METROLOGY & MEASUREMENT METROLOGY & MEASUREMENTS [COMMON TO III SEM MECHANICAL / I&P] MME 3104 METROLOGY & MEASUREMENTS [3 0 0 3] METROLOGY & MEASUREMENTS No. of Lecture hours: 36 Measurements and measurement systems: Methods of Measurement, Generalized Measurement System & its elements, Static Characteristics of Instruments & measurement systems: Accuracy, Precision, Sensitivity, Reproducibility, Repeatability, Linearity, Hysteresis. Threshold, Dead zone, Resolution. Errors in Measurement. [03] Measurement of pressure: Definition of Pressure. List of instruments used to measure pressure. Methods of pressure measurement Elastic pressure elements (Bourdon Tube, Bellows, Diaphragm), McLeod Gauge and Bridgman gauge, Related problems. [04] Measurement of temperature: Methods of temperature measurement Pressure thermometer, Electrical Resistance thermometer, Thermocouples, Pyrometer (Disappearing filament type optical pyrometer) & Problems, Bimetallic thermometer. [03] Measurement of strain: Types of electrical resistance strain gauges, Theory of operation of wire wound strain gauge, Gauge Factor, Strain gauge bridge circuit, Calibration Circuit, Temperature compensation, Strain measurement on static and rotary shaft, Orientation of strain gauges. Simple problems related to measurement of strain using strain gauge. [05] Measurement of force, torque and shaft power: Measurement of Force - Hydraulic & Pneumatic load cells, Proving ring, Strain gauge load cell & related problems. Methods of Torque & Shaft power Cradled dynamometer, Torque Meter, Band Brake dynamometer, Water Brake dynamometer. [03] Limits, Fits and Tolerances: Terminology (as per Indian Standards IS 919), Grades of Tolerances, Letter symbols for tolerances, Fits – definition, Types of fits – Clearance, Interference and Transition. Numerical on limits and fit. [03] Department of Mechanical & Manufacturing Engineering, MIT, Manipal 1 METROLOGY & MEASUREMENTS METROLOGY & MEASUREMENT Gauges: Taylor’s principle for design of gauges – Statements and explanation, Gauge Maker’s tolerance – as per 3rd system (present British standards), Numerical on design of gauges (complete shaft and hole pair) ,Types of gauges – Plug gauge, Ring gauge, Taper plug gauge, Taper Ring gauge and slip gauges. [03] Measurement of form errors: Straightness measurement– using straight edge, using Autocollimator. Squareness measurement – Engineer’s Square tester, Optical Square. Simple numerical on Straightness, Flatness and Squareness measurement. [04] Surface texture measurement: Definitions - I, II, III, IV order (including their causes), Roughness and Waviness, Lays, Indian standards symbols for Roughness, Analysis of traces – Ra, Rz, Rt, Rq, Sampling length, hrms and Centerline Average (CLA), Simple numerical on surface roughness. [04] Screw threads: Definitions of elements of external screw threads, Pitch error in threads: Progressive and Periodic, Measurement of the elements of the threads – Effective diameter using screw thread micrometer, two wire and three wire methods, Best size wire, Simple numerical on screw threads. [04] MME 3104 METROLOGY & MEASUREMENTS [3 0 0 3] References: 1. Beckwith Thomas G., Mechanical Measurements, Pearson Education, Delhi, 2003. 2. Jain R.K., Engineering Metrology, Khanna Publishers, New Delhi, 1997. 3. Sawhney A.K., Mechanical Measurement & Instrumentation, Dhanpat Rai & Co, New Delhi, 2002. 4. Nakra B.C. and Chaudry K.K., Instrumentation, Measurement & Analysis, Tata McGraw Hill, New Delhi, 2002. 5. Gupta I. C., Engineering Metrology, Dhanpat Rai Publications, New Delhi, 1997 6. ASTME, Handbook of Engineering Metrology, Prentice Hall of India, New Delhi, 1972 7. Raghavendra N.V. and Krishnamurthy L., Engineering Metrology and Measurements, Oxford University Press, 2013. Department of Mechanical & Manufacturing Engineering, MIT, Manipal 2 METROLOGY & MEASUREMENT Temperature Measurements Introduction Temperature measurement is the most common and important measurement in controlling any process. Temperature may be defined as an indication of intensity of molecular kinetic energy within a system. It is a fundamental property similar to that of mass, length and time, and hence it is difficult to define. Temperature cannot be measured using basic standards through direct comparison. It can only be determined through some standardized calibrated device. Change in temperature of a substance causes a variety of effects such as: i) Change in physical state, ii) Change in chemical state, iii) Change in physical dimensions, iv) Change in electrical properties and v) Change in radiating ability. And any of these effects may be used to measure the temperature The change in physical and chemical states cannot be used for direct temperature measurement. However, temperature standards are based on changes in physical state. A change in physical dimension due to temperature shift forms the basis of operation for liquid-in-glass and bimetallic thermometers. Changes in electrical properties such as change in electrical conductivity and thermoelectric effects which produce electromotive force forms the basis for thermocouples. Another temperature-measuring method using the energy radiated from a hot body forms the basis of operation of optical radiation and infrared pyrometers. Temperature Measurement by Electrical Effects Electrical methods of temperature measurement are very convenient because they provide a signal that can be easily detected, amplified, or used for control purposes. In addition, they are quite accurate when properly calibrated and compensated. Several temperature-sensitive electrical elements are available for measuring temperature. Thermal emf and both positive and negative variations in resistance with temperature are important among them. Thermo resistive Elements The electrical resistance of most materials varies with temperature. Resistance elements which are sensitive to temperature are made of metals and are good conductors of electricity. Examples are nickel, copper, platinum and silver. Any temperature-measuring device which uses these elements are called resistance thermometers or resistance temperature detectors (RTD). If semiconducting materials like combination of metallic oxides of cobalt, manganese and nickel having large negative resistance co- efficient are used then such devices are called thermistors. Electrical Resistance Thermometers The desirable properties of resistance-thermometer materials are: i) The material should permit fabrication in convenient sizes. ii) Its thermal coefficient of resistivity should be high and constant iii) They must be corrosion-resistant and should not undergo phase changes within the temperature ranges iv) Provide reproducible and consistent results. Unfortunately, there is no universally acceptable material and the selection of a particular material depends on the compromises. Department of Mechanical & Manufacturing Engineering, MIT, Manipal 3 METROLOGY & MEASUREMENT Although the actual resistance-temperature relation must be determined experimentally, for most metals the following empirical equation may be used: Rt = Ro (l + aT + bT2) Where, Rt is the resistance at temperature T, Ro is the resistance at the reference temperature, T is the temperature and a & b are constants depending on the material. Usually platinum, nickel and copper are the most commonly used materials, although others like tungsten, silver and iron can also be used. However, over a limited temperature range around 00 C (273 K), the following linear relationship can be applied: Rt = Ro (l + α t) Where, α = the temperature coefficient of resistance of material in (Ω/Ω)/0C, Ro is the resistance at 00C, t is the temperature relative to 00C. If a change in temperature from t1 to t2 is considered, the above equation becomes: R2 = R1 + Ro α (t2 – t1), Rearranging gives: t2 = t1 + [(R2 – R1) / α R0] Some typical values of α are: Copper = 0.00430C-1, Nickel = 0.00680C-1, Platinum = 0.00390C-1 The construction of the resistance thermometer is as shown in the figure, where the wire of metal is wound on the grooved hollow insulating ceramic former covered with protective cement. The ends of the coils welded to stiff copper leads that are taken out to be connected in one of the arms of the Wheatstone bridge circuit. The resistance thermometer is introduced in to the media whose temperature is to be measured. Due to a change in temperature, the resistance wire of the thermometer gets heated and due to this heats the resistance of the wire changes. Now this change in resistance of the wire is measured using the Wheatstone bridge. Example: The element of a resistance thermometer is constructed of a 50 cm length and of 0.03 mm diameter nickel wire. The resistivity of nickel wire is wire is 7.8 μΩcm. Nominal resistance R0 of the element is given by, R0 = ρ L / A ρ = 7.8 x 10-8 Ω-m and L= 50 x 10-2m and A = (π / 4) x (0.03 x 10-3)2 R0 = [(7.8 x 10-8) x (50 x 10-2)] / 7.07 x 10-10 = 3.9 x 10-8 / 7.07 x 10-10 = 55.16Ω Over a limited temperature range around 0ºC, the linear relationship is given by Rt = R0 (1 + α t) If a change in temperature from t1 to t2 is considered, the above equation becomes: R2 = R1 + R0 α (t2 - t1) i.e., (R2 - R1) / (t2 - t1) = R0 α Department of Mechanical & Manufacturing Engineering, MIT, Manipal 4 METROLOGY & MEASUREMENT By assuming temperature coefficient of resistance (0.0068ºC-1) is constant over the common range of ambient temperatures, the change in resistance of the element per degree centigrade is given by, ∆R / ∆t = R0 x α = 55.16 x 0.0068 = 0.3751Ω / ºC Thermo-electric Sensors: 1. See beck Effect: When two dissimilar metals are joined together as shown in the Fig. an electromotive force (emf) will exists between the two points A and B, which is primarily a function of the junction temperature. This phenomenon is called the see beck effect. Junction of Two Dissimilar Metals 2. Peltier effect If the two metals are connected to an external circuit in such a way that a current is drawn, the emf may be altered slightly owing to a phenomenon called the peltier effect. 3. Thomson effect Further, if a temperature gradient exists along either or both of the metals, the junction emf may undergo an additional slight alteration. This is called the Thomson effect. Hence there are, three emfs present in a thermoelectric circuit: i) The See beck emf, caused by the junction of dissimilar metals ii) The Peltier emf, caused by a current flow in the circuit and iii) The Thomson emf, resulting from a temperature gradient in the metals. The See beck emf is important since it depends on the junction temperature. If the emf generated at the junction of two dissimilar metals is carefully measured as a function of temperature, then such a junction may be used for the measurement of temperature. The above effects forms the basis for a thermocouple which is a temperature measuring element. Thermocouple If two dissimilar metals are joined an emf exists which is a function of several factors including the temperature. When junctions of this type are used to measure temperature, they are called thermocouples The principle of a thermocouple is that if two dissimilar metals A and B are joined to form a circuit as shown in the Fig. It is found that when the two junctions J1 and J2 are at two different temperatures T1 and T2, small emf's e1 and e2 are generated at the junctions. The resultant of the two emf's causes a current to flow in the circuit. If the temperatures T1 and T2 are equal, the two emf's will be equal but opposed, and no current will flow. The net emf is a function of the two materials used to form the circuit and the temperatures of the two junctions. The actual relations, however, are empirical and the temperature-emf data must be based on experiment. It is important Department of Mechanical & Manufacturing Engineering, MIT, Manipal 5 METROLOGY & MEASUREMENT that the results are reproducible and therefore provide a reliable method for measuring temperature. Basic Thermocouple Circuit It should be noted that two junctions are always required, one which senses the desired or unknown temperature is called the hot or measuring junction. The other junction maintained at a known fixed temperature is called the cold or reference junction. Laws of Thermocouples The two laws governing the functioning of thermocouples are: Law of Intermediate Temperature: The emf generated in a thermocouple with junctions at temperatures T1 and T3 is equal to the sum of the emf generated by similar thermocouples, one acting between the temperatures T 1 and T2 and the other between T2 and T3 when T2 lies between T1 and T3. This law permits the thermocouple calibration for a given temperature to be used with any other reference temperature through the use of a suitable correction. Also, the extension wires having the same thermo-electric characteristics as those of the thermocouple wires can be introduced in the circuit without affecting the net emf of the thermocouple. Law of Intermediate Metals: Insertion of an intermediate metal in to a thermocouple circuit will not affect the net emf, provided the two junctions introduced by third metal are at identical temperatures. Application of this law is as shown in Fig. In Figure, if the third metal C is introduced and the new junctions R and S are held at temperature T3, the net emf of the circuit will remain unchanged. This permits the insertion of a measuring device or circuit without affecting the temperature measurement of the thermocouple circuit In the Figure the third metal is introduced at either a measuring or reference junction. As long as junctions P1 and P2 are maintained at the same temperature TP the net emf of the circuit will not be altered. This permits the use of joining metals, such as solder used in fabricating the thermocouples. In addition, the thermocouple may be Department of Mechanical & Manufacturing Engineering, MIT, Manipal 6 METROLOGY & MEASUREMENT embedded directly into the surface or interior of a conductor without affecting the thermocouple's functioning. Thermocouple materials and Construction Any two dissimilar metals can be used to form thermocouple, but certain metals and combinations are better than others. The desirable properties of thermocouple materials are: i) Ability to withstand the temperature at which they are used, ii) Immunity from contamination/oxidation, etc. which ensures maintenance of prcise thermo-electric properties with continuous use, iii) Linear temperature-emf relationship The thermocouple materials can be divided into two types 1. Base-metal thermocouples, and 2. Rare-metal thermocouple. Base-metal thermocouples are the combination of pure metals and alloys of iron, copper and nickel and are used for temperature up to 1450 K. These are most commonly used in practice as they are more sensitive, cheaper and have nearly linear characteristics. Their chief limitation is the lower operating range because of their low melting point and vulnerability to oxidation. On the other hand, rare-metal thermocouples are the combination of pure metals and alloys of platinum for temperature up to 16000C and tungsten, rhodium and molybdenum for temperature up to 30000C. Example: A copper-constantan thermocouple was found to have linear calibration between 0C to 400C with emf at maximum temperature (reference junction temperature 0C) equal to 20.68 mV. If the indicated emf is 8.92 mV in the thermocouple circuit and the cold junction temperature is 25C, determine the temperature of the hot junction by using the law of intermediate temperature. Law of intermediate Temperatures states that the emf generated in a thermocouple with junctions at temperatures T1 and T3 is equal to the sum of the emf’s generated by similar thermocouples, one acting between the temperatures T 1 and T2 and the other between T2 and T3 when T2 lies between T1 and T2. E3 = E1 + E2 Department of Mechanical & Manufacturing Engineering, MIT, Manipal 7 METROLOGY & MEASUREMENT A copper-constantan thermocouple was found to have linear calibration between 0C to 400C with emf at maximum temperature (reference junction temperature 0C) equal to 20.68 mV. Sensitivity of the thermocouple = 20.68 / (400 – 0) = 0.0517 m V/ C. If the indicated emf is 8.92 mV in the thermocouple circuit and the cold junction temperature is 25C, then according to the law of intermediate temperature, E3 = E1 + E2 = (0.0517 x 25C) + 8.92 = 1.293 + 8.92 = 10.213 mV. Temperature of the hot junction = 10.213 / 0.0517 = 197.54C. Temperature measurement by Radiation methods (Pyrometry): Disappearing filament type optical pyrometer are a type of telescope having a filament inside it. When the telescope is aimed and focused towards the red hot object, the filament will be visible because of the difference in the two light intensities (red hot object and the filament). Now the filament is fed current from a standard battery through an adjustable resistance. The current is gradually increased until the tip of the filament just disappears; i.e., the difference in two light intensities becomes zero. At this instance, the current flowing through the lamp which is indicated by the mille voltmeter connected to the lamp becomes a measure of the temperature of the source when calibrated. Department of Mechanical & Manufacturing Engineering, MIT, Manipal 8 METROLOGY & MEASUREMENT Temperature measurement by non-electrical methods: Bimetallic Thermometer: The bimetallic thermometer uses the following two principles: All metals change in dimension, that is expand or contract when there is a change in temperature. The rate at which this expansion or contraction takes place depend on the temperature coefficient of expansion of the metal and this temperature coefficient of expansion is different for different metals. Hence the difference in thermal expansion rates is used to produce deflections which are proportional to temperature changes. A bimetallic strip is in the form of a cantilever beam. An increase in temperature will result in the deflection of the free end of the strip as shown. This deflection is linear and can be related to temperature change by R = {t [3 (1 + m)2 + (1 + m n) x (m2 + 1/ m n)]} / [6 (αH – αL) (T2 - T1) (1 + m)2] Where R = Radius of curvature at temperature T2 t = Total thickness of bimetallic strip = (t1 + t2) m = Thickness of lower expansion metal / Thickness of higher expansion metal = t 1 / t2 n = Modulus of elasticity of lower expansion metal / Modulus of elasticity of higher expansion metal αH = Coefficient of expansion of higher expansion metal αL = Coefficient of expansion of lower expansion metal T1 = Initial température T2 = Température of the source Example: A bimetallic cantilever with invar & brass as two metal strips of equal thickness has a total thickness of 0.125 cm & length 5 cm. Its one end is fixed; estimate the end deflection for change of temperature of 40C. The thermal coefficient of expansion of Invar & brass are respectively 1.7 x 10 -6/C and 20.2 x 106/C & their modulus of elasticity are respectively 147 GN/m 2 and 96.5 GN/m2. The radius of curvature of a bimetallic strip due to change in temperature is given by R = {t [3 (1 + m)2 + (1 + m n) x (m2 + 1/ m n)]} / [6 (αH – αL) (T2 - T1) (1 + m)2] Where R = Radius of curvature at temperature T2 t = Total thickness of bimetallic strip = (t1 + t2) m = Thickness of lower expansion metal / Thickness of higher expansion metal Department of Mechanical & Manufacturing Engineering, MIT, Manipal 9 METROLOGY & MEASUREMENT = t 1 / t2 = 1 n = Modulus of elasticity of lower expansion metal / Modulus of elasticity of higher expansion metal = 147 / 96.5 = 1.52 αH = Coefficient of expansion of higher expansion metal αL = Coefficient of expansion of lower expansion metal T1 = Initial température T2 = Température of the source T2 - T1 = 40ºC R = {1.25 [3 (1 + 1)2 + (1 + 1.52) x (12 + 1/ 1.52)]} / [6 (20.2 x 10-6 – 1.7 x 10-6) (40) (1 + 1)2] = {1.25 [12 + (2.52 x 1.66)]} / [6 x 18.5 x 10-6 x 40 x 4] = 20.229 / 0.0178 = 1139 mm Pressure Thermometer: Pressure thermometer is based on the principle of fluid expansion due to an increase in the pressure in a given volume of the temperature measuring systems. It is one of the most economical, versatile and widely used devices in industrial temperature measurements. It has relatively large metal bulb (often stainless steel) instead of glass. This results in a robust, easy-to-read thermometer that may be read remotely by connecting the bulb to a Bourdon gauge by means of a capillary tube as shown in figure. The entire assembly of the bulb, capillary and gauge is calibrated directly on the basis of pressure change corresponding to the temperature change. The bulb of the thermometer may be filled with either a liquid (usually mercury) or gas or a liquidvapour mixture and depending upon the type of fluid, the thermometer is termed as mercury-in-steel thermometer or constant volume gas thermometer or vapour pressure thermometer respectively. Department of Mechanical & Manufacturing Engineering, MIT, Manipal 10 METROLOGY & MEASUREMENT Review Questions Q1) Explain with neat sketch the method of measurement of temperature with resistance thermometer. Q2) A platinum resistance thermometer is used at room temperature. Assuming a linear resistance variation with temperature, calculate the sensitivity of the thermometer. Q3) The element of a resistance thermometer is constructed of a 50 cm length and of 0.03 mm diameter nickel wire. The resistivity of nickel wire is 7.8 μΩ-cm. By assuming temperature coefficient of resistance (0.0068ºC-1) is constant over the common range of ambient temperatures, what will be the change in resistance of the element per degree centigrade? Solved in Notes Q4) State the laws of thermo-electricity. Q5) State and explain laws of thermocouples (with sketches). Write expression for the relationship between thermoelectric emf and temperature gradient. Q6) A copper constantan thermocouple was found to have linear calibration between 0C to 400C with emf at maximum temperature (reference junction temperature 0C) equal to 20.68 mV(i) determine the correction which must be made to the indicated emf if the cold junction temperature is 25C. (ii) if the indicated emf is 8.92 mV in the thermocouple circuit, determine the temperature of the hot junction. Solved in PPT Q7)The hot junction of a chromel-alumel thermocouple is connected to a potentiometer terminal at 24C. The potentiometer whose terminals are at 24C reads 25.76 mV. What is the temperature of the thermocouple junction? The Solved in PPT calibration chart of the thermocouple is: 20 24 28 ………….…. 480 488 493 Temperature, C Voltage, mV 0.8 0.95 1.12 …………….. 26.25 26.72 26.04 Q8) What are pyrometers? Explain the working of an optical pyrometer with neat sketch. Q9) Explain the working of disappearing filament optical pyrometer with neat sketch. List its fields of application. Q10) Explain the basic principle on which the bimetallic thermometer works. How the deflection of the bimetallic strip is related to temperature change. Q11) A bimetallic strip is constructed of strips of yellow brass & Invar bonded together at 30C. Each has a thickness of 0.3mm. Calculate the radius of curvature when a 60mm strip is subjected to a temperature of 100C. One end of the bimetallic strip is fixed. The thermal coefficient of expansion of yellow brass & Invar are respectively 20.2 x 10 -6/ C & 1.7 x 10-6/ C & their modulus of elasticity are respectively 96.5 GN/m2 & 147 GN/m2. Solved in PPT Q12) Explain with a neat sketch the working of a pressure thermometer. Q13) A mercury in steel thermometer employs a Bourdon pressure gauge which has a range of 0 to 6.0MPA for a pointer rotation from 0-270ºc. In the temperature calibration process the pointer measurement set to 0º rotation at 0ºc and the instrument indicated 250 º rotations corresponding to 200ºc. Determine the sensitivity of the instrument in rad / ºc. Solved in PPT Q14) A platinum resistance thermometer has a resistance of 140.5Ω and 100Ω at 1000C and 00C, respectively. If its resistance becomes 305.3Ω when it is in Department of Mechanical & Manufacturing Engineering, MIT, Manipal 11 METROLOGY & MEASUREMENT contact with a hot gas, determine the temperature of the gas. The temperature Solved in PPT coefficient of platinum is 0.00390C-1. Q15) Explain the different thermocouple materials and their designation. Q16) Explain See beck, Thomson and Peltier effects. Department of Mechanical & Manufacturing Engineering, MIT, Manipal 12