it has the potential to produce a bare metal appearance that is similar to Sa 2.5. 41 It is important to note that consistent with other power tools, the potential for cross-contamination of the surface remains. Results are based on flat plate trials only. Page 44 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group approach to leak sealing was inadequate at the time of repair installation [12]. The presence of any leak sealing device should be considered at the design stage and the size/geometry of defect selected to encompass the device and any filler used. A4 Cure A4.1 General It is important that the same level of cure (or glass transition temperature) is achieved during the manufacture of the repair as was qualified and used in the design. Cure duration and any post cure requirements should be considered in the repair assessment to ensure a suitable repair system is applied. A4.2 Cure Schedule The cure schedule describes the temperature time/ profile. It should have been established that the cure schedule is suitable to achieve the necessary Tg value. Where, based on qualification testing, the supplier can demonstrate that the required glass transition temperature is achieved by ambient cure alone, then heat treatment may be omitted. In all other cases the supplier shall provide a heat treatment procedure (temperature profiles and hold times) which has been demonstrated to achieve the required glass transition temperature during qualification. Post curing should only be undertaken once the resin has hardened and on equipment that is depressurised and drained. Any heat applied to cure must be controlled and known. Taking credit for heat treatment due to heating from process fluid is not permitted. The operator should be aware of the time required for cure and the requirement that the repair is to be cured to an acceptable level (see A4.3) before the pressure is brought back to normal operating conditions. Not doing so has been identified as the principal reason for repair failure during this phase of the repair installation [12]. Consideration needs to be afforded to the total number of layers that make up the repair laminate, the number of layers that can cured at one time, and the cumulative time this will take. A4.3 Quality Assurance Checks Hardness testing (Shore or Barcol) is not a direct measurement of cure but can provide an indication that the repair system has cured to an acceptable level. When measured, the hardness should not be less than 90% of the minimum value obtained from repair system qualification42. Hardness testing alone should not be relied upon to infer an acceptable level of cure. Temperature profiles and hold times should also be scrutinised. A4.4 Special Considerations Design temperature should be carefully considered. If a line has a high design temperature but operates at a lower temperature, the use of a high temperature resin system may result in under curing of the laminate leading to a failed repair - unless the repair is post-cured before being put in service. 42 BS EN ISO 24817: 2017, Section 7.5.3 Page 45 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group A5 In-service Inspection A5.1 General Inspection requirements are a key input at the decision making stage when evaluating options for remedial action. The three candidate areas for inspection are: (1) the repair laminate; (2) the substrate; (3) the bond between the repair laminate and the substrate. A range of inspection techniques are available with different capabilities and limitations. Depending on defect type, consequences of failure, extent of the inspection and data requirements, it is possible that more than one technique will be required A5.2 Extent and Periodicity When determining the extent and periodicity of inspection, consideration should be given to the degradation mechanism(s) of the substrate as well as consequences of failure. A risk based inspection (RBI) type approach (or suitable equivalent) is advised. The accuracy of the defect report is important as it informs the appropriate selection of NDT techniques. For non-safety critical applications it is likely that any inspection schedule will be limited to a periodic visual examination only. Appendix B provides an overview of some possible defects. These are limited to the external surface of the repair and substrate. For safety critical applications, in addition to visual inspection, inspections should employ available non-destructive testing (NDT) equipment to confirm the condition of the substrate. For external substrate defects that are not through-wall, the maintenance strategy should consider the condition of the repaired substrate as well as the repair. Along with ensuring that the repair laminate remains intact, there should be no evidence of damage to the laminate, edge lifting/disbonding, or corrosion at the edges of the repair. The periodicity of any inspection should be such that the integrity of the line remains assured. The threat of internal corrosion must be considered throughout the life of the repair. If internal corrosion is determined as active, then the end user should discuss implications with the repair supplier; particularly the suitability of the installed repair in the context of this additional threat. In some cases a suitable strategy to mitigate the threat may be determined (e.g. change in process conditions, use of inhibitors or reduced life of repair, etc.). For internal or through-wall defects further deterioration or growth of the defect may continue despite application of the repair, unless other measures are taken and are verified to be effective. In addition to the requirements of the external corrosion case, the maintenance strategy should ensure that the internal defect does not grow to a size greater than that assumed in the design or that the repair laminate does not disbond from the substrate. It is important to be aware of, and take account of, the increased risk profile when a defect is through-wall and the repair is acting as the primary means of containment. This may have been due to an external and/or internal mechanism. The integrity of the repair must be ensured throughout its lifecycle. A5.3 Capabilities and Limitations A range of NDT techniques are available each with their own capabilities and limitations. Appendices C-E provides a summary with respect to the key areas to inspect [28]. These summaries Page 46 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group should be used as a basic guide, identifying candidate techniques for subsequent detailed discussions with inspection companies, as appropriate. It is notable that for a number of NDT techniques, whilst their capability to detect absolute values is restricted, they can be used to identify change. i.e. comparing before and after. Whilst some NDT techniques can identify and size bondline defects, there remains no validated inspection technique to establish the integrity of the bond, emphasising the importance of appropriate surface preparation and adherence to qualified procedures. It has been found [29] that whilst there are a range of techniques available, pulsed eddy current (PEC), radiography and dynamic response spectroscopy (DRS) are the most established techniques for the inspection of composite repairs, despite each technique having its own limitations. Depending on a range of factors, both radiography and DRS have the potential to identify both laminate and bondline defects. This is a particular strength of the DRS technique and, as such, it has been used as a quality assurance tool post installation. The application of a composite repair prevents the subsequent use of some NDT techniques to establish the condition of the substrate. This includes standard ultrasonic testing, including phased array, as well as surface NDT methods such as dye penetrant testing, visual examination and magnetic particle inspection. Further details on in-service inspection is provided in Section 6.3. A5.4 Practical Considerations In addition to the points raised in Section A5.3, the viability of successfully deploying any NDT techniques should be considered at the decision making stage. Consideration should be given to conducting an inspection to confirm that the selected inspection techniques are viable from a capability and practical standpoint. A5.5 Baseline Inspection For safety critical repairs, a baseline inspection should be conducted pre43 and post repair installation. The post installation inspection serves two purposes. Firstly, for some techniques it affords an opportunity to establish the quality of the repair installation. Secondly, it permits a comparison of future inspection data to ‘as installed’. This is particularly applicable for techniques that can be used to identify change over time. A6 Training and Competency A6.1 General All end user employees involved in the specification, application and management of engineered composite repairs should have had sufficient training and experience to be deemed competent [30]. Composite repair technology is a specialised field, potentially employing a range of materials and processes that are unfamiliar to many. A review [30] has recommended the following training: 43 This depends on how comprehensive/time since the anomaly report was prepared and whether sufficient data was acquired during the viability inspection to preclude this additional step. Page 47 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group 1. Training for operator/client personnel involved in engineered composite repair installation to give them the knowledge of the systems and awareness of the potential issues and increased likelihood of failure if the repair is not prepared, installed and cured as specified. 2. Training for installers, supervisors and client personnel in human factors aspects surrounding the management, installation and inspection of engineered composite repairs may help with the understanding of the nature and type of human errors and the factors that may make errors and short cuts more likely. A6.2 Applicability Candidates for (tailored) training programmes are: 1. Technical Authority (or equivalent) 2. On-site field engineers (or equivalent) 3. On-site inspection engineers (or equivalent) The ‘Technical Authority’ (or equivalent) should have a sufficient level of competency to review repair supplier design proposals and verify that they are fit for purpose. Further, they should be aware of the general capabilities and limitations of composite repair technology and NDT techniques. This will inform the decision making process as to whether a composite repair is feasible/appropriate. In addition, when the repair has been installed and added to the repair register, the ‘Technical Authority’ should be able to review the repair close out documentation and establish that the repair reflects what was proposed and is fit for purpose. For safety critical repairs, an end user representative should be at the repair site to verify hold points and act as a further level of quality assurance/control. With this in mind, ‘on-site field engineers’ (or equivalent) should have an awareness of the key hold points as well as the pre/post installation quality assurance checks. They should have the necessary competence to sign-off the repair following inspection and reviewing any associated documentation/paperwork. On-site inspection engineers (or equivalent) should have a sound appreciation of composite repair technology. Specifically, they should be aware of the key areas to inspect and allowable limits for defects. They should be competent in reviewing inspection data (visual and/or more sophisticated forms of NDT) and highlighting anomalies for further investigation. A6.3 Training Competence can be developed through training and/or operational experience. The most effective is likely to be a combination of the two. A number of repair suppliers now offer composite repair awareness training courses which present an ideal opportunity to learn about the technology. The courses often take the form of theoretical and practical sessions. In many cases, bespoke courses can be provided, catering for the direct needs of the client. A7 Applications A7.1 General BS EN ISO 24817 covers the qualification and design, installation, testing and inspection procedures for composite repair systems involving damage commonly encountered in oil, gas, utility pipework Page 48 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group systems and vessels. For pipework systems, this can mean repairing a range of geometries including: straights, tees, bends, reducers and flanges. A7.2 Performance and Reliability A review of in-service failures [13] suggests that for pipework systems the rate of failure is highest for repairs to reducers and tees. Vessels require special consideration, with over one in ten repairs subsequently failing in service [13]. This failure rate is significantly higher than for all other repair types. A large number of these failures were attributed to difficulties in consolidating the repair onto the side of the vessel. Such repairs often take the form of a patch rather than a circumferential wrap and can be more challenging to apply successfully. A7.3 Special Considerations For novel repairs, perhaps infrequently applied, or repairs with specific considerations (e.g. restricted access), consideration should be given to undertaking full-scale feasibility trials [30]. Such trials can prove informative for both the repair supplier and the client. They can help establish whether a composite repair is viable, as well as informing and optimising any procedures which may take place at the repair site. The time and effort afforded to such an activity is likely to only be warranted for safety and potentially business critical repairs. A8 Repair Lifetime A8.1 General All engineered composite repairs should have a design life and a defined life. These should be clearly stipulated in all relevant documentation, including the defined life repair register. A8.2 Design Life The design life is the maximum application lifetime of the repair. It is defined by the owner and used by the repair supplier for the purposes of design. It may transpire that the owner defined design life is not feasible given the defect type and service conditions. Ultimately, it should be agreed between the repair supplier and the client. It is important that the client ensures that any information/data used for the purposes of design by the repair supplier is robust and accurate. Each engineered repair shall have a design life which may be the same, but shall never be less than the defined life of the repair. Composite repairs shall have a specified minimum design life of two years44. As the repair design is based on the (initial) input data provided by the client, for safety critical repairs it is important that any potential deviations (through-life) are discussed with the repair supplier. This may be informed by, for example, inspection data or a change in process conditions. The revised input data may mean that an engineered composite repair is no longer an appropriate solution or result in the design life being reduced unless some form of remediation is undertaken. 44 BS EN ISO 24817:2017, Section 7.3 Page 49 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group Once a repair has exceeded its design life it shall be removed or re-evaluated. Section 6.4 provides a more comprehensive overview of design life reduction and extension. A8.3 Defined Life The defined life is the actual application or intended service lifetime of the repair. The defined life is set by the end-user with due consideration of the risks associated with each repair and defines the time after which the repair needs to be re-validated or its removal scheduled. Defined life extension does not generally require repair supplier input, rather re-consideration of the risks associated with the repair. For safety critical applications the defined life should be set by the risk assessment on a case by case basis. For safety critical applications, if the repair is intended to provide the primary means of containment (either immediately after application or at any time during the life of the repair) it should be considered for short-term use only45. Special consideration should be afforded to scenarios where there is an active internal degradation mechanism where damage has not yet broken through wall but could do so during the life of the repair. In this case, the ability of the repair to provide primary containment must be demonstrated for the largest defect that is considered may develop. Initial, successful performance of the repair, shall not be considered to provide any indication of future reliability because of the changes expected in the defect. It should be noted that the risk profile associated with each repair can change over time, for example, this may be influenced by changes in process conditions, inspection findings etc. As such, for safety critical repairs the defined life should be subject to periodic review to confirm that the design basis is still appropriate and valid. 45 Consideration should be given to bringing shutdowns forward if the risk profile warrants such action – the integrity of the repair must be ensured throughout its lifecycle. Page 50 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group APPENDIX B – VISUAL INSPECTION CHECKLIST Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group APPENDIX C – NDT TECHNIQUE SELECTION CHART (PART A) [29] Page 52 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group APPENDIX D – NDT TECHNIQUE SELECTION CHART (PART B) [29] Page 53 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group APPENDIX E - NDT TECHNIQUE SELECTION CHART (PART C) [29] Aspect Large pipe diameters Thick walled pipe Thin walled pipe Substrate magnetic properties Repair material(s) Small pipe diameters Wrap thickness Wrap surface quality Liquid within pipe Presence of welded features, attachments or component edges Extent of wrap coverage Principal effects on inspection techniques Radiography: May limit application for tangential radiography, typical upper limit 8” for Schedule 40 pipes, increasing to 14” for thinnest walls; exact limit depends on pipe wall thickness and radiation source being used PEC: Probe contact limitations, Typical lower limit 1” DRS: Probe contact limitations, Typical lower limit 4” Radiography: May limit application depending on radiation source being used in the case of tangential radiography PEC and DRS: Typically 3 mm lower wall thickness, limit increases with wrap thickness for DRS PEC: Requires magnetic material such as C-steel; cannot be used on austenitic, duplex or super-duplex steels Microwave: cannot be used on carbon fibre wraps (Material must be non-conducting) Visual: Less effective on carbon fibre wraps or painted wraps due to reduced contrast DRS: Putty/filler used for repair of external defects can potentially prevent WT measurements in those areas PEC: Wrap thickness increases lift-off and therefore exacerbates wall thickness averaging effect DRS: Limited to 12 mm wrap thickness in most cases, up to 19 mm by exception Radiography: Thick wraps can decrease image resolution Laser Shearography: Limited to ~10 mm thick Laser Shearography: Surface scratches or gouges can affect image quality DRS: Poor surface quality such as wrinkles limits applicability of method Radiography: Presence of oil or water reduces image resolution and increases required exposure time GWU: Length range of inspection is reduced by presence of high viscosity fluids PEC: Reduced resolution at locations nearer to an edge or attachment than one probe footprint diameter GWU: Welded attachments and flanges can affect results GWU: Requires access to a bare pipe surface on at least one side of the wrap Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group APPENDIX F – HOLD POINTS AND MANUFACTURING CONSIDERATIONS Method statement (and supporting design information) Check cure requirements are appropriate and achievable. Confirm defect details and location. Confirm substrate geometry and material. Confirm surface preparation requirements and that the repair supplier has undertaken qualification testing using the methods to be employed on-site. Confirm verification activities have taken place, if required. Confirm assumptions are valid and realistic. Verify worksite requirements. Confirm who is responsible for what and liaise with all parties, as appropriate. Materials Preparation Check all materials to be used for repair: o Fibre reinforcement o Resin o Filler o Hardener o Batch numbers o Dates etc. Environmental conditions Verify environmental conditions repair: o Relative humidity o Dew point o Substrate surface temperature If required, confirm the following has been provided: o Access o Lighting o Shelter o Work area/table for material preparation Surface preparation Confirm that exposure times between steps has been kept to an absolute minimum. Verify that the substrate is free from contamination - water, service fluids, oils etc. Undertake salt test, if required. Confirm that the preparation grade achieved on-site is the same as assumed in the design/method statement – including extent of surface preparation. Confirm that surface preparation method/tool used on site is the same as that assumed in the design/method statement. Ensure that the correct number of surface profile measurements are taken. Confirm within limits. Confirm acceptable stipple test result. Page 55 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group Filler Profile Check correct filler used, as appropriate, so that there is a smooth profile prior to application of the laminate. Installation Ensure that the correct materials are used / are in date etc. Ensure all mixing is done correctly. Ensure that the lamination process occurs as soon as possible after surface preparation activities are completed. Ensure that the correct number of layers are applied. Ensure that each consecutive layer of reinforcing fabric is wetted out with resin and is appropriately consolidated. Ensure the fibre direction is as per the design. Ensure the layers of the repair are free from foreign matter and contamination Tests on repair laminate Ensure that the curing cycle has been completed in accordance with the requirements. Ensure hardness check completed and recorded. Verify within limits. Review temperature profiles and hold times. Verify repair thickness. Verify axial length and taper length of the repair. Verify inspection has been completed and the results recorded. Check within limits. Verify that a photographic record has been taken. Verify the corrosion barrier been reinstated. Verify that baseline NDT has been carried out (if required). Verify the repair been identified and tagged. QA Records Ensure the repair process (as undertaken on site) is fully documented in a close out report, to include: o Repair reference number o Visual inspection report o Thickness measurement o Repair axial extent measurement o Curing Details o Personnel who applied repair o Hardness measurement (if undertaken) o DSC measurement (if undertaken) o Bond strength measurements (if undertaken) o Inspection and NDT results (if undertaken) Pressure Testing Undertaken if required. Page 56 of 56 Commercial in Confidence Strictly not to be circulated outside SRP Engineered Composite Repair Sponsor Group HSE’s Buxton operations are certified to: ISO 9001 OHSAS 18001 Health and Safety Executive Science Division Harpur Hill Buxton Derbyshire SK17 9JN UK www.hsl.gov.uk www.hse.gov.uk/research 1.2 Redgrave Court Merton Road Bootle L20 7HS T: +44 (0)20 3028 2000 E: hslinfo@hsl.gsi.gov.uk help employers reduce injuries, accidents, and ill health amongst their workforce, increasing productivity and delivering healthier workplaces. In addition to the wide range of analytical services, HSL social Page 57 of 56 scientists can help customers identify ways to