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PRACTICAL Physical and chemical changes

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General Chemistry Unit 2
Physical and chemical changes
Name: __________________________________ Class: _____________
Change
1. Copper (II) sulphate and water (Demo)
Watch while your teacher dissolves some copper
(II) sulphate in water.
2. Sucrose and concentrated sulphuric acid
(Demo)
Observations
Word equation for change
Chemical or physical change? Why?
Before
Word equation:
After
Chemical or physical? Why?
Before
Word equation:
After
Chemical or physical? Why?
Before
Mass: ____________
Word equation:
Watch while your teacher reacts sucrose (sugar)
with concentrated sulphuric acid.
3. Magnesium and oxygen
Weigh a ~5cm magnesium ribbon. Place your
Bunsen on a heat mat.
Light your Bunsen (air holes closed). Open the air
holes, if necessary, to get a short flame that’s blue
at the bottom and yellow at the top.
Hold the magnesium ribbon at one end with the
crucible tongs and place the other end in the
purple part of the flame. Don’t look directly at the
flame! Once all the magnesium has turned to ash,
try to collect all the ashes and weigh them.
Chemical or physical? Why?
After
Mass: ____________
Change
4. King Kong’s hand (Demo)
Watch while your teacher solves a problem
that has to do with their Halloween costume.
5. Copper (II) sulphate and iron
Obtain the following materials: one pair of safety
glasses per person, test tube rack, test tube, iron
nail. Pour some copper(II)sulphate solution into a
test tube. About half a test-tube should be
enough.
Carefully place an iron nail into the test tube and
wait for the reaction to happen. It’s slow, so clean
up a bit and do some post lab questions and then
come back to have a look at it. Come back after a
couple of days and have a look at it again.
Observations
Word equation for change.
Chemical or physical change? Why?
Before
Word equation:
After
Chemical or physical? Why?
Before
Word equation:
Chemical or physical? Why?
After
Questions (answer on a separate sheet of paper)
1. Which was your favourite change? Why? [2]
2. Explain what happened in change #2 [2]
3. The mass of magnesium oxide at the end of change #3 should have been greater than the mass of magnesium at the beginning. Why?
[2]
4. Chances are some magnesium was lost in change #3. Suggest one way to improve this procedure so that little/no magnesium oxide is
lost. This improvement must be specific and achievable in a school laboratory. [3]
5. State and try to explain what the brown precipitate was in change #5. (Hint: it’s not rust)[2]
6. A lit Bunsen burner is also an example of a chemical change. Explain why. [1]
TEACHER INSTRUCTIONS
1. Copper sulphate + water
This is simply a demonstration of how to make a standard solution. There is no need to mass the copper sulphate, just show them the
steps and emphasise how to read the meniscus, as well as introducing volumetric flasks.
2. Dehydrating sugar with sulfuric acid
-
Best do this in an extraction hood.
Safety goggles must be worn.
Beaker gets very hot. Leave to cool or ask for a tray to move it around.
Wear gloves
The resulting black carbon “tower” should be neutralised prior to disposal.
3. Burning magnesium
-
Wear safety goggles
Place the Bunsen on a heat mat
Mass a piece of magnesium ribbon (~5cm) and get students to write down the mass
Use crucible tongs to hold end of magnesium in the hottest part of the Bunsen flame (the violet/blue bit in the middle of the flame)
Tell students squint their eyes (nearly shut) and not look at the magnesium directly as soon as it lights up. The resulting white
powder is magnesium oxide
Recover as much magnesium oxide as you can and mass it – it should have a greater mass than the Mg by itself because now it also
contains oxygen atoms. Use this to introduce the idea of combination reactions where two elements react together to form a
compound.
Discard MgO in rubbish bin when cool
4. King Kong's Hand
This is FUN. Good for reinforcing states of matter too.
-
Wear safety goggles
Have students draw “hairs” onto the glove.
Pour vinegar into two of the fingers in a glove, and sodium hydrogencarbonate in another.
Pull together the top of the glove and mix the reactants together. Best do this over a sink, as the carbon dioxide produced inflates the
glove and it might burst.
Disposal: The contents may be safely poured down the drain.
5. Copper (II) sulphate and iron
This is a displacement reaction – the sulphate “changes hands” and copper is deposited onto the nail. This happens because iron is more
reactive than copper so it tends to be in a compound.
copper sulphate + iron

iron sulphate
+
copper
Blue solution
grey metal
clear and colourless solution
red metal
Use the copper sulphate you made in 1. Make a point of explaining the red solid that appears is not rust. Rusting is a much much slower
process than this. You will be able to see results nearly straight away and they will become really obvious within 30 mins or so. This is a
good experiment to reinforce safety rules and expectations without much of a hazard so students can do it themselves. Ask them to pour the
left over solution into a big waste beaker and to give the nail back to you. Place the nails on a paper towel. The reaction might stain the test
tube.
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