13 Joining processes for powder metallurgy parts C. S e l c u k, Brunel Innovation Centre, UK DOI: 10.1533/9780857098900.3.380 Abstract: Powder metallurgy (PM) processes are ideal for rapid production of near net shape parts with complex geometries from a range of materials that would often not be possible to combine otherwise. Certain alloy combinations, chemical compositions in powder form are more favourable for synthesis of materials. This allows PM to be extremely versatile, maximising material utilisation. The net shape capability directly reduces or eliminates secondary operations like machining. Despite this obvious advantage of PM processes, joining materials synthesised from powders has been associated with difficulties related to their inherent characteristics, like porosity, contamination and inclusions, at levels which tend to influence the properties of a welded joint. This chapter presents an overview of joining PM components. It seeks to identify preferred joining processes and identify apparent technology gaps, with an emphasis on offering solutions to welding problems. It also highlights developing approaches. Key words: joining, near net-shape processing, powder metallurgy, welding. 13.1 Introduction In PM materials processing techniques, all or some constituents of a part are employed in particulate form with certain characteristics of composition, morphology and size, compacted into a high precision product (Figs 13.1 and 13.2). The ability of PM to produce high quality, complex parts with close tolerances and high productivity presents significant advantages, such as energy efficiency, with potentially low capital costs. PM is widely used for a range of applications, such as dental restorations, implants, bearings and automotive transmission parts, from biomedical to automotive industry sectors. PM components are becoming increasingly attractive as substitutes for wrought and cast materials in various applications. However, it is possible to increase further the use of PM by exploiting the ability to manufacture complex geometrical configuration by joining PM parts to one another or to other cast/wrought products. The main issues restricting the welding of PM parts have been porosity, impurities and the fact that some PM parts have a high carbon content. Of these, the most important characteristic of a 380 © Woodhead Publishing Limited, 2013 Joining processes for powder metallurgy parts 381 Design & development Product Particulate composition Secondary processing Joining Machining Heat treatment Green/ sintered part Particulate size Particulate shape 13.1 Important factors to consider in development of PM products. Joining is an enabling step. High quality Construction & engineering tooling bearings Automotive transmission parts, gears medical dental restoration, impants Mining Oil & gas exploration Power Renewables Generators Magnets Electronics Aerospace Defence Household Sports PM Energy efficiency Part complexity (Joining) High productivity 13.2 Ability of PM to create complex geometries for industry with the help of joining. PM part for welding has been porosity, created either deliberately to make a porous part or incidentally due to insufficient densification. Powder particle characteristics (such as particle shape, size and surface area) determine the porosity or relative density of a powder compact, which in turn influences several important physical properties of the preform, such as thermal conductivity and hence hardenability, as well as thermal expansion. It has © Woodhead Publishing Limited, 2013 382 Advances in powder metallurgy been noted that porosity can also act as a trap for impurities/inclusions that could potentially have an impact on secondary operations such as welding when entrapped impurities in the pores could be deleterious to the weldability of the PM part, for example by encouraging solidification cracking. PM parts have been reported to be susceptible to cracking in the heat affected zone when welded, owing to the porosity of the preform and limited area of interparticle bonding giving low ductility adjacent to the joint. Hence these locations may be unable to resist the thermal stresses generated as a result of contraction in a fusion weld. In addition, welding is commonly associated with resultant distortion, whereas PM parts are known to provide good dimensional and geometrical accuracy and thus, if machining operations are to be avoided, distortion must be minimised via selection of appropriate joining technology. Therefore, widespread success in welding PM parts requires understanding of the influence of porosity, chemical composition, impurity level and overall cleanliness, upon weldment properties such as weld metal and heat affected zone (HAZ) cracking, ductility and toughness, residual stresses and distortion. These issues are addressed in this review. 13.2 Welding processes for powder metallurgy parts 13.2.1 Introduction Joining processes applicable for PM parts can be categorised as solid state and liquid state. The solid state processes such as diffusion bonding and brazing have been predominantly used for lower density porous parts. In comparison, parts with higher densities or minimal porosity are typically treated as fully dense wrought materials, and these are typically welded using fusion-based joining processes, including arc welding, that is gas tungsten arc (GTA), gas metal arc (GMA), electron beam (EB) and laser welding. Further joining techniques such as adhesive bonding and shrink fitting may be used for some applications but are not considered here. 13.2.2 Arc welding Arc welding of PM parts may give porosity with an associated detrimental influence on the weld integrity.1 Gas metal arc (GMA) welding of powder compacts, which are not fully dense, can result in porous welds and weld toe cracking, the latter presumably resulting from low ductility of the original PM part. The density of a PM part and its composition are expected to affect the tendency for porosity during welding.2,3 Welding of ferrous PM parts can form a soft pearlitic microstructure as a result of slow cooling, caused by porosity reducing the thermal conductivity, © Woodhead Publishing Limited, 2013 Joining processes for powder metallurgy parts 383 which can allow strains to be accommodated that would otherwise give rise to cracking. An additional benefit of the porous structure is that hydrogen can diffuse out of the metal into and through the interconnected pores, hence reducing susceptibility to fabrication hydrogen cracking. Sintered steels are thus considered to be more resistant than wrought steels. It is also worth mentioning that, when subjecting ferrous PM parts to steam treatment (heating the parts to a temperature in the region of 550°C and exposing them to water vapour) which is a common secondary process in production environment, a thin layer of Fe3O4 is formed both on the outer surface and on the surfaces of the interconnected porosity. This treatment is for improved corrosion resistance, increased surface hardness, compressive strength and wear resistance. This or a similar post sintering heat treatment of ferrous sintered parts will, however, prevent satisfactory welding. The problem is due to a resulting oxide film, which is slightly porous, probably containing moisture and has an insulating effect and hence is potentially a source of weld metal porosity and a potential cause of cracking in weldments. Arc welding (gas tungsten arc welding, GTAW, and gas metal arc welding, GMAW) has also been attempted for non-ferrous metal matrix composite (MMC) systems, for example, SiC particle-reinforced aluminium. Gross porosity and delaminations in both weld metal and HAZ were reported to be frequent. It was claimed that despite large volumes of particulates in the Al alloy matrix, a wide range of MMCs can be fusion welded, with weldability similar to Al.4 However, particulate characteristics (shape, size and distribution) of reinforcement, their proportion within the matrix, along with the homogeneity of the material and chemistry are critical for welding. Any interfacial reactions between the reinforcement and matrix that may result in the presence of secondary compounds or flux derivatives can influence the weldability and its success. Filler metal compositions, with respect to inclusions such as oxides and impurity contents (e.g. silicon and phosphorous levels in notably ferrous parts), can change the output of welding by influencing the microstructures attainable, especially in the heat affected regions. This can manifest itself in formation of low melting point eutectic phases at grain boundaries owing to segregation of impurities which can lead to solidification cracks in the heat affected zone (HAZ). Porosity distribution across the weld metal, HAZ and parent metal will affect the strength of the joint. PM components have the potential to replace their wrought counterparts in several applications owing to the advantages of net shape capability, low cost of production and high added value in terms of performance (e.g. strength, wear and fatigue). However, this can only be fully achieved if they can be confidently joined to other components especially with respect to design and structural considerations. Weldability of PM parts is therefore crucial to establish when it comes to widening the horizons for PM and future applications. © Woodhead Publishing Limited, 2013 384 Advances in powder metallurgy Consumable electrode Flux covering Weld metal Core wire Evolved gas shield Slag Arc Weld pool Parent metal (a) Gas nozzle Filler rod Non-consumable tungsten electrode Gas shield Arc Weld pool Parent metal Weld metal (b) 13.3 Schematic representations of manual metal arc: (a) gas–metal arc GMAW welding and (b) tungsten–inert gas gas–tungsten arcGTAW welding (courtesy of TWI Ltd). 13.2.3 Laser welding There are advantages of laser welding for PM parts, as it is a highly automated process, offering precision and control (Fig. 13.4). Welding speeds of several © Woodhead Publishing Limited, 2013 Joining processes for powder metallurgy parts 385 Key bole (a) (b) 13.4 Representation of key hole laser welding and a typical weld (courtesy of TWI Ltd). metres per minute are possible, with a low heat input, resulting in a small HAZ and limited thermal distortion and residual stress.5 However, various defects, such as blowholes that are probably due to entrapment of gases that cannot leave the melt during rapid solidification, were observed in laser welding of sintered steel parts in general, together with the occurrence of hydrogen cracking of medium carbon parts, cold, and hot cracking which have been observed in laser welding of sintered steel parts.6 It was recommended by one author that a filler wire could be used to prevent all of these types of defect, although filler wire addition is an extra complication in laser welding. Low C-steels (typically up to 0.3% C) can be satisfactorily laser welded and it has been reported that a sintered steel part can be acceptably laser welded to a wrought counterpart, as long as both components have low carbon content.7 However, laser welding of medium C‑steels (typically 0.3–0.6% C) appears to be difficult, owing to the formation of a hard, brittle and hydrogen crack sensitive martensitic structure in the joint, caused by rapid cooling. Pre-heating may help by inducing a softer bainitic microstructure with some fine pearlite, which will increase toughness and hence improve the defect tolerance of the joint and reduce sensitivity to hydrogen cracking. Gas carburised and oil quenched steels are considered to be difficult to weld, because of significant blowhole formation, probably due to entrapped oil and gas in the pores. Elsewhere, it was noted that smooth, discontinuityfree welds can be produced at slower travel speeds and lower beam powers.8 It was also reported that a beam weaving laser welding technique would suppress porosity and that an increased width to depth ratio of the molten metal was beneficial for the escape of bubbles in the weld zone.9 © Woodhead Publishing Limited, 2013 386 Advances in powder metallurgy Laser welding of sintered austenitic stainless steel (grade 316L) was reported to be very easy, resulting in good joints.7 In trials with sintered Al alloys, it proved difficult to obtain a sound joint because of porosity formation, resulting in spongy welds.7 It is thought that oxidation was the probable cause, possibly creating locally overheated spots when more laser energy is absorbed by the oxides than the metal; another possibility is that the oxide absorbs moisture and this is released during welding. 13.2.4 Electron beam (EB) welding EB welding is normally carried out in high vacuum (e.g. 10–6 mbar). Therefore it is a batch process and may be expensive and thus restricted to high value parts only. It has a tendency to give high cooling rates and high hardness in C-steels, similar to laser welding, but is likely to have a greater tendency towards pore formation as the vacuum encourages trapped gas to try to escape during welding. It is reported that porosity increased with reduced travel speed. However, it has been demonstrated that weld metal porosity content in sintered ferrous compacts with a range of porosities can be controlled by beam parameters10 and a non-vacuum EB welding process has been used for sintered parts.11 Any residual films, such as heat treatment quench oil trapped in the pores of a PM part, were found to have a detrimental effect on EB welding.12 A fine grain size (< ASTM 8–9) in a sintered PM part was reported to be essential for good EB weldability, presumably due to improved ductility, in high temperature PM superalloys.13 This is related to increased ductility and toughness of a fine grained material for absorbing strains upon solidification. Cracking has been observed in EB welding of PM superalloys designed for aerospace applications (engine components such as turbine discs) which required further investigation.14 However, despite the problems described above, EB welding has the ability to give low distortion, again similar to laser welding, or at least uniform distortion effects, which is important for preserving the dimensional stability of near net shape PM components (Fig. 13.5). 13.2.5 Resistance projection welding Projection welding is one of the most widely applied welding processes for sintered PM parts. A significant aspect of projection welding is the limited distortion associated with it, which is certainly advantageous in terms of geometrical stability. However, one potential difficulty for the success of projection welding is the cleanliness of the parts or presence of surface films that can inhibit bonding. This can manifest itself in the likely presence of an oxide layer on some parts, for example ones subjected to steam treatment, © Woodhead Publishing Limited, 2013 Joining processes for powder metallurgy parts 387 Vacuum pumping Workspace pressure ~10–2 – 10–4 mbar (a) 10 mm (b) 13.5 Example of (a) EB welding configuration with reduced pressure and (b) reduced pressure EB welds in C-Mn steel (courtesy of TWI Ltd). typically on ferrous sintered parts. Such a layer could prevent satisfactory welding through an insulation effect at the interface and as a potential source of moisture and hence porosity.15,16 It is therefore recommended that any steam treatment on PM parts, as described earlier, should be done after welding. It has been possible to weld high carbon PM steels and case hardened parts using resistance projection welding.17 Light alloys have also been projection welded and the combined effect of pressure and temperature at the joint can, in fact, help to densify the region by closing the pores. This can help improve the strength of the weld region. The process enables PM parts to © Woodhead Publishing Limited, 2013 Advances in powder metallurgy 388 be joined to wrought materials and therefore allows a degree of flexibility in creating complex geometries and dissimilar joints (Fig. 13.6). 13.2.6 Friction welding Friction welding is a solid phase joining process, mainly used for wrought products (e.g. light alloys of Al and Ti) in a range of geometries such as extrusions (Fig. 13.7). Particular advantages are the absence of flux, filler or need for a protective atmosphere, which makes the process extremely attractive.15 The friction welding process is highly suitable for welding PM parts as it enables pore closure, which can potentially lead to a pore-free weld interface and a refined microstructure. This is particularly valid for Al-based PM parts and MMCs.18 An additional advantage of friction welding for Al alloy PM components, is that it is useful in breaking down any oxide layer deposited on the particles by intense deformation within the weld region. This in turn results in exfoliation of oxide and its rejection from the joint. As a consequence, a clear bond line is achieved and often the bond homogeneity and strength is improved. One potential disadvantage of friction welding may be associated with the change in microstructure caused by reorientation and deformation of sintered metal grains, which may create a potential weak region in the joint, thereby reducing fatigue performance.16 Since its invention in the early 1990s at TWI in the UK, friction stir welding (FSW), which is a variant of friction welding, has come a long way and it is widely applied in various industry sectors notably transport and aerospace. Al has been a good material to demonstrate the applicability of process in its fully industrialised form. The tooling and agility of the process have been critical for complex parts and relatively difficult to weld materials. FSW presents a good opportunity for PM materials, not only for joining but also for creating MMCs in bulk or on the surface. The process can be utilised to combine what would otherwise be difficult to co-exist alloy systems. This is partly due to the fact that it is a solid state process like PM. Projection Sheet (a) (b) (c) 13.6 Projection welding configurations: (a) embossed projection section, (b) stud to plate, (c) annular projection, and an example microstructure from a typical weld (courtesy of TWI Ltd). © Woodhead Publishing Limited, 2013 Joining processes for powder metallurgy parts 389 (a) Load Motion (b) Sufficient downward force to maintain registered contact Advancing side of weld Joint Leading edge of the rotating tool Shoulder Probe Trailing edge of the rotating tool Retreating side of weld (c) 13.7 Examples of friction welding: (a) rotary, (b) linear, (c) friction stir configurations, and typical weld macrograph and microstructure in Ti alloy forging, shown in (d) and (e) respectively (images courtesy of TWI Ltd). © Woodhead Publishing Limited, 2013 390 Advances in powder metallurgy 10 mm (d) 100 µm (e) 13.7 Continued 13.3 Other joining processes for powder metallurgy parts 13.3.1 Brazing In brazing, the porosity of the PM part can, in fact, draw away the brazing alloy from the joint region. This can leave insufficient material for bonding. To overcome this problem, techniques have been developed where brazing is integrated in the sintering process.19,20 Another potential issue which is encountered commonly in brazing is the presence of secondary products, for example due to flux reactions which would stop further infiltration by blocking the pores. Factors that can affect the brazed joint in terms of strength are surface condition of the particles (as is the case for other techniques) and the part’s surface roughness;21 their influence can be significant. There are new brazing techniques, such as laser brazing, and new brazing alloys being developed for joining sintered components in large volume.22 Brazed assemblies can typically consist of PM to PM or PM to wrought or cast © Woodhead Publishing Limited, 2013 Joining processes for powder metallurgy parts 391 structures, which can end up as a functionally graded material. Brazing, however has been selected as a joining method for hot isostatically pressed (HIP) parts. 13.3.2 Diffusion bonding Diffusion bonding is typically utilised for ferrous parts which are fairly small in size. Hence, part geometry can be a concern. To avoid this complication, sintering and diffusion bonding can potentially be carried out in the same furnace. A eutectic reaction is often employed to provide a transient liquid phase for bonding at the interface.23 The presence of resulting reaction products such as oxide compounds may reduce the bond strength.24 To induce high bond strength diffusion can be activated via the addition of suitable elements, such as Cu in, for example, ferrous PM parts.25 When compared with other joining techniques, rather low strength joints can be expected from diffusion bonding, which may be limited to certain geometries and alloy compositions. Diffusion bonding has been a choice when handling more exotic compositions where the chemistry of the part plays a significant role in the joining process and its feasibility. Hence, applications have been focused on light materials such as Ti alloys, MMCs and special products. More conventional C–Mn steels have not been commonly diffusion bonded. Although an attractive option, the success of the bond strength gained by this joining technique critically depends on compositions and hence phase transformations and may require protective atmospheres (inert such as argon, or reducing, such as hydrogen) which bring additional considerations such as complexity and cost of production. Small volume high performance and added value components may therefore be more favourable for diffusion bonding and the technique may well be the only option for joining such materials. Similar to brazing, diffusion bonding has also found applications in HIP components. 13.3.3 Shrink fitting (press fitting) In shrink fitting, dimensional changes between parts are employed to form the joint, which will not be necessarily gas-or liquid-tight. This may be a disadvantage in some applications.15 It has been demonstrated that, for ferrous PM parts, dimensional change will be dependent on the powder selection and the nature of the constituents.26 Shrink fitting is a cost effective option for many applications, reducing machining, especially for parts that could be manufactured by other methods such as metal injection moulding (MIM) for particular geometrical reasons.19 Cylindrical and ring-shaped compacts are most often joined by press fitting. Joint strength is dependent on variations in densities between the parts, fitting pressure and degree of taper angle, if any.27 © Woodhead Publishing Limited, 2013 392 Advances in powder metallurgy 13.3.4 Adhesive bonding The porosity of sintered parts is ideal for adhesive bonding, since surface porosity can facilitate mechanical keying of the adhesive. Most PM parts can simply be joined by gluing.12 However, the surface has to be cleaned and free of contaminants. Potential advantages include uniform distribution of stress and the ability to join thin to thick parts, making complex geometries possible. The major disadvantage tends to be poor resistance to elevated temperatures where the adhesive degrades; as a result the strength of the joint can be significantly reduced. It is worth noting that the performance of any adhesive strongly depends on the loading mode and therefore any testing should be representative of the actual loading conditions in the application of interest.19 13.3.5 Joining metal injection moulded (MIM) parts At this juncture it is worth noting that the above considerations for different processes are also valid for MIM parts even more so than PM parts owing to the higher binder content in MIM which can affect the weldability, porosity content and impurity levels in the parts. Therefore, careful handling of the component chemistry, including residual levels as well as geometrical considerations and strength/porosity of the parts to be welded, is paramount in defining a window for joining and will enable choice of a suitable process for MIM parts. To date both diffusion bonding and brazing have been favourable processes for joining. It is worth highlighting that powder injection moulding (PIM) of ceramics and metals can also be regarded as a potential route for creating tool materials for friction stir welding of metals and alloys. 13.3.6 Laser metal deposition Laser metal deposition (LMD) is a unique technique, combining laser and powder processing, which enhances material utilisation by enabling manufacture of high precision near net shape components from powders. Owing to the cost of specialised powder feedstock and laser equipments with protective atmosphere in many cases, the technique is regarded as an expensive but versatile option. Therefore, LMD has been of most interest in high value added applications such as in aerospace and medicine which can afford this developing process as a whole, in spite of the criticality of performance and acceptance criteria in these industry sectors. There are several benefits to using LMD for repair. Highly complex parts can be repaired in an automated fashion and, because the heat input is low, the heat affected zone is small. Therefore the strength of material is not © Woodhead Publishing Limited, 2013 Joining processes for powder metallurgy parts 393 affected. Distortion is also lower than for conventional welding techniques. Anisotropy in the mechanical properties occurs, however, due to the layered microstructure and residual stresses that are commonly present because of steep thermal gradients. These are usually detrimental to the mechanical properties of the parts produced. A current concern with LMD is that it is very hard to predict the properties of LMD fabricated components because there are so many process variables involved in the process. The parts have very complex thermal histories, which depend on process variables. The effects of process parameters on the microstructure are complex with a strong dependence on the material system. Despite the major advantages of LMD, there is, however, a continuous need to develop a full understanding of the process–structure–property relationships, with a particular emphasis on the effect of powder characteristics, such as powder particle size, shape and distribution on process variables, and the metallurgy and resulting mechanical properties, which are crucial for many in service applications (Fig. 13.8, Table 13.1).28 13.4 Discussion A broad range of powder metallurgy parts is available, in a wide range of alloys, and there is no single best way to join them. However, there are a number of welding characteristics of PM parts that are different from those associated with wrought or cast equivalents, either as a consequence of the PM production route or the typical applications of PM parts. For example, as PM parts are used in a variety of high precision applications, it is desirable to weld with a process that gives minimal distortion. This favours low heat input processes such as laser and EB welding but any low heat input process will also inevitably give rapid cooling and hence high hardness in steel parts, particularly for higher C contents. It is not clear whether sintered parts can be EB welded in a vacuum however, considering inherent porosity where gases and impurities can be retained and entrapped in the weld. Reduced pressure EB welding, which only requires a vacuum of the order of 10–3 mbar, may be more suitable for welding sintered PM parts, to overcome difficulties in achieving an adequate vacuum, but this is still under development. As with any welding, the main requirements for welding PM parts is that the process should not introduce defects (Fig. 13.9). Powder metallurgy parts contain porosity, either deliberately, and hence with a fairly high volume fraction, or as a consequence of the inability to obtain complete densification, in which case it is typically at a low level. Any porosity in the PM part will tend to trap contaminants and gas, which can cause pores in the weld metal and introduce species that increase sensitivity to both hot and cold cracking mechanisms, for example sulphur and phosphorus © Woodhead Publishing Limited, 2013 394 Advances in powder metallurgy Ti alloys Laser DMD Ferrous and non-ferrous Friction welding Al PM, MMCs Diffusion bonding Laser welding Super alloys Light materials, MMCs EB welding Brazing Porous Arc welding Shrink fitting Resistance/ projection welding Ferrous 13.8 Layout showing relative disposition of joining processes with respect to applications in terms of the nature of materials. contamination will encourage solidification cracking, whilst moisture and carbon contamination will encourage hydrogen cracking. In order to minimise these problems, cleanliness of parts is vital. In this respect, avoiding steam treatment will be beneficial and degreasing is important prior to welding. Where contamination exists, use of a filler metal that is more tolerant of contamination than the parent material, for example a nickel alloy, may be beneficial, in which case arc welding processes are preferred. One possible advantage of an interconnected porosity may be that hydrogen can diffuse out via the open porous structure, in welding PM steel parts, which may make them more resistant to hydrogen fabrication cracking. Where present at significant levels, porosity of the parent material may lead to tearing of the material adjacent to the weld, simply due to the development of plastic strain beyond the capacity of the PM part, perhaps exacerbated by geometric effects at the joint. In such cases, use of low heat input is preferred, to reduce the amount of material strained, and friction welding may be advantageous, as the compression involved tends to close pores. Indeed friction welding may be generally useful for PM parts owing © Woodhead Publishing Limited, 2013 Joining processes for powder metallurgy parts 395 Table 13.1 Qualitative ranking of joining processes for PM parts in terms of relative distortion, geometrical constraint, porosity and cost as high (H), medium (M) or low (L) Joining process Distortion Geometrical Porosity constraint Cost Typical applications Arc welding H/M H/M H/M M/L Ferrous and nonferrous materials Laser welding M/L M/L H/M H/M Ferrous and nonferrous materials EB welding M/L M/L H/M H/M PM superalloys Resistance projection welding M/L M/L M/L M/L Ferrous materials Friction welding M/L M/L M/L H/M Al based PM parts, MMCs Brazing M/L M/L M/L M/L Ferrous: PM to PM or PM to wrought materials Diffusion bonding M/L H/M M/L M/L Ferrous, light materials, Ti, MMCs Shrink fitting M/L M/L M/L M/L Porous materials (a) (c) (b) (d) 13.9 Representation of typical welding flaws: (a) HAZ hydrogen cracking and (b) weld metal hydrogen cracking, (c) lamellar tearing and (d) solidification (hot) cracking (courtesy of TWI Ltd). © Woodhead Publishing Limited, 2013 396 Advances in powder metallurgy to the compressive force involved and the fact that friction welding squeezes the original surface layer, which may be contaminated, out of the joint. It is apparent that powder particle characteristics, which influence densification of a PM part and therefore its final porosity, have not received much emphasis in relation to welding studies. In order to achieve better control of porosity and minimise its detrimental effects in welding, consideration should be given to the influence of powder particle characteristics such as particle shape, size and surface area on the density and porosity of a powder compact, as well as any interfacial reactions and subsequent formations such as secondary phases for improved weldability and joint strength. 13.5 Conclusions The following conclusions are drawn: ∑ Welding is widely used for a range of PM components for diverse applications across several industry sectors but limitations exist owing to the inherent porosity, contamination within the pores and the effect of porosity on the ductility of the material and hence its ability to withstand strain in a weld heat affected zone. ∑ For porous materials, use of low heat input is recommended to reduce strains that develop in the heat affected zone and minimise the risk of tearing adjacent to the weld. Where applicable, friction welding and projection welding may be advantageous as they involve compression, which tends to close pores in the joint area. Porosity in the weld metal is likely to result when any fusion-based process is used and rapid cooling rates may increase porosity owing to the limited opportunity for bubbles to escape from the molten metal. ∑ Where contamination causes weld metal cracking, the use of a welding process that allows introduction of a consumable filler material, such as the various common arc welding processes, is beneficial. In extreme cases, use of a tolerant nickel-based filler metal may be necessary to avoid cracking. Any process that introduces contamination or oxide to porous parts, such as steam treatment is likely to be detrimental to the ability to make sound welded joints and should be avoided. Similarly, cleaning the joint surfaces prior to welding is beneficial. ∑Laser and EB welding have also found application in welding PM components when the inherent low distortion of these processes is an advantage, that is for high precision parts, but these processes have rapid thermal cycles, which encourage hardening and cracking of the weld metal, with limited opportunity for filler addition, and are not always applicable. EB welding in particular is likely to suffer from porosity and the necessary high vacuum might not be achieved when gas contamination © Woodhead Publishing Limited, 2013 Joining processes for powder metallurgy parts 397 is extensive. Reduced pressure EB welding, which operates with higher gas pressures, is attractive for sintered porous parts. 13.6 References 1. J. C. Thornley, Welding Design and Metal Fabrication, 1973, 12, 399–402. 2.K. Couchman, M. Kesterholt and R. White, ‘Seminar on secondary operations’, Proceedings International Conference PM 1988, Orlando, 33–9. 3. M. A. Greenfield, R.F. Geisendorfer, D. K. Haggend and L.P. Clark, Welding Research Supplement, 1977, May, 43–148. 4. J. H. Devletian, Welding Journal, 1987, June, 33–9. 5. A. Rocca and G. Capra, SPEI GCL-7th International Symposium on Gas Flow and Chemical Lasers, Austria 1988, Vol. 1031, 635–45. 6. A. Joskin, J. Wildermuth and D. F. Stein, International Journal Powder Metallurgy and Powder Technology, 1975, 11(2), 137–142. 7.E. Mosca, A. Marchetti and U. Lampugnani, Proceedings International Conference PM Powder Metallurgy, Florence, 1982, 193–200. 8. S. Chiang and C. E. Albright, Journal of Laser Applications, 1988, 1(1), 18–24. 9. X. Zhang, W. Chen, G. Bao and C. Zhao, Science and Technology of Welding and Joining, 2004, 9(4), 379–76. 10. G. M. Alexander-Morrison, A. G. Dobbins, R. K. Holbert and M. W. Doughty, Journal Materials for Energy Systems, 1986, 8(2), 79. 11. J. A. Hamill, Jr, Welding Journal, 1993, February 37–45. 12. G. W. Halldin, S. N. Patel and G. A. Duchon, Progress in Powder Metallurgy, 39, 267–280. 13. J. H. Davidson and C. Aubin, Proceedings: High Temperature Alloys for Gas Turbines, 1982, Liege, Belgium, 853–86. 14. P. Adam and H. Wilhelm, Proceedings: High Temperature Alloys for Gas Turbines, 4–6 October 1982, Liege, Belgium, 909–30. 15. W. V. Knopp, Automobile Engineering Meeting Toronto, Canada, Oct 21–25, Society of Automotive Engineers, 1974, 740984. 16. J. E. Middle, Chartered Mechanical Engineer, 1980, 27(7), 55–60. 17.L. J. Johnson, G. J. Holstand, M. J. O’Hanlon, Fall Powder Metallurgy Conference, 19–20, Detroit, Michigan, MPIF/APMI, 1971, 193–203. 18. W. A. Baeslack III and K. S. Hagey, Welding Research Supplement, 1988, July 1395–495. 19. P. Beiss, Powder Metallurgy, 1989, 32(4), 277–84. 20. W. V. Knopp, Materials Engineering, 1975, 12–75, 34. 21.K. Okimoto and T. Satoh, International Journal Powder Metallurgy, 1987, 23(3), 163–69. 22. N. Janissek, DVS Berichte, Proceedings Brazing, High Temperature Brazing and Diffusion Welding Conference, no. 243, Auchen, 19–21 June 2007, 1–5. 23. H. Duan, M. Kocak, K. -H. Bohm and V. Ventzke, 2004, Science and Technology of Welding and Joining, 2004, 9(6), 513–17. 24. A. Akutso and M. Iijima, 1985, Modern Developments in Powder Metallurgy, 16, 195–208. 25. T. Tabata, Nasaki, H. Susuki and B.G Zhu, International Journal Powder Metallurgy, 1989, 25(1), 37–41. © Woodhead Publishing Limited, 2013 398 26. 27. 28. Advances in powder metallurgy J. C. Thornley, Welding and Metal Fabrication, 1972, 390–5. T. Tabata and S. Masaki, International Journal Powder Metallurgy Powder Technology, 1979, 15(3), 239–44. C. Selcuk, Powder Metallurgy, 2011, 54(2), 94–9. © Woodhead Publishing Limited, 2013