QS-B220
DESKTOP EXPLOSIVES & DRUGS TRACE DETECTION SYSTEM
USER MANUAL
500 Research Drive Unit 3
Wilmington, MA 01887 USA
Document Number 42400026 Rev.G
NOTICES
WARRANTY INFORMATION
© 2015 Implant Sciences Corporation
All Rights Reserved
The information contained herein is proprietary
and is provided solely for the purpose of allowing
customers to operate and/or service Implant
Sciences Corporation manufactured equipment and
is not to be released, reproduced, or used for any
other purposes without written permission of
Implant Sciences Corporation (Implant Sciences).
Implant Sciences has made every reasonable
attempt to ensure that the system is in optimum
working condition. Failure to operate the
equipment precisely as described in this manual
may result in personal injury and void system
warranty. Implant Sciences will not be held liable in
instances of improper or unauthorized operation of
equipment.
Information and specifications in this manual are
subject to change without notice. Quantum Sniffer,
inCal, Implant Sciences, and the Implant Sciences
logo are trademarks of Implant Sciences
Corporation. Throughout this manual, trademarked
names may be used. Use of trademark symbols is
not used in every instance as the names are used
only in an editorial fashion, with no intention of
infringement.
The
software
contained
in
the
QS-B220 system and accompanying materials are
copyrighted.
Unauthorized copying of the
software, including software that has been
modified, merged, or included with other software
or the written materials is expressly forbidden
without the prior written consent of Implant
Sciences. All right, title, and interest in all copies of
this software are and shall at all times remain the
sole and exclusive property of Implant Sciences.
Customer may be held legally responsible for any
copyright infringement that is caused or
encouraged by its failure to abide by these terms.
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QS-B220 User Manual
The QS-B220 comes with a standard one-year
warranty from date of shipment that covers parts and
labor. Extended service plans are available through
the factory. Authorized personnel must install the
QS-B220. The warranty or service agreement may be
voided if the system is installed or serviced by
unauthorized personnel.
The standard training program included in the
purchase of the equipment must be scheduled
through the distributor or through the factory. This
training covers typical hardware and software
operation. The customer is responsible for training
personnel on proper protocol when dealing with
alarms and alarm resolution.
The customer is responsible for shipping charges
when returning a system to the factory. The unit
MUST be shipped in its original shipping container.
Implant Sciences is not responsible for damages
incurred from misuse (e.g. unit dropped,
inappropriate use, or failure to follow standard
maintenance protocols).
Implant Sciences Corporation
500 Research Drive, Unit 3
Wilmington, MA 01887
USA
Technical and Service Support, USA
+1-978-752-1700
service@implantsciences.com
1
About This Guide
H OW
WARNING / CAU TIONS / NOTES ARE DISPLAYED
Several conventions used throughout this manual are described below. When a symbol is displayed,
the user should carefully read the details accompanying the symbol to determine if precautions must
be taken to maintain a safe work environment.
WARNING
!
Indicates a WARNING! The warning symbol indicates that improper use or
handling could cause personal injury and/or damage to the equipment. The
text following the symbol describes the specific warning and the precautions
that should be taken by the user.
CAUTION
!
Indicates a Caution. A caution symbol indicates that improper use or failure
to execute a critical step may cause damage to the equipment.
N O T E O F I N T E R E ST
Indicates a Note of Interest. Notes are statements that either provide extra
information about a topic or contain special instructions for handling a particular
condition or set of circumstances.
T YPOGRAPHIC C ONV ENTIONS
ENTERING TEXT
When instructions in the manual require the user to enter text by typing on the touchscreen keyboard,
the text will appear in bold letters as shown:
bold text
P R E S SI N G B U T T O N S
When instructions in the manual require the user to press a button on the screen, the text appears in
capital bold letters as shown:
Press ENTER
S Y ST E M P R O M P T S O R M E S SA G E S
Messages or system prompts will be displayed in italicized, bold font as shown:
“Save changes?”
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U NIT F EATURES - C OMMERCIAL
QS-B220 S T A N D A R D F E A T U R E S












Simple-to-use software with multiple access levels for
security purposes
Wiping mode analysis using sample traps
inCal™ automatic internal calibration
Automatic system self-cleaning
Internal universal AC power supply 100/240VAC, 4763Hz with 6 foot (1.8 meter) cable for operation with AC
power source
Audible and visual alarm indicators
(indicators can be disabled)
Built-in CPU and analysis software
Internal long-life calibrant and dopant
Verification cans
User manual on CD
Internal printer for printing sample spectrograms
Transport case, with retractable handle and wheels
OPTIONAL FEATURES



Sample wand
6-month maintenance kit
External printer for printing sample spectrograms
S P E C I A L F E A T U R E S F O R C O M ME R C I A L U S E R S

Customizable user accounts

Configurable visual and audible alarms

Automatic clear down after alarm samples

Built-in Printer

I/O Panel allows connection to external USB keyboard/mouse

Able to export sample data to a USB or to a FTP Network Site.

Ability to add a network printer (via the QS-B220 Touchscreen Settings Menu)
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C ONSUMABLES
AND
S PARE P ARTS
The following list contains part numbers and descriptions for spare parts and consumables that may be required to
keep your system running properly.
Please contact Implant Sciences for price and availability.
Description
Part Number
Consumables
Sample Traps, 100 per can
42200191
Sieve Canister (single)
10011329
Sieve Canister, 4-pack
10011340
Sieve Canister, 12-pack
10011341
Cotton Swabs, low-lint, pkg of 100
42200164
Alcohol Swabs, box of 100
42200165
Nitrile Gloves, box of 100, large
40000148
Nitrile Gloves, box of 100, medium
40000183
Cabinet Fan Filters, pkg of 5
42200160
Desorber Screen
20051736
Printer Paper, roll
42200172
Spare Parts
User Manual
42400028
Quick Operating Guide
42400030
Verification Sample, A
10010156
Verification Sample, B
10011326
Sieve canister O-ring, large (outer)
42200180
Sieve Canister O-ring, small (inner)
42200181
500 Research Drive, Unit 3
Wilmington, MA 01887
USA
Technical and Service Support, USA
+1-978-752-1700
service@implantsciences.com
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ContentsHow warning/cautions/notes are displayed ............................................................................2
Typographic Conventions ......................................................................................................................................2
Unit Features - Commercial .......................................................................................................................................3
Consumables and Spare Parts ...................................................................................................................................4
1
2
- INTRODUCTION .................................................................................................................. 8
1.1
QS-B220 Introduction...................................................................................................................................9
1.2
Theory of Operation .....................................................................................................................................9
1.3
Physical Characteristics ..............................................................................................................................10
1.4
Hardware Description ................................................................................................................................11
1.5
Safety Summary .........................................................................................................................................12
1.6
System ........................................................................................................................................................13
– OPERATING INSTRUCTIONS................................................................................................. 15
2.1
Power On the System .................................................................................................................................16
2.2
Log In and Warm-Up ..................................................................................................................................17
2.3
Logout ........................................................................................................................................................20
2.4
Power Off the System ................................................................................................................................21
2.5
Respond to System Messages ....................................................................................................................22
2.5.1
Calibration Required ..............................................................................................................................22
2.5.2
Verification Required .............................................................................................................................22
2.6
Maintenance ..............................................................................................................................................23
2.6.1
Maintenance Menu ...............................................................................................................................23
2.6.2
Calibration..............................................................................................................................................23
2.6.3
Verification.............................................................................................................................................26
2.6.4
Cleaning .................................................................................................................................................30
2.6.5
Automatic Cleaning ................................................................................................................................31
2.6.6
Regeneration .........................................................................................................................................32
2.6.7
Automatic Regeneration ........................................................................................................................33
2.6.8
Sieve Maintenance ................................................................................................................................36
2.7
Sampling .....................................................................................................................................................43
2.7.1
Blank Sample..........................................................................................................................................43
2.7.2
Sampling with Traps...............................................................................................................................44
2.7.3
Reusing Sample Traps ............................................................................................................................47
2.7.4
Sample Details .......................................................................................................................................48
2.7.5
Clear Down.............................................................................................................................................49
2.8
Resolve Alarms ...........................................................................................................................................50
2.9
Add a Comment .........................................................................................................................................51
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2.10
Sampling History ........................................................................................................................................52
2.11
User Accounts ............................................................................................................................................54
2.11.1
Add a user..........................................................................................................................................55
2.11.2
Update a user ....................................................................................................................................56
2.11.3
Delete a user .....................................................................................................................................57
2.11.4
Unlock a user .....................................................................................................................................58
2.12
2.12.1
QS-B220 Settings ...............................................................................................................................59
2.12.2
System Settings .................................................................................................................................65
2.12.3
Substances .........................................................................................................................................71
2.13
Upgrade Software ......................................................................................................................................74
2.14
Export/Import ............................................................................................................................................76
2.14.1
Export Function .................................................................................................................................76
2.14.2
Import Function .................................................................................................................................76
2.15
Purge Database ..........................................................................................................................................82
2.16
Reports .......................................................................................................................................................83
2.16.1
Administrator Summary ....................................................................................................................84
2.16.2
Sample History ..................................................................................................................................84
2.16.3
Event Summary .................................................................................................................................85
2.16.4
Equipment Summary .........................................................................................................................85
2.16.5
Uptime Summary...............................................................................................................................86
2.17
3
4
System Settings ..........................................................................................................................................59
Diagnostics .................................................................................................................................................89
2.17.1
Hardware Parameters .......................................................................................................................89
2.17.2
Event Log ...........................................................................................................................................90
2.17.3
System Warm-Up ..............................................................................................................................90
– MAINTENANCE INSTRUCTIONS ............................................................................................ 91
3.1
Recommended Maintenance Schedule .....................................................................................................92
3.2
Change Sieve Canisters ..............................................................................................................................93
3.3
Calibrant and Dopant Replacement ...........................................................................................................93
3.4
Cleaning the Desorber ................................................................................................................................93
3.5
Desorber Screen Check ..............................................................................................................................93
3.6
Replacing Cabin Filter .................................................................................................................................97
3.7
Loading Printer Paper (Optional Integrated Printer) .................................................................................98
3.8
Sample Wand Maintenance .....................................................................................................................102
– TROUBLESHOOTING ........................................................................................................ 103
4.1
Introduction .............................................................................................................................................104
4.2
Implant Sciences Corporation Contact Information ................................................................................104
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5
4.3
Message Table..........................................................................................................................................105
4.4
Troubleshooting Table .............................................................................................................................107
-GUIDELINES FOR HAND SAMPLING....................................................................................... 113
5.1
Preparing to sample .................................................................................................................................114
5.2
How efficiently sample hands ..................................................................................................................114
5.2.1
hand sampling......................................................................................................................................114
5.2.2
recommended sampling techniques without sampling wand .............................................................115
5.2.3
Recommended Sampling Technique with Sampling Wand .................................................................116
5.3
6
How NOT to Sample .................................................................................................................................119
– SOFTWARE USER ACCESS LEVELS ....................................................................................... 120
6.1
Software User Access Levels ....................................................................................................................121
7
– GLOSSARY ................................................................................................................... 123
8
- TABLE OF FIGURES .......................................................................................................... 127
9
- INDEX.......................................................................................................................... 131
10 APPENDIX: MATERIAL SAFETY DATA SHEETS ........................................................................... 135
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Section 1 – Introduction
1 - INTRODUCTION
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Section 1 – Introduction
1.1 QS-B220 I NTRODU CTION
The QS-B220 is a real-time explosives and drugs trace detector. The spectrometry component of the
detector is an Ion Mobility Spectrometer with novel non-radioactive ion sources utilizing patented
photon-ionization and corona technologies developed by Implant Sciences Corporation. The QS-B220 is
designed to detect the presence of trace explosives and drugs on a surface.
1.2 T HEORY
OF
O PERAT ION
A trace sample is collected onto a trap material which is inserted into the system. The sample trap is
heated to release vapor from any explosive and narcotic traces that were collected. The vapor is drawn
into the ionization chamber, ionized, analyzed, and exhausted from the system. If an organic
compound of interest is found, the system processes an Alarm.
Explosives and drugs detection and identification is based on the measurements of molecular ion
mobility within a drift tube. The ion source is tuned to ionize specific classes of molecules. After pulsed
ionization, ions start their journey to the collector, pulled or drawn by an electrical field within the drift
tube. Small ions arrive earlier, the larger ions move slower and arrive at the collector later. Every
molecular ion has its signature in the arrival time, which allows the ions to be identified.
Figure 1: System Schematic Cross Section
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Section 1 – Introduction
1.3 P HYSICAL C HARACT ERISTICS
Warm-up Time:
30 minutes max.
Relative Humidity:
0-95% non-condensing
Input Power:
100-240VAC, 47-63Hz, 4A (max) via provided
universal power supply
Power Consumption
350 watts peak, 225 typical
Display:
12.5” (32cm) High-resolution color touch screen
Analyzer Unit Dimensions:
L 15.6” (39.6cm) x H 14.4” (36.6cm) x D 16.2”
(41.1cm) without printer
L 15.6” (39.6cm) x H 15.7” (39.7cm) x D 16.2”
(41.1cm) with printer
Analyzer Unit Weight:
34.7 lbs (15.7 kg)
Power Supply Cable:
6 ft. (1.8 meters)
Contact Sensitivity:
Particles – Nano gram level
Sampling & Analysis Time:
8 seconds (default); 5-30 seconds (user/configuration
variable)
Clear down Time:
10 seconds or less under normal sampling methods
Operating Temperature:
-10 to 55C ( 14 to 131F)
Sample Acquisition:
Particle collection by wiping surface with sample
trap
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Section 1 – Introduction
1.4 H ARDWARE D ESCRIPTION
The major components of the QS-B220 are indicated below:
Figure 2: Major components of QS-B220 system
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Section 1 – Introduction
Figure 3: External connections
1.5 S AFET Y S UMMARY
To keep personnel safe during operation of the equipment and for optimum performance of the
equipment, the following cautions and warnings must be reviewed and understood before operating
the QS-B220.
!
WARNING! Do not perform service or repair without authorization
from the factory as it could damage the equipment, cause injury,
and/or void system warranty.
!
WARNING! The desorber of the QS-B220 is very hot. Do not touch
any part or insert any material other than what is described in this
manual. Failure to comply will void warranty and may cause serious
damage to the system and/or personal harm.
!
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WARNING! Only trained, certified personnel are authorized to repair
the QS-B220 system. Removal of the cover or attempting to preform
repairs without proper training may cause personal injury.
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Section 1 – Introduction
!
Caution! The system is sensitive to the operating environment.
Smoking and spraying of aerosols should be avoided around the
system while the system is in operation.
!
Caution! Ensure that system is plugged into ONLY protective earth
outlets rated to 4 amps or better.
!
Caution! Use only recommended spare parts and consumables.
!
Caution! Do not cover ventilation openings.
!
Caution! Allow system to cool for a minimum of 30 minutes before
placing into any type of container.
1.6 S YSTEM
The QS-B220 contains a built-in computer and analysis software with a touch screen user interface that
that guides the user through system operation. Analysis begins by inserting a sample trap into the
sample desorber or pressing the BLANK SAMPLE button on the touch screen. The function/menu
buttons allow the user to maneuver through screens to set operating preferences and perform various
functions.
Note: In cases of an alarm condition, the user must be familiar with applicable protocol on how to
handle an actual threat. Personal safety is of utmost importance.
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Section 2 – Operating Instructions
2 – OPERATING
INSTRUCTIONS
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Section 2 – Operating Instructions
2.1 P OWER O N
THE
S YSTEM
How to connect the AC power cord
The QS-B220 power cord is attached to the AC input box on the back of the unit. Ensure the cord is
securely connected to the unit, and is not going to be jostled by movement occurring near the QS-B220.
Figure 5: Power cord
Figure 4: AC input location
!
!
Caution! Ensure that system is plugged into ONLY protective earth outlets.
Caution! Do not use line cord with inappropriate rating. Line cord must be rated
to 4 amps or better.
Figure 6: AC panel and power switch
Powering On Instructions:
1. Plug the power cord into the back of the QS-B220.
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2.
Plug the other end of the power cord into a protected earth outlet.
3.
Press the upper half of the white switch on the AC panel.
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Section 2 – Operating Instructions
2.2 L OG I N
AND
W ARM -U P
The user names and passwords for accounts shown in this section will be configured on the QS-B220
when it is first received from Implant Sciences. They should be removed and replaced with organization
specific user accounts by an administrator after installation of the unit.



Screener
o User ID: screener Password: customer
o Abilities: can sample, blank sample, view basic sample details, verification/calibration,
sampling history
Supervisor
o User ID: supervisor Password: customer
o Abilities: all screener abilities, user accounts, administrator report, access to some
settings, sieve replacement, desorber cleaning
Administrator
o User ID: administrator Password: customer
o Abilities: all supervisor abilities, access to system settings, access to all reports,
export/import
!
Caution! The user names and passwords shown above are part of the factory
configuration of the system. Implant Sciences recommends changing them
immediately! The administrator is responsible for logging onto the system with the
default password, changing it, then adding users as described in the section titled
‘User Accounts’.
Figure 7: Log in screen
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Section 2 – Operating Instructions
The system must complete warm-up before calibration and sampling can take place. The warmup
period from a cold start is typically 30 minutes. This allows the system to reach proper operation
temperature and be ready for detection. The system monitors its parameters automatically and will
notify the user when the warm-up is complete.
Figure 8: System warm-up (administrator)
Figure 9: System warm-up (screener)
Note: System Warm-Up Time is dependent on the length of time the system has been powered off,
and may be less than 30 minutes.
After system warm-up, the system will initiate an automatic calibration, and then will prompt for a
verification with a “Verification Required” status bar. When verification is complete, the system will
display the Main Menu with a status bar indicating “Ready to Sample”.
Figure 10: Verification required
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Figure 11: Ready to sample
18
Section 2 – Operating Instructions
Log In and Warm-Up Instructions:
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1.
Touch the box next to “User ID”. When the box has a thick outline the system
is ready for the user ID to be entered.
2.
Use the touchscreen keyboard to enter a username.
3.
Touch the box next to “Password”. When the password field has a thick
outline the system is ready for the password to be entered.
4.
Use the touchscreen keyboard to enter a password.
5.
Touch the Login button in the lower left corner or ENTER key when complete.
6.
If the QS-B220 has not reached operating temperature, the system will display
a warm-up screen. Wait for the warm-up period to elapse, or press “Main
Menu” to advance to the main menu and allow the warm-up to continue in the
background.
7.
Once the QS-B220 has reached operating temperature, the system will
automatically perform a calibration. When the QS-B220 has passed calibration,
perform a verification to bring the system into a Ready to Sample state.
8.
If the system remains in a “Calibration Required” or “Verification Required”
state see the troubleshooting section of the user manual.
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Section 2 – Operating Instructions
2.3 L OGOUT
To preserve system security, the QS-B220 has an auto-logout feature that will log the current user out
after a period of inactivity. The auto logout time is factory configured to 15 minutes. Auto logout can
be disabled or the time changed by administrators in the Settings menu.
Figure 12: Main menu with logout button
Figure 13: Auto logout rate
Logout Instructions
1.
Use the <Back button in the lower left corner to navigate to the Main Menu
screen.
2.
Press the Logout button in the lower left corner.
3.
When the “Are you sure you want to log out?” screen is displayed, press Yes.
Change Auto Logout Rate Instructions
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1.
Log into the system as an administrator level user.
2.
Press the Advanced tab.
3.
Use the up and down arrow buttons to set the Auto Logout rate.
4.
Press or depress the checkbox next to “Enabled” to enable/disable auto logout.
5.
Press the <Back button twice to return to the Main Menu.
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Section 2 – Operating Instructions
2.4 P OWER O FF
THE
S YS TEM
Figure 14: Main menu with shutdown button
Figure 15: Power switch
Power Off Instructions
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1.
Navigate to the Main Menu screen.
2.
Press the Shutdown button.
3.
When the system displays the “It is now safe to turn off your computer”
message, locate the AC panel on the back side of the QS-B220, and press the
lower part of the white switch.
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Section 2 – Operating Instructions
2.5 R ESPOND
TO
S YSTEM M ESSAGES
2.5.1 C A LI BR AT I O N R EQ UI R E D
The QS-B220 will require manual calibration when the automatic calibration fails or because auto
calibration has been disabled in the QS-B220 Settings Menu. The Calibration Required warning banner
at the top of the screen will list the detection modes that require verification (positive, negative or
both). Follow the steps in the User Manual section on Calibration (page 23) to resolve the error.
Figure 16: Calibration required
2.5.2 V ER I FI CA T I O N R EQ UI R E D
To ensure proper system operation, the QS-B220 requires periodic verification. The system will require
verification when it is first powered on, and then every 8 hours (or another interval as set by a system
administrator). The warning Verification Required banner displayed at the top of the screen will list the
detection modes that require verification (positive, negative or both). To respond to this, the user will
need to perform a verification - see User Manual section on Verification (page Error! Bookmark not
defined.) for detailed instructions.
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Section 2 – Operating Instructions
Figure 17: Verification required
2.6 M AINTENANCE
2.6.1 M AI N T EN AN C E M E N U
The maintenance menu is accessible from the main menu and allows access to cleaning, regeneration,
sieve, calibration and verification functions.
Figure 18: Maintenance menu
2.6.2 C A LI BR AT I O N
Access: Screener, Supervisor, Administrator
Calibration adjusts the QS-B220 to ensure that samples are analyzed accurately. Two types of
calibration methods are available on the QS-B220; automatic calibrations called “Chemical”
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Section 2 – Operating Instructions
calibrations, and “Trap” calibrations which require a user to insert a sample trap with a pre-applied
calibration substance.
The chemical calibration is fully programmed and does not require any user intervention. It is initiated
automatically by the QS-B220 on a time-based interval. Chemical calibrations happen automatically
after startup, login, and before verification. The calibration frequency is determined by the relative
change in atmospheric pressure.
In instances where a chemical calibration is unsuccessful, the system will prompt the user to perform a
trap calibration. The user may perform a trap calibration by selecting OK, or decline trap calibration by
selecting CANCEL. Once OK is selected, the user will be prompted to insert a Calibration Trap. Once a
Calibration Trap is inserted, the system will automatically perform a calibration.
Figure 19: Calibration screen
Calibration Instructions for User Initiated Chemical Calibration:
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1.
From the Main Menu, press the Maintenance button
2.
From the Maintenance menu press Calibrate.
3.
Enable the Positive and/or Negative IMS checkboxes. The QS-B220 will perform
calibration for the selected detection modes.
4.
Set the Calibrant Type to Chemical.
5.
Press the Start button.
6.
After Calibration completes, return to the Main Menu by pressing the <Back
button twice.
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Section 2 – Operating Instructions
Calibration Instructions for Trap-Based Calibration:
1.
From the Main Menu, press the Maintenance button.
2.
From the Maintenance menu press Calibrate.
3.
Enable the Positive or Negative IMS checkboxes. The QS-B220 will perform
calibration for the selected detection modes.
4.
Set the Calibrant Type to Trap.
5.
Using a sample trap, wipe the mesh inside Verification can “A” once to create a
negative calibration trap, or wipe the mesh inside Verification can “B” once to
create a positive calibration trap.
6.
When the screen prompts “Please insert a NEGATIVE Calibration trap…” insert
a negative calibration trap into the desorber.
7.
Remove the trap from the desorber when the system prompts “Please Remove
Trap Before Continuing”
8.
When the screen prompts “Please insert a POSITIVE Calibration trap…” insert a
positive calibration trap into the desorber.
9.
Remove the trap from the desorber when the system prompts “Please Remove
Trap Before Continuing”
10. Press OK when the “Calibration Successful” message displays. If Calibration
repeatedly fails, refer to the Troubleshooting section of the User Manual on
page 107.
11. Return to the Main Menu by pressing the <Back button twice.
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Section 2 – Operating Instructions
2.6.3 V ER I FI CA T I O N
Access: Screener, Supervisor, Administrator
The Verification button allows the user to access the Verification screen in order to test that the QSB220 is properly calibrated. The QS-B220 will prompt to run a Verification when the system is powered
on and after every 8 hours of operation (or other interval as specified by the Administrator).
The Verification Required banner will be displayed at the top of the User Interface Screen when the
system requires verification. If only one mode requires verification only that mode will run verification
when the start button is pressed. If the system requires verification of both modes, when the start
button is pressed both negative and then positive mode verification will be performed.
Figure 20: Verification screen
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Section 2 – Operating Instructions
VERIFICATION BY CAN
Verification Instructions for Positive AND Negative:
1.
From the Main Menu, press the Maintenance button
2.
From the Maintenance menu press Verification.
3.
Ensure that the Positive and Negative IMS checkboxes are enabled. If the
system is in a Verification Required (Positive/Negative) state the checkboxes
will be automatically enabled upon entry into the Verification screen.
4.
Press the Start button. If the most recent calibration occurred more than ten
minutes prior to start of the Verification, the system will prompt for a
calibration before Verification can proceed.
5.
Using a sample trap, wipe the mesh inside Verification can “A” once.
6.
When the screen prompts “Please insert a NEGATIVE Verification sample…”
insert the trap into the desorber sample side up.
7.
Remove the trap from the desorber when the system prompts “Please Remove
Trap Before Continuing”
8.
Press OK when the “Negative Verification Successful” message displays. If
Verification is not successful the system will display a Verification Failed
message, and prompt the user to repeat steps 5 to 7. If Verification repeatedly
fails, manually initiate a calibration and then retry verification. If verification
continues to fail, refer to the Troubleshooting section of the User Manual on
page 107.
9.
Using a sample trap, wipe the mesh inside Verification can “B” once.
10. When the screen prompts “Please insert a POSITIVE Verification sample…”
insert the trap into the desorber sample side up.
11. Remove the trap from the desorber when the system prompts “Please Remove
Trap Before Continuing”
12. Press OK when the “Positive Verification Successful” message displays.
13. Return to the Main Menu by pressing the <Back button twice.
14. If verification is successful, the system will report that it is “Ready to Sample”.
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Verification Instructions for Positive OR Negative:
1.
From the Main Menu, press the Maintenance button.
2.
From the Maintenance menu press Verification.
3.
Enable the Positive or Negative IMS checkboxes.
4.
Press the Start button. If the most recent calibration occurred more than ten
minutes prior to start of the Verification, the system will prompt for a
calibration before Verification can proceed.
5.
Using a sample trap, wipe the mesh inside Verification can “A” once for a
negative verification, or the mesh inside Verification can “B” once for a positive
verification.
6.
When the screen prompts “Please insert a NEGATIVE/POSITIVE Verification
sample…” insert the trap into the desorber sample side up.
7.
Remove the trap from the desorber when the system prompts “Please Remove
Trap Before Continuing”
8.
Press OK when the “Verification Successful” message displays. If Verification is
not successful the system will display a Verification Failed message, and
prompt the user to repeat steps 5 to 7. If Verification repeatedly fails, refer to
the Troubleshooting section of the User Manual on page 107.
9.
Return to the Main Menu by pressing the <Back button twice.
10. If verification is successful, the system will report that it is “Ready to Sample”.
VERIFICATION BY DUAL-MODE VERIFICATION TRAP
Verification Instructions using Dual-Mode Verification Trap:
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1.
From the Main Menu, press the Maintenance button.
2.
From the Maintenance menu press Verification.
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3.
Enable the Positive or Negative IMS checkboxes.
4.
Press the button to select Trap.
5.
Press the Start button. If the most recent calibration occurred more than ten
minutes prior to start of the Verification, the system will prompt for a
calibration before Verification can proceed.
6.
When the screen prompts “Please insert a dual verification trap…” insert the
trap into the desorber sample side up.
7.
Remove the trap from the desorber when the system prompts “Please Remove
Trap Before Continuing”
8.
Press OK when the “Verification Successful” message displays. If Verification is
not successful the system will display a Verification Failed message, and
prompt the user to repeat steps 5 to 7. If Verification repeatedly fails,
manually initiate a calibration and then retry verification. If verification
continues to fail, refer to the Troubleshooting section of the User Manual.
9.
Return to the Main Menu by pressing the <Back button twice.
10. If verification is successful, the system will report that it is “Ready to Sample”.
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2.6.4 C L E AN I N G
Access: Screener, Supervisor, Administrator
The Cleaning feature increases the temperature of the sample path for 30 minutes to burn off any
contamination that may have accumulated during system usage or from a sample with excess amounts
of explosives, drugs or contamination. Cleanings can be manually initiated as a response to repeated
failed calibrations or contamination that leads to a long clear down time. Cleanings can also be
automatically initiated by the software based on total ion charge measurements.
Figure 21: Cleaning screen
Cleaning Instructions:
42400026 Rev G
1.
From the Main Menu, press the Maintenance button
2.
From the Maintenance menu press Cleaning.
3.
Press Start.
4.
Wait for the Cleaning Timer to complete. The system includes a cool down
period in the Cleaning timer.
5.
After Cleaning completes, return to the Main Menu by pressing the <Back
button twice.
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2.6.5 A U T O M AT I C C L E AN I N G
The QS-B220 initiates automatic cleaning procedures to clear contamination from the system and to
keep the system in optimum condition. Automatic cleaning is triggered by the total ion charge levels.
The QS-B220 displays a “Cooling Down...” banner when a user logs in while a cleaning is active to allow
the system time to exit the cleaning procedure and return to a ready to sample state. The QS-B220
allows for scheduled cleaning to occur during off-peak hours – see the QS-B220 Settings section for
more information.
Figure 22: Automatic cleaning cool down
Figure 23 Automatic cleaning (low positive charge)
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2.6.6 R E G EN ER AT I O N
Access: Screener, Supervisor, Administrator
The Regeneration feature increases the temperature of the negative ion source and other components
of the system to remove contamination.
Figure 24: Regeneration
Regeneration Instructions:
42400026 Rev G
1.
From the Main Menu, press the Maintenance button
2.
From the Maintenance menu press Regeneration.
3.
Press Start.
4.
Wait for the Regeneration Timer to complete. The system includes a cool
down period in the regeneration timer.
5.
After the Regeneration completes, return to the Main Menu by pressing the
<Back button twice.
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2.6.7 A U T O M AT I C R E G EN E R A T I O N
The QS-B220 initiates automatic regenerations to clear contamination from the system, triggered by
the charge levels of the last five samples/calibrations. The QS-B220 displays a Cooling Down... banner
when a user logs in while a regeneration is active to allow the system time to exit the cleaning
procedure and return to a ready to sample state.
The QS-B220 allows for scheduled regenerations on a multi-day basis – see the QS-B220 Settings
section for more information.
Figure 25: Automatic regeneration cool down
Figure 26 Automatic regeneration ( Low negative charge)
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Desorber Cleaning
Access: Supervisor, Administrator
The Desorber Cleaning feature allows the user to turn off the desorber heaters and monitor the
temperature in order to determine when the desorber has cooled sufficiently to perform desorber
cleaning. During normal use, the desorber should be cleaned monthly. In dirtier environments, the
desorber may need to be cleaned more often.
Figure 27: Desorber cleaning
!
CAUTION! Allow the desorber to cool down for approximately 30 minutes.
Figure 28: Desorber cleaning with alcohol swab
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Desorber Cleaning Instructions:
42400026 Rev G
1.
From the Main Menu, press the Maintenance button
2.
From the Maintenance menu press Desorber Cleaning.
3.
Press Start.
4.
Wait for the Desorber temperature to cool (approximately 30 minutes).
5.
Using either a cotton swab (Q-Tip) dipped in IPA or an alcohol swab, clean the
inside of the desorber by scrubbing with the swab.
6.
Repeat step 6 using a fresh swab two (2) to three (3) times or until the swab
comes out clean.
7.
Allow the IPA to fully dry; approximately 30 minutes.
8.
On the QS-B220 touch screen press the DONE button. Allow the desorber to
come up to temperature; approximately 5 minutes.
9.
After the desorber cleaning completes, return to the Main Menu by pressing
the <Back button twice.
10.
Perform a Cleaning.
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2.6.8 S I EV E M AI N T E N A N C E
Access: Supervisor, Administrator
The QS-B220 sieve is a type of desiccant, used to dry the air inside of the drift region and to filter
organic molecules from the dry air stream. The QS-B220 system employs alumina-based molecular
sieves with a porosity sieve of 5 Ǻ. The sieve must be replaced periodically to ensure accurate detection
of trace explosives and drugs. The Sieve Maintenance feature allows the user to change the sieve
canisters without powering off the system.
Figure 29: Sieve maintenance
The frequency of sieve changes is dependent on the atmosphere surrounding the QS-B220. A system
that is running in a humid environment is likely to require a sieve change every few weeks, and a
system that is operating in a dry location may not need to change the sieve for several months.
The QS-B220 monitors internal humidity, and when the humidity exceeds a pre-set threshold the
system will display a “High Humidity” message at the top of the screen. This warning indicates that the
sieve material needs to be replaced.
The QS-B220 allows for sieve replacement reminders to display on a multi-week basis – see the QSB220 Settings section for more information.
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Figure 30: High humidity warning
Sieve Change Instructions:
42400026 Rev G
1.
From the Main Menu, press the Maintenance button
2.
From the Maintenance menu press Sieve Maintenance.
3.
Press Replace .
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Section 2 – Operating Instructions
4.
From the rear panel, gently pull the sieve compartment cover from both sides
of the panel. The sieve canisters are accessed in pairs, each pair is accessed by
one of the two levers.
Figure 31: Sieve chamber lever
5.
As the lever is moved to the side, the pair of canisters tilts up.
Figure 32: Tilting sieve canisters
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6.
Gently twist the sieve canister in a counterclockwise motion to unscrew it from
the sieve manifold. Repeat for second canister.
Figure 33: Unscrewing sieve canister
7.
Remove the orifice filter replacement tool from the sieve assembly cover as
shown below.
Figure 34: Orifice Filter Replacement Tool
8.
Look inside the end of the orifice filter replacement tool. Note the locating pin.
This pin makes contact with a key on the sieve orifice filter to turn it in either
direction.
Figure 35: Locate the Pin on the Orifice Filter
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9.
Push the tool onto the orifice filter at the bottom-rear of the sieve assembly
housing until fully seated.
Figure 36: Orifice Installation
10. WARNING: Gently turn the orifice filter replacement tool to remove the filter.
Excessive force can result in damage to the key.
Turn the orifice filter replacement tool in a counter-clockwise direction until
the orifice filter disengages and remove the tool and filter.
Figure 37: Turn Orifice Filter Replacement Tool
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Section 2 – Operating Instructions
11. Remove the old orifice filter from the orifice filter tool and discard.
Figure 38: Discard Old Orifice Filter
12. Place a new orifice filter in the orifice filter replacement tool. NOTE: ensure
that the keyed end of the filter goes into the tool first as illustrated below.
Figure 39: Replace Orifice Filter
13. Carefully turn the orifice filter replacement tool clockwise until the filter is
seated. Care should be taken not to strip the key on the filter by overtightening.
14. To install a new sieve canister, unscrew the cap of a new sieve canister.
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15. Inspect canister to ensure that 2 O-Rings are in place.
Figure 40: Inspecting for O-rings
16. Reinstall new sieve canisters, screwing them in a clockwise motion into the
sieve manifold
17. On the QS-B220 touch screen press the Resume button.
18. The system starts auto calibration.
19.
Return to the Main Menu by pressing the <Back button twice .
!
!
CAUTION! Always wear clean, powder-free nitrile gloves when changing the sieve.
CAUTION! Never touch any surfaces of the mating surface of the sieve bottle or O-Rings with nonprotected hands.
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2.7 S AMPLING
2.7.1 B L AN K S A MP L E
Access: Screener, Supervisor, Administrator
The Blank Sample button manually initiates a sample analysis. This can be used to initiate samples
without inserting a trap. This button also allows samples to be manually initiated if the trap sensor in
the desorber malfunctions.
Figure 41: Blank sample – ready to sample
Figure 42: Blank sample – sampling
Figure 43: Sample alarm
Figure 44: Sample no alarm
Blank Sample Instructions:
1.
2.
3.
4.
Log on to the QS-B220 as any level user. If the system is not
Ready to Sample, perform calibration and verification procedures
and return to the Main Menu.
From the Main Menu, press the Blank Sample button
The system will enter a Sampling state. At this time the user may
choose to insert a trap into the desorber for a trap sample, or
may choose not to insert a trap for an air sample.
At the conclusion of sampling, the QS-B220 will display an alarm
popup or no alarm popup.
5.
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2.7.2 S A MP LI N G
WITH
T R AP S
Access: Screener, Supervisor, Administrator
Taking a sample involves collecting or transferring the sample onto a sample trap and then analyzing
the trap with the QS-B220. Explosive and narcotic compounds can be detected on a variety of surfaces,
e.g. clothing, luggage, packages, vehicles, etc. Using a sample trap is an effective way to search quickly.
Implant Sciences strongly recommends the use of sample traps provided with the QS-B220, as they are
contaminant-free. Implant Sciences cannot guarantee system performance if an unapproved trap
material is used, as the use of unapproved traps may degrade detection performance.
Sample traps may be used several times unless they have collected a substance that produces an alarm,
have been torn or shredded, or have become excessively dirty or oily. Any of the conditions mentioned
would be cause to discard the sample trap and use a new one.
Samples with traps can be taken by hand or with the Implant Sciences Sample Wand. The QS-B220
sample wand is a means of sampling various surfaces without the user using his or her hand to swipe
the surface. The sample wand is an effective tool for taking samples in tight spaces.
It is not recommended that one vigorously wipe surfaces. In cases of volatile substances, such as
nitroglycerine, TATP and HMTD, the heat generated by the friction of rubbing can cause the microscopic
quantities of explosives and drugs to decompose.
Figure 45: Implant Sciences sample wand and sample trap
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The following is a list of possible results and messages that may appear on the unit after a sample:
Status
Bar
Color
Example Screenshot
Result
Description
RED
ALARM
Follow alarm protocol
GREEN
NO
ALARM
System ready for next sample
WAIT
System may be sampling, selfcalibrating or self-cleaning. Wait
for ‘Ready to Sample’ screen.
YELLOW
Figure 46: Possible trap sample results
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Trap Sample by Hand Instructions:
1.
Use clean, powder-free Nitrile gloves to prevent excessive hand contamination
from soiling the trap.
2.
Place index finger onto the top center of the trap and allow your thumb to hold
the underside edge of the trap.
Figure 47: Holding a trap
3.
Press firmly and wipe the target area in one direction only. DO NOT wipe back
and forth as this may redeposit the sample back onto the sampled surface.
Figure 48: Sampling by hand
42400026 Rev G
4.
The sample is now ready for analysis.
5.
Verify that the system status is displaying Ready to Sample. Insert the sample
trap to begin analysis. The sample trap must be inserted into the desorber
with the swabbed side facing up.
6.
When prompted, remove the sample trap
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7.
At the conclusion of sampling, the QS-B220 will display an alarm popup or no
alarm popup.
Note:
The above sampling practice does not apply for hand sampling. Please refer to section 5 for hand
sampling instructions.
2.7.3 R E U SI N G S A MP L E T R A P S
A sample trap may be reused many times provided;
a)
b)
c)
d)
it is not physically damaged by tears,
it is not contaminated,
the trap has not produced an alarm,
the surface of the trap is still rough enough to reasonably collect a sample.
It is not unusual for traps to be reused in fairly clean environments. However, in a cargo environment or
when sampling vehicles where sample-collecting locations are more likely to be contaminated by oil, as
few as 1-2 uses may be more normal.
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2.7.4 S A MP LE D ET AI L S
Access: Screener, Supervisor, Administrator
The sample details screen displays information about the most recent sample. Screener level users are
able to see the sample number, time, and type. Supervisor and Administrator level users are able to
see alarm details and spectrogram charts on additional tabs.
Figure 49: Sample Details (Screener View)
Figure 50: Sample Details (Administrator View)
Figure 51: Sample Alarms (Administrator View)
Figure 52: Sample Spectrogram (Administrator View)
View Sample Details Instructions:
42400026 Rev G
1.
From the Main Menu, press the Sample Details button.
2.
Select the Details, Alarm, Negative or Positive tabs to see sample information.
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2.7.5 C L E AR D O W N
Access: Screener, Supervisor, Administrator
The Clear Down button allows the user to initiate a clear down cleaning sequence. The Clear Down
button is also the mechanism for acknowledging an alarm when in silent alarm mode. Clear downs are
performed automatically after each sample and calibration/verification to remove remaining
substances from the IMS detection cells.
The software will attempt a preset number of clear down cycles if the system is identified as being
contaminated. If these clear downs are successful, the display will indicate “Ready to Sample”. If the
unit has failed to clear down, the user may choose to perform manual clear down cycle, which is
initiated on the Main Menu by selecting Clear Down. This is the recommended method for most
situations, since all users can access it.
A stronger cleaning procedure is to perform a Cleaning from the Maintenance menu. This heat
cleaning process requires 30 minutes to complete and is usually successful at removing any
contamination in the sample pathway.
Figure 53: Clearing down popup
Figure 54: Clearing down banner
Manual Clear Down Instructions:
1.
42400026 Rev G
From the Main Menu, press the Clear Down button.
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2.8 R ESOLVE A LARMS
Access: Screener, Supervisor, Administrator
When an alarm occurs, the system will display alarm information. If audible alarm is enabled, an
audible signal will also sound during an alarm. To resolve an alarm condition, the user must FIRST
FOLLOW THE LOCAL AUTHORITY’S ESTABLISHED PROTOCOL FOR ALARMS. After following established
protocol, the user presses the Acknowledge Alarm button to clear the alarm.
The alarm file will be saved to the system hard drive. All alarm files are saved along with all pertinent
system conditions at the time of the alarm.
!
WARNING! In cases of an alarm condition, the user must be familiar with site
protocol on how to handle an actual threat. Personal safety is of the utmost
importance.
Figure 55: Resolve alarm popup
Figure 56: Resolve alarm banner
Note: If the visual alarm indicator is turned off the user MUST press the Clear Down button in order to
acknowledge the alarm and initiate a clear down to be able to perform further sampling.
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2.9 A DD
A
C OMMENT
Access: Screener, Supervisor, Administrator
Users are able to add optional comments to both alarm and non-alarm samples to record a description
of the object that was sampled or observations on the sampling conditions.
Figure 57: Add comment
Add Comment Instructions:
1.
Open the Sample Details screen from the Main Menu to show the results
from the most recent sample, OR open the Sampling History screen and
highlight a specific sample then press Select.
2.
Press the Add button in the Comment field.
3.
Use the touch screen keyboard to enter a comment.
4.
Press the Accept button.
View Comment Instructions:
1.
Open the Sample Details screen from the Main Menu to show the results
from the most recent sample, OR open the Sampling History screen and
highlight a specific sample then press Select.
2.
Press the View button in the Comment field.
3.
Select a comment in the Date list to view the comment text.
4.
Press the Close button.
Note: Comments are only available for samples (not for calibrations and verifications).
Note: Previously entered comments may not be deleted or edited.
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2.10
S AMPLING H ISTORY
Access: Screener, Supervisor, Administrator
The Sampling History screen allows appropriate level users to review data from samples taken, such as
sample number, date, time, user name, peak information and user added comments.
The Query option allows the user to filter the list of samples by date, by type and/or by ID. The Query
screen also allows easy access to the last alarm or last sample.
Figure 58: Sampling history
Select Sample Instructions:
1. From the Main Menu, press the Sampling History button.
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2.
Highlight a sample, and press the Select button to display details about the
specific sample.
Figure 59: Sampling history, sample details
3.
Press the <Back button to return to the Sampling History screen.
Query Sampling History Instructions:
1. From the Main Menu, press the Sampling History button.
2.
Press the Query button to display a filter for the sample list.
Figure 60: Sampling history query
42400026 Rev G
3.
Select conditions for the filter (date range, sample type, etc…) and press
Execute. The query screen will close and display a list of samples that meets
the criteria specified in the filter.
4.
Press the <Back button to return to the Main Menu.
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2.11
U SER A CCOUNTS
Access: Supervisor, Administrator
The User Accounts screen is allows users to manage user access to the QS-B220. From the User
Accounts screen a user can create, modify, delete and enable/disable user accounts.
Each account requires a User ID and a Password. If desired, the First Name, Last Name and Company
can be used to identify users. Each account is assigned a permission level: Administrator, Supervisor or
Screener. For information on what functionality is available to each user levels see Section 6: Software
User Access Levels.
Accounts also have two status settings:
Locked: A user is locked out of the system if he or she fails login with an incorrect password
three times in a row. The user can be unlocked by a user with a higher access level.
Enabled: Disabling a user prevents that user from any access to the QS-B220, but does not
remove the user from the user account list. A user can only be enabled/disabled by a user with a
higher access level.
The level hierarchy of the QS-B220 is Administrator > Supervisor > Screener. A user is only able to
access and modify accounts of equal or lesser authority.
Administrator level users have the ability to export a user account list from one QS-B220 and import the
list on other QS-B220 systems. For detailed instructions see the user manual sections on Export and
Import.
A set of default accounts comes pre-loaded on the QS-B220, and should be removed and replaced with
organization specific user accounts by an administrator after installation of the unit.
Default Accounts:



Screener
o User ID: screener Password: customer
Supervisor
o User ID: supervisor Password: customer
Administrator
o User ID: administrator Password: customer
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Figure 61: User accounts screen
2.11.1
ADD
A U SE R
Instructions to Add a User:
1. From the Main Menu, press the User Accounts button.
2.
From the User Accounts screen, press the Add button.
Figure 62: Add a user account
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3.
Select a field to enter data. When the field is outlined with a dark blue box, it is
selected. The touch screen keyboard will appear automatically.
Figure 63: Add a user account with keyboard
2.11.2
U P D AT E
4.
Enter the User’s ID, Password field, and Confirm Password in the appropriate
fields. To help prevent mistakes in entering passwords, the Password and
Confirm Password fields are required to contain identical information.
5.
The First Name, Last Name and Company fields are optional – these can be left
blank if desired.
6.
Press the Keyboard Icon to hide the touch screen keyboard.
7.
Choose the level, and ensure that the new user is enabled and is not locked.
8.
Press Apply and view the new user in the User Accounts list.
A US E R
Instructions to Update a User:
42400026 Rev G
1.
From the Main Menu, press the User Accounts button.
2.
Select a user by highlighting the row with the User ID, and press the Modify
button. You must be a user of an authority level equal to or higher than the
user you are modifying.
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3.
Update the user data.
Figure 64: Modify user account
4.
2.11.3
D E L ET E
Press the Apply button.
A U S ER
Delete User Instructions:
1.
From the Main Menu, press the User Accounts button.
2.
Select a user by highlighting the row with the User ID.
3.
Press the Delete button. You must be a user of an authority level equal to or
higher than the user you are deleting.
Figure 65: Delete user account
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4.
2.11.4
U N LO CK
Press Yes on the “Are you sure you want to delete this User Account” popup.
A U S ER
Unlock User Instructions:
1. From the Main Menu, press the User Accounts button.
2. Select a user by highlighting the row with the User ID, and press the Modify
button. You must be a user of an authority level equal to or higher than the
user you are modifying.
3. Uncheck the Locked checkbox. Ensure that the Enabled box is selected.
Figure 66: Enable User Account
4. Press the Apply button.
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2.12
S YSTEM S ETTINGS
2.12.1
QS-B220 S E T T I N GS
PRINTER SETTINGS TAB
Access: Supervisor, Administrator
Figure 67: QS-B220 settings system tab
Set Printer/Auto Print Instructions:
1. In the Print Options box – Sample Printer field use the drop down menu to
select a printer for sample printouts.
2. If a sample printout should include a spectrogram, check the “Include
Spectrogram” checkbox.
3. In the Auto Print Option field choose whether the system should print on Every
Sample, Every Alarm, or Never using the radio button.
4. In the Auto Print Option field choose whether the system should print errors by
enabling or disenabling the checkbox. When the Print Errors checkbox is
enabled the system will print a short summary each time the system enters an
error state (example would be high humidity state or low charge state).
5. In the Print Options box – Report Printer field use the drop down menu to
select a printer for report printouts, and a page size.
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6. In the Orientation field choose whether the printout should be portrait or
landscape orientation.
Set Alarm Indicator Instructions:
1. In the Alarm Indicator box, press the radio button next to On or Off to enable or
disable the alarm indicator. When the Alarm Indicator is on, an alarm sample
will result in a full screen alarm popup. When the Alarm Indicator is off an
alarm sample will result in a less conspicuous banner at the top of the screen.
Figure 68: Resolve alarm popup (indicator =
ON)
Figure 69: Resolve alarm banner (indicator =
OFF)
Note: When the alarm indicator is turned OFF, a warning will be posted when an alarm is detected. A
clear down must be performed before the system will accept more samples.
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ADVANCED TAB
Access: Administrator
Figure 70: QS-B220 settings – advanced tab
Save Hard Drive Space Instructions:
1. In the Save Spectrograms box check the “Alarms Only” checkbox. The Alarms
Only option will conserve hard drive space on the QS-B220 by only saving
spectrograms for alarm samples.
2. Press the Accept button.
Disable/Enable Automatic Calibration Instructions:
1. In the Auto Calibration box select the checkboxes next to Negative, Positive or
High Voltage to enable/disable automatic calibration.
Negative controls auto calibration for the negative IMS mode. Positive controls
auto calibration for the positive IMS mode. When the field is disabled the
negative mode does not auto calibrate, and the user is required to manually
initiate calibration to bring the system into a ready state. High Voltage controls
automatic checks on high voltage levels. When the field is disabled the QSB220 does not automatically adjust high voltage levels during calibrations.
2. Press the Accept button.
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Require Comments on Samples Instructions:
1. Enabling the Required Alarms checkbox will prompt the user for a comment
after each alarm sample. Enabling the Required Settings checkbox will prompt
the user for a comment each time a setting is updated.
2. Press the Accept button.
Change Auto Logout Rate Instructions:
1. In the Auto Logout Rate box, select the interval in minutes for automatic user
logout, and enable or disable the feature by selecting or deselecting the
“Enabled” checkbox.
The Auto Logout Rate field controls the interval for auto logout. When the
system records no user input for the auto logout interval the system will log the
current user out and return to the login screen.
2. Press the Accept button.
Active Cleaning instructions:
1
2


Enable the “Level 1” checkbox to trigger an automatic cleaning after
consecutive positive or negative samples with low charge warnings. These
automatic cleanings produce a “Negative/Positive Charge Too Low, Perform
Regeneration/Cleaning” popup.
Enable the “Level 2” checkbox to trigger an automatic cleaning after any type
of consecutive samples with low charge warnings. These automatic cleanings
produce a “Positive Charge Too Low, Perform Regeneration/Cleaning” popup.
Press the Accept button.
Alarm Mode
o The alarm mode controls the length of sampling. Fixed mode requires the duration all
samples to be a fixed interval of time, and a sample in fixed mode may return multiple
types of alarms. Stop If Detected mode will terminate the sample after the first alarm
substance is detected.
Verification Rate
o The Verification Rate controls the interval between required verifications. The default
value is 24 hours.
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SCHEDULED TASKS
Access: Administrator
Figure 71: QS-B220 settings – scheduled tasks tab
Set Daily Clean Instructions:
3. In the Daily Clean box enable or disable an automatic daily cleanings and
regenerations by checking or unchecking the “Enabled” checkbox.
4. Select the time for the daily clean.
5. Select the duration of the daily clean.
6. Press the Accept button.
Set Regeneration Frequency Instructions:
1. In the Daily Clean box enable or disable an automatic regenerations and
cleanings by checking or unchecking the “Enabled” checkbox.
2. In the Regeneration Frequency box select the interval in days for automatic
regenerations.
3. Press the Accept button.
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Set Sieve Replacement Reminder Instructions:
1. In the Sieve Replacement Reminder box on the Scheduled Tasks tab, select the
interval in weeks for a reminder to change the system sieve.
2. Press the Accept button.

Sieve Replacement Reminder
o The Sieve Replacement Reminder will remind the user to change the sieve soon via a
banner on the Main Menu, which will persist until the sieve is changed. See page 36 for
sieve change instructions.
Figure 72: Sieve replacement reminder
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2.12.2
S Y ST E M S ET T I N G S
SYSTEM SETTINGS
Access: Supervisor, Administrator
Figure 73: QS-B220 system settings
Change Volume Instructions:
1. Press the arrow buttons to increase or decrease the volume.
2. Press the speaker icon button to mute the QS-B220. The icon in the upper left
corner will change to a mute icon.
Change Language Instructions:
1. In the Supported Languages field, use the drop down list to select a system
language.
2. Press the Accept button.
Change Time/Date Instructions:
1. In the Date field select the month, day and year from the drop down boxes.
2. In the Time field select the hour, minute, second and AM/PM from the drop
down boxes.
3. Press the Accept button. The system will prompt for a restart to change the
system time and date.
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FTP S E T T I N G S
Access: Administrator

FTP settings allow a user to establish a connection to an FTP (File Transfer Protocol) server for
export/import and software update functions.
Figure 74: QS-B220 system settings – FTP tab
Add FTP Connection Instructions:
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1.
From the Main Menu, press the Settings button.
2.
From the Settings Menu, press the System Settings button.
3.
From the System Settings page, press the FTP Settings tab.
4.
Add the path to a network FTP Site in the FTP Site field.
5.
Insert user credentials (User ID and Password) for connection to the FTP site.
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6.
Press the Test Connection button.
Figure 75: Tested FTP connection
7.
The FTP connection will be available in the Select Drives screen in the
Import/Export screen (see Export/Import on page 76).
Figure 76: Select drive (FTP)
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NETWORK SETTINGS
Access: Administrator
Network Settings Tab Features:


The Network Settings tab allows a user to enter the path of a network printer. Once a printer has
been added via this screen the printer name will show up in the QS-B220 settings page as an option
to print reports or sample data.
The Network Settings tab allows a user to test the whether or not the QS-B220 is connected to the
internet by pressing the Test Internet Connection button, and will display the unit’s IP Address.
Figure 77: QS-B220 system settings – FTP tab
Add Network Printer Instructions:
1. From the Main Menu, press the Settings button.
2. From the Settings Menu, press the System Settings button.
3. From the System Settings page, press the Network Settings tab.
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4. Enter the path to a network printer in the Name field. In this example, the
network printer is located at \\atlas\back_mp_3351
Figure 78: Insert network printer name
5. Press the Add button.
Figure 79: Adding network printer
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6. Wait for feedback that the network printer has been added successfully.
Figure 80: Network printer added successfully
7. Once the printer has been successfully added, press the <Back button to return
to the settings menu.
8. Press the QS-B220 Settings button.
9. The printer will be available in the drop down list for report and sample
printers. Choose the printer from these lists and press the Accept button to set
the printer to the network printer.
Figure 81: Choose network printer
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PERIPHERALS SETTINGS
Access: Administrator
Peripherals Settings Tab Features:
The peripherals settings tab allows a user to calibrate the sensitivity of the QS-B220’s touch screen.
Pressing the Start Wizard button will display a Windows application that provides access to click speed
settings and to touch screen calibration.
Figure 82: Peripherals tab
2.12.3
S UB ST AN C ES
Access: Administrator
Substances settings include calibration time (in MS), minimum alarm level, and whether each substance
is enabled or disabled.
Figure 83: QS-B220 substances
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OPTIONAL CONFIGURATION: The ability for Administrator level users to add or modify substances is
factory configurable. A QS-B220 with Administrator Substance Table editing enabled will have display
Add, Modify, Remove and Mode buttons.
Figure 84: Substances with edit capability
OPTIONAL CONFIGURATION: The modify substance screen allows an administrator the ability to add a
new substance or modify an existing substance in the substance table.
Figure 85: Add/Modify substance
Add or Modify Substance Instructions:
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1.
From the Main Menu, press the Settings button.
2.
From the Settings menu press the Substances button.
3.
In the Substances screen highlight the substance to be modified, and press the
Modify button. To add a new substance, press the Add button.
4.
In the Modify Substance screen, enter or edit the substance values. Substances
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can be individually disabled by checking or unchecking the Enable field.
5.
Press the Accept button.
OPTIONAL CONFIGURATION: The substance mode screen allows an administrator to enable or disable
detection of groups of substances to put the QS-B220 in Explosives Mode or Drugs Mode or Dual Mode.
Figure 86: Substance modes
Substance Mode Instructions:
1. From the Main Menu, press the Settings button.
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2.
From the Settings menu press the Substances button.
3.
In the Substances screen press the Mode button.
4.
Select one of the three modes by pressing the Explosives Mode, Drugs Mode
or Dual Mode buttons, or customize the selection with the explosives and
drugs checkboxes.
5.
Press the Accept button.
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2.13
U PGRADE S OFTWARE
Access: Administrator
The Upgrade Software function prompts an administrator through the necessary steps to upgrade
system software by inserting a USB drive containing the upgrade files. Software can be loaded from a
USB or from an FTP server. See page 66 for details on how to set up a connection to a FTP server.
Figure 87: Upgrade software
Upgrade Software Instructions:
1. From the Main Menu, press the Administration button.
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2.
From the Administration menu press the Upgrade Software button.
3.
Insert a USB that contains the software upgrade file into the I/O port on the
QS-B220 OR ensure the software upgrade file is available via FTP server.
4.
Press the Browse… button.
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Figure 88: Upgrade software select folder
5.
Press the Select Drive button.
Figure 89: Upgrade software directory browser
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6.
Choose the drive (USB or FTP) that contains the software upgrade file and
press OK.
7.
Locate the software upgrade file in the file structure, highlight the file and
press OK.
8.
Ensure that the location field shows the correct file location, and press the
Upgrade button.
9.
The QS-B220 will upgrade and restart the software, and after the upgrade will
leave the user on the login screen.
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2.14
E XPORT /I MPORT
Access: Administrator
The Export/Import function allows the user to select data to be imported or exported to/from a USB
drive or FTP server. The Export/Import file location is determined by use of the Export Location and
Import Location buttons and the Select Drive option. The Export/Import function allows users to copy
a user list to all of an organization’s QS-B220 units by exporting a user list from one unit, and importing
that list on to a different unit.
2.14.1
E XP O R T F UN CT I O N
The Export function allows a user to back up sampling data from a unit by exporting sample files onto
an external USB drive or FTP network site. Two types of file export are available:
Export by Date:





Configuration Files: A snapshot of the environmental settings and software settings at the given
time. This includes the substance table and unit configuration files.
Event Log: A log of recent user activity.
Log Files: Hardware and software logs.
User Accounts: A list of user accounts.
Sample Data: Spectrograms and relevant environmental data.
o Alarms Only: Only alarm samples will be exported.
o Exclude Calibration: Only samples and verifications will be exported.
o Purge Spectrograms: Export the files, sample records (number, time, date, alarms) are
retained by the QS-B220, while the spectrograms are deleted.
Export by Sample ID:

2.14.2
Sample ID: Spectrograms and relevant environmental data organized by Sample ID, and are
individually selectable files.
I MP O R T F UN C T I O N
The Import function allows a user to transfer data from one unit to another via an external USB drive or
FTP site. Import options include:



Environment Settings: Software settings.
User Accounts: User account list.
Substance Table: Updates to the substance table
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Export by Date Instructions:
1. Log on to the QS-B220 as an administrator level user.
2.
From the Main Menu, press the Administration button.
3.
From the Administration menu press the Export/Import button.
4.
At the bottom of the screen ensure that the Export Option Type field is set to
Date.
5.
Highlight the checkboxes next to the file types for export.
Figure 90: Export file types
6.
Use the calendar drop down boxes to select a date range for export.
Figure 91: Export calendar drop down
7.
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Insert a USB to store exported files into the I/O port on the QS-B220 OR ensure
there is a connection to a viable FTP server in the QS-B220 Settings screen.
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8.
Press the Export Location button.
Figure 92: Export folder location
9.
Press the Select Drive button.
Figure 93: Export select drive
10. Choose the desired export drive (USB or FTP) and press OK.
11. Locate the export folder location in the file structure and press OK.
12. Ensure that the location field shows the correct file location, and press the
Start button.
13. The QS-B220 will complete export and display an Export Successful or Export
Failed popup.
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Export by Sample ID Instructions:
1.
Log on to the QS-B220 as an administrator level user.
2.
From the Main Menu, press the Administration button.
3.
From the Administration menu press the Export/Import button.
4.
At the bottom of the screen ensure that the Export Option Type field is set to
Sample ID.
5.
Use the calendar dropdown options to select the start date and end date for
the Sample ID range.
6.
Check the checkboxes next to the Sample IDs of the samples for export.
Figure 94: Export by sample ID
7.
Insert a USB to store exported files into the I/O port on the QS-B220 OR ensure
there is a connection to a viable FTP server in the QS-B220 Settings screen.
8.
Press the Export Location button.
9.
Press the Select Drive button.
10. Choose the desired export drive (USB or FTP) and press OK.
11. Locate the export folder location in the file structure and press OK.
12. Ensure that the location field shows the correct file location, and press the
Start button.
13. The QS-B220 will complete export and display an Export Successful or Export
Failed popup.
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Import Instructions:
1.
Log on to the QS-B220 as an administrator level user.
2.
From the Main Menu, press the Administration button.
3.
From the Administration menu press the Export/Import button.
4.
Click the Import tab.
5.
Highlight the checkboxes next to the file type for import.
Figure 95: Import file types
6.
Insert a USB to store exported files into the I/O port on the QS-B220 OR ensure
there is a connection to a viable FTP server in the QS-B220 Settings screen.
7.
Press the Import Location button.
Figure 96: Import folder location
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8.
Press the Select Drive button.
Figure 97: Import choose directory
9.
Choose the desired export drive (USB or FTP) and press OK.
10. Locate the file to import in the file structure and press OK.
11. Ensure that the location field shows the correct file location, and press the
Start button.
12. The QS-B220 will complete import and display an Import Successful or Import
Failed popup.
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2.15
P URGE D AT ABASE
Access: Administrator
The purge tool allows a user to erase data from the QS-B220 database. Three purge options are
available:
 Event Log: This option will purge the data from the QS-B220 event log that is available via the
diagnostics menu.

Sample Data: This option will delete all samples in the sampling history screen, and will reset the
current sample number to 1.

Configuration Files: This option will delete old configuration file backups from the database.
Figure 98: Purge database
Purge Database Instructions:
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1.
Log on to the QS-B220 as an administrator level user.
2.
From the Main Menu, press the Administration button.
3.
From the Administration menu press the Purge Database button.
4.
In the Purge Database screen, press the check boxes next to Event Log, Sample
Data or Configuration Files to select the type of data to purge.
5.
Press the Start button. When the purge has completed the message
“Transaction Complete” will be displayed on the screen.
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2.16
6.
Press the Close button to return to the Administration menu.
7.
Press the <Back button to return to the Main Menu.
R EPORTS
Access: Supervisor, Administrator
Note: Supervisors can only access the Administrator Summary report.
Note: The default time period for report generation is one month, ending on the current date.
The reports menu allows a user to generate reports on QS-B220 login history, QS-B220 sample history,
and individual sample details. Reports can be printed to an external printer (configured in the QS-B220
Settings screen) or exported to Microsoft Excel, XML and PDF files.
Figure 99: Reports menu
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2.16.1

A D MI N I ST R AT O R S U M M AR Y
The Administrator Summary report can be accessed by Supervisor and Administrator level users. The
report contains the login and logout date and time, the number of samples, and alarm rate for each
user.
Figure 100: Administrator summary report
2.16.2

S A MP LE H I ST O R Y
The Sample History report contains the date, time, and ID number of each sample, whether or not
the sample alarmed as well as any substances it alarmed on. The report also displays the User ID of
the person who was logged in at the time of the sample.
Figure 101: Sample history report
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2.16.3

E V EN T S U MM A R Y
The Event Summary displays the details of a specific event. On the reports page, when the user
selects the Event Summary report, they are to enter a specific Sample #. The report is generated and
displays: login ID, sample count (Sample #), alarm type, sample date and time, and any comments
that were added to the sample.
Figure 102: Event summary report
2.16.4

E Q UI P M EN T S U M M AR Y
The Equipment Summary report allows the user to select start date and end date of data to be
displayed in the report and whether the report is displayed as a daily report, weekly report, monthly
report, or yearly report. The report displays the date range of the summary, the sample count #, the
alarm count, the peak hour, and the breakdown of alarms by type for each time period in the report.
Figure 103: Equipment summary report
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2.16.5

U P T I ME S U M MA R Y
The Uptime Summary report allows the user to view the time that the machine has been powered on
and is available for use.
Figure 104: Uptime summary report
Report Instructions FOR SUPERVISORS:
1. From the Main Menu, press the Reports button.
2.
Select the Administrator Summary report type.
3.
Select the start and end dates using the calendar drop down panels.
4.
Press Show Report.
5.
Press the <Back button three times to return to the Main Menu.
Report Instructions FOR ADMINISTRATORS:
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1.
From the Main Menu, press the Administration button.
2.
From the Administration Menu press the Reports button.
3.
Select report type. Event summary reports and equipment summary reports
require a secondary filter (by sample ID or by time interval) selection.
4.
Select the start and end dates using the calendar drop down panels.
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5.
Press Show Report.
6.
Press the <Back button three times to return to the Main Menu.
Print Report Instructions FOR ADMINISTRATORS:
1.
Ensure that the report printer is configured in the QS-B220 Settings screen.
2.
From the Main Menu, press the Administration button.
3.
From the Administration Menu press the Reports button.
4.
Select report type.
5.
Select the start and end dates using the calendar drop down panels.
6.
Press Show Report.
7.
Press the Print button at the bottom of the report.
8.
Press the <Back button three times to return to the Main Menu.
Export Report Instructions FOR ADMINISTRATORS:
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1.
From the Main Menu, press the Administration button.
2.
From the Administration Menu press the Reports button.
3.
Select report type.
4.
Select the start and end dates using the calendar drop down panels.
5.
Press Show Report.
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6.
Press the Export button at the bottom of the report.
Figure 105: Export report
7.
Insert a USB for the export file in the I/O panel of the QS-B220.
8.
Select a file type for export (to XML, PDF or Excel).
9.
Press the Browse… button and select an export location on the USB.
10. Press the Export button.
11. The QS-B220 will complete export and display an Export Successful or Export
Failed popup.
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2.17
2.17.1
D IAGNOSTICS
H AR DW AR E P AR A M ET E RS
Access: Administrator
The Hardware Parameters screen allows the user to view all system hardware parameters. The
Counters tab records a count of system functions including verification, regenerations and sieve
replacement.
Figure 106: Hardware parameters
Figure 107: Hardware parameters – counters
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2.17.2
E V EN T L O G
Access: Administrator
The Event Log screen displays all system events that have occurred, including user log in information,
and system errors. The event log is instrumental in diagnosing problems with the system.
Figure 108: Event log
2.17.3
S Y ST E M W AR M -U P
Access: Administrator
The System Warm-Up screen displays the warm-up status and various heater values.
Note: All users will see a system warm-up after login after a system shut down. Administrator level
users can visit this system warm-up screen to view a snapshot of hardware values when the system is
not in a warm-up state.
Figure 109: System warm-up
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SectionSection
3 – Maintenance
Instructions
2 – QS-B220
“How To”
3 – MAINTENANCE
INSTRUCTIONS
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SectionSection
3 – Maintenance
Instructions
2 – QS-B220
“How To”
Outer Housing Cleaning
Cabin Filter Cleaning
Cleaning
Mirror Regeneration
Cabin Filter Replacement
Desorber Cleaning
Sieve Change:
Sieve Orifice Filter Replacement
Sample Path Filter Replacement
N-Hexachloroethane (Dopant)
Replacement
N-Nitrovanillin (Calibrant) Replacement
P-Nicotinamide (Dope/Cal) Replacement
O
O
Auto
Note 1
Auto
Note 1
O
S
S
S
Note 2
Note 2
S
F
Note 3
F
LEGEND
O: Operator
S: Supervisor
F: Field Service
Figure 110: Recommended maintenance schedule
NOTES
1. Cleaning and Mirror Regeneration maintenance items are performed automatically per the schedule
specified above and also by the automated cleaning system as necessary. These maintenance items can
also be performed manually as part of the troubleshooting procedures.
2. The sieve canister change frequency is the average. There are many factors that go into the life
expectancy of the sieve canisters such as humidity in the environment. You can expect more frequent
sieve changes in very humid environments. The sieve orifice filter is replaced at the time of the sieve
canister change.
3. Nitro vanillin has an extremely slow dissipation rate. It is expected that the Nitro vanillin cartridges will
last the life of the unit.
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As Needed
Two Years
One Year
Quarterly
Monthly
Weekly
QS- B220
Recommended Maintenance Schedule
Daily
3.1 R ECOMMENDED M AINTENANCE S CHEDULE
92
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Instructions
2 – QS-B220
“How To”
3.2 C HANGE S IEVE C ANISTERS
See QS-B220 “How To” Sieve Maintenance section on page 36.
3.3 C ALIBRANT
AND
D OPANT R EPLACEMENT
Calibrant and dopant chemicals are contained in heated chambers within the system. The calibrant and
dopants last for approximately 2 years in normal operation, since calibrations are performed
automatically at specific intervals as needed.
Contact the local service center for calibrant and dopant replacement.
3.4 C LEANING
THE
D ESORBER
See QS-B220 desorber cleaning instructions section on page 33.
3.5 D ESORBER S CREEN C HECK
During normal use the desorber screen should be checked annually. If a build-up of foreign material is
observed, replace the screen every year or as needed.
Desorber Screen Check Instructions:
1. Power down the QS-B220 and allow the Desorber to cool for 45 minutes.
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“How To”
Remove the two (2) Phillips head screws from the bottom of the Desorber
Cover, remove the Desorber Cover and set it aside.
Figure 111: Desorber cover removal
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“How To”
2.
Gently pull the desorber screen tray out of the desorber and inspect the filter
screen.
Figure 112: Removal of desorber filter screen tray
Figure 113: Desorber filter screen tray
NOTE: There is a desorber filter screen retaining ring holding the filter
screen in place. Care should be taken to ensure the retaining ring is
not dislodged during removal.
3.
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If the filter screen is dirty, replace with the following steps:
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“How To”
4.
Turn the desorber filter screen tray upside down (screen facing up) over a clean
surface to remove the desorber filter screen retaining ring.
Figure 114: Filter screen retainer ring removal
5.
Gently push the filter screen out of the desorber filter screen tray from the
bottom.
Figure 115: Filter screen removal
6.
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Place the new filter screen into the desorber filter screen tray from the top,
ensuring the filter screen is sitting flat
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2 – QS-B220
“How To”
7.
Reinstall the desorber filter screen retaining ring, and ensure that it is sitting
flush with the top of the desorber filter screen tray.
Figure 116: Desorber filter screen retainer installation
8.
Reinstall the desorber filter screen tray into the desorber with a slight side-toside motion ensuring it is fully seated in the desorber.
9.
Replace the desorber cover.
10. Restore power to the QS-B220 system.
3.6 R EPLACING C ABIN F ILTER
During normal use, the cabin filter should be cleaned or replaced once a week. In dirtier environments,
the filter may need to be cleaned or replaced more often.
Replace Cabin Filter Instructions:
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1.
The cabin filter is accessed by removing the filter guard on the side of the
console.
2.
The cabin filter can be cleaned by gently shaking it to dislodge any surface or
embedded dirt.
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Instructions
2 – QS-B220
“How To”
Figure 117: Accessing cabin filter
3.7 L OADING P RINTER P APER (O PTIONAL I N TEGRATED P RINTER )
Manual load printer paper instructions (recommended):
1. Open outer printer cover.
2.
Gently push (2) tabs labeled “Push” on each side of the printer housing. This
will give you access to the inner printer componentry.
Figure 118: Open printer housing
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Instructions
2 – QS-B220
“How To”
3.
Gently lift the lever labeled “Lift this lever for paper loading”.
Figure 119: Lift lever for paper loading
4.
Place a new paper roll in the paper tray with the leading edge of the roll
feeding from the bottom. Cut leading edge of the paper roll at an angle.
Figure 120: Paper roll cut on an angle
Figure 121: Insert paper roll
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Instructions
2 – QS-B220
“How To”
5.
Carefully feed the paper under the printer roller taking care not to crease or
jam the leading edge as you feed it through. Feed the roll through until a few
inches are fed through the upper roller opening.
Figure 122: Feed paper through printer
6.
Pull enough slack to feed the leading edge through the bottom side of the
printer opening. Once the roll is completely through the printer opening
continue feeding the paper directly through the outer printer cover opening.
Figure 123: Feed paper through printer cover
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Instructions
2 – QS-B220
“How To”
7.
Close the lever labeled “Lift this lever for paper loading”.
Figure 124: Close printer load lever
8.
Hold the leading edge of the paper roll up as you gently close the printer
housing. The housing should lock into place. Close the outer printer cover.
Figure 125: Close outer printer housing
Auto Feed Printer Paper Instructions:
1.
Open outer printer cover.
2.
Place a new paper roll in the paper tray with the leading edge of the roll
feeding from the bottom.
3.
Gently feed the leading edge of the paper roll under the printer roller until the
printer automatically feeds the paper roll.
4.
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Instructions
2 – QS-B220
“How To”
operation.
5.
Close outer printer cover and print test page to ensure proper operation.
3.8 S AMPLE W AND M AINTENANCE
To avoid contamination, the rubber pad area should be cleaned with a wipe containing isopropyl
alcohol (IPA). Weekly cleaning is recommended but can be more or less often, based on the
environment conditions. The pad should dry for at least 5 minutes prior to next use. If debris
accumulates on other areas of the sample wand, a wipe containing isopropyl alcohol (IPA) can be used
to dislodge the debris from the sample wand.
Figure 126: Sample wand
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Section 4 – Troubleshooting
4 – TROUBLESHOOTING
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Section 4 – Troubleshooting
4.1 I NTRODUCTION
The purpose of this troubleshooting section is to recognize certain environmental conditions that may
prevent the system from operating optimally. The table below will explain basic troubleshooting
techniques to determine the cause of the problem and present information on potential ways to
overcome these conditions and return the system to an operational state.
The system’s IMS detectors contain heaters and provide airflow in order to maintain its environment.
The heat and airflow allows the QS-B220 to operate cleanly and efficiently.
During periods of inactivity when the QS-B220 is not powered on, some contamination may build up
that can cause problems such as calibration failure and false/repeated alarms. Additionally, humidity
levels may elevate inside the system and compromise its detection capabilities.
It is recommended that the system is powered ON whenever possible. If this is not possible, and the
QS-B220 has been in storage for a significant amount of time, the QS-B220 should be powered up 12
hours prior to its expected use to obtain optimal performance.
If the system has been shipped via air an extended powered ON period of 24 hours is recommended
prior to use to achieve optimal performance levels.
4.2 I MPLANT S CIENCES C ORPORATION C ONT ACT I NFORMATION
If technical assistance is required, contact Implant Sciences at:
Phone: +1 978-752-1700
Email: service@implantsciences.com
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Section 4 – Troubleshooting
4.3 M ESSAGE T ABLE
This table is a brief overview of the messages that may appear in the QS-B220 banner at the top center
of the user interface touchscreen.
Message
Description
Solution
Calibration
Required
The Calibration Required message is displayed Perform a Calibration.
after a calibration fails or when auto calibration
is disabled from the QS-B220 Settings menu
Cleaning Failed
A Cleaning failure will be reported if the system Shut Down the system from the Main Menu
did not reach the cleaning temperature set
screen, power off the unit, and then power
point by the end of the warm-up period or the the unit back on.
normal operating set point by the end of the
cool down period.
Clear Down
Incomplete
The Clear Down Incomplete message indicates Clear down must be initiated again manually
that the system has not cleared down within 10 from the Main Menu until the system is
minutes.
ready.
Cooling Down…
The QS-B220 includes a unique automatic
Wait for the Cool Down period to complete.
cleaning system to maintain optimal detection
sensitivity. The Cooling Down… message
indicates that the system is returning to the
operating state after an automated cleaning
procedure.
Equilibrating
This message is displayed while the QS-B220 is Wait for equilibration to complete (expected
adjusting system parameters to adapt to
to complete within 30 seconds).
changes in humidity and voltage.
Hardware Comms An internal communications failure has
Error
occurred.
Shut Down the system from the Main Menu
screen, power off the unit, and then power
the unit back on.
High Humidity
The High Humidity warning is displayed when
the internal humidity of the QS-B220 exceeds
the allowable threshold.
Change the sieve. See the Sieve Maintenance
section in QS-B220 How To.
Low Air Flow
The internal air flow through the system is
system is below system threshold settings.
Contact Implant Sciences Technical Service.
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Section 4 – Troubleshooting
Message
Description
Solution
Low Makeup Air
Flow
The internal air flow through the system is
below system threshold settings.
Contact Implant Sciences Technical Service.
Low Charge
(Negative)
This warning may be issued when the negative Run a Cleaning procedure (see page 30). If
mode ionizing source does not work efficiently. the negative charge is still low, run a
This can be caused from a buildup of
regeneration procedure.
contamination on the source.
Low Charge
(Positive)
This warning may be issued when the positive Run a Cleaning procedure. See page 30.
mode ionizing source does not work efficiently.
This can be caused from a buildup of
contamination on the source.
Ready to Sample
The system is ready to accept and analyze
sample traps.
Regeneration
Failed
The system did not reach the regeneration
Shut Down the system from the Main Menu
temperature set point by the end of the warm- screen, power off the unit, and then power
up period or the normal operating set point by the unit back on.
the end of the cool down period.
Verification
Required
The QS-B220 requires verification after the
system is powered on and then every eight
hours. A verification should be performed to
check that automatic calibration results are
accurate.
Perform a Verification. See page 26.
Warm-Up Failed
This error indicates that one or more heaters
did not reach their set points.
Shut Down the system from the Main Menu
screen, power off the unit, and then power
the unit back on.
System is ready.
Figure 127: Message Table
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Section 4 – Troubleshooting
4.4 T ROUBLESHOOTING T ABLE
Problem
Action
QS-B220 DOES NOT
POWER UP
Check the system power source:
 Is the power switch ON? The switch should be in the ‘I’
position.
 Check that the power cord is fully plugged in.
 Check the power cord for damage
 Check the AC Main power.
If the QS-B220 will not power up after performing these checks, please
contact Implant Sciences Technical Service.

Ensure that there are no Humidity or Low Charge warnings.

Perform a Manual Calibration by pressing the CALIBRATE
button. Perform trap based calibration as prompted by the
system.
Shut the system down via the Main screen, turn the power
OFF, then switch it back ON and allow it to warm-up and auto
calibrate.
If calibration is still required, perform CLEANING from the
Maintenance menu.
After Cleaning concludes, perform a manual calibration from
the Maintenance menu.


CALIBRATION
REQUIRED


If calibration is still required replace the sieve material as
explained in the Maintenance section of this manual.
 Perform another manual calibration from the Maintenance
menu.
 It is possible there are contaminants in the area preventing
calibration (i.e. cigarette smoke, cleaning vapors). If calibration
is still required after performing these steps, move the QSB220 to a different location and try these steps again.
If calibration is still required after performing these steps, contact
Implant Sciences Technical Service.
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Problem
Action
The Humidity too high warning is displayed when the humidity of the
QS-B220 exceeds the allowable threshold.

HIGH HUMIDITY
Ensure that the system has been powered on for a minimum of
1 hour to allow system to stabilize.


Perform a manual calibration.
If the warning persists, replace the sieve canisters as explained
in the How To – Sieve Maintenance section of this manual.
 Power up the system. Perform a calibration to test the
humidity and clear the warning. Note that the warning may
remain for a few minutes while the system stabilizes.
 If the warning persists, replace the sieve canisters.
If the problem persists after performing these steps, contact Implant
Sciences Technical Service.
This warning may be issued when the negative mode ionizing source
does not work efficiently. This can be caused from a buildup of
contamination on the source.

Perform a CLEANING from the Maintenance Menu.

LOW CHARGE
(NEGATIVE)
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At the conclusion of the CLEANING cycle, perform a manual
calibration from the Maintenance Menu.
 If the negative total charge is still too low, perform a
REGENERATION from the Maintenance menu.
 At the conclusion of the regeneration cycle, perform a manual
calibration from the Maintenance Menu.
 If the situation is not resolved, perform a DESORBER
CLEANING followed by another CLEANING.
 At the conclusion of the CLEANING cycle, perform a manual
calibration from the Maintenance Menu.
If the problem persists after performing these steps, contact Implant
Sciences Technical Service.
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Problem
Action
This warning may be issued when the positive mode ionizing source
does not work efficiently. This can be caused from a buildup of
contamination on the source.
LOW CHARGE
(POSITIVE)

Perform a CLEANING cycle from the Maintenance Menu.

At the conclusion of the CLEANING cycle, perform a manual
calibration from the Maintenance Menu.
If the situation is not resolved, perform a DESORBER
CLEANING followed by another CLEANING.


At the conclusion of the CLEANING cycle, perform a manual
calibration from the Maintenance Menu.
If the problem persists after performing these steps, contact Implant
Sciences Technical Service.
REPEATED ALARMS
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Repeated alarms may occur if the QS-B220 has become contaminated.
Allow sufficient time for any contamination to dissipate as explained in
the introductory section of the Troubleshooting section.
 Insert a fresh, clean, blank trap into the system. If the system
alarms, the system may still be contaminated.
 Clean the outside of the DESORBER cover using an IPA wipe.
Allow the DESORBER cover to dry for 10 minutes.
 Using a fresh, clean, blank trap, insert it into the system. If the
system alarms, the system may still be contaminated.
 If the problem persists, perform a CLEANING cycle from the
Maintenance menu. At the conclusion of the CLEANING cycle,
perform a manual calibration from the Maintenance Menu.
 Insert a fresh, clean, blank trap into the system. If the system
alarms, the system may still be contaminated.
 If the contamination persists, perform a DESORBER CLEANING
cycle followed by another CLEANING.
 At the conclusion of the CLEANING cycle, perform a manual
calibration from the Maintenance Menu.
 Insert a fresh, clean, blank trap into the system. If the system
alarms, the system may still be contaminated.
If the problem persists after performing these steps, contact Implant
Sciences Technical Service.
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Section 4 – Troubleshooting
Problem
Action
SYSTEM DOESN’T
SAMPLE WHEN TRAP
INSERTED

Check to make sure that the infrared sensor light located in the
DESORBER is on. The light is red.

Shut down the system via the Main screen, power it off and
then restart the system.

After warm-up and auto calibration run a blank trap sample.
If the problem persists after performing these steps, contact Implant
Sciences Technical Service.
The “Hardware Error” indicates an internal problem with the QS-B220.
HARDWARE ERROR

Shut down the system via the Main screen, power it off and
then restart the system.

After warm-up and auto calibration the system should be
ready to sample.
If the problem persists after performing these steps, contact Implant
Sciences Technical Service.
In the event that the touch screen is unresponsive:
TOUCH SCREEN NOT
WORKING

Connect a mouse and keyboard to the USB ports located on
the side of the system.

Use the mouse and keyboard to shut down the system from
the Main screen.

Power cycle the system.

After warm-up and auto calibration the system should be
ready to sample.
If the problem persists after performing these steps, contact Implant
Sciences Technical Service.
In the event that the system is unresponsive:
SYSTEM NOT
RESPONDING

Power cycle the system.

After warm-up and auto calibration the system should be
ready to sample.
If the problem persists after performing these steps, contact Implant
Sciences Technical Service.
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Section 4 – Troubleshooting
Problem
Action
CLEANING FAILED

A problem occurred during a cleaning cycle. Shut down the
system via the Main screen.

Power cycle the system.

After warm-up and auto calibration the system should be
ready to sample.
If the problem persists after performing these steps, contact Implant
Sciences Technical Service.
A problem occurred during a regeneration cycle.
REGENERATION FAILED

Shut down the system via the Main screen.

Power cycle the system.

After warm-up and auto calibration the system should be
ready to sample.
If the problem persists after performing these steps, contact Implant
Sciences Technical Service.
WARM-UP FAILED

The QS-B220 did not reach the proper operating state during
warm-up. Shut down the system via the Main screen.

Power cycle the system.

After warm-up and auto calibration the system should be
ready to sample.
If the problem persists after performing these steps, contact Implant
Sciences Technical Service.
The normal cleardown procedure was unable to remove all detectable
traces from the system.
CLEARDOWN FAILED

Perform a CLEANING from the Maintenance menu.

At the conclusion of the CLEANING cycle, clear down the
system again.

Perform a manual calibration from the Maintenance Menu
If the problem persists after performing these steps, contact Implant
Sciences Technical Service.
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Section 4 – Troubleshooting
Problem
Action
If Verification fails:

Try repeating the Verification Sample using a firmer touch to
load the sample trap.

If it still fails, perform a Calibration and then perform a
Verification.

If it still fails even though the verification peak is of sufficient
amplitude, perform a trap calibration, then retry verification.

If verification fails but there is no peak of sufficient amplitude,
check the total charge levels. If the total charge levels are
lower than normal, but a warning hasn’t been presented,
follow the steps for a LOW CHARGE condition and then
perform verification again.
VERIFICATION FAILED
If the problem persists after performing these steps, contact Implant
Sciences Technical Service.
On occasion, the Windows Operating System will display an error if
there is a serious system failure (memory problem, software crashed,
hard disk error, etc.) In any of these cases:
OTHER ERRORS

Shut down the system via the Main Screen.

Power off the System and restart.
If the problem persists after performing these steps, contact Implant
Sciences Technical Service.
Figure 128: Troubleshooting Table
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Section 5 – Guidelines for hand Sampling
5
-Guidelines for Hand
Sampling
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Section 5 – Guidelines for hand Sampling
5.1
P REPARING
TO SAMPLE
Sample traps
Implant Sciences’ Sample Traps are certified for use up to 25 times. However, after repeated use,
contaminants may accumulate on the sample trap. Before sampling, visually inspect traps for any
discoloration (figure 1). Always discard sample traps after a positive alarm, as well as after the
verification procedure or if the trap appears dirty.
Figure 129 Sample Traps
Using gloves
It is essential for all operators to wear powder-free nitrile gloves when sampling passengers, as to not
contribute any excess hand contaminants to the sample.
5.2
H OW
5.2.1
HA N D SA M P LI N G
EFFICIENTLY S AMPL E HANDS
When sampling hands during passenger screening, it is important to not apply excessive pressure onto
the sample trap. Detection is more effective when the trap is applied to the hands with light pressure.
Furthermore, using light pressure also prevents excessive hand contaminants, such as hand oils, lotions,
and cosmetics from being introduced into the system. These substances may interfere with the
detection of certain target substances
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Section 5 – Guidelines for hand Sampling
5.2.2
RE CO M M EN D E D S AM P LI N G T E CH N I Q U E S W I T HO UT S A MP LI N G W AN D
Hold sample trap at the base end and, in a sweeping motion, lightly graze the surface of back of the hand
AND palm of the hand. Repeat on the opposite hand and analyze. Do not apply any pressure (figures 2,
3). Sample hands in a unidirectional motion (figures 4, 5). When searching for trace amounts, this is
sufficient enough for detection of target substances.
Figure 130 Sampling technique 1
Figure 131 Sample technique 2
Figure 132 Front side
Figure 133 Back Side
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Section 5 – Guide Lines for hand sampling
5.2.3 Recommended Sampling Technique with Sampling Wand
1.
Use clean, powder-free Nitrile gloves to prevent excessive hand contamination
from soiling the trap.
With the sample wand in one hand, use your free hand to grip a sample trap
from the straight end. Insert the trap into the inlet area on the opened portion
of the sample wand. The sample trap should be placed into the insert inlet area
notched end first.
Figure 134: Insert trap into sample wand
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Section 5 – Guide Lines for hand sampling
2.
With the sample trap securely in place, grip the end tab of the sample wand
head and push in to close.
Figure 135: Close sample wand on trap
3.
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If necessary, pull gently on the top exposed end of the sample trap to tighten.
Pulling too hard may remove the trap from the sample wand.
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Section 5 – Guide Lines for hand sampling
4.
In a unidirectional sweeping motion, lightly graze the surface of back of the
hand.
Figure 136 Back Side
5.
In a unidirectional sweeping motion, lightly graze the surface of the palm of
the hand
Figure 137Front Side
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6.
Verify that the system status is displaying Ready to Sample. The sample wand
is now ready to use for sampling. To analyze, open the sample wand head,
remove the sample trap and insert into the QS-B220.
7.
When prompted, remove the sample trap
8.
At the conclusion of sampling, the QS-B220 will display an alarm popup or no
alarm popup.
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Section 5 – Guide Lines for hand sampling
5.3 How NOT to Sample
When sampling, do NOT place finger near the insertion end of the sample trap and apply downward
pressure onto the hands/palms of the passenger (figure 8). By doing so, more hand contaminants are
being harvested, which may actually interfere with or suppress the detection of target substances.
Figure 138 How NOT to sample
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Section 6 – Software User Access Levels
6 – SOFTWARE USER
ACCESS LEVELS
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Section 6 – Software User Access Levels
6.1 S OFTWARE U SER A CCESS L EVELS
Screener
Supervisor
Administrator
Login/Logout
X
X
X
Manually start sample
X
X
X
Automatically start sample
X
X
X
View sample details and Add Comments
X
X
X
Print Sample Data
X
X
X
Clear Down
Shutdown
Acknowledge Alarm
View Sample History
Calibrate
Cleaning
Regeneration
Verification
Sieve Maintenance
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
Control Alarm Data Printing
X
X
Control Full Screen Alarm Indication
X
X
Control Audio Volume
Set Language
X
X
X
X
Schedule Daily Maintenance
Export/Import system Data
Run a Report on Administrator Summary
X
X
Run Reports on Sample History, Event
Summary and Equipment Summary
View System Parameters
View Event log
View Warm-up Status
View Substance Values
Control System Settings
Set Date/Time
Check Network Connectivity, Add Network
Printer, Control FTP Network Settings
Upgrade Software
X
X
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X
X
X
X
X
X
X
View Substance Values
Manage User Accounts
X
X
X
X
X
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Section 7 - Glossary
Section 6: Glossary
7 – GLOSSARY
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Section 7 – Glossary
Section 6: Glossary
Term
Desorber
Definition
The desorber heats the
sample trap to release
collected traces into the
QS-B220. Inserting a
sample trap into the
desorber slot begins the
detection process.
Main Menu
Touchscreen menu
located on QS-B220
system screen. Used to
navigate through system
options.
Orifice Filter
A filter that is changed as
part of the sieve
replacement procedure.
Orifice Filter
Replacement Tool
Stored on the sieve
housing cover, the
Orifice filter replacement
tool is used to screw and
unscrew the orifice filter
during the sieve
replacement procedure.
Sample Trap
Also called a swab. Used
to wipe surfaces to
collect traces for
analysis.
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Section 7 – Glossary
Section 6: Glossary
Sample Wand
Sieve
Used during sampling to
prevent contamination
from screener hands, and
to facilitate easy
sampling inside/around
cargo.
A desiccant substance
that removes water from
air. Used by the QS-B220
to control internal
humidity.
Sieve Canister
Convenient quickchange packaging for QSB220 sieve material.
Verification Can A
Used to verify the
calibration of the
negative spectrometer.
Verification Can B
Used to verify the
calibration of the positive
spectrometer.
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Section 8 – Table of Figures
Section 6: Glossary
8 - TABLE OF FIGURES
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Section 8 – Table of Figures
Section 6: Glossary
Figure 1: System Schematic Cross Section .....................................................................................................................9
Figure 2: Major components of QS-B220 system ........................................................................................................11
Figure 3: External connections ....................................................................................................................................12
Figure 4: AC input location ..........................................................................................................................................16
Figure 5: Power cord ....................................................................................................................................................16
Figure 6: AC panel and power switch ..........................................................................................................................16
Figure 7: Log in screen .................................................................................................................................................17
Figure 8: System warm-up (administrator) .................................................................................................................18
Figure 9: System warm-up (screener) .........................................................................................................................18
Figure 10: Verification required ...................................................................................................................................18
Figure 11: Ready to sample .........................................................................................................................................18
Figure 12: Main menu with logout button ..................................................................................................................20
Figure 13: Auto logout rate .........................................................................................................................................20
Figure 14: Main menu with shutdown button.............................................................................................................21
Figure 15: Power switch ..............................................................................................................................................21
Figure 16: Calibration required ....................................................................................................................................22
Figure 17: Verification required ...................................................................................................................................23
Figure 18: Maintenance menu ....................................................................................................................................23
Figure 19: Calibration screen .......................................................................................................................................24
Figure 20: Verification screen ......................................................................................................................................26
Figure 21: Cleaning screen ...........................................................................................................................................30
Figure 22: Automatic cleaning cool down ...................................................................................................................31
Figure 23 Automatic cleaning (low positive charge)....................................................................................................31
Figure 24: Regeneration ..............................................................................................................................................32
Figure 25: Automatic regeneration cool down ............................................................................................................33
Figure 26 Automatic regeneration ( Low negative charge) .........................................................................................33
Figure 27: Desorber cleaning .......................................................................................................................................34
Figure 28: Desorber cleaning with alcohol swab .........................................................................................................34
Figure 29: Sieve maintenance......................................................................................................................................36
Figure 30: High humidity warning ...............................................................................................................................37
Figure 31: Sieve chamber lever ...................................................................................................................................38
Figure 32: Tilting sieve canisters ..................................................................................................................................38
Figure 33: Unscrewing sieve canister ..........................................................................................................................39
Figure 34: Orifice Filter Replacement Tool ..................................................................................................................39
Figure 35: Locate the Pin on the Orifice Filter .............................................................................................................39
Figure 36: Orifice Installation ......................................................................................................................................40
Figure 37: Turn Orifice Filter Replacement Tool ..........................................................................................................40
Figure 38: Discard Old Orifice Filter .............................................................................................................................41
Figure 39: Replace Orifice Filter...................................................................................................................................41
Figure 40: Inspecting for O-rings .................................................................................................................................42
Figure 41: Blank sample – ready to sample .................................................................................................................43
Figure 42: Blank sample – sampling ............................................................................................................................43
Figure 43: Sample alarm ..............................................................................................................................................43
Figure 44: Sample no alarm .........................................................................................................................................43
Figure 45: Implant Sciences sample wand and sample trap ........................................................................................44
Figure 46: Possible trap sample results .......................................................................................................................45
Figure 47: Holding a trap .............................................................................................................................................46
Figure 48: Sampling by hand .......................................................................................................................................46
Figure 49: Sample Details (Screener View) ..................................................................................................................48
Figure 50: Sample Details (Administrator View) ..........................................................................................................48
Figure 51: Sample Alarms (Administrator View) .........................................................................................................48
Figure 52: Sample Spectrogram (Administrator View) ................................................................................................48
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Section 8 – Table of Figures
Section 6: Glossary
Figure 53: Clearing down popup..................................................................................................................................49
Figure 54: Clearing down banner ................................................................................................................................49
Figure 55: Resolve alarm popup ..................................................................................................................................50
Figure 56: Resolve alarm banner .................................................................................................................................50
Figure 57: Add comment .............................................................................................................................................51
Figure 58: Sampling history .........................................................................................................................................52
Figure 59: Sampling history, sample details ................................................................................................................53
Figure 60: Sampling history query ...............................................................................................................................53
Figure 61: User accounts screen ..................................................................................................................................55
Figure 62: Add a user account .....................................................................................................................................55
Figure 63: Add a user account with keyboard .............................................................................................................56
Figure 64: Modify user account ...................................................................................................................................57
Figure 65: Delete user account ....................................................................................................................................57
Figure 66: Enable User Account ...................................................................................................................................58
Figure 67: QS-B220 settings system tab ......................................................................................................................59
Figure 68: Resolve alarm popup (indicator = ON) .......................................................................................................60
Figure 69: Resolve alarm banner (indicator = OFF) .....................................................................................................60
Figure 70: QS-B220 settings – advanced tab ...............................................................................................................61
Figure 71: QS-B220 settings – scheduled tasks tab .....................................................................................................63
Figure 72: Sieve replacement reminder .....................................................................................................................64
Figure 73: QS-B220 system settings ............................................................................................................................65
Figure 74: QS-B220 system settings – FTP tab.............................................................................................................66
Figure 75: Tested FTP connection................................................................................................................................67
Figure 76: Select drive (FTP) ........................................................................................................................................67
Figure 77: QS-B220 system settings – FTP tab.............................................................................................................68
Figure 78: Insert network printer name ......................................................................................................................69
Figure 79: Adding network printer ..............................................................................................................................69
Figure 80: Network printer added successfully ...........................................................................................................70
Figure 81: Choose network printer ..............................................................................................................................70
Figure 82: Peripherals tab ............................................................................................................................................71
Figure 83: QS-B220 substances ...................................................................................................................................71
Figure 84: Substances with edit capability ..................................................................................................................72
Figure 85: Add/Modify substance ...............................................................................................................................72
Figure 86: Substance modes ........................................................................................................................................73
Figure 87: Upgrade software .......................................................................................................................................74
Figure 88: Upgrade software select folder ..................................................................................................................75
Figure 89: Upgrade software directory browser .........................................................................................................75
Figure 90: Export file types ..........................................................................................................................................77
Figure 91: Export calendar drop down ........................................................................................................................77
Figure 92: Export folder location .................................................................................................................................78
Figure 93: Export select drive ......................................................................................................................................78
Figure 94: Export by sample ID ....................................................................................................................................79
Figure 95: Import file types .........................................................................................................................................80
Figure 96: Import folder location.................................................................................................................................80
Figure 97: Import choose directory .............................................................................................................................81
Figure 98: Purge database ...........................................................................................................................................82
Figure 99: Reports menu .............................................................................................................................................83
Figure 100: Administrator summary report ................................................................................................................84
Figure 101: Sample history report ...............................................................................................................................84
Figure 102: Event summary report ..............................................................................................................................85
Figure 103: Equipment summary report .....................................................................................................................85
Figure 104: Uptime summary report ...........................................................................................................................86
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Section 8 – Table of Figures
Section 6: Glossary
Figure 105: Export report ............................................................................................................................................88
Figure 106: Hardware parameters...............................................................................................................................89
Figure 107: Hardware parameters – counters.............................................................................................................89
Figure 108: Event log ...................................................................................................................................................90
Figure 109: System warm-up .......................................................................................................................................90
Figure 110: Recommended maintenance schedule ....................................................................................................92
Figure 111: Desorber cover removal ...........................................................................................................................94
Figure 112: Removal of desorber filter screen tray .....................................................................................................95
Figure 113: Desorber filter screen tray ........................................................................................................................95
Figure 114: Filter screen retainer ring removal ..........................................................................................................96
Figure 115: Filter screen removal ................................................................................................................................96
Figure 116: Desorber filter screen retainer installation ..............................................................................................97
Figure 117: Accessing cabin filter ................................................................................................................................98
Figure 118: Open printer housing ................................................................................................................................98
Figure 119: Lift lever for paper loading .......................................................................................................................99
Figure 120: Paper roll cut on an angle .........................................................................................................................99
Figure 121: Insert paper roll ........................................................................................................................................99
Figure 122: Feed paper through printer ....................................................................................................................100
Figure 123: Feed paper through printer cover ..........................................................................................................100
Figure 124: Close printer load lever ..........................................................................................................................101
Figure 125: Close outer printer housing ....................................................................................................................101
Figure 126: Sample wand ..........................................................................................................................................102
Figure 127: Message Table ........................................................................................................................................106
Figure 128: Troubleshooting Table ............................................................................................................................112
Figure 129 Sample Traps ...........................................................................................................................................114
Figure 130 Sampling technique 1 ..............................................................................................................................115
Figure 131 Sample technique 2 .................................................................................................................................115
Figure 132 Front side .................................................................................................................................................115
Figure 133 Back Side ..................................................................................................................................................115
Figure 136: Insert trap into sample wand .................................................................................................................116
Figure 137: Close sample wand on trap ....................................................................................................................117
Figure 138 Back Side ..................................................................................................................................................118
Figure 139Front Side..................................................................................................................................................118
Figure 140 How NOT to sample .................................................................................................................................119
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Section – Index
9 - INDEX
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Section 9 – Index
AC power cord .........................................................16
Acknowledge Alarm ................................................50
Administrator Summary Report ..............................84
Alarm Indicator ........................................................60
Alarm Protocol .........................................................50
Alarms ......................................................................50
Alcohol Swabs ............................................................4
Analysis Time ...........................................................10
auto-logout ..............................................................20
automatic cleaning ..................................................31
B220 Settings ...........................................................59
Blank Sample ...........................................................43
Cabin Filter ...............................................................97
Calibrant and Dopant Replacement ........................93
Calibration ...............................................................23
Calibration Required ................................................22
Change Sieve Soon...................................................64
Cleaning ............................................................. 30, 31
Cleaning the Desorber .............................................93
Clear Down ..............................................................49
Cleardown ................................................................10
collector .....................................................................9
Comment .................................................................51
Consumables .............................................................4
conventions ...............................................................2
Cotton Swabs .............................................................4
default accounts ......................................................17
Delete Database ......................................................82
desorber cleaning ....................................................34
Desorber Cleaning ............................................. 34, 36
Desorber screen.........................................................4
Desorber Screen Check ............................................93
Dimensions ..............................................................10
Display .....................................................................10
drift tube ....................................................................9
Equilibrating...........................................................105
Equipment Summary Report ...................................85
Event Log .................................................................90
Event Summary Report ............................................85
Export ......................................................................76
Export Report ..........................................................87
filter guard ...............................................................97
filter, cabin ...............................................................97
filter, replacing.........................................................97
filters ..........................................................................4
gloves .........................................................................4
Hardware Parameters .............................................89
humidity...................................................................36
Humidity ..................................................................10
Implant Sciences ....................................................104
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Import ......................................................................76
Ion Mobility Spectrometer ........................................9
Maintenance ..........................................................106
molecules ...................................................................9
Nitrile gloves ..............................................................4
Operating Temperature ...........................................10
O-Rings.....................................................................42
Parameters ..............................................................89
photon-ionization ......................................................9
Print Options............................................................59
Printer ......................................................................98
Printer Paper............................................................98
Protocol, Alarm ........................................................50
Purge Database ........................................................82
Query .......................................................................52
Recommended Maintenance Schedule ...................92
Regeneration ...........................................................32
Regeneration Frequency .........................................64
Reorder ......................................................................4
replacing cabin filter ................................................97
Replacing Cabin Filter ..............................................97
Report Export ..........................................................87
Reports ....................................................................83
Resolve Alarms ........................................................50
Reusing Sample Traps ..............................................47
Safety .......................................................................12
Sample Acquisition ..................................................10
Sample Details .........................................................48
Sample History Report .............................................84
Sample Traps .............................................................4
sample wand............................................................44
Sample Wand Maintenance ..................................102
Sampling ..................................................................43
Sampling History ......................................................52
Sensitivity.................................................................10
Shutdown ................................................................21
Sieve .................................................................. 36, 93
Sieve Replacement Reminder ..................................64
Software Upgrade ....................................................74
Spare Parts .................................................................4
Spectrogram ............................................................48
Start Sample ............................................................43
Substances ...............................................................71
Substances Table .....................................................71
Swabs .........................................................................4
symbol .......................................................................2
caution ...................................................................2
note of interest ......................................................2
warning ..................................................................2
System Settings........................................................65
132
Section 9 – Index
trace detection ..........................................................9
Transfer User List .....................................................76
Trap handling ...........................................................46
Trap Sample .............................................................44
troubleshooting .....................................................104
Troubleshooting ....................................................107
Typographic Conventions ..........................................2
Unlock a user ...........................................................58
Upgrade Software ....................................................74
Uptime Summary Report .........................................86
User Access ............................................................121
User Accounts ..........................................................54
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User Accounts – Add................................................55
User Accounts – Delete ...........................................57
User Accounts – Modify...........................................56
User Accounts – Unlock ...........................................58
User Accounts – Update ..........................................56
Verification ..............................................................26
Verification Rate ......................................................62
Verification Required ...............................................22
Wand .......................................................................44
Warm-up Time .........................................................10
warning ......................................................................2
Weight .....................................................................10
133
Section 10 – Appendix: Material
Safety Data Sheets
Section 9: MSDS Sheets
10 APPENDIX:
MATERIAL SAFETY
DATA SHEETS
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Section 9: MSDS Sheets
SIGMA-ALDRICH sigma-aldrich.com
Material Safety Data Sheet
Product: XM-101-T TNT Simulant
Date of Preparation: 8/1/00
8/1/00 TNT Simulant MSDS
Page 2 of 4
Section 1 - Chemical Product and Company Identification
Product/Chemical Name: Simulant for Trinitrotoluene (TNT), KTN-01-AA
Chemical Formula: for TNT C7H5N3O6, for Silica O2Si
CAS Number:
Other Designations: Fused Silica with Trinitrotoluene
General Use: To have the vapor signature of an explosive, but will not explode.
Manufactured for: XM division of Van Aken International, 9157 Rochester Court, Rancho Cucamonga,
CA 91730,
TEL (909) 980-2001, FAX (909) 980-2333 (hours 8:00am till 4:30pm of operation), emergency TEL (909)
260-2561.
Emergency Overview 
Section 2 - Composition / Information on Ingredients
Ingredient Name CAS Number % wt
Silica, fused 60676-86-0 >92%
2,4,6-Trinitrotoluene 118-96-7 <8%
Trace Impurities: None
OSHA PEL ACGIH TLV NIOSH REL NIOSH
Ingredient TWA STEL TWA STEL TWA STEL IDLH
Silica 80mg/m3 none estab.
.
none estab. . none estab. none estab. none estab. none estab.
TNT 1500mg/m3
(SKIN)
none estab. none estab. none estab. none estab. none estab. none estab.
Toxicity Data: Exposure Limits 0.1 mg/m 3 (resp), 1.5 mg/m3 (skin)
Section 3 - Physical and Chemical Properties
Physical State: granular solid
Appearance and Odor: light brown to white
Odor Threshold: None
Density: 2.2 gm/cc
Specific Gravity (H2O=1, at 4 °C):1.1
pH:
Water Solubility: 0.5%
Other Solubilities:
Freezing/Melting Point: 240ofor TNT
Section 4 - Fire-Fighting Measures
Flash Point: N/A
Burning Rate:
Autoignition Temperature: none
LEL: N/A
UEL: N/A
Flammability Classification: Non-Flammable
Extinguishing Media: Water Spray, carbon dioxide or dry chemical
Unusual Fire or Explosion Hazards: none
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Hazardous Combustion Products: CO, Co2, NO
Fire-Fighting Instructions: Do not release runoff from fire control methods to sewers or waterways.
Fire-Fighting Equipment: Because fire may produce toxic thermal decomposition products, wear a selfcontained breathing
apparatus (SCBA) with a full face piece operated in pressure-demand or positive-pressure mode.
Section 5 - Stability and Reactivity
Stability: Product is stable at room temperature in closed containers under normal storage and handling
conditions.
Polymerization: Hazardous polymerization cannot occur.
Chemical Incompatibilities: none known
8/1/00 TNT Simulant MSDS
Page 3 of 4
Conditions to Avoid: none known
Hazardous Decomposition Products: none
Section 6 - Health Hazard Information
Potential Health Effects
Primary Entry Routes: Inhalation
Target Organs: Lungs
Acute Effects
Inhalation: High intraperitoneal, intratracheal, intravenous. Cause pulmonary dust disease.
Eye: none
Skin: none
Ingestion: same as above
Carcinogenicity: IARC, NTP, and OSHA do not list product or chemical as a carcinogen.
Medical Conditions Aggravated by Long-Term Exposure: silicosis
Chronic Effects: Same
Emergency and First Aid Procedures
Inhalation: Remove affected person to well ventilated area.
Eye Contact: Wash with water.
Skin Contact: Wash with water.
Ingestion: Induce vomiting.
After first aid, get appropriate in-plant, paramedic, or community medical support.
Note to Physicians:
Special Precautions/Procedures:
Section 7 - Spill, Leak, and Disposal Procedures
Spill /Leak Procedures: Dispose of powder as a non-explosive waste.
Small Spills: Same
Large Spills: Same
Containment: For large spills, dike far ahead of liquid spill for later disposal. Do not release into sewers
or waterways.
Cleanup: Do not use acetone, use water as necessary.
Regulatory Requirements: Follow applicable OSHA regulations (29 CFR 1910.120).
Disposal: Contact your supplier or a licensed contractor for detailed recommendations. Follow applicable
Federal, state, and
local regulations.
Disposal Regulatory Requirements: As an inert material.
Container Cleaning and Disposal: Use water. Collect material in 50 micro meter mesh filter
Ecological Information: None
EPA Regulations:
RCRA Hazardous Waste Number: Not listed (40 CFR 261.33)
RCRA Hazardous Waste Classification (40 CFR 261.): Not classified
CERCLA Hazardous Substance (40 CFR 302.4) unlisted specific per RCRA, Sec. 3001; CWA, Sec. 311
(b)(4); CWA, Sec.
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Section 9: MSDS Sheets
307(a), CAA, Sec. 112
CERCLA Reportable Quantity: none known
SARA 311/312 Codes: none known
SARA Toxic Chemical (40 CFR 372.65): Not listed
SARA EHS (Extremely Hazardous Substance) (40 CFR 355): Not listed.
OSHA Regulations:
Air Contaminant (29 CFR 1910.1000, Table Z-1, Z-1-A): Not listed
OSHA Specifically Regulated Substance (29CFR 1910.109)
State Regulations: Same
Section 8 - Exposure Controls / Personal Protection
Engineering Controls: Handle as an inert material.
Ventilation: Provide general or local exhaust ventilation systems to maintain airborne concentrations
below OSHA PELs
(Sec.Ê2). Local exhaust ventilation is preferred because it prevents contaminant dispersion into the work
area by controlling it
at its source.
Administrative Controls: Maintain in approved storage area.
8/1/00 TNT Simulant MSDS
Page 4 of 4
Respiratory Protection: Seek professional advice prior to respirator selection and use. Follow OSHA
respirator regulations
(29 CFR 1910.134) and, if necessary, wear a MSHA/NIOSH-approved respirator. Select respirator based
on its suitability to
provide adequate worker protection for given working conditions, level of airborne contamination, and
presence of sufficient
oxygen. For emergency or non-routine operations (cleaning spills, reactor vessels, or storage tanks),
wear an SCBA.
Warning! Air-purifying respirators do not protect workers in oxygen-deficient atmospheres. If respirators
are used, OSHA
requires a written respiratory protection program that includes at least: medical certification, training, fittesting, periodic
environmental monitoring, maintenance, inspection, cleaning, and convenient, sanitary storage areas.
Protective Clothing/Equipment: Wear chemically protective gloves, boots, aprons, and gauntlets to
prevent prolonged or
repeated skin contact. Wear protective eyeglasses or chemical safety goggles, per OSHA eye- and faceprotection regulations
(29 CFR 1910.133). Contact lenses are not eye protective devices. Appropriate eye protection must be
worn instead of, or in
conjunction with contact lenses. Handle behind a barrier.
Safety Stations: Make emergency eyewash stations, safety/quick-drench showers, and washing facilities
available in work area.
Contaminated Equipment: Separate contaminated work clothes from street clothes. Launder before
reuse. Remove this
material from your shoes and clean personal protective equipment.
Comments: Never eat, drink, or smoke in work areas. Practice good personal hygiene after using this
material, especially before
eating, drinking, smoking, using the toilet, or applying cosmetics.
Section 9 - Special Precautions and Comments
Handling Precautions: none
Storage Requirements: none
DOT Transportation Data (49 CFR 172.101):
Shipping Name: Simulant, not
an explosive
Shipping Symbols: none
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Safety Data Sheets
Section 9: MSDS Sheets
Hazard Class: not applicable
ID No.:
Packing Group:
Label:
Special Provisions:
Packaging Authorizations
a) Exceptions:
b) Non-bulk Packaging:
c) Bulk Packaging: N/A
Quantity Limitations
a) Passenger, Aircraft, or Railcar:
b) Cargo Aircraft Only:
Vessel Stowage Requirements
a) Vessel Stowage:
b) Other:
Prepared By: B. MacDonald
Revision Notes: RVA 1/29/08
Disclaimer:
Material Safety Data Sheet
Version 4.5
Revision Date 10/26/2012
Print Date 02/21/2013
1. PRODUCT AND COMPANY IDENTIFICATION
Product name : H EXACHL OROETHANE
Product Number : 185442
Brand : Aldrich
Supplier : Sigma-Aldrich
3050 Spruce Street
SAINT LOUIS MO 63103
USA
Telephone : +1 800-325-5832
Fax : +1 800-325-5052
Emergency Phone # (For both supplier and manufacturer) : (314) 776-6555
Preparation Information : Sigma-Aldrich Corporation
Product Safety - Americas Region 1-800-521-8956
2. HAZARDS IDENTIFICATION
Emergency Overview
OSHA Hazards
Carcinogen, Irritant
Target Organs
Central nervous system, Liver, Kidney
GHS Classification
Acute toxicity, Oral (Category 5)
Skin irritation (Category 2)
Eye irritation (Category 2A)
Carcinogenicity (Category 2)
Specific target organ toxicity - single exposure (Category 3)
Acute aquatic toxicity (Category 1)
Chronic aquatic toxicity (Category 1)
GHS Label elements, including precautionary statements
Pictogram
Signal word Warning
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Hazard statement(s)
H303 May be harmful if swallowed.
H315 Causes skin irritation.
H319 Causes serious eye irritation.
H335 May cause respiratory irritation.
H351 Suspected of causing cancer.
H410 Very toxic to aquatic life with long lasting effects.
Precautionary statement(s)
P261 Avoid breathing dust/ fume/ gas/ mist/ vapours/ spray.
P273 Avoid release to the environment.
P281 Use personal protective equipment as required.
P305 + P351 + P338 IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present
and easy to do. Continue rinsing.
P501 Dispose of contents/ container to an approved waste disposal plant.
HMIS Classification
Health hazard: 2
Chronic Health Hazard: *
Flammability: 0
Physical hazards: 0
NFPA Rating
Health hazard: 2
Fire: 0
Reactivity Hazard: 0
Potential Health Effects
Inhalation May be harmful if inhaled. Causes respiratory tract irritation.
Skin May be harmful if absorbed through skin. Causes skin irritation.
Eyes Causes eye irritation.
Ingestion May be harmful if swallowed.
3. COMPOSITION/INFORMATION ON INGREDIENTS
Synonyms : Perchloroethane
Formula : C2Cl6
Molecular Weight : 236.74 g/mol
Component Concentration
Hexachloroethane
CAS-No.
EC-No.
67-72-1
200-666-4
4. FIRST AID MEASURES
General advice
Consult a physician. Show this safety data sheet to the doctor in attendance. Move out of dangerous area.
If inhaled
If breathed in, move person into fresh air. If not breathing, give artificial respiration. Consult a physician.
In case of skin contact
Wash off with soap and plenty of water. Consult a physician.
In case of eye contact
Rinse thoroughly with plenty of water for at least 15 minutes and consult a physician.
If swallowed
Never give anything by mouth to an unconscious person. Rinse mouth with water. Consult a physician.
5. FIREFIGHTING MEASURES
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Conditions of flammability
Not flammable or combustible.
Suitable extinguishing media
Use water spray, alcohol-resistant foam, dry chemical or carbon dioxide.
Special protective equipment for firefighters
Wear self contained breathing apparatus for fire fighting if necessary.
Hazardous combustion products
Hazardous decomposition products formed under fire conditions. - Carbon oxides, Hydrogen chloride gas
6. ACCIDENTAL RELEASE MEASURES
Aldrich - 185442 Page 3 of 8
Personal precautions
Use personal protective equipment. Avoid dust formation. Avoid breathing vapors, mist or gas. Ensure adequate
ventilation. Evacuate personnel to safe areas. Avoid breathing dust.
Environmental precautions
Prevent further leakage or spillage if safe to do so. Do not let product enter drains. Discharge into the environment
must be avoided.
Methods and materials for containment and cleaning up
Pick up and arrange disposal without creating dust. Sweep up and shovel. Keep in suitable, closed containers for
disposal.
7. HANDLING AND STORAGE
Precautions for safe handling
Avoid contact with skin and eyes. Avoid formation of dust and aerosols. Provide appropriate exhaust ventilation at
places where dust is formed.
Conditions for safe storage
Keep container tightly closed in a dry and well-ventilated place.
8. EXPOSURE CONTROLS/PERSONAL PROTECTION
Components with workplace control parameters
Components CAS-No. Value Control parameters
Basis
Hexachloroethane
67-72-1 TWA
1 ppm
USA. ACGIH Threshold Limit Values (TLV)
Remarks Liver & kidney damage Confirmed animal carcinogen with unknown relevance to humans Danger of
cutaneous absorption
TWA
1 ppm
10 mg/m3
USA. OSHA - TABLE Z-1 Limits for Air Contaminants -1910.1000
Skin notation
TWA
1 ppm
10 mg/m3
USA. Occupational Exposure Limits (OSHA) - Table Z-1
Limits for Air Contaminants
Skin designation The value in mg/m3 is approximate.
TWA
1 ppm
10 mg/m3
USA. NIOSH Recommended Exposure Limits
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Potential Occupational Carcinogen See Appendix C See Appendix A Potential for dermal
absorption
Personal protective equipment
Respiratory protection
Where risk assessment shows air-purifying respirators are appropriate use a full-face particle respirator type N100
(US) or type P3 (EN 143) respirator cartridges as a backup to engineering controls. If the respirator is the sole
means of protection, use a full-face supplied air respirator. Use respirators and components tested and approved
under appropriate government standards such as NIOSH (US) or CEN (EU).
Hand protection
Handle with gloves. Gloves must be inspected prior to use. Use proper glove removal technique (without touching
glove's outer surface) to avoid skin contact with this product. Dispose of contaminated gloves after use in
accordance with applicable laws and good laboratory practices. Wash and dry hands.
Immersion protection
Material: Nitrile rubber
Minimum layer thickness: 0.11 mm
Break through time: > 480 min
Material tested: Dermatril® (Aldrich Z677272, Size M)
Splash protection
Material: Nitrile rubber
Minimum layer thickness: 0.11 mm
Break through time: > 30 min
Material tested:Dermatril® (Aldrich Z677272, Size M)
data source: KCL GmbH, D-36124 Eichenzell, phone +49 (0)6659 873000, e-mail sales@kcl.de, test method: EN374
If used in solution, or mixed with other substances, and under conditions which differ from EN 374, contact the
supplier of the CE approved gloves. This recommendation is advisory only and must be evaluated by an Industrial
Hygienist familiar with the specific situation of anticipated use by our customers. It should not be construed as
offering an approval for any specific use scenario.
Eye protection
Safety glasses with side-shields conforming to EN166 Use equipment for eye protection tested and approved
under appropriate government standards such as NIOSH (US) or EN 166(EU).
Skin and body protection
impervious clothing, The type of protective equipment must be selected according to the concentration and
amount of the dangerous substance at the specific workplace.
Hygiene measures
Handle in accordance with good industrial hygiene and safety practice. Wash hands before breaks and at the end
of workday.
9. PHYSICAL AND CHEMICAL PROPERTIES
Appearance
Form crystalline
Colour white
Safety data
pH no data available
Melting point/freezing point: Melting point/range: 183 - 185 °C (361 - 365 °F)
Boiling point no data available
Flash point no data available
Ignition temperature no data available
Autoignition temperature: no data available
Lower explosion limit no data available
Upper explosion limit no data available
Vapour pressure 0.5 hPa (0.4 mmHg) at 20.0 °C (68.0 °F)
Density 2.091 g/mL at 25 °C (77 °F)
Water solubility no data available
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Partition coefficient: n-octanol/water, no data available
Relative vapour density: no data available
Odour no data available
Odour Threshold no data available
Evaporation rate no data available
10. STABILITY AND REACTIVITY
Chemical stability
Stable under recommended storage conditions.
Possibility of hazardous reactions
no data available
Conditions to avoid
no data available
Materials to avoid
Strong oxidizing agents, Strong bases
Hazardous decomposition products
Hazardous decomposition products formed under fire conditions. - Carbon oxides, Hydrogen chloride gas Other
decomposition products - no data available
11. TOXICOLOGICAL INFORMATION
Acute toxicity
Oral LD50
LD50 Oral - guinea pig - 4,970 mg/kg
TDLo Oral - rat - female - 5,500 mg/kg
TDLo Oral - rat - 6,944 mg/kg
Remarks: Liver:Changes in liver weight. Kidney, Ureter, Bladder:Changes in tubules (including acute renal failure,
acute tubular necrosis). Kidney, Ureter, Bladder:Other changes.
TDLo Oral - rat - 48,750 mg/kg
Remarks: Brain and Coverings:Other degenerative changes. Liver:Changes in liver weight. Kidney, Ureter,
Bladder:Other changes.
TDLo Oral - rabbit - 12,000 mg/kg
Remarks: Liver:Other changes. Kidney, Ureter, Bladder:Other changes. Nutritional and Gross Metabolic:Weight loss
or decreased weight gain.
Inhalation LC50
Behavioral:Muscle weakness.
Dermal LD50
LD50 Dermal - rabbit - 32,000 mg/kg
Other information on acute toxicity
LD50 Intraperitoneal - mouse - 4,500 mg/kg
LDLO Intraperitoneal - rat - 2,900 mg/kg
LDLO Intravenous - dog - 325 mg/kg
Skin corrosion/irritation
no data available
Serious eye damage/eye irritation
no data available
Respiratory or skin sensitization
no data available
Germ cell mutagenicity
Genotoxicity in vivo - Hamster
Sister chromatid exchange
Carcinogenicity
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This product is or contains a component that has been reported to be possibly carcinogenic based on its IARC,
ACGIH, NTP, or EPA classification. Limited evidence of carcinogenicity in animal studies
IARC: 2B - Group 2B: Possibly carcinogenic to humans (Hexachloroethane)
NTP: Reasonably anticipated to be a human carcinogen (Hexachloroethane)
OSHA: No component of this product present at levels greater than or equal to 0.1% is identified as a carcinogen or
potential carcinogen by OSHA.
Reproductive toxicity
no data available
Teratogenicity
no data available
Specific target organ toxicity - single exposure (Globally Harmonized System)
no data available
Specific target organ toxicity - repeated exposure (Globally Harmonized System)
no data available
Aspiration hazard
no data available
Potential health effects
Inhalation May be harmful if inhaled. Causes respiratory tract irritation.
Ingestion May be harmful if swallowed.
Skin May be harmful if absorbed through skin. Causes skin irritation.
Eyes Causes eye irritation.
Signs and Symptoms of Exposure
To the best of our knowledge, the chemical, physical, and toxicological properties have not been thoroughly
investigated.
Synergistic effects
no data available
Additional Information
RTECS: KI4025000
12. ECOLOGICAL INFORMATION
Toxicity
Toxicity to fish NOEC - Cyprinodon variegatus (sheepshead minnow) - 1 mg/l - 96 h
Toxicity to daphnia
and other aquatic
invertebrates
LC50 - Daphnia magna (Water flea) - 1.36 mg/l - 48 h
Persistence and degradability
Biodegradability Result: - Not biodegradable
Method: OECD Test Guideline 301
Bioaccumulative potential
Bioaccumulation Lepomis macrochirus (Bluegill) - 28 d
Bioconcentration factor (BCF): 139
Aldrich - 185442 Page 7 of 8
Mobility in soil
no data available
PBT and vPvB assessment
no data available
Other adverse effects
An environmental hazard cannot be excluded in the event of unprofessional handling or disposal.
Very toxic to aquatic life with long lasting effects. No data available.
13. DISPOSAL CONSIDERATIONS
Product
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Offer surplus and non-recyclable solutions to a licensed disposal company. Contact a licensed professional waste
disposal service to dispose of this material. Dissolve or mix the material with a combustible solvent and burn in a
chemical incinerator equipped with an afterburner and scrubber.
Contaminated packaging
Dispose of as unused product.
14. TRANSPORT INFORMATION
DOT (US)
UN number: 3077 Class: 9 Packing group: III
Proper shipping name: Environmentally hazardous substances, solid, n.o.s. (Hexachloroethane)
Reportable Quantity (RQ): 100 lbs
Marine pollutant:
Poison Inhalation Hazard: No
IMDG
UN number: 3077 Class: 9 Packing group: III EMS-No: F-A, S-F
Proper shipping name: ENVIRONMENTALLY HAZARDOUS SUBSTANCE, SOLID, N.O.S. (Hexachloroethane)
Marine pollutant: No
IATA
UN number: 3077 Class: 9 Packing group: III
Proper shipping name: Environmentally hazardous substance, solid, n.o.s. (Hexachloroethane)
Further information
EHS-Mark required (ADR 2.2.9.1.10, IMDG code 2.10.3) for single packagings and combination packagings
containing inner packagings with Dangerous Goods > 5L for liquids or > 5kg for solids.
15. REGULATORY INFORMATION
OSHA Hazards
Carcinogen, Irritant
SARA 302 Components
SARA 302: No chemicals in this material are subject to the reporting requirements of SARA Title III, Section 302.
SARA 313 Components
The following components are subject to reporting levels established by SARA Title III, Section 313:
Hexachloroethane
CAS-No.
67-72-1
Revision Date
2007-07-01
SARA 311/312 Hazards
Acute Health Hazard, Chronic Health Hazard
Massachusetts Right To Know Components
Hexachloroethane
CAS-No.
67-72-1
Revision Date
2007-07-01
Aldrich - 185442 Page 8 of 8
Pennsylvania Right To Know Components
Hexachloroethane
CAS-No.
67-72-1
Revision Date
2007-07-01
New Jersey Right To Know Components
Hexachloroethane
CAS-No.
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67-72-1
Revision Date
2007-07-01
California Prop. 65 Components
WARNING! This product contains a chemical known to the State of
California to cause cancer.
Hexachloroethane
CAS-No.
67-72-1
Revision Date
2007-09-28
16. OTHER INFORMATION
Further information
Copyright 2012 Sigma-Aldrich Co. LLC. License granted to make unlimited paper copies for internal use only. The
above information is believed to be correct but does not purport to be all inclusive and shall be used only as a
guide. The information in this document is based on the present state of our knowledge and is applicable to the
product with regard to appropriate safety precautions. It does not represent any guarantee of the properties of
the product. Sigma-Aldrich Corporation and its Affiliates shall not be held liable for any damage resulting from
handling or
from contact with the above product. See www.sigma-aldrich.com and/or the reverse side of invoice or packing
slip for additional terms and conditions of sale.
SIGMA-ALDRICH sigma-aldrich.com
Material Safety Data Sheet
Version 3.2
Revision Date 08/03/2012
Print Date 02/21/2013
1. PRODUCT AND COMPANY IDENTIFICATION
Product name : 5-N ITROVANILLIN
Product Number : N28000
Brand : Aldrich
Supplier : Sigma-Aldrich
3050 Spruce Street
SAINT LOUIS MO 63103
USA
Telephone : +1 800-325-5832
Fax : +1 800-325-5052
Emergency Phone # (For both supplier and manufacturer) : (314) 776-6555
Preparation Information : Sigma-Aldrich Corporation
Product Safety - Americas Region 1-800-521-8956
2. HAZARDS IDENTIFICATION
Emergency Overview
OSHA Hazards
Irritant
GHS Classification
Skin irritation (Category 2)
Eye irritation (Category 2A)
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Specific target organ toxicity - single exposure (Category 3)
GHS Label elements, including precautionary statements
Pictogram
Signal word Warning
Hazard statement(s)
H315 Causes skin irritation.
H319 Causes serious eye irritation.
H335 May cause respiratory irritation.
Precautionary statement(s)
P261 Avoid breathing dust/ fume/ gas/ mist/ vapours/ spray.
P305 + P351 + P338 IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present
and easy to do. Continue rinsing.
HMIS Classification
Health hazard: 2
Flammability: 0
Physical hazards: 0
NFPA Rating
Health hazard: 2
Fire: 0
Reactivity Hazard: 0
Potential Health Effects
Inhalation May be harmful if inhaled. Causes respiratory tract irritation.
Skin May be harmful if absorbed through skin. Causes skin irritation.
Eyes Causes eye irritation.
Ingestion May be harmful if swallowed.
3. COMPOSITION/INFORMATION ON INGREDIENTS
Synonyms : 4-Hydroxy-3-methoxy-5-nitrobenzaldehyde
Formula : C8H7NO5
Molecular Weight : 197.14 g/mol
Component Concentration
5-Nitrovanillin
CAS-No.
EC-No.
6635-20-7
229-633-2
4. FIRST AID MEASURES
General advice
Consult a physician. Show this safety data sheet to the doctor in attendance. Move out of dangerous area.
If inhaled
If breathed in, move person into fresh air. If not breathing, give artificial respiration. Consult a physician.
In case of skin contact
Wash off with soap and plenty of water. Consult a physician.
In case of eye contact
Rinse thoroughly with plenty of water for at least 15 minutes and consult a physician.
If swallowed
Never give anything by mouth to an unconscious person. Rinse mouth with water. Consult a physician.
5. FIREFIGHTING MEASURES
Suitable extinguishing media
Use water spray, alcohol-resistant foam, dry chemical or carbon dioxide.
Special protective equipment for firefighters
Wear self-contained breathing apparatus for fire-fighting if necessary.
Hazardous combustion products
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Hazardous decomposition products formed under fire conditions. - Carbon oxides, nitrogen oxides (NOx)
6. ACCIDENTAL RELEASE MEASURES
Personal precautions
Use personal protective equipment. Avoid dust formation. Avoid breathing vapors, mist or gas. Ensure adequate
ventilation. Evacuate personnel to safe areas. Avoid breathing dust.
Environmental precautions
Do not let product enter drains.
Methods and materials for containment and cleaning up
Pick up and arrange disposal without creating dust. Sweep up and shovel. Keep in suitable, closed containers for
disposal.
7. HANDLING AND STORAGE
Precautions for safe handling
Avoid contact with skin and eyes. Avoid formation of dust and aerosols. Provide appropriate exhaust ventilation at
places where dust is formed. Normal measures for preventive fire protection.
Conditions for safe storage
Keep container tightly closed in a dry and well-ventilated place. Keep in a dry place.
8. EXPOSURE CONTROLS/PERSONAL PROTECTION
Contains no substances with occupational exposure limit values.
Personal protective equipment
Respiratory protection
For nuisance exposures use type P95 (US) or type P1 (EU EN 143) particle respirator. For higher level protection
use type OV/AG/P99 (US) or type ABEK-P2 (EU EN 143) respirator cartridges. Use respirators and components
tested and approved under appropriate government standards such as NIOSH (US) or CEN (EU).
Hand protection
Handle with gloves. Gloves must be inspected prior to use. Use proper glove removal technique (without touching
glove's outer surface) to avoid skin contact with this product. Dispose of contaminated gloves after use in
accordance with applicable laws and good laboratory practices. Wash and dry hands.
Eye protection
Safety glasses with side-shields conforming to EN166 Use equipment for eye protection tested and approved
under appropriate government standards such as NIOSH (US) or EN 166(EU).
Skin and body protection
impervious clothing, The type of protective equipment must be selected according to the concentration and
amount of the dangerous substance at the specific workplace.
Hygiene measures
Handle in accordance with good industrial hygiene and safety practice. Wash hands before breaks and at the end
of workday.
9. PHYSICAL AND CHEMICAL PROPERTIES
Appearance
Form powder
Colour no data available
Safety data
pH no data available
Melting point/freezing point
Melting point/range: 172 - 175 °C (342 - 347 °F) - lit.
Boiling point no data available
Flash point no data available
Ignition temperature no data available
Autoignition temperature no data available
Lower explosion limit no data available
Upper explosion limit no data available
Vapour pressure no data available
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Density no data available
Water solubility no data available
Partition coefficient:
n-octanol/water
no data available
Relative vapour density
no data available
Odour no data available
Odour Threshold no data available
Evaporation rate no data available
10. STABILITY AND REACTIVITY
Chemical stability
Stable under recommended storage conditions.
Possibility of hazardous reactions
no data available
Conditions to avoid
no data available
Materials to avoid
Strong oxidizing agents, Strong bases
Hazardous decomposition products
Hazardous decomposition products formed under fire conditions. - Carbon oxides, nitrogen oxides (NOx)
Other decomposition products - no data available
11. TOXICOLOGICAL INFORMATION
Acute toxicity
Oral LD50
no data available
Inhalation LC50
Dermal LD50
no data available
Other information on acute toxicity
no data available
Skin corrosion/irritation
no data available
Serious eye damage/eye irritation
no data available
Respiratory or skin sensitization
no data available
Germ cell mutagenicity
no data available
Carcinogenicity
IARC: No component of this product present at levels greater than or equal to 0.1% is identified as probable,
possible or confirmed human carcinogen by IARC.
ACGIH: No component of this product present at levels greater than or equal to 0.1% is identified as a carcinogen
or potential carcinogen by ACGIH.
NTP: No component of this product present at levels greater than or equal to 0.1% is identified as a known or
anticipated carcinogen by NTP.
OSHA: No component of this product present at levels greater than or equal to 0.1% is identified as a carcinogen or
potential carcinogen by OSHA.
Reproductive toxicity
no data available
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Teratogenicity
Aldrich - N28000 Page 5 of 6
no data available
Specific target organ toxicity - single exposure (Globally Harmonized System)
Inhalation - May cause respiratory irritation.
Specific target organ toxicity - repeated exposure (Globally Harmonized System)
no data available
Aspiration hazard
no data available
Potential health effects
Inhalation May be harmful if inhaled. Causes respiratory tract irritation.
Ingestion May be harmful if swallowed.
Skin May be harmful if absorbed through skin. Causes skin irritation.
Eyes Causes eye irritation.
Signs and Symptoms of Exposure
To the best of our knowledge, the chemical, physical, and toxicological properties have not been thoroughly
investigated.
Synergistic effects
no data available
Additional Information
RTECS: Not available
12. ECOLOGICAL INFORMATION
Toxicity
no data available
Persistence and degradability
no data available
Bioaccumulative potential
no data available
Mobility in soil
no data available
PBT and vPvB assessment
no data available
Other adverse effects
no data available
13. DISPOSAL CONSIDERATIONS
Product
Offer surplus and non-recyclable solutions to a licensed disposal company. Contact a licensed professional waste
disposal service to dispose of this material.
Contaminated packaging
Dispose of as unused product.
14. TRANSPORT INFORMATION
DOT (US)
Not dangerous goods
IMDG
Not dangerous goods
IATA
Not dangerous goods
Aldrich - N28000 Page 6 of 6
15. REGULATORY INFORMATION
OSHA Hazards
Irritant
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SARA 302 Components
SARA 302: No chemicals in this material are subject to the reporting requirements of SARA Title III, Section 302.
SARA 313 Components
SARA 313: This material does not contain any chemical components with known CAS numbers that exceed the
threshold (De Minimis) reporting levels established by SARA Title III, Section 313.
SARA 311/312 Hazards
Acute Health Hazard
Massachusetts Right To Know Components
No components are subject to the Massachusetts Right to Know Act.
Pennsylvania Right To Know Components
5-Nitrovanillin
CAS-No.
6635-20-7
Revision Date
New Jersey Right To Know Components
5-Nitrovanillin
CAS-No.
6635-20-7
Revision Date
California Prop. 65 Components
This product does not contain any chemicals known to State of California to cause cancer, birth defects, or any
other
reproductive harm.
16. OTHER INFORMATION
Further information
Copyright 2012 Sigma-Aldrich Co. LLC. License granted to make unlimited paper copies for internal use only. The
above information is believed to be correct but does not purport to be all inclusive and shall be used only as a
guide. The information in this document is based on the present state of our knowledge and is applicable to the
product with regard to appropriate safety precautions. It does not represent any guarantee of the properties of
the product. Sigma-Aldrich Corporation and its Affiliates shall not be held liable for any damage resulting from
handling or
from contact with the above product. See www.sigma-aldrich.com and/or the reverse side of invoice or packing
slip for additional terms and conditions of sale.
Material Safety Data Sheet
Part Number: 10011326 Verification Sample B (Positive)
SECTION 1 – CHEMICAL PRODUCT AND COMPANY IDENTIFICATION
Product Name: Verification Sample B (Positive)
Product Use: For use as a verification sample containing narcotics simulant for the purpose of verifying
the detection of Implant Sciences Corporation’s Trace Detection Equipment.
Manufacturer: Implant Sciences Corporation
500 Research Drive Unit 3
Wilmington, MA 01887
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Section 9: MSDS Sheets
978-752-1700 Fax: 978-725-1711
%
SECTION 2 –
COMPOSITION/I
NFORMATION
ON
INGREDIENTS
CAS Number
Ingredients
Procaine
50
Hydrochloride
Adhesive, Crystalbond 509:
Phthalic
Anhydride
Ethylene Glycol
51-05-8
37.5
85-44-9
12.5
107-21-1
SECTION 3 – HAZARDS IDENTIFICATION
Emergency Overview: Toxic if swallowed.
HMIS Rating:
Health: 2
Flammability: 1
Reactivity: 0
SECTION 4 – FIRST AID MEASURES
Skin Contact: Rinse with soap and water.
Eye Contact: Flush with copious amounts of water for at least 15 minutes. If irritation occurs, seek
medical attention.
Inhalation: Not applicable.
Ingestion: Not applicable.
SECTION 5 – FIRE FIGHTING MEASURES
Suitable Extinguishing Media: Use Foam, Carbon Dioxide or Dry Powder. DO NOT USE WATER.
Flashpoint: Not Available
Autoignition Temperature: Not Available
Hazardous Combustion Products: Burning produces irritant fumes.
SECTION 6 – ACCIDENTAL RELEASE MEASURES
General Information: Sweep up and dispose of in a metal container. Provide adequate ventilation. Avoid
excessive heat, sparks, open flames or other sources of ignition. Dispose of in accordance with all local,
state and federal regulations.
SECTION 7 – HANDLING AND STORAGE
Handling Procedures and Equipment: Protective gloves recommended.
Storage Requirements: Keep containers tightly closed and store in a cool, dry area. Avoid excessive
heat, sparks, open flames or other sources of ignition.
SECTION 8 – EXPOSURE CONTROL/PERSONAL PROTECTION
Engineering Controls: Use with adequate ventilation.
Personal Protective Equipment:
Eyes: Not Applicable
Skin: Protective gloves recommended.
Clothing: Not Applicable
Hygiene Measures: Handle in accordance with good industrial hygiene and safety practice.
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SECTION 9 – PHYSICAL AND CHEMICAL PROPERTIES
Physical State: Solid
Appearance: Amber Color
Odor: Odorless
pH: Not Available
Vapor Pressure: 1.05 mmHg (Crystalbond); Procaine Hydrochloride <10-7 kpa (1.2 10-5 mg/L)
Vapor Density: (Air = 1): 1.0
Evaporation Rate: Nil
Flash Point: Not Available
Autoignition Temperature: Not Available
SECTION 10 – STABILITY AND REACTIVITY
Chemical Stability: Stable
Conditions to Avoid: Excessive heat, sparks, open flames or other sources of ignition.
Hazardous Decomposition of Products: Carbon Monoxide, Carbon Dioxide, Chloride/Hydrochloric Acid,
Nitrogen Oxides (NOx)/Ammonia/CNSECTION 11 – TOXICOLOGICAL INFORMATION
Product Information
LD50:
Oral: 361 mg/kg
Dermal: No Data Available
Inhalation: 2140 mg/m3 for Phthalic Anhydride
200 mg/m3 for Ethylene Glycol
No Data Available for Procaine Hydrochloride
Carcinogenic Effects: None of the ingredients is listed by ACGIH, IARD, NTP, or CA Prop 65
Mutagenic Effects: No Data Available
Reproductive Toxicity: No Data Available
SECTION 12 – ECOLOGICAL INFORMATION
Exotoxicity:
Procaine Hydrochloride: Not Listed
Phthalic Anhydride: No data Available
Ethylene Glycol: Fish, Rainbow Trout, LC50 = 41000 mg/Liter, 96 hours
Fish, Bluegill/Sunfish, LC50 = 27500 – 41000 mg/Liter, 96 hours
SECTION 13 – DISPOSAL CONSIDERATIONS
Waste Disposal: Waste disposal must be in accordance with appropriate Federal, State and Local
regulations.
SECTION 14 – TRANSPORT INFORMATION
US DOT Hazard Class: Not Hazardous
IATA: Non Hazardous for Air Transport.
SECTION 15 – REGULATORY INFORMATION
OSHA: No Data Available.
SARA:
Section 313: Procaine Hydrochloride is not listed.
This material contains Phthalic anhydride (CAS # 85-44-9) which is subject to the reporting requirements
of section 313 of SARA Title III and 40 CFR Part 373.
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This material contains Ethylene glycol (CAS# 107-21-1) which is subject to the reporting requirements of
Section 313 of SARA Title III and 40 CFR Part 373.
TSCA: Phthalic Anhydride and Ethylene Glycol are both listed on the TSCA Inventory. None of the
chemicals in this product are listed on the Health & Safety Reporting List. None of the chemicals in this
product is under a Chemical Test Rule. None of the chemicals in this product have a SNUR under TSCA.
None of the chemicals in this product is listed under TSCA Section 12b.
SECTION 16 – OTHER INFORMATION
Disclaimer: The information and recommendations contained herein are taken from sources believed to
be accurate as of the date hereof. However, Implant Sciences Corporation does not guarantee the
accuracy or completeness NOR SHALL ANY OF THIS INFORMATION CONSTITUTE A WARRANTY,
WHETHER EXPRESSED OR IMPLIED, AS TO THE SAFETY OF THE GOODS, THE MERCHANTABILITY OF THE
GOODS, OR THE FITNESS OF THE GOODS FOR A PARTICULAR PURPOSE. Adjustment to conform to actual
conditions of usage may be required. Implant Sciences Corporation assumes no responsibility for results
obtained or for incidental or consequential damages, including lost profits arising from the use of these
data. No warranty against infringement of any patent, copyright or trademark is made or implied. The
information contained in this sheet does not constitute a hazard assessment and should not be used in
place of the user’s own assessment of work place risks as required by other health and safety legislation.
Remember that it is always, at all times, the user’s responsibility to determine the suitability of any
material for any specific purpose and to adopt such safety precautions as may be necessary.
Material Safety Data Sheet
Part Number: 10011326 Verification Sample B (Positive)
SECTION 1 – CHEMICAL PRODUCT AND COMPANY IDENTIFICATION
Product Name: Verification Sample B (Positive)
Product Use: For use as a verification sample containing narcotics simulant for the purpose of verifying
the detection of Implant Sciences Corporation’s Trace Detection Equipment.
Manufacturer: Implant Sciences Corporation
500 Research Drive Unit 3
Wilmington, MA 01887
978-752-1700 Fax: 978-725-1711
%
CAS Number
SECTION 2 –
COMPOSITION/I
NFORMATION
ON
INGREDIENTS
Ingredients
Procaine
50
Hydrochloride
Adhesive, Crystalbond 509:
Phthalic
Anhydride
Ethylene Glycol
51-05-8
37.5
85-44-9
12.5
107-21-1
SECTION 3 – HAZARDS IDENTIFICATION
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Emergency Overview: Toxic if swallowed.
HMIS Rating:
Health: 2
Flammability: 1
Reactivity: 0
SECTION 4 – FIRST AID MEASURES
Skin Contact: Rinse with soap and water.
Eye Contact: Flush with copious amounts of water for at least 15 minutes. If irritation occurs, seek
medical attention.
Inhalation: Not applicable.
Ingestion: Not applicable.
SECTION 5 – FIRE FIGHTING MEASURES
Suitable Extinguishing Media: Use Foam, Carbon Dioxide or Dry Powder. DO NOT USE WATER.
Flashpoint: Not Available
Autoignition Temperature: Not Available
Hazardous Combustion Products: Burning produces irritant fumes.
SECTION 6 – ACCIDENTAL RELEASE MEASURES
General Information: Sweep up and dispose of in a metal container. Provide adequate ventilation. Avoid
excessive heat, sparks, open flames or other sources of ignition. Dispose of in accordance with all local,
state and federal regulations.
SECTION 7 – HANDLING AND STORAGE
Handling Procedures and Equipment: Protective gloves recommended.
Storage Requirements: Keep containers tightly closed and store in a cool, dry area. Avoid excessive
heat, sparks, open flames or other sources of ignition.
SECTION 8 – EXPOSURE CONTROL/PERSONAL PROTECTION
Engineering Controls: Use with adequate ventilation.
Personal Protective Equipment:
Eyes: Not Applicable
Skin: Protective gloves recommended.
Clothing: Not Applicable
Hygiene Measures: Handle in accordance with good industrial hygiene and safety practice.
SECTION 9 – PHYSICAL AND CHEMICAL PROPERTIES
Physical State: Solid
Appearance: Amber Color
Odor: Odorless
pH: Not Available
Vapor Pressure: 1.05 mmHg (Crystalbond); Procaine Hydrochloride <10-7 kpa (1.2 10-5 mg/L)
Vapor Density: (Air = 1): 1.0
Evaporation Rate: Nil
Flash Point: Not Available
Autoignition Temperature: Not Available
SECTION 10 – STABILITY AND REACTIVITY
Chemical Stability: Stable
Conditions to Avoid: Excessive heat, sparks, open flames or other sources of ignition.
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Section 9: MSDS Sheets
Hazardous Decomposition of Products: Carbon Monoxide, Carbon Dioxide, Chloride/Hydrochloric Acid,
Nitrogen Oxides (NOx)/Ammonia/CNSECTION 11 – TOXICOLOGICAL INFORMATION
Product Information
LD50:
Oral: 361 mg/kg
Dermal: No Data Available
Inhalation: 2140 mg/m3 for Phthalic Anhydride
200 mg/m3 for Ethylene Glycol
No Data Available for Procaine Hydrochloride
Carcinogenic Effects: None of the ingredients is listed by ACGIH, IARD, NTP, or CA Prop 65
Mutagenic Effects: No Data Available
Reproductive Toxicity: No Data Available
SECTION 12 – ECOLOGICAL INFORMATION
Exotoxicity:
Procaine Hydrochloride: Not Listed
Phthalic Anhydride: No data Available
Ethylene Glycol: Fish, Rainbow Trout, LC50 = 41000 mg/Liter, 96 hours
Fish, Bluegill/Sunfish, LC50 = 27500 – 41000 mg/Liter, 96 hours
SECTION 13 – DISPOSAL CONSIDERATIONS
Waste Disposal: Waste disposal must be in accordance with appropriate Federal, State and Local
regulations.
SECTION 14 – TRANSPORT INFORMATION
US DOT Hazard Class: Not Hazardous
IATA: Non Hazardous for Air Transport.
SECTION 15 – REGULATORY INFORMATION
OSHA: No Data Available.
SARA:
Section 313: Procaine Hydrochloride is not listed.
This material contains Phthalic anhydride (CAS # 85-44-9) which is subject to the reporting requirements
of section 313 of SARA Title III and 40 CFR Part 373.
This material contains Ethylene glycol (CAS# 107-21-1) which is subject to the reporting requirements of
Section 313 of SARA Title III and 40 CFR Part 373.
TSCA: Phthalic Anhydride and Ethylene Glycol are both listed on the TSCA Inventory. None of the
chemicals in this product are listed on the Health & Safety Reporting List. None of the chemicals in this
product is under a Chemical Test Rule. None of the chemicals in this product have a SNUR under TSCA.
None of the chemicals in this product is listed under TSCA Section 12b.
SECTION 16 – OTHER INFORMATION
Disclaimer: The information and recommendations contained herein are taken from sources believed to
be accurate as of the date hereof. However, Implant Sciences Corporation does not guarantee the
accuracy or completeness NOR SHALL ANY OF THIS INFORMATION CONSTITUTE A WARRANTY,
WHETHER EXPRESSED OR IMPLIED, AS TO THE SAFETY OF THE GOODS, THE MERCHANTABILITY OF THE
GOODS, OR THE FITNESS OF THE GOODS FOR A PARTICULAR PURPOSE. Adjustment to conform to actual
conditions of usage may be required. Implant Sciences Corporation assumes no responsibility for results
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Section 9: MSDS Sheets
obtained or for incidental or consequential damages, including lost profits arising from the use of these
data. No warranty against infringement of any patent, copyright or trademark is made or implied. The
information contained in this sheet does not constitute a hazard assessment and should not be used in
place of the user’s own assessment of work place risks as required by other health and safety legislation.
Remember that it is always, at all times, the user’s responsibility to determine the suitability of any
material for any specific purpose and to adopt such safety precautions as may be necessary.
Product Name NICOTINAMIDE, 99+%
Product Number 240206
Brand ALDRICH
Company Sigma-Aldrich
Address 3050 Spruce Street
SAINT LOUIS MO 63103 US
Technical Phone: 800-325-5832
Fax: 800-325-5052
Emergency Phone: 314-776-6555
Section 2 - Composition/Information on Ingredient
Substance Name CAS # SARA 313
NICOTINAMIDE 98-92-0 No
Formula C6H6N2O
Synonyms Acid amide * Amide PP * Amid kyseliny nikotinove
(Czech) * Aminicotin * m-(Aminocarbonyl)pyridine
* Amixicotyn * Amnicotin * Austrovit PP * Benicot
* 3-Carbamoylpyridine * Delonin amide * Dipegyl *
Endobion * Factor PP * Hansamid * Inovitan PP *
NAM * Niacevit * Niacinamide * Niavit PP *
Nicamindon * Nicasir * Nicobion * Nicofort *
Nicogen * Nicomidol * Nicosan 2 * Nicotamide *
Nicotilamide * Nicotinic acid amide * Nicotinic
amide * Nicotinsaureamid (German) * Nicotylamide
* Nicovit * Nicovitol * Nicozymin * Niko-Tamin *
Nikotinsaeureamid (German) * Niocinamide *
Niozymin * Pelmine * Pelonin amide * PP-Faktor *
Pyridine-3-carboxylic acid amide *
3-Pyridinecarboxamide * 3-Pyridinecarboxylic acid
amide * Savacotyl * VI-Nicotyl * Vitamin B *
Vitamin B3 * Vitamin PP * Witamina PP *
Niacinamide
RTECS Number: QS3675000
Section 3 - Hazards Identification
EMERGENCY OVERVIEW
Irritant.
Irritating to eyes, respiratory system and skin.
Target organ(s): Eyes. Kidneys.
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HMIS RATING
HEALTH: 2*
FLAMMABILITY: 0
REACTIVITY: 0
NFPA RATING
HEALTH: 2
FLAMMABILITY: 0
REACTIVITY: 0
*additional chronic hazards present.
For additional information on toxicity, please refer to Section 11.
Section 4 - First Aid Measures
ORAL EXPOSURE
If swallowed, wash out mouth with water provided person is
conscious. Call a physician.
INHALATION EXPOSURE
If inhaled, remove to fresh air. If not breathing give
artificial respiration. If breathing is difficult, give oxygen.
DERMAL EXPOSURE
In case of contact, immediately wash skin with soap and copious
amounts of water.
EYE EXPOSURE
In case of contact, immediately flush eyes with copious amounts
of water for at least 15 minutes.
Section 5 - Fire Fighting Measures
FLASH POINT
302 °F 150 °C Method: closed cup
AUTOIGNITION TEMP
N/A
FLAMMABILITY
N/A
EXTINGUISHING MEDIA
Suitable: Water spray. Carbon dioxide, dry chemical powder, or
appropriate foam.
FIREFIGHTING
Protective Equipment: Wear self-contained breathing apparatus
and protective clothing to prevent contact with skin and eyes.
Specific Hazard(s): Emits toxic fumes under fire conditions.
Section 6 - Accidental Release Measures
PROCEDURE(S) OF PERSONAL PRECAUTION(S)
Wear respirator, chemical safety goggles, rubber boots, and
heavy rubber gloves.
METHODS FOR CLEANING UP
Sweep up, place in a bag and hold for waste disposal. Avoid
raising dust. Ventilate area and wash spill site after material
pickup is complete.
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Section 7 - Handling and Storage
HANDLING
User Exposure: Do not breathe dust. Avoid contact with eyes,
skin, and clothing. Avoid prolonged or repeated exposure.
ALDRICH - 240206 www.sigma-aldrich.com Page 2
STORAGE
Suitable: Keep tightly closed.
Section 8 - Exposure Controls / PPE
ENGINEERING CONTROLS
Safety shower and eye bath. Mechanical exhaust required.
PERSONAL PROTECTIVE EQUIPMENT
Respiratory: Use respirators and components tested and approved
under appropriate government standards such as NIOSH (US) or CEN
(EU). Where risk assessment shows air-purifying respirators are
appropriate use a dust mask type N95 (US) or type P1 (EN 143)
respirator.
Hand: Compatible chemical-resistant gloves.
Eye: Chemical safety goggles.
GENERAL HYGIENE MEASURES
Wash thoroughly after handling.
Section 9 - Physical/Chemical Properties
Appearance Physical State: Solid
Color: White
Form: Fine crystals
Property Value At Temperature or Pressure
Molecular Weight 122.13 AMU
pH N/A
BP/BP Range N/A
MP/MP Range 128 °C
Freezing Point N/A
Vapor Pressure N/A
Vapor Density N/A
Saturated Vapor Conc. N/A
SG/Density N/A
Bulk Density N/A
Odor Threshold N/A
Volatile% N/A
VOC Content N/A
Water Content N/A
Solvent Content N/A
Evaporation Rate N/A
Viscosity N/A
Surface Tension N/A
Partition Coefficient N/A
Decomposition Temp. N/A
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Flash Point 302 °F 150 °C Method: closed cup
Explosion Limits N/A
Flammability N/A
Autoignition Temp N/A
Refractive Index N/A
Optical Rotation N/A
Miscellaneous Data N/A
Solubility N/A
N/A = not available
Section 10 - Stability and Reactivity
STABILITY
ALDRICH - 240206 www.sigma-aldrich.com Page 3
Stable: Stable.
Materials to Avoid: Strong oxidizing agents.
HAZARDOUS DECOMPOSITION PRODUCTS
Hazardous Decomposition Products: Carbon monoxide, Carbon dioxide,
Nitrogen oxides.
HAZARDOUS POLYMERIZATION
Hazardous Polymerization: Will not occur
Section 11 - Toxicological Information
ROUTE OF EXPOSURE
Skin Contact: Causes skin irritation.
Skin Absorption: May be harmful if absorbed through the skin.
Eye Contact: Causes eye irritation.
Inhalation: Material is irritating to mucous membranes and upper
respiratory tract. May be harmful if inhaled.
Ingestion: May be harmful if swallowed.
TARGET ORGAN(S) OR SYSTEM(S)
Kidneys. Eyes. Liver.
SIGNS AND SYMPTOMS OF EXPOSURE
To the best of our knowledge, the chemical, physical, and
toxicological properties have not been thoroughly investigated.
Other symptoms of exposure can include anorexia, excessive
salivation, pupillary constriction, bronchoconstriction,
respiratory failure, tightness of the chest, coma, pulmonary,
ureter, and bladder effects.
CONDITIONS AGGRAVATED BY EXPOSURE
May produce reversible liver damage
TOXICITY DATA
Oral Oral
Rat Rat
3500 mg/kg 3500 mg/kg
LD50 LD50
Subcutaneous Subcutaneous
Rat Rat
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1680 MG/KG 1680 MG/KG
LD50 LD50
Remarks: Lungs, Thorax, or Respiration:Other changes. Lungs,
Thorax, or Respiration:Other changes.
Oral Oral
Mouse Mouse
2500 mg/kg 2500 mg/kg
LD50 LD50
Intraperitoneal Intraperitoneal
Mouse Mouse
2050 MG/KG 2050 MG/KG
LD50 LD50
Subcutaneous Subcutaneous
Mouse Mouse
2 GM/KG 2 GM/KG
LD50 LD50
ALDRICH - 240206 www.sigma-aldrich.com Page 4
CHRONIC EXPOSURE - MUTAGEN
Species: Human Human
Dose: 10 MMOL/L 10 MMOL/L
Cell Type: lymphocyte lymphocyte
Mutation test: Sister chromatid exchange Sister chromatid
exchange
Species: Rat Rat
Dose: 20 MMOL/L 20 MMOL/L
Cell Type: liver liver
Mutation test: DNA inhibition DNA inhibition
Species: Rat Rat
Dose: 25 MG/KG 25 MG/KG
Cell Type: ovary ovary
Mutation test: Body fluid assay Body fluid assay
Species: Hamster Hamster
Dose: 5 MMOL/L 5 MMOL/L
Cell Type: ovary ovary
Mutation test: Sister chromatid exchange Sister chromatid
exchange
Section 12 - Ecological Information
No data available.
Section 13 - Disposal Considerations
APPROPRIATE METHOD OF DISPOSAL OF SUBSTANCE OR PREPARATION
Dissolve or mix the material with a combustible solvent and burn in a chemical incinerator equipped
with an afterburner and scrubber. Observe all federal, state, and local environmental regulations.
Section 14 - Transport Information DOT
Proper Shipping Name: None
Non-Hazardous for Transport: This substance is
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considered to be non-hazardous for transport.
IATA
Non-Hazardous for Air Transport: Non-hazardous for air
transport.
Section 15 - Regulatory Information
EU ADDITIONAL CLASSIFICATION
Symbol of Danger: Xi
Indication of Danger: Irritant.
R: 36/37/38
Risk Statements: Irritating to eyes, respiratory system and skin.
S: 26-36
Safety Statements: In case of contact with eyes, rinse
immediately with plenty of water and seek medical advice. Wear
suitable protective clothing.
US CLASSIFICATION AND LABEL TEXT
Indication of Danger: Irritant.
ALDRICH - 240206 www.sigma-aldrich.com Page 5
Risk Statements: Irritating to eyes, respiratory system and skin.
Safety Statements: In case of contact with eyes, rinse
immediately with plenty of water and seek medical advice. Wear
suitable gloves and eye/face protection.
US Statements: Target organ(s): Eyes. Kidneys.
UNITED STATES REGULATORY INFORMATION
SARA LISTED: No
TSCA INVENTORY ITEM: Yes Yes
CANADA REGULATORY INFORMATION
WHMIS Classification: This product has been classified in
accordance with the hazard criteria of the CPR, and the MSDS
contains all the information required by the CPR.
DSL: Yes
NDSL: No
Section 16 - Other Information
DISCLAIMER
For R&D use only. Not for drug, household or other uses.
WARRANTY
The above information is believed to be correct but does not
purport to be all inclusive and shall be used only as a guide. The information in this document is
based on the present state of our knowledge and is applicable to the product with regard to
appropriate safety precautions. It does not represent any
guarantee of the properties of the product. Sigma-Aldrich Inc., shall not be held liable for any
damage resulting from handling or from contact with the above product. See reverse side of invoice
or packing slip for additional terms and conditions of sale.
Copyright 2008 Sigma-Aldrich Co. License granted to make unlimited paper copies for internal use
only.
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ALDRICH - 240206 www.sigma-aldrich.com Page 6
KALTRON|PETTIBONE
1241 Ellis Street, Bensenville, Illinois 60106 630-350-1116 FAX 630-350-1606
info@kaltron.com www.kaltron.com
MATERIAL SAFETY DATA SHEET
MOLECULAR SIEVE 5A
SECTION 1 – PRODUCT IDENTIFICATION
Product Name: Molecular Sieve 5A
Chemical Name: Molecular Sieve
Synonyms: Aluminosilicate 5A, Zeolite 5A
Trade Names: N/A
Formula: Ca4.5Na3 [(AlO2)12(SiO2)12] _ X H2O
Molecular Weight: 285
CAS Number: 1344-00-9
EINECS Number: N/A
SECTION 2 – COMPOSITION, INFORMATION ON INGREDIENTS
Chemical Name: Calcium Aluminum Silicate
Percent: 100
CAS Number: 1344-00-9
ACGIH TLV (1992-1993) Not established
OSHA Pel: Not established
NIOSH (RTECS) Number: 1000369SS
SECTION 3 – HAZARD INFORMATION
SECTION 4 – FIRST AID MEASURES
Eyes: Flush eyes with plenty of water for at least 15 minutes, occasionally lifting the upper and lower eyelids. Get
medical aid.
Skin: Get medical aid. Flush skin with plenty of water for at least 15 minutes while removing contaminated clothing
and shoes. Wash clothing before reuse.
Ingestion: Never give anything by mouth to an unconscious person. Get medical aid. Do NOT induce vomiting. If
conscious and alert, rinse mouth and drink 2-4 cupfuls of milk or water.
Inhalation: Remove from exposure and move to fresh air immediately. If not breathing, give artificial respiration. If
breathing is difficult, give oxygen. Get medical aid. Do NOT use mouth-to-mouth resuscitation.
Notes to Physician: Treat symptomatically and supportively.
KALTRON|PETTIBONE
1241 Ellis Street, Bensenville, Illinois 60106 630-350-1116 FAX 630-350-1606
info@kaltron.com www.kaltron.com
Routes of Exposure:
Eye: Causes eye irritation, redness, pain.
Skin: May cause skin irritation with dryness and abrasion.
Ingestion: No adverse reaction expected.
Inhalation: May cause respiratory tract irritation and dryness. Symptoms may include coughing, sore throat, and
wheezing.
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SECTION 5 – FIRE FIGHTING MEASURES
Extinguishing Methods: Use media appropriate for surrounding fire.
Inappropriate Extinguishing Methods: Unknown.
Specific Hazards: Used product may contain products of a hazardous nature. Inform fire fighters of hazards of
retained chemicals.
Protective Measures in Case of Intervention: When exposed to water, product will get hot. Flood with water to
reduce to sage temperature.
Other Precautions: None.
SECTION 6 – ACCIDENTAL RELEASE MEASURES
General Information: Use proper personal protective equipment as indicated in Section 8.
Spills / Leaks: Clean up spills immediately, observing precautions in the Protective Equipment section. Sweep up,
and then place into a suitable container for disposal. Avoid generating dusty conditions. Provide ventilation.
Handling: Wash thoroughly after handling. Use with adequate ventilation. Minimize dust generation and
accumulation. Avoid contact with eyes, skin, and clothing. Keep container tightly closed. Avoid ingestion and
inhalation. Wash clothing before reuse.
Storage: Store in a tightly closed container. Store in a cool, dry, well-ventilated area away from combustible
substances.
SECTION 7 – PHYSICAL DATA
Physical State: Powder, extrudate or bead
Appearance: Tan
Odor: None Reported
pH: Not Available
Vapor Pressure: Not Available
Vapor Density: Not Available
Evaporation Rate: Not Available
Viscosity: Not Available
Boiling Point: Not Available
Melting Point: 1713 °C
Decomposition Temperature: Not Available
Solubility: Insoluble
Specific Gravity / Density: Not Available
SECTION 8 – EXPOSURE CONTROLS, PERSONAL PROTECTION
Engineering Controls: Facilities storing or utilizing this material should be equipped with an eyewash facility and a
safety shower. Use adequate ventilation to keep airborne
KALTRON|PETTIBONE
1241 Ellis Street, Bensenville, Illinois 60106 630-350-1116 FAX 630-350-1606
info@kaltron.com www.kaltron.com
concentrations low.
Personal Protective Equipment:
Eyes: Wear appropriate protective eyeglasses or chemical safety goggles as described by OSHA’s eye and face
protection regulations in 29 CFR 1910.133 or European Standard EN166.
Skin: Wear appropriate protective gloves to prevent skin exposure.
Clothing: Wear appropriate protective clothing to prevent skin exposure.
Respirators: A respiratory protection program that meets OSHA’s 29 CFR 1910.134 and ANSI Z88.2 requirements
or European Standard EN 149 must be followed whenever workplace conditions warrant respirator use.
SECTION 9 – TRANSPORT INFORMATION
D.O.T. Shipping Name: N/A D.O.T. Hazardous Classification: NonHazardous
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D.O.T. Labeling Requirements: None Hazardous Waste: Non-Hazardous
SECTION 10 – STABILITY AND REACTIVITY
Stability: Yes.
Conditions to Avoid: Addition of water without flooding will generate heat and can cause skin burns.
Materials to Avoid: No information available.
Hazardous Decomposition Products: None
Other Information: None.
SECTION 11 – DISPOSAL CONSIDERATIONS
Waste Treatment: Dispose in accordance with all local, state, and federal regulations.
SECTION 12 – OTHER INFORMATION
Edition Date: June 1995
Revision Number: 5
Updated: February 2006
The information above is believed to be accurate and represents the best information currently available to us.
However, we make no warranty of merchantability or any other warranty, express or implied, with respect to such
information, and we assume no liability resulting from its use. Users should make their own investigations to
determine the suitability of the information for their particular purposes. In no event shall Kaltron-Pettibone be
liable for any claims, losses, or damages of any third party or for lost profits or any special, indirect, incidental,
consequential or exemplary damages, howsoever arising, even if Kaltron-Pettibone has been advised of the
possibility of such damages.
Material Safety Data Sheet
U.S. Department of Labor
Occupational Safety and Health Administration
This form is consistent with ANSI standard for
preparation of MSDS’s in accordance with
OSHA's Hazard Communication Standard,
29 CFR 1910.1200.
Product Type: COCO PLUS 4x10 Activated
Product Code: 2293 Profile No: 2
Effective Date: March 31, 2008 Supersedes:
Charcoal
SECTION I - PRODUCT AND COMPANY INFORMATION
Company Identification (USA)
Calgon Carbon Corporation
P.O. Box 717
Pittsburgh, PA 15230-0717
Telephone Number(s) Information 412-787-6700
Emergency 412-787-6700
Company Identification
(Europe)
Chemviron Carbon
Zoning Industriel de Feluy
B-7181 Feluy, Belgium
Telephone Number(s) Information 32 64 51 18 11
Emergency 32 64 51 18 11
Date Prepared
November 3, 2008
Signature of Preparer
(optional)
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SECTION II – COMPOSITION /INFORMATION ON INGREDIENTS
Nonhazardous components are listed at 3% or greater; acute hazards are listed when present at 1% or greater and
chronic hazards are listed when present at 0.01% or greater. This is not intended to be a complete compositional
disclosure.
Ingredient / Component CAS No % by Wt
Activated Carbon (Coconut based) 7440-44-0 100
Material Safety Data Sheet Profile No 2
SECTION III – HAZARD(S) IDENTIFICATION
Emergency Overview: Black particulate solid, pellet or powder. Contact may cause eye irritation. Dust may be
slightly irritating to eyes and respiratory tract. Avoid generation of dust or fines during handling.
CAUTION: Wet activated carbon removes oxygen from air causing a severe hazard to workers in
enclosed or confined space. Before entering such an area, sampling and work procedures for low
oxygen levels should be taken to ensure ample oxygen availability, observing all local, state and federal regulations
OSHA Regulatory Status Not regulated
HMIS Ratings Health 0
(NFPA) Flammability 1
Reactivity 0
Special
4 = Extreme/Severe
3 = High/Serious
2 = Moderate
1 = Slight
0 = Minimum
W = Water Reactive
OX = Oxidizer
Protective Equipment Safety glasses with side shields or goggles, gloves, long sleeve shirt or lab coat, long pants
recommended.
Health Effects See Section IV
Environmental Effects See Section XII
SECTION IV – FIRST-AID MEASURES
Route of exposure
Eyes Dust may cause mild irritation, possibly reddening.
Skin Dust may cause mild irritation, possibly reddening.
Inhalation Dust may cause mild irritation to the upper respiratory tract.
Ingestion Dust may cause mild irritation to digestive track resulting in
nausea or diarrhea.
Signs/Symptoms of Exposure
Dust may cause irritation and redness of eyes, irritation of skin and respiratory system. The effects of long-term,
low-level exposures to this product have not been determined.
Emergency and First Aid
Procedures
For eye contact, immediately flush with copious amounts of water for at least 15 minutes, lifting both the upper
and lower lids occasionally; seek medical attention. For skin contact, wash with soap and water; seek medical
attention.
For inhalation, Remove to fresh air and rest as needed; seek medical attention for any breathing difficulty.
For ingestion, drink plenty of water; seek medical attention.
Medical Conditions Generally
Aggravated by Exposure
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People with pre-existing skin conditions or eye problems or impaired respiratory function may be more susceptible
to the potential effects of the dust.
Material Safety Data Sheet Profile No 2
SECTION V – FIRE FIGHTING MEASURES
Suitable Extinguishing Media Use an extinguishing media suitable for the surrounding fire
Unsuitable Extinguishing
Media None known
Specific Hazards
As with most organic solids, fire is possible at elevated temperatures or by contact with an ignition source.
Activated carbon is difficult to ignite and tends to burn slowly (smolder) without producing smoke or flame.
Carbon monoxide and carbon dioxide gas may be emitted upon combustion of
material. Contact with strong oxidizers such as ozone or liquid oxygen may cause rapid combustion.
Protective Equipment and
Procedures
Wear NIOSH approved self-contained breathing apparatus suitable for the surrounding fire.
SECTION VI – ACCIDENTAL RELEASE MEASURES
Personal Precautions Wear protective equipment, keep unnecessary personnel away,
ventilate area of spill
Environmental Precautions
The material is not soluble but can cause a particulate emission if discharged to waterways; therefore, dike all
entrances to sewers and drains to avoid introducing the material into the
waterways.
Containment & Clean-up
Dike all entrances to sewers and drains. Vacuum or shovel spilled material and place in closed container for
disposal. Remove product to appropriate storage area until it can be properly disposed of in accordance with local,
state and federal regulations. Avoid dust formation. See section XIII
Other information NA
SECTION VII – HANDLING AND STORAGE
Handling
Avoid prolonged contact with eyes and skin. Keep away from ignition sources. Use in
well ventilated areas. Protect containers from physical damage. Wash hands after
handling.
Storage Store in cool, dry, ventilated area and in closed containers. Keep away from oxidizers,
heat or flames. Store away from ignition sources.
SECTION VIII – EXPOSURE CONTROLS/PERSONAL PROTECTION
Component OSHA
PEL
ACGIH
TLV
Other limits
Activated Carbon 5 mg/M3 (Resp) 5 mg/M3 (Resp)
Exposure Guidelines
Wet activated carbon removes oxygen from air posing a hazard to workers in enclosed or confined space. Before
entering such an area, sample the air to assure sufficient oxygen supply. Use work procedures for low oxygen
levels, observing all local, stated and federal regulations.
Engineering Controls
No special ventilation requirements. Good general ventilation should be adequate for open areas. Mechanical
ventilation is recommended for enclosed or confined spaces
Personal Protective
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Equipment
Use of NIOSH approved particulate filter is recommended if dust is generated in handling. The usual precautionary
measures for handling chemicals should be followed, i.e. gloves, safety glasses w/side shields or goggles, long
sleeve shirt or lab coat, dust respirator if dusty. Other
protective clothing/equipment as appropriate.
General Hygiene
The usual precautionary measures for handling chemicals should be followed: i.e. Keep away from food and
beverage; remove contaminated clothing immediately; wash hands before breaks or eating; avoid contact with
eyes and skin.
SECTION IX – PHYSICAL AND CHEMICAL PROPERTIES
Boiling Point NA Melting Point NA
Vapor Pressure (mm Hg.) 0 Evaporation Rate NA
Vapor Density (AIR = 1) solid Flash Point NA
Specific Gravity 0.4 to 0.7 UEL NA
LEL NA
Flammability Limits Ignition Temperature > 220º C
Odor None
Solubility in Water Product is not soluble.
Appearance Black granular or powder material.
SECTION X – STABILITY AND REACTIVITY
UNSTABLE STABILITY STABLE XX
CONDITIONS TO AVOID:
None
HAZARDOUS MAY OCCUR
REACTION WILL NOT OCCUR XX
CONDITIONS TO AVOID:
None
Caution: High concentrations of organics in air will cause temperature rise due to heat of adsorption. At very high
concentration levels this may result in a thermal excursion, referred to as a bed fire. High concentrations of Ketones and
Aldehydes may cause a bed temperature rise due to adsorption and oxidation.
Incompatible Materials Alkali Metals and Strong Oxidizers such as ozone, oxygen,
permanganate, chlorine
Hazardous Decomposition
Products
Carbon monoxide and carbon dioxide gas may be generated during combustion of this material.
SECTION XI – TOXICOLOGICAL INFORMATION
Acute Effects
Oral LD50 Not determined on the finished product. Toxicity Studies Dermal LD50 Not determined on the finished
product.
Inhalation See section IV
Ingestion See section IV
Eye Irritation See section IV
Skin Irritation See section IV
Sensitization Not determined on the finished product.
Target Organ (s) or System Eyes, Skin and Upper Respiratory System
Signs and symptoms of
Exposure
Irritation and redness of eyes, irritation of skin and respiratory
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system may result from exposure to carbon dust
See Sections III and IV
Chronic Effects
Carcinogenicity Not Determined on the finished product.
Mutagenicity Not Determined on the finished product.
Reproductive Effects Not Determined on the finished product.
Developmental Factors Not Determined on the finished product.
SECTION XII – ECOLOGICAL INFORMATION
Ecotoxicity Not Determined on the finished product.
Persistence/degradability Not Determined on the finished product.
Bioaccumulation/Accumulation Not Determined on the finished product.
Mobility in Environmental Media Not Determined on the finished product.
Other Adverse Effects Not Determined on the finished product.
SECTION XIII – DISPOSAL CONSIDERATIONS
Vacuum or shovel material into a closed container. Storage and disposal should be in accordance
with applicable local, state and federal laws and regulations. Local regulations may be more stringent than state or
federal requirements. Consult with the US EPA Guidelines listed in 40 CFR Part 261.3 for the classifications of
hazardous waste prior to disposal
SECTION XIV – TRANSPORT INFORMATION
This information as presented below only applies to the material as shipped. The identification based on
characteristic(s) or listing may not apply if the material has been used or otherwise contaminated. It is the
responsibility of the waste generator to determine the toxicity and physical properties of the material generated
to determine the proper waste identification and disposal methods in compliance with applicable regulations.
DOT Regulations Proper Shipping
Description
COCO PLUS 4x10
(Steam Activated Carbon)
Land Canadian WHMIS Hazard Class NA See note below
UN/NA UN 1362
IMO / IMDG Proper Shipping
Description
COCO PLUS 4x10
(Steam Activated Carbon)
Water Hazard Class NA See note below
UN/NA UN 1362
IACO / IATA Proper Shipping
Description
COCO PLUS 4x10
(Steam Activated Carbon)
Hazard Class NA See note below
UN/NA UN 1362
Air
Information reported for product/size: 0.5 Kg
This product has been tested according to the United Nations Transport of Dangerous Goods test protocol for a
“self-heating substance”. It has been specifically determined that this product does not meet the definition of a
self-heating substance or any other hazard class, and therefore is not a hazardous material. Please note that this
information is applicable only for the Activated Carbon Product identified in this document.
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SECTION XV – REGULATORY INFORMATION
SARA Title III 302 Product is not subject to SARA Title III, section 302 regulation.
SARA Title III 313 Product is not subject to SARA Title III, section 313 regulation.
TSCA Product is listed
California Proposition 65 Product is not listed
WHMIS Product is listed. Canadian classification DSL # Product is listed.
EEC Council Directives relating to the classification, packaging, and labeling of dangerous substances and
preparations.
Risk and Safety Phrases
R36: Irritating to the eyes,
R37: Irritating to the respiratory system,
R38: Irritating to the skin,
SECTION XVI – OTHER INFORMATION
Intended Use The material is generally used for treatment of gases (and liquids)
The information contained in this document applies to this specific material as supplied. It may not be valid for this
material if it is used in combination with any other materials. It is the user’s responsibility to determine the
suitability and completeness of this information for their particular use. While the information and
recommendations set forth herein are believed to be accurate as of the date hereof, Calgon Carbon Corporation
makes no warranty with respect to same and disclaims all liability for reliance there on.
References:
NA not applicable
Legend:
ACGIH - American Conference of Governmental Industrial Hygienists
ANSI - American National Standards Institute
ATSDR - Agency for Toxic Substances and Disease Registry
Ceil - Ceiling (limit value)
CAS # - Chemical Abstracts Service Registry Number
CERCLA - Comprehensive Environmental Response, Compensation, and Liability Act
CEPA - Canadian Environmental Protection Act
CFR - Code of Federal Regulations
DOT - Department of Transportation
DSL - Domestic Substances List
EINECS - European Inventory of Existing Commercial Chemical Substances
ERAP - Emergency Response Assistance Plan
IATA - International Air Transportation Association
IARC - International Agency for Research on Cancer
ICAO - International Civil Aviation Organization
IDLH - Immediately Dangerous to Life and Health
IMO - International Maritime Organization
IMDG - International Maritime Dangerous Goods
LC50 - The concentration of material in air expected to kill 50% of a group of test animals
LD50 - Lethal Dose expected to kill 50% of a group of test animals
NFPA - National Fire Protection Association
NIOSH - National Institute for Occupational Safety and Health
NTP - National Toxicology Program
OSHA - Occupational Safety and Health Association
PEL - Permissible Exposure Limit
RCRA - Resource conservation and Recovery Act
RQ - Reportable Quantity
SARA - Superfund Amendments and Reauthorization Act
STEL - Short Term Exposure Limit
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TDG - Transportation of Dangerous Goods Act/Regulation
TLV - Threshold Limit Value
TSCA - Toxic Substances Control Act
TWA - Time Weighted Average
WHMIS - Workplace Hazardous Material Information System
* * * END OF MATERIAL SAFETY DATA SHEET * * *
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