Importance of testing for vacuum ejectors in refinery service Efforts should be made to identify and avoid errors in the specification, engineering, and manufacturing of vacuum system equipment before they manifest at start-up V acuum systems are critically important to the performance of refinery crude vacuum distillation units. Vacuum tower flash zone pressure is a result of vacuum system suction pressure plus pressure drop through the overhead vapour line and column internals. To maximise recovery of gasoil from vacuum residue, the flash zone should operate at the lowest possible pressure without exceeding tower capacity. Unfortunately, many vacuum towers operate above their design or expected pressure, resulting in lower vacuum gasoil yields and reduced profitability. Many papers and articles in the technical literature discuss the performance and troubleshooting of vacuum ejector systems in refinery service.1,2. This article focuses on the importance of shop testing vacuum ejectors to ensure they meet their design parameters of pressure versus capacity and consequently prevent significant economic losses that can result from their underperformance. An additional benefit is the ejector performance curves derived from actual testing are paramount to any future troubleshooting, optimisation, and revamping of vacuum systems in operating units. Crude unit vacuum systems Multi-stage steam jet vacuum ejector systems are almost universally used to produce vacuum in refinery crude distillation units. They are particularly well suited to the large vapour volumetric rates present and high compression ratios normally required. The systems are arranged in two to four stages, with each stage consisting of an ejector www.digitalrefining.com Vacuum resid yeild (LV% on crude) EDWARD HARTMAN and TONY BARLETTA Process Consulting Services, Inc. LAURENT SOLLIEC and PETER TREFZER GEA Wiegand GmbH 40% 39% 38% 37% 36% 35% 34% 33% 32% Unit 1 31% 30% 20 22 24 26 28 30 32 34 Flash zone pressure, mmHg absolute Unit 2 36 38 40 Figure 1 Flash zone pressure impact on vacuum residue yield and discharge surface condenser. Depending on unit capacity and desired flexibility, each stage may have ejectors or surface condensers in parallel. Steam works as the motive fluid providing the energy for compression. Load to each stage consists of non-condensable gas, condensable hydrocarbons vapour, and water vapour. Surface condensers minimise the quantity of condensable vapours and cool the non-condensable gas mixture flowing to the next ejector stage and leaving the system. This reduction in load results in smaller ejector size in the intermediate and final stages, as well as lower overall energy usage. Discussed in further detail under vacuum ejector fundamentals, ejector suction pressure is a function of its load and performance curve, as long as its discharge pressure is below its maximum discharge pressure (MDP). In a multi-stage crude vacuum unit system, overall suction pressure is a function of vapour overhead load from the vac- uum tower and first-stage ejector performance curve. This holds true provided the first-stage condenser, as well as ejectors, condensers, and interconnecting piping in subsequent stages do not cause the first-stage MDP to be exceeded. In some cases, high vacuum system suction pressure, and consequently high tower pressure, is caused by process loads pushing the ejectors out on their curves. However, Process Consulting Services (PCS) has encountered several instances of ejector design errors leading to tower pressures up to 10 mmHgA above design right from start-up. When vacuum system fails to deliver from day one, system performance can further degrade rapidly with normal exchanger fouling and the initial 10 mmHgA miss can increase to 20 mmHgA or more above design suction pressure. The impact of flash zone pressure on refinery profitability is magnified in units processing heavy crudes. Figure 1 shows vacuum res- PTQ Q2 2022 01 Motive nozzle Diffuser throat Diffuser Discharge Motive steam Pd m=mm + ms Pm, m m Suction chamber Ps, m s Suction load P = Absolute pressure m = Mass flow rate Figure 2 Steam jet vacuum ejector diagram Suction pressure (mmHg absolute) idue yields for two different vacuum columns over a range of flash zone pressures. Unit 1 runs a blend of heavy Canadian crudes, while Unit 2 processes a blend of heavy Venezuelan and light US crudes. As pressure increases from 20 to 40 mmHgA, Unit 1 residue yield increases by about 3 LV% on crude and Unit 2 residue yield increases by about 4 LV% on crude. For a crude capacity of 100 MBpd, this corresponds to 3 and 4 MBpd of incremental vacuum residue, respectively. Considering a vacuum gasoil to residue downgrade penalty of $15/Bbl, the higher flash zone pressure results in profit losses of $16MM/yr and $21MM/yr. Troubleshooting and diagnosis of crude vacuum systems underperformance can be difficult and time consuming. The process of determining ejector loads in an operating unit is full of uncertainties. It requires good field data, laboratory analysis, and flow measurements that are often unavailable. Furthermore, it relies heavily on process simulation models that are only as good as the simulation inputs. For units that have been in operation for more than 19 18 17 16 15 14 13 12 11 10 9 8 7 6 5 4 3 2000 3000 4000 5000 6000 7000 8000 a few months, additional uncertainties can further complicate efforts to narrow the root cause(s) of high vacuum column operating pressure. These include, but are not limited to, condenser fouling, ejector motive steam nozzle erosion, and tower internals damage that increases system load. Therefore, every effort should be made to identify and avoid errors in the specification, engineering, and manufacturing of vacuum system equipment before they manifest themselves at start-up. In vacuum surface condensers, undersized shell nozzles, over-optimistic heat transfer coefficients, and vapour internal bypass are common problems. In vacuum ejectors, motive steam nozzle size and position are common culprits. In addition to generating accurate performance curves, shop testing vacuum ejectors provides a unique and valuable opportunity to prevent such problems. Steam jet vacuum ejector fundamentals Steam jet vacuum ejectors are essentially compressors with no moving parts. Figure 2 is a diagram of a 9000 10000 11000 12000 13000 14000 15000 Equivalent water vapour load @ 70˚F (lb/hr) Figure 3 Suction pressure vs load performance curve 02 PTQ Q2 2022 steam jet vacuum ejector that establishes nomenclature and symbology used throughout this article. The basic operating principle of a steam jet ejector is momentum transfer. The motive nozzle converts steam pressure energy into velocity energy, resulting in a supersonic velocity jet of steam that entrains the vapour and gas mixture from the suction chamber. The resulting mixture of motive steam and suction load enters the diffuser where velocity energy is converted back to pressure. At the diffuser throat, a pressure discontinuity or shock wave occurs which is responsible for an important property of steam jet ejectors – suction pressure is independent of discharge pressure up to a certain limit, and is only influenced by the amount of suction load. Figure 3 presents the performance curve of a large first-stage ejector, showing the relationship between suction pressure and load. As mentioned above, suction pressure is independent of discharge pressure only up to a certain point. When discharge pressure becomes too high, the shock wave in the ejector throat can become unstable, leading to ‘broken’ ejector operation that produces high and sometimes fluctuating suction pressure. When an ejector is operating in a broken state, the suction pressure is unpredictable and depends on both suction load and discharge pressure. The discharge pressure that breaks the ejector is known as maximum discharge pressure, or MDP. MDP is commonly represented as a single number for a given ejector, but it actually varies with suction load. Figure 4 shows a combined plot of suction pressure and MDP curves versus suction load for an actual first-stage ejector. Note that the axes on this figure are reversed from the typical pressure versus load capacity curve, with X-axis indicating pressure and Y-axis representing load. This arrangement makes it easier to combine the individual capacity curves of a multi-stage system in the same plot. Although ejectors can handle a wide variety of suction gasses with varying temperature and molecular weight, ejector curves and ejector www.digitalrefining.com Equivalent water vapour load @ 300˚F (lb/hr) 15000 14000 13000 12000 11000 10000 9000 8000 7000 6000 5000 4000 3000 2000 1000 0 make up those ratios and with the proper correction factors. Test stand setup and limitations Suction 0 10 20 30 40 MDP 50 60 70 80 90 100 110 120 Pressure (mmHg absolute) Figure 4 Suction pressure and MDP vs load performance curves testing are based on the principle of equivalent load. Any combination of suction vapours can be converted to equivalent water vapour (EWV) or dry air equivalent (DAE) load by simple corrections for molecular weight and temperature. Using equivalent load makes it easy to convert and plot any given suction load onto the equivalent load curve to check performance. Equivalent load can also be represented at different reference temperatures. This process is described in detail in industry standards.3,4 All loads discussed herewith are on an EWV basis. Entrainment ratio: . ω = mm . ms Ejectors are scalable devices in terms of both physical size and non-dimensional parameters. Similitude laws allow ejectors to be scaled by applying appropriate ratios to all critical geometric parameters, including throat area, motive steam nozzle throat area, and motive steam nozzle distance to throat, among others. A family of ejectors sharing identical geometric ratios also shares all combinations of Cr, Er, and ω. The entrainment ratio ω is not exactly constant because it is affected by friction through the throat – an ejector with a larger throat always performs better than a similar scaled down ejector with a smaller throat. Therefore, for a defined ejector geometry, testing at any set of fixed Cr, Er, and ω is valid, regardless of the absolute values that Ejector similitude and scaling Ejectors are commonly defined by the following three non-dimensional parameters: Compression ratio: Cr = Pd PS Expansion ratio: Er = Pm Ps Liquid ring vacuum pump or atmosphere TI Motive steam Air Superheater (optional) Separator Condensate drain Load steam TI Direct contact condenser PI HEI nozzle Separator Condensate drain Figure 5 Test stand configuration 03 PTQ Q2 2022 Cooling water supply PI PI Cooling water return Previously referenced industry standards cover many testing related topics in detail. The standards are written to cover testing of ejectors for a wide range of services. Ejectors designed for refinery vacuum systems normally bring additional challenges due to size and utilities consumption. Their testing should include a range of suction loads, with suction pressure and MDP recorded at each load point. Although formal testing guidelines allow testing only three points, adding additional test points is trivial after going through the effort of setting up the ejector on the test stand. Depending on unit process design and modes of operation, it may also be advisable to check unusual loads corresponding to expected process swings. Ejectors that may operate during periods of very low load should be tested all the way down to zero load to ensure suction pressure stability. In addition, the zero-load suction and discharge pressures are essential at start-up of the vacuum column for comparison with in-situ measurements. Refinery ejectors are typically tested with steam as load rather than air. Figure 5 shows a representative test stand setup. This test setup allows for control of motive steam pressure, suction load, and ejector discharge pressure. Motive steam is let down to the test pressure through a pressure control valve. If the vacuum system design conditions specify superheated motive steam, then superheat may be added by an electric superheater or motive steam pressure can be adjusted to account for the lack of superheat.4 Suction load is metered by adjusting steam pressure upstream of a Heat Exchange Institute (HEI) nozzle under critical flow. Ejector discharge is routed to a direct contact condenser where motive and load steam are condensed by mixing with cooling water. Condenser pressure is maintained by a downstream vacuum producing equipment (liquid ring vacuum pump) and it can be adjusted by an air intake control valve. www.digitalrefining.com Equation 1 can be used for motive steam flow calculations, as well as suction load flow calculations using steam through an HEI nozzle under critical flow. The unit conversion factor U (see Table 1) combines the nozzle flow coefficient and discharge function at supercritical flow: Values of unit conversion factor U Unit conversion factor U 867.9 0.5804 ṁ lb/hr kg/hr Manufacturer’s test stands are limited in physical size, steam boiler capacity, steam pressure, and cooling water heat removal capability. Given size limitations, most large first-stage ejectors and many larger second-stage ejectors do not physically fit in the existing test facilities. Additionally, large ejectors that consume thousands of pounds per hour of motive steam or ejectors designed for high pressure motive steam may exceed test stand capabilities. The ability to add superheat to the motive steam can also pose a challenge. Therefore, test methods based on model ejectors, scaled process conditions or a combination thereof may be required. General guidance is to use the simplest test possible, while resorting to rigorous scaling factors and accurate empirical correction factors when needed. A. Direct test Testing is most straightforward for small ejectors that fit on the test stand and require motive and load steam that are within steam generation capacity both in terms of flow rate and pressure. In these cases, motive steam is set at design, and the measured suction pressures, discharge pressures, and equivalent loads can be plotted directly on the final ejector curves without any correction factors. Due to its simplicity, direct test is the preferred method whenever possible. B. Scale test For ejectors that physically fit on the test stand but that require more motive steam flow or higher motive steam pressure than available, the actual ejector can be tested by scaling the process conditions. Scaled test results are then translated to the final ejector curves by using Cr, Er, www.digitalrefining.com P psia bar ρ lb/ft3 Kg/m3 Note: P and ρ are for the motive steam upstream of the nozzle. Table 1 m.steam,critical =U * Dn2 * √P * ρ [1] Testing methods Dn in mm and ω non-dimensional parameters. C. Superheated or saturated steam test Ejector performance is based on mass flow. For typical refinery levels of superheat (100-300°F), the extra energy due to superheat generally has a negligible impact on ejector performance. However, superheat is important because of its effect on motive steam density, which changes the mass flow of steam through the critical flow motive nozzle. Steam with more superheat has lower density, so, for the same pressure, mass flow of superheated steam through a fixed orifice is less than it would be for saturated steam. In terms of testing an ejector designed for superheated steam, options are: If the test stand can supply superheated steam For direct and model testing, superheat the steam to achieve the exact motive steam design pressure and temperature. For scale testing, superheat the steam such that both expansion ratio Er and steam mass flow rate scale correctly. The ratio of superheated steam density to saturated steam density should be the same in both cases. If the test stand cannot supply superheated steam For model testing, the model’s motive steam nozzle throat area can be reduced to account for the higher density of the saturated steam used on the test stand. For direct or scale testing, motive steam pressure can be adjusted to get the correct motive mass flow. Superheated steam has a lower density than saturated steam of the same pressure, so density can be matched by lowering test steam pressure until motive flow rate at the lower pressure matches the superheated motive flow rate at design pressure. This calculation is straightforward with steam tables and Equation 1. Adjusting steam pressure to account for superheat impacts the expansion ratio Er, such that the test points Cr, Er, and ω are no longer equal to those for the ejector curve points. Correcting the test point for the difference in Er requires adjusting the entrainment ratio ω by an empirical factor which, similarly to the efficiency factor, is also based on manufacturer’s experience. D. Model test Ejectors are scalable devices, so performance of a geometrically scaled ejector can be accurately ratioed up to predict performance of the fullsize ejector. For large ejectors, it is common practice for the manufacturer to use a scaled model of the actual jet to optimise steam nozzle position and complete the factory performance tests. Ejector efficiency is significantly impacted by wall friction inside the jet. As ejector size increases, ejector throat area increases more quickly than wall surface area, so that larger ejectors are more efficient because less energy is lost to wall friction. Therefore, performance of a fullsize ejector always exceeds that of a smaller scaled version of the same ejector. In terms of ejector testing and certification, this efficiency difference can be accounted for by an empirical efficiency factor to produce accurate ejector capacity curves, or the curves can be used as tested and the increased efficiency thought of as ‘bonus’ or ‘safety margin’. The technique explained in testing method B (scaling of the process conditions) can also be applied to a model ejector if required by the test stand capabilities. Crude vacuum unit ejectors testing A revamp designed by PCS of a major US Gulf Coast crude vacuum unit illustrates the application of the PTQ Q2 2022 04 1st stage model test results and translation to full-size ejector Model test results Pm,test Ps,test Pd,test psia mmHgA mmHgA 194.4 11.1 90.0 m·s,test lb/hr 89 m·s lb/hr 9,634 Full-size ejector results Pm Ps Pd psia mmHgA mmHgA 194.4 11.1 90.0 Table 2 3rd stage ejector scaled test results and translation to design conditions m·s,test lb/hr 325 Scaled test results Pm,test Ps,test Pd,test m·s psia mmHgA mmHgA lb/hr 28.7 27.8 123.8 1,408 Design test results Pm Ps psia mmHgA 128.8 111.0 Pd mmHgA 495.0 Table 3 testing methods. Unit charge consists of atmospheric residue from a blend of heavy Venezuelan and light US crudes. In order to maximise refinery profitability, one of the main revamp objectives is to improve heavy vacuum gasoil (HVGO) cutpoint to over 1050°F, thus minimising vacuum residue yield. Therefore, required vacuum unit design conditions are stringent: heater outlet temperature in the 780°F range, stripping steam rate in excess of 8.0 lb/bl of residue and 30 mmHgA vacuum tower flash zone pressure. The fourstage existing vacuum system was revamped with all new ejectors, as well as new first- and second-stage intercondensers. 1st stage ejectors – model test with adjustment for steam superheat The first-stage ejectors cannot be directly tested due to their sheer size, requiring a model test. The model ejector is scaled down based on the similitude laws, resulting in a scale factor of 100 to 1 ratio. As previously mentioned, the model ejector is less efficient than the actual ejector due to wall friction effects. This efficiency difference is accounted for on the translation of each test point to the full-sized ejector curves by an empirical factor. Although the friction correction factor is correlated to Reynolds number, in practice GEA relies on an extensive database of test results, compiled over decades, to determine this empirical factor. Design motive steam conditions include superheat, which cannot be delivered on the test stand. 05 PTQ Q2 2022 Therefore, the model ejector is fitted with a motive nozzle throat area sized to account for the higher density of the saturated steam used on the test stand, such that the correct motive steam mass rate is delivered. Test results from one of the measuring points and its respective translation to the full-sized ejector is exemplified in Table 2. 3rd stage ejectors – scale test with adjustment for steam superheat The third-stage ejectors physically fit in the test stand but their motive steam rate exceeds test stand capacity. Therefore, a scale test is performed with a scale factor of 4 to 1 ratio. Again, the design motive steam conditions include superheat, which cannot be delivered on the test stand. In order to achieve the same motive steam mass rate through the motive nozzle, a superheat temperature correction factor calculated from steam properties is applied to the motive pressure in conjunction with the scale factor. As previously mentioned, adjusting steam pressure to account for superheat results in a different expansion ratio Er between design and test conditions, while the compression ratio Cr remains constant. Therefore, the entrainment ratio ω is adjusted by an empirical factor based on GEA’s experience. Test results from one of the third- stage test measuring points and its respective translation to the design conditions is exemplified in Table 3. All ejector elements in this system were tested by one of the methods illustrated above. This acceptance testing allowed GEA to demonstrate the expected design performance of each ejector, as well as to generate accurate suction and MDP performance curves. Overall vacuum system performance and its impact on post-revamp unit operations will be discussed in a future article. Conclusion Acceptance or shop testing of vacuum ejectors is used to generate an accurate set of ejector performance curves. More importantly, it provides an opportunity to prevent ejector underperformance by identifying and correcting design or manufacturing errors. Given the significant profit loss that can result from a ‘broken’ ejector in a crude vacuum distillation unit, shop testing of new ejectors should be mandatory. This is not a topic to cut corners on cost. References 1 Lieberman N, Cardoso R, Troubleshoot operation of a steam ejector vacuum system, Hydrocarbon Processing, Feb 2016, 59-64. 2 Cantley G, et al, Maximise VGO yield, PTQ Revamps & Operations, 2005, 22-25. 3 Heat Exchange Institute, Inc., Standards for Steam Jet Vacuum Systems. 4 German Standard DIN 28 430, Rules for the Measurement of Steam Jet Vacuum Pumps and Steam Jet Compressors. Edward Hartman is a process engineer with Process Consulting Services Inc, in Houston, TX, USA. He has 35 years of experience in studies and design packages of refinery units, specialising in distillation equipment design. Tony Barletta is Vice President with Process Consulting Services. Inc. He has over 34 years of experience with refinery revamps and process design for heavy oil units. Laurent Solliec is an R&D Manager at GEA Wiegand GmbH, Germany. He specialises in customer oriented solutions and ejector technology, and heads the test bench facility. He holds a PhD in fluid dynamics engineering. Peter Trefzer is Product Manager for vacuum systems and ejectors at GEA Wiegand. He specialises in multi-stage ejector applications and holds a degree in mechanical engineering. LINKS More articles from: Process Consulting Services More articles from the following categories: Crude and Vacuum Units www.digitalrefining.com