ECE350 Semiconductor Electronic Devices LAB 2 ECE350 Semiconductor Electronic Devices Lab 2 (Part B)– Optical Analogue of X-Ray Crystal Diffraction Edward S. Rogers Sr. Department of Electrical and Computer Engineering University of Toronto Last Revised Aug. 2022 1 Introduction In this part, you will analyze the structure of periodic 1D and 2D arrays by their optical diffraction patterns. This is analogous to using X-rays to study the structure of crystals. 2 Background and Key Concepts Diffraction of a wave by a periodic array is due to phase differences that result in constructive and destructive interference. The diffraction pattern of a crystal is a picture of the reciprocal lattice and therefore yields the structural information of the crystal. Diffraction can be observed when a wave passes through a periodic array if the period spacing is similar to the wavelength of the incident wave. As the lattice constant of a crystal is on the order of 10s of Angstroms (Å), X-rays are required to produce the diffraction patterns. In this experiment, you will make a change of lengthscale. By using the periodic arrays with spacing 10-4 m-10-5 m, visible light from a laser can be used instead of X-rays to produce diffraction patterns. Reference: Kittel. Introduction to Solid State Physics. Ch.2 3 Equipment JDS Uniphase He-Ne Gas Laser (wavelength: 632.8 nm) PASCO Educational diffraction grating slide with three vertical line arrays labelled A, B, and C PASCO Diffraction pattern slide: array of square apertures shown in Figure 3; array of equilateral triangular apertures shown in Figure 4 Optical rail (2 m in length), optical rail carriers, posts, slide holder, screen, ruler 4 Cautionary Notes NEVER LOOK DIRECTLY INTO A LASER BEAM OR SHINE A LASER TOWARD OTHER PERSON. Rev. 2022 Page 1 of 5 ECE350 Semiconductor Electronic Devices LAB 2 AVOID SCRATCHING THE EXPENSIVE SLIDES. HOLD THE SLIDES ONLY BY ITS EDGES. 5 Procedure The experimental setup is shown in Figure 1. A Helium-Neon (He-Ne) laser (632.8 nm) is used as the light source. The laser, slide, and screen are placed on an optical rail with the beam aligned along it. When laser light is incident on a slide containing periodic arrays, the Fraunhofer diffraction pattern of the arrays appears on the projection screen. Figure 1 Optical diffraction experiment setup Mathematically, the Fraunhofer diffraction equation and the Bragg diffraction equation are similar, both of which are dependant on the array spacing (d), wavelength (λ), and diffraction angle (θ) as follows: (a) Rev. 2022 (b) Page 2 of 5 ECE350 Semiconductor Electronic Devices LAB 2 Figure 2 A comparison of (a) Fraunhofer diffraction with (b) Bragg diffraction As can be seen in Figure 2, the path difference of the top and bottom rays is 𝑑 ∙ 𝑠𝑖𝑛𝜃 for the Fraunhofer diffraction case and 2𝑑 ∙ 𝑠𝑖𝑛𝜃 for the Bragg diffraction. This leads to the conditions: 𝑑 ∙ 𝑠𝑖𝑛𝜃 = 𝑛𝜆 (Fraunhofer) and 2𝑑 ∙ 𝑠𝑖𝑛𝜃 = 𝑛𝜆 (Bragg), where 𝑛 is integer number representing the diffraction order. In the experiment, you will first observe how the size and direction of the diffraction pattern are related to the periodic arrays. Then you will measure the diffraction pattern spacing 𝑍, the distance between the slide and the screen, 𝐿, and then calculate the diffraction angle 𝜃 . For a given wavelength 𝜆, you can then calculate the array spacing 𝑑. (1) Turn on the He-Ne laser. Move the screen back and forth on the optical rail and observe the laser beam on the screen. (2) Insert a PASCO Educational Diffraction Grating on the slide holder which should be placed between laser and the screen. Each grating slide has three vertical line gratings A, B, and C, each with different line densities (lines/mm). (3) Adjust the grating slide to let the laser light to be incident on grating A. Move the screen closer and away from slide, observe and record the diffraction pattern. Does the pattern change as change L? (4) Adjust the grating laterally. Observe the diffraction pattern. Does the diffraction pattern move as you move the gratings laterally? Why/Why not? (5) Measure the diffraction pattern spacing and the distance L as shown in Figure 1, then calculate the grating density (lines/mm) of grating A by using the Fraunhofer diffraction equation. (6) Repeat Procedure (3)-(5) for slide gratings B, and C. (7) Remove the grating slide and insert the Diffraction Pattern slide. (8) Adjust the slide to let laser light be incident on the array of square apertures shown in Figure 3. Observe and record the diffraction pattern. Measure the diffraction pattern spacings and the distance between the slide and the screen. Does the diffraction pattern move as you move the gratings laterally? Why/Why not? From your measurements, determine the lattice constant of the square array. (9) Adjust the slide to let the laser light be incident on the array of the triangular apertures shown in Figure 4. Observe and record the diffraction pattern. Measure the diffraction pattern spacings and the distance between the slide and screen. Does the diffraction pattern move as you move the gratings laterally? Why/Why not? From your measurements, determine the lattice constants of the triangular apertures. Rev. 2022 Page 3 of 5 ECE350 Semiconductor Electronic Devices LAB 2 (10) Turn the laser off, then hold the PASCO Educational Diffraction Grating by its edges and look at a fluorescent light tube through the grating. What do you see? (11) After finishing the experiment, put the slides back into the box and ensure the laser is turned off. 6 Hypothesis Draw the diffraction patterns of a vertical array of lines and a horizontal array of lines. Draw the diffraction pattern of an array of square apertures (X=0.025 mm, Y=0.075 mm) as shown in Figure 3. Assume a=X+Y is the pattern period/lattice constant. Draw the diffraction pattern of an array of triangle apertures (X=0.025 mm, Y=0.075 mm) as shown in Figure 4. Assume a=X+Y is the pattern period/lattice constant. Figure 3 Array of square apertures (Lattice constant a = X+Y = 0.100 mm) Figure 4 array of triangle apertures (Lattice constant a = X+Y = 0.100 mm) 7 Pre-Lab Questions 1. How does a periodic array of scatterers produce a diffraction pattern? 2. How can you use Fraunhofer diffraction to measure the lattice constant a 1D or 2D periodic array? 8 Results Include the following data in your post-lab report: Rev. 2022 Page 4 of 5 ECE350 Semiconductor Electronic Devices Diffraction patterns for the three 1D and two 2D arrays. Data needed to calculate the lattice constants. LAB 2 9 Post-Lab Questions (1) What are the geometries of the lattices and the lattice constant of gratings A, B, and C? (2) Calculate the lattice constant of the square apertures array. How do your results compare to the specifications in Figure 3? How does the diffraction pattern vary as you move the arrays along x, y, z? (3) What is the lattice constant of the array of the triangle apertures? How do your results compare to the specifications in Figure 4? How do the results compare with your hypothesis? How does the diffraction pattern vary as you move the arrays along x, y, z? Rev. 2022 Page 5 of 5