Modeling of Adhesively Bonded Joints Lucas Filipe Martins da Silva · Andreas Öchsner (Eds.) Modeling of Adhesively Bonded Joints 123 Editors Lucas Filipe Martins da Silva Departamento de Engenharia Mecânica e Gestão Industrial Faculdade de Engenharia Universidade do Porto Rua Dr. Roberto Frias 4200-465 Porto Portugal lucas@fe.up.pt ISBN: 978-3-540-79055-6 Prof. Dr. Andreas Öchsner Technical University of Malaysia Faculty of Mechanical Engineering Department of Applied Mechanics 91310 UTM Skudai, Johor Malaysia andreas.oechsner@gmail.com e-ISBN: 978-3-540-79056-3 Library of Congress Control Number: 2008927234 c 2008 Springer-Verlag Berlin Heidelberg This work is subject to copyright. All rights are reserved, whether the whole or part of the material is concerned, specifically the rights of translation, reprinting, reuse of illustrations, recitation, broadcasting, reproduction on microfilm or in any other way, and storage in data banks. Duplication of this publication or parts thereof is permitted only under the provisions of the German Copyright Law of September 9, 1965, in its current version, and permission for use must always be obtained from Springer. Violations are liable to prosecution under the German Copyright Law. The use of general descriptive names, registered names, trademarks, etc. in this publication does not imply, even in the absence of a specific statement, that such names are exempt from the relevant protective laws and regulations and therefore free for general use. Cover design: eStudio Calamar S.L. Printed on acid-free paper 9 8 7 6 5 4 3 2 1 springer.com Preface Adhesives have been used for thousands of years, but until 100 years ago, the vast majority were from natural products such as bones, skins, fish, milk, and plants. Since about 1900, adhesives based on synthetic polymers have been introduced, but these were at first of limited use as they were expensive and had poor mechanical properties. Since 1940, there has been a rapid expansion of the chemical knowledge of polymers from which structural adhesives can be made, with a consequent improvement in their properties and reduction of their cost. Today, there are many industrial uses of structural adhesives, particularly in aerospace, but increasingly in automotive applications where the need is to join sheets of dissimilar adhesives to produce lightweight car bodies. In the old days, adhesive use was based on trial and error, together with experience of what was known to work, without any real means of optimisation. With modern technological needs and assisted by modern computers and experimental techniques, it is now possible to asses the performance of adhesively bonded joints before committing a design to manufacture. At least, that is the intention. Reality is such that we need continually to improve and develop these techniques as definitive and certain answers are still not available. Even now, we rely to a significant extent on trial and error and to test prototypes or coupons to validate (or to check) the theoretical predictions. The objective of this book is to bring together some of the latest thinking on available predictive technology for structural bonded joints, using internationally renowned authors who are authorities in their fields. There are two basic ways of analysing the performance of a joint. In the old days, before we had advanced computers, we relied on algebraic methods, using a range of simple or complex formulae. It was difficult or impossible to solve most of these algebraic formulations in a closed form and so we relied to some extent on numerical solutions. Even those solutions we could obtain were often so complex that it took several minutes to calculate a single point by hand. However, modern computers can now be programmed to solve these complex formulae on a point by point basis since they can calculate the values in microseconds. These “old” algebraic formulae have therefore gained a new lease of life and can, for relatively simple v vi Preface joint geometries, give a good indication of the stresses and strains in a joint. Since 1970, the numerical technique called finite element analysis has been developed from a crude and essentially a research tool into a sophisticated commercially available system. The facilitator has been the parallel development of digital computers. These computers have become faster and able to tackle large numerical calculations on even a lap top computer. Indeed, a modern lap top can give results in seconds that in 1980 would have had a turn round time of a day or more using a large main frame computer such as might be found in a university or a large industrial company. For example, a modern motor car contains more computing power than was used for the first space landings in 1970. For anyone wanting to understand how adhesive joints will behave under significant loads and how you might go about getting a design load, this book provides an excellent review of the most up to date thinking and practice. Department of Mechanical Engineering, University of Bristol, Bristol BS8 1TR, UK Robert D Adams Contents Part I Analytical Modeling 1 Simple Lap Joint Geometry . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Andrew D. Crocombe and Ian A. Ashcroft 2 Analysis of Cracked Lap Shear (CLS) Joints . . . . . . . . . . . . . . . . . . . . 25 Liyong Tong and Quantian Luo 3 Analytical Models with Stress Functions . . . . . . . . . . . . . . . . . . . . . . . . 53 Toshiyuki Sawa 3 Part II Numerical Modeling 4 Complex Constitutive Adhesive Models . . . . . . . . . . . . . . . . . . . . . . . . . 95 Erol Sancaktar 5 Complex Joint Geometry . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 131 Andreas Öchsner, Lucas F.M. da Silva and Robert D. Adams 6 Progressive Damage Modelling . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 155 Marcelo F.S.F de Moura 7 Modelling Fatigue in Adhesively Bonded Joints . . . . . . . . . . . . . . . . . . 183 Ian A. Ashcroft and Andrew D. Crocombe 8 Environmental Degradation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 225 Andrew D. Crocombe, Ian A. Ashcroft and Magd M. Abdel Wahab 9 Non-Linear Thermal Stresses in Adhesive Joints . . . . . . . . . . . . . . . . . 243 Mustafa Kemal K. Apalak vii viii Contents 10 Impact . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 279 Chiaki Sato 11 Stress Analysis of Bonded Joints by Boundary Element Method . . . . 305 Madhukar Vable Index . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 327 List of Contributors Andrew D. Crocombe Division of Mechanical, Medical and Aerospace Engineering, School of Engineering, University of Surrey, Guildford, GU2 7XH, UK, e-mail: A.Crocombe@surrey.ac.uk Andreas Öchsner Department of Applied Mechanics, Faculty of Mechanical Engineering, Technical University of Malaysia, 81310 UTM Skudai, Johor, Malaysia; University Centre for Mass and Thermal Transport in Engineering Materials, School of Engineering, The University of Newcastle, Callaghan, NSW 2308, Australia, e-mail: andreas.oechsner@gmail.com Chiaki Sato Precision and Intelligence Laboratory, Tokyo Institute of Technology, 4259 Nagatsuta, Midori-ku, Yokohama 226-8503, Japan, e-mail: csato@pi.titech.ac.jp Erol Sancaktar Professor, Polymer Engineering, Adjunct Professor, Mechanical Engineering, The University of Akron, Akron, OH 44325-0301, e-mail: erol@uakron.edu Ian A. Ashcroft Wolfson School of Mechanical and Manufacturing Engineering, Loughborough University, Loughborough, Leicestershire, LE11 3TU, UK, e-mail: i.a.ashcroft@lboro.ac.uk Liyong Tong School of Aerospace, Mechanical and Mechatronic Engineering, J11- Aeronautical Engineering Building, The University of Sydney, NSW 2006, Australia, e-mail: ltong@aeromech.usyd.edu.au Lucas F.M. da Silva Departamento de Engenharia Mecânica e Gestão Industrial, Faculdade de Engenharia, Universidade do Porto, Rua Dr. Roberto Frias, 4200-465 Porto, Portugal, e-mail: lucas@fe.up.pt ix x List of Contributors Madhukar Vable Mechanical Engineering - Engineering Mechanics, Michigan Technological University, Houghton, MI 49931, USA, e-mail: mavable@mtu.edu Magd M. Abdel Wahab Division of Mechanical, Medical and Aerospace Engineering, University of Surrey, Guildford, GU2 7XH, UK, e-mail: M.Wahab@surrey.ac.uk Marcelo F.S.F de Moura Departamento de Engenharia Mecânica e Gestão Industrial, Faculdade de Engenharia, Universidade do Porto, Rua Dr. Roberto Frias, 4200-465 Porto, Portugal, e-mail: mfmoura@fe.up.pt Mustafa Kemal K. Apalak Department of Mechanical Engineering, Erciyes University, Kayseri 38039, Turkey, e-mail: apalakmk@erciyes.edu.tr Quantian Luo School of Aerospace, Mechanical and Mechatronic Engineering, J11- Aeronautical Engineering Building, The University of Sydney, NSW 2006, Australia, e-mail: qtluo@aeromech.usyd.edu.au Robert D. Adams Department of Mechanical Engineering, University of Bristol, Bristol BS8 1TR, UK, e-mail: R.D.Adams@bristol.ac.uk Toshiyuki Sawa Hiroshima University, 1-4-1, Kagamiyama, Higashihiroshima, Hiroshima, Japan, e-mail: sawa@mec.hiroshima-u.ac.jp Part I Analytical Modeling Chapter 1 Simple Lap Joint Geometry Andrew D. Crocombe and Ian A. Ashcroft Abstract The chapter outlines the basic mechanics of adhesively bonded simple lap joints, focusing on the analytical solutions that have been developed. This can be viewed as foundational material for the chapters in this book that deal with numerical modelling of adhesive joints. It begins with a discussion of the shear-lag concept which governs the development of adhesive shear stresses arising from load transfer between substrates. From this starting point a number of design analysis approaches are outlined, all of which seek to provide easy access to adhesive stresses within joints under a range of service loading conditions. The chapter concludes by considering approaches that have been made to enhance the accuracy of the closed form analytical adhesive joint models. Although improving the accuracy, these developments also result in a considerable increase in complexity with the result that analytical solutions are more difficult to utilise. 1.1 Introduction A large number of adhesively bonded joint configurations use an overlap in their construction. These are generically referred to as simple lap joint geometries. The most common of these simple lap joint geometries is the axially loaded single overlap joint (sometimes referred to simply as a single overlap joint). This chapter will consider the analytical stress analyses of the generic range of simple lap joints. Later chapters deal with the numerical modelling of such configurations. Andrew D. Crocombe Division of Mechanical, Medical and Aerospace Engineering, School of Engineering, University of Surrey, Guildford, GU2 7XH, UK, e-mail: A.Crocombe@surrey.ac.uk Ian A. Ashcroft Wolfson School of Mechanical and Manufacturing Engineering, Loughborough University, Leicestershire, LE11 3TU, UK, e-mail: i.a.ashcroft@lboro.ac.uk L.F.M. da Silva, A. Öchsner (eds.), Modeling of Adhesively Bonded Joints, c Springer-Verlag Berlin Heidelberg 2008 3 4 Andrew D. Crocombe and Ian A. Ashcroft 1.1.1 Limiting Joint Strengths Adhesives are not generally as strong as the materials they join and hence use is often made of an overlap to increase the load carrying capacity of a joint. Generally, when designing a bonded joint, the ideal approach is to ensure that the bonded joint is stronger than the parts being jointed. However, it can be shown that the load carrying capacity of an overlap joint is not proportional to the length of the overlap. Consider the simple single overlap joint illustrated in Fig. 1.1. The axial load is transferred from one substrate to the other through shear in the adhesive. This shear will only occur over a finite zone of the adhesive layer and any increase in overlap length beyond this maximum transfer zone length will not result in any increase in joint strength. Where load transfer beyond this limiting value is required (as in the case of very thick substrates) a different type of joint design will be required, such as the scarf or stepped lap joint, as shown in Fig. 1.2. In both these configurations the load is distributed more uniformly across the entire adhesive layer than in the single lap joint. 1.1.2 Load Transfer in Lap Joints In some lap joints complete load transfer occurs from one set of substrates to another as shown in the joints in Figs. 1.1 and 1.2. In other configurations, such as that shown in Fig. 1.3, only partial load transfer occurs across the adhesive. However, even this partial load transfer may be sufficient to cause the bond line to fail and thus stresses and strains in the adhesive layer are required to assess the joint strength. τ Fig. 1.1 Single lap joint configuration and shear stress distribution in the adhesive layer Scarf Joint Fig. 1.2 Scarf and stepped lap joints Step Joint 1 Simple Lap Joint Geometry 5 Fig. 1.3 Partial load transfer within a joint 1.1.3 Overview Methods of determining the adhesive stress and strain in a range of lap joints will be considered in this chapter. The next section outlines the simplest form of axial loaded single lap joint analysis and presents results in an accessible way in order to understand basic joint mechanics. This is followed by a section that discusses the various tools that are available to analyse a range of practical lap joint configurations. The analyses outlined in these two sections are subject to a number of simplifying assumptions. These tend to include: • substrate deformation due to tension and bending only • adhesive stresses restricted to peel and shear and assumed to be constant across the adhesive layer The penultimate section addresses more advanced analyses, generally of the axially loaded single overlap joint, that make less simplifying assumptions at the cost of analytical complexity and hence general usefulness. 1.2 Single Lap Joint Mechanics 1.2.1 Qualitative Understanding of Adhesive Stresses The simplest approach is to assume that the substrates are effectively rigid. This means that as the load passes from substrate to substrate a uniform shear stress distribution is generated, as shown in Fig. 1.4. In reality the substrates are not rigid and they stretch more nearest their loaded end, as shown in Fig. 1.5. Thus the shear stress that is generated is not uniform but peaks at the overlap ends where the differential substrate extension is greatest, as illustrated in Fig. 1.1. In practice, as well as shearing the adhesive, the offset loading causes bending in the loaded substrate, which tries to separate from the adjacent unloaded substrate. In τ Fig. 1.4 Uniform adhesive shear stress x 6 Andrew D. Crocombe and Ian A. Ashcroft Fig. 1.5 Non-uniform adhesive shearing σ x Fig. 1.6 Peel stresses in a single lap joint addition to the non-uniform shear stress, this bending action gives rise to transverse direct stresses, sometimes known as peel or cleavage stresses, which are maximum at the joint ends, as shown schematically in Fig. 1.6. Thus what appears to be a simple joint in reality gives rise to a fairly complex state of adhesive stresses. 1.2.2 Volkersen’s Shear Lag Analysis This approach was developed by Volkersen (1938) and accounts for the variable shear stress distribution shown in Fig. 1.1. Referring to Fig. 1.7 the adhesive shear stress (τ ) at distance x from the centre of the overlap (length L and adhesive thickness η ) is defined in terms of the shear strain γ as δ (δ0 + u2 − u1 ) τ = Gγ = G = G (1.1) η η u1 and u2 represent the extension of the substrates and can be derived in terms of substrate strains (ε1 and ε2 ) as x ε1 dx; u1 = −L/2 x u2 = ε2 dx (1.2) −L/2 These strains at distance x can be obtained from the upper and lower substrate stresses, which can be expressed by the substrate force P, thickness ti and tensile modulus Ei , as shown in Fig. 1.8 and Eq. (1.3). L/2 + x + u1 P δ δ0 A B L/2 + x + u2 Fig. 1.7 Deformation in the shear lag analysis P 1 Simple Lap Joint Geometry 7 Fig. 1.8 Substrate forces P – Fτ P Fτ Fτ ε1 = [P − Fτ ]/E1t1 = [P − x τ dx]/E1t1 −L/2 ε2 = Fτ /E2t2 = x τ dx/E2t2 (1.3) −L/2 If the substrates are made from the same material then E1 = E2 = Es . By substituting Eq. (1.1) into (1.3), then (1.3) into (1.2) and then differentiating twice the following second order differential equation governing the adhesive shear stress is obtained d 2 τ ω 2 = τ dx2 L (1.4) where ω 2 = (1 + t1 /t2 )k and k = GL2 /(Est1 η ). This can be solved and non-dimensionalised fairly readily to give a solution of t1 − t2 ω sinh ω X τ ω cosh ω X + = τa 2 sinh ω /2 t1 + t2 2 cosh ω /2 where τa is the average shear stress (P/L) and X = x/L. The above can be considerably simplified, by considering only the peak stress at the joint ends (X = +/ − 0.5) and assuming that the joint is sufficiently long such that sinh ω /2 = cosh ω /2, giving t1 − t2 τ ω = ± τa 2 t1 + t2 This clearly shows that for a joint with different substrates the adhesive stress is maximum (and thus failure most likely) at the overlap end where the loaded substrate is thinnest. Further, the lowest adhesive stresses are obtained when the substrates are identical (t1 = t2 = t). τ ω = = τa 2 GL2 2Est η (1.5) This is an extremely useful formula which shows a number of very important features about the size of the peak adhesive stress in a single overlap joint, namely – for long joints it is independent of the joint length, – it increases with increasing adhesive shear modulus, – it increases with decreasing substrate modulus and thickness and adhesive thickness. 8 Andrew D. Crocombe and Ian A. Ashcroft 1.3 Simple Design Tools 1.3.1 General Adhesive Sandwich Analysis The analysis developed by Goland and Reissner (1944) for the single lap joint has been generalised by Bigwood and Crocombe (1989) so that it can be applied to an arbitrary end loaded single overlap configuration. The resulting analyses can be applied to single overlap joints but also to many other configurations, as shown in Fig. 1.9. The substrate loads and adhesive stresses acting on small elements of the upper and lower substrates are shown in Fig. 1.10. Force and moment equilibrium of the upper and lower substrates gives dTi = τ; dx ti dMi −Vi + τ = 0 dx 2 dVi = σ; dx (1.6) where i = 1 or 2, representing the upper and lower substrate respectively and all other terms have been defined in Fig. 1.10. The axial and transverse displacements of the upper and lower substrates (ui and vi ) can be expressed in terms of the substrate surface strain and moments respectively as (1 − νi2 ) dui Miti2 (1 − νi2 )Mi d 2 vi = =− (1.7) Pi + ; 2 dx Eiti 2Ii dx Ei Ii V12 V11 T11 M11 T21 M12 x M21 V21 T12 T22 V22 M22 Fig. 1.9 Arbitrarily end loaded single overlap unit T1 + dT1 M1 T2 Fig. 1.10 Elemental substrate stresses in the lap joint V1 + dV1 V1 T1 V2 τ M1 + dM1 σ σ dx τ V2 + dV2 T2 + dT2 M2 M2 + dM2 1 Simple Lap Joint Geometry 9 where νi and Ii are respectively the Poisson’s ratio and second moment of area of substrate i. Finally expressions for the adhesive shear and transverse direct stresses in terms of the adhesive strains and hence substrate displacements are τ = Gγ = G (u1 − u2 ) ; η σ = Eε = E (v1 − v2 ) η (1.8) Equations (1.8) can be differentiated an appropriate number of times and substitutions made from (1.7). The resulting expressions can be differentiated further and substitutions made from (1.6) to give the governing differential equations as d5τ d3τ dτ d7τ =0 − K1 5 + K3 3 − K5 7 dx dx dx dx d6σ d4σ d2σ − K1 4 + K3 2 − K5 σ = 0 6 dx dx dx (1.9) Now these can be solved with appropriate boundary conditions. This cannot be done analytically for the general adhesive sandwich shown in Fig. 1.9 but they can be easily solved numerically. However for the case of the axially loaded single lap joint discussed in Sect. 1.2 the 12 unknown end loads shown in Fig. 1.9 are reduced to 6 (left end of the upper substrate and right end of the lower substrate). An analytical solution for this simplified configuration was first derived by Goland and Reissner (1944) and this is outlined in the following section. 1.3.2 Axially Loaded Single Overlap Joints The Goland and Reissner (1944) solution of this configuration consists of two parts. The first is a solution for the load boundary conditions and the second is the derivation of the equations for the adhesive shear (τ ) and peel stresses (σ ). The generalised adhesive sandwich analysis outlined in the previous section is an extension of the second part of the Goland and Reissner analysis and hence this will not be repeated here. Instead this section outlines the solution for the load boundary conditions or what is now known as Goland and Reissner’s bending moment factor. Figure 1.11 shows a single lap joint in its undeformed position. If the joint is sufficiently long then approximate expressions for the end loads are T11 = T22 = P M11 = M22 = −P(t/2) The shear forces V11 ,V22 can be determined to maintain moment equilibrium. However, in practice, the joint will rotate on loading as illustrated in Fig. 1.6 and the line of action of the load will move closer to the substrate centre line thus 10 Andrew D. Crocombe and Ian A. Ashcroft P t P V11 T11 M11 T22 V22 M22 Fig. 1.11 Simplified single lap joint end loads reducing the moment. This is accommodated by introducing a factor (k) to reduce the bending moment i.e. M11 = M22 = −kP(t/2) In an axially loaded single overlap joint the substrate moment makes a significant contribution to the adhesive stresses and thus it is important that the correct value is used. To account for the joint rotation Goland and Reissner split the joint into two regions, the free substrate region and the overlap region as shown in Fig. 1.12 and the transverse deflection is determined for each region. All parameters are known except the deflection of the neutral axes of the two regions, wa and wb . Equations for the bending moment and thus the curvature can be written for both the regions wa = −Ma /(EI)a = −P(α xa − wa )/(EI)a (1.10) wb = −Mb /(EI)b = −P(α (La + xb ) − wb − (t + η )/2)/(EI)b (1.11) The adhesive thickness (η ) is disregarded in the classical Goland and Reissner approach. These are 2nd order differential equations in wa and wb respectively and can be easily solved. The boundary conditions are that the deflection is zero at the left end of region a and the right end of region b while the deflections and slopes at the wa P t xa La wb η xb c Fig. 1.12 Deflection of the single overlap joint α 1 Simple Lap Joint Geometry 11 connection of regions a and b are continuous. These can be simplified and solved for the reasonable assumption that the free substrate length is large to give sandwich moment (M11 ) of (1.12) M11 = −k(Pt/2) where cosh u2 c √ cosh u2 c + 2 2sinh u2 c u2 = 3(1 − ν 2 )P/2η Es k= The parameter k is a factor of the undeformed moment and varies from a value of 1 at low loads to a minimum of around 0.26 for high loads. Again the shear forces V11 ,V22 can be determined to maintain moment equilibrium. When these boundary conditions are used in conjunction with the analysis for adhesive stresses the following closed form equations are derived for adhesive shear and peel stresses in an axially loaded single overlap joint ⎤ ⎡ βc x cosh ⎥ τ 1 ⎢βc t c (1.13) (1 + 3k) + 3(1 − k)⎥ = ⎢ ⎦ ⎣ βc τav 4 t sinh t where β 2 = 8tG Es η t 2 1 k λx λx σ = cos R2 λ 2 − λ k cos λ cosh λ cosh P/t c R1 2 c c k λx λx sin + R3 λ 2 − λ k sin λ sinh λ sinh 2 c c where c λ= t 6Et Es η 1 4 R1 = (sinh 2λ + sin 2λ )/2 R2 = sinh λ cos λ − cosh λ sin λ R3 = sinh λ cos λ + cosh λ sin λ Goland and Reissner’s derivation of the bending moment factor for symmetric single lap joints assumed that the overlap region deformed as a single block of composite stiffness ((EI)b in Eq. (1.11)). This has been developed by a number of subsequent researchers. Hart-Smith (1973a) argued that it was better to model the deformation of the upper and lower substrates in the overlap region separately. His approach 12 Andrew D. Crocombe and Ian A. Ashcroft involved the solution of the adhesive stresses and the bending moments at the same time and provides a bending moment factor k in Eq. (1.12) of: η k = 1+ t 1 1+ξc+ ξ 2 c2 6 √ where ξ = u2 c.2 2 (see Eq. (1.12)). The expression derived for the moment factor varies from unity at low loads to zero with increasing loads. Thus at higher loads the moment and hence the adhesive stress predicted by Hart-Smith are a little lower than those predicted by Goland and Reissner. Tsai and Morton (1994) review both these approaches and a third by Oplinger (1994) that includes large deformation of the overlap as well as the free substrate. All three are only applicable to joints with balanced substrates. They also investigate the assumption that the overlap is much smaller than the free substrate length. Overall, based on comparison with numerical studies, they conclude that Hart-Smith and Oplinger give better end moments for short and long overlaps respectively. However with regard adhesive stresses, the Goland and Reissner approach is accurate enough for short and long overlaps. 1.3.3 Simplified Design Formulae Although the equations outlined in the general adhesive sandwich analysis section above require a numerical solution, a simplification (neglecting the adhesive shear and peel stress in turn) can be made resulting in simple design formulae. This simplification decouples the governing equations presented in Eq. (1.9). In fact it turns out that this simplification is completely valid when the substrates are the same and this is common practice. By making the same assumptions as those in the shear lag analysis it is possible to find approximate expressions for the stresses at the end of the overlap in terms of simple design formulae. Unlike the shear lag analysis these formulae give both adhesive stress components due to all possible substrate loading, not just axial loads. These formulae are shown in Fig. 1.13 and Bigwood and Crocombe (1989) provide further detail. T τT = − α1T ( α1 + α2 ) 0.5 σV = − 2 β1V ( β1 + β2 ) 0.75 V τV = 3V σM = − β1 M ( β1 + β2 ) 0 . 5 M τM = 4t1 3α1 M t1 ( α1 + α2 ) 0.5 Fig. 1.13 Peel and shear stress design formulae for tensile shear and moment loading in the substrate 1 Simple Lap Joint Geometry 13 The parameters α1,2 and β1,2 are called the shear and peel compliance factors and are defined as follows α1 = G(1 − ν12 )/(E1t1 η ); β1 = 12E(1 − ν12 )/(E1t13 η ) with similar expressions for the lower substrates. Although a good guide, the simplifications made in the analysis are only completely valid for identical substrates (t1 = t2 = t), in this case the design formulae simplify further still to give σV = −V (β /2)0.25 ; τT = −T (α /2)0.5 ; 2 σM = −M(β /2)0.5 τV = 3V /4t; τM = M 3(α /2)0.5 t (1.14) It is interesting to compare τT in the above to that given by Volkersen. Substituting in for α above gives 1 τT = P 2 G(1 − ν 2 ) 2Es η t By comparison with Eq. (1.5) it can be seen that in addition to the factor (1 − ν 2 ) (this arises by assuming plane strain rather than plane stress behaviour) the stresses given by Volkersen are exactly twice that found from the more general analysis. This difference is caused by the fact that, in Volkersen the substrate is assumed to be in tension only. This is clearly wrong as, from simple static considerations, the adhesive shear stress must induce a moment in the substrate. This acts in a way to reduce the adhesive shear stress and the result is quite significant. Thus we may say that Volkersen formulae overestimates the peak adhesive stresses by a factor of two and use of the simple formulae produced by Crocombe and Bigwood should be used. 1.3.4 Design Formulae for Environmentally Degraded Single Lap Joints Fig. 1.14 Illustrating moisture transport and degradation in the joint x Stress Moisture When bonded joints are exposed to moisture, the moisture diffuses through, and degrades the adhesive. This is illustrated in Fig. 1.14. Increasing time Increasing moisture x Strain 14 Andrew D. Crocombe and Ian A. Ashcroft In many adhesive systems it can be shown that the ultimate adhesive strength essentially degrades linearly with increasing moisture content (cm ) up to the maximum moisture content (cm∞ ). A simple yet effective limit state approach (Crocombe, 2007) has been applied to develop design tools. This limit state approach was first suggested for use with adhesive joints by Crocombe (1989) using the term global yielding. The failure load (Pmax ) is found by assuming that all the adhesive reaches its maximum load carrying capacity (τmax , which is a function of cm /cm∞ , reducing where the adhesive is wetter) before joint failure occurs i.e. L Pmax = τmax (cm /cm∞ ) dx (1.15) 0 The moisture distribution shown in Fig. 1.14 (cm ) can be found by using the Fickian diffusion coefficient D. Combining this with Eq. (1.15) and the linear reduction in adhesive strength τmax with moisture cm finally provides the following equation for degraded joint strength 2 Pmax 1 8 ∞ −(2 j+1)2 Dπ2 t L = 1 − Fτ 1 − 2 ∑ e (1.16) τdry L π 0 (2 j + 1)2 where Fτ = 1 − τwet and τwet and τdry are the saturated and dry adhesive strengths. τdry 1.4 Advanced Analytical Models The previous two sections have outlined lap joint analyses based on the following assumptions (a) (b) (c) that the adhesive stresses do not vary across the adhesive thickness, that the substrates response is a simple combination of tension and bending, both adhesive and substrate behave elastically. This section reviews work by various authors that go beyond these basic simplifying assumptions. 1.4.1 Advances in Strain-Displacement Models Renton and Vinson (1977) made the next significant contribution to the analysis of single lap joints. The effect of shearing in the substrate is included and the substrate is modelled as a generally orthotropic system, to extend the application to composite materials. As with previous analyses the adhesive shear and peel stress have been assumed constant across the thickness of the adhesive. Equations were derived 1 Simple Lap Joint Geometry τou V1 T1 15 σou V2 x M1 σoL T2 h L τoL M2 Fig. 1.15 Model substrate block according to Renton and Vinson for the stress resultants (Mx , Nx and Vx ) for the model substrate element shown in Fig. 1.15, which shows the block end loads and the upper (τou , σou ) and lower (τoL , σoL ) surface shear and normal stresses. Mx = −D11 Nx = A d 3 τoL d2w d 3 τou d τou d3φ dφ d τoL +H + H∗ +F 3 +G +J + J∗ 2 3 3 dx dx dx dx dx dx dx d 3 τoL du d 3 τou d τou d3φ dφ d τoL +C +C∗ + Ā − N(x)T +B +D + D∗ 3 3 dx dx dx dx dx3 dx dx h Vx = (τou + τoL ) + Lφ 2 (1.17) In these equations parameters A to L are problem specific constants, D11 is the main flexural stiffness and φ is a function of x defining the transverse shear stress distribution. Importantly, these included a parabolic shear stress distribution across the thickness of the block. This block is used to model both substrates in the overlap region, Fig. 1.16. Assuming that the adhesive shear (τo ) and peel (σo ) stress is constant across the adhesive thickness, using the same adhesive strain-displacement equations as Goland and Reissner, considering equilibrium of the substrate blocks and setting appropriate surface tractions and stress resultants either to zero or to the adhesive V1 T1 τo M1 τo σo τo τo σo V2 T2 M2 Fig. 1.16 Blocks in the overlap region 16 Andrew D. Crocombe and Ian A. Ashcroft shear or peel stress, an 8th order differential equation is obtained for the adhesive shear stress in single lap joints with different substrates. This simplifies considerably for symmetric single lap joints. From the solution of this, the adhesive peel and shear stresses and the stress resultants in the substrate blocks can be found. Goland and Reissner’s moment factor was used to provide boundary conditions. When compared with the Goland and Reissner solution for a typical joint configuration, the maximum peel and shear stresses are reduced by around 20% and 40% respectively and, unlike the Goland and Reissner analysis, the adhesive shear stress now drops rapidly to zero at the very end of the overlap, as it should for a free surface. Further advances to single lap joint analyses have been made by Ojalvo and Eidinoff (1978). They incorporate a fuller description for adhesive shear strain on the upper and lower interfaces (i = 1 or 2 respectively) γi = u1 − u2 dwi + η dx (1.18) Further, the displacements in the adhesive are assumed to vary linearly between the values on the upper and lower interface as w(x, z) = (w1 + w2 ) z + (w1 − w2 ) 2 η (1.19) with a similar expression for u(x, y). This allows for a linear variation across the adhesive thickness of the shear stress while the peel stress does not vary. Substrate shearing has not been included. Balanced joints are considered and the adhesive shear and peel stresses both reach a peak at the end of the overlap. For typical joint parameters the maximum shear and peel stresses are increased and decreased respectively over the values given by Goland and Reissner (1944). It was shown that shear stress could exhibit significant variation across the overlap at the joint ends. However, unlike Renton and Vinson (1977), the formulation does not allow the adhesive shear stress to drop to zero at the ends of the overlap. Delale et al. (1981) include the adhesive longitudinal stress in addition to the shear and peel stresses, however these adhesive stresses are assumed to be constant across the adhesive thickness and as with all previous analyses, except Renton and Vinson (1977), the formulation does not allow the adhesive shear stress to become zero at the overlap ends. The formulation is derived for unbalanced orthotropic lap joints and substrate shearing has been incorporated though substrate rotation (θi ). The adhesive shear strain is now defined in terms of substrate mid-plane displacements (ūi ) and rotations. 1 h1 h2 γ= ū1 − θ1 − ū2 − θ2 (1.20) η 2 2 The adhesive longitudinal strain (εx ) is taken as the average of the upper and lower interface strains which is expressed as 1 Simple Lap Joint Geometry εx = 17 1 2 du1 h1 d θ1 du2 h2 d θ2 − + − dx 2 dx dx 2 dx (1.21) Adhesive shear stresses are expressed as a 7th order differential equation. The boundary conditions used do not incorporate the bending moment factor and thus it is not possible to make a comparison between this and other solutions. Tsai et al. (1998) present a different way to model substrate shear, allowing it to vary linearly through the substrate thickness. They argue that as the adhesive shear stress is highest towards the end of the overlap then there will be high shear stresses acting on the adjacent substrate that forms the interface with the adhesive. Neglecting this substrate shear deformation can have important effects, particularly with shear compliant substrates like laminated composites. This shear goes to zero on the opposite free surface of the substrate and Tsai et al. assume the simplest linear variation. The substrate in-plane displacement (ui ) due to tension now has an extra term that varies across the substrate thickness (yi ) ui = ui,os + τ 2 y 2Gi hi i (1.22) where ui,os is the displacement on the outer (shear free) surface of the substrate and τ is the adhesive shear stress and i refers to the substrate. Whilst this is not as accurate a representation for substrate shear as others such as Renton and Vinson (1977) it has the advantage of being readily incorporated into the earlier solutions of Volkersen (1938) and Goland and Reissner (1944). Only adhesive shear stress is considered as the substrate shear was not expected to affect the adhesive peel stresses. The result of including this parameter is to modify the governing differential equation. For example Volkersen’s equation (1.4) is modified by the term α to d 2 τ αω 2 = τ; dx2 L −1 t1 G t2 where α = 1 + + η 3G1 3G2 2 (1.23) As the substrate shear deformations become smaller α tends to 1 and the original Volkersen equation is recovered. Similar modifications are derived for the Goland and Reissner solution where the shear stress is still given by Eq. (1.13), repeated again here for convenience, but now the parameter β 2 is defined differently. ⎤ ⎡ βc x cosh ⎥ τ 1 ⎢βc t c ⎥ (1.24) (1 + 3k) + 3(1 − k) = ⎢ ⎦ βc τav 4 ⎣ t sinh t 1 8tG where β 2 = Es η 1 + 2Gt/(3Gs η ) In the Goland and Reissner’s analysis the term in parenthesis in the expression for β 2 is unity. It is shown that including the substrate shear will smooth and reduce the shear stress distribution along the overlap. 18 Andrew D. Crocombe and Ian A. Ashcroft Fig. 1.17 Three strips with end loads and interface tractions (shown dashed) considered by Sawa et al. (2000) Sawa et al. (2000) modelled an unbalanced single lap joint by considering the two substrates and the adhesive layer as three separate strips, Fig. 1.17, subjected to common but unknown tractions along the interfaces (illustrated schematically) and appropriate tractions on the other faces. All three stress components are included in each strip (σx , σy and τxy ) thus a complete 2D elasticity problem is formulated and solved. A series of 9 separate polynomial and Fourier series Airy stress functions X = ΣXi were derived for each strip involving 18 + 48N unknown coefficients, where N is the number of terms in the Fourier series (between 50 and 60 were found to be an adequate number of terms). Stresses in each strip can be defined in terms of the Airy stress function as σx = d2X ; dy2 σy = d2X ; dx2 τx = − d2X dxdy (1.25) The first 18 of these unknown coefficients can be found from the known boundary conditions and the remainder are found by solving 48 simultaneous equations for each term included in the series. Solution of this is likely to be as complex as carrying out finite element (FE) analysis and so is of limited use as an analytical tool. They found the same sort of trends in adhesive stress as were found in the simpler closed form solutions but with the inclusion of sufficient terms were able to model the bi-material stress singularity reasonably. 1.4.2 Energy Based Approaches A number of authors, including, Chen and Cheng (1983) and Adams and Mallick (1992) have adopted a different approach to obtain a global stress analysis of adhesive joints. They use the equilibrium equations ∂ σx ∂ τxy + = 0; ∂x ∂y ∂ σy ∂ τxy + =0 ∂y ∂x (1.26) to develop general expressions for stresses (σx , σy and τxy ) in both substrates and adhesive. Thus tensile, bending and shearing in the substrate are all included. Boundary and continuity conditions are then imposed to partially solve these equations. As 1 Simple Lap Joint Geometry 19 the substrate and adhesive sections are treated separately the condition for zero adhesive shear stress at the overlap ends can be imposed, as Renton and Vinson (1977). The remaining unknown parameters are found by applying the variational principle (minimising) of complementary energy. Chen and Cheng (1983) use the Goland and Reissner (1944) moment factor and determined the shear force using equilibrium. The substrate longitudinal stresses are assumed to vary linearly across the substrate thickness and the shear stresses parabolically. They assume that the adhesive shear stress does not vary across the thickness and show that from the equilibrium equations this implies that adhesive longitudinal stress is zero. The peel stress however varies linearly across the adhesive thickness. It is shown that all stress components can be expressed in terms of two unknown independent functions of x (Φ and Φ ∗ ). Expressions for adhesive peel and shear stress are given below: dΦ h dΦ ∗ + dx 2 dx y σ = Φ + (Φ − Φ ∗ ) η τ=h (1.27) The complementary energy is expressed in terms of these unknowns. Minimising this produces two coupled 4th order differential equations for these unknowns. These can be solved and used to find adhesive and substrate stresses. Although closed form in nature the resulting expressions are highly complex. A good match with the solution of Goland and Reissner is found except at the overlap ends where Chen and Cheng’s analysis correctly show the adhesive shear stress to drop rapidly to zero and the adhesive peel stress to vary significantly across the adhesive thickness. Adams and Mallick (1992) extended the work of Chen and Cheng by formulating the problem to include different substrates, thermal stresses and both single and double lap joints solutions. In addition, adhesive longitudinal stresses were included and all stresses were allowed to vary across the adhesive thickness. Due to the increased complexity in adhesive stresses and dissimilar substrates the entire stress field was expressed in terms of four independent functions, rather than the two in the work of Chen and Cheng. Owing to this added complexity the authors have not determined a closed form solution but instead have discretised the problems by breaking the joint into a number of intervals with the functions and their first derivatives forming the unknown parameters at each node. {σ } = [N]{Φ } + {C(x)} + {k} (1.28) Where {σ } is a vector containing the 3 stress components of each of the substrates and the adhesive, {Φ } is the vector of the 4 stress functions (Φ11 , Φ12 , Φ21 , Φ22 ) and their first and second derivatives with respect to x. The arrays [N], {C(x)} and {k} are known from the configuration. The entire problem is then solved numerically as a matrix problem similar to the FE method. 20 Andrew D. Crocombe and Ian A. Ashcroft 1.4.3 Non-linear Material Models Many modern adhesive systems exhibit significant non-linearity in their constitutive response and hence analyses based on linear material behaviour may be of limited use for strength assessment. Hart-Smith (1973b) extended the double lap joint analysis modelling the adhesive as an elasto-plastic material. He showed that the actual form of the adhesive stress strain curve was less important than the area under it (energy dissipated) and thus used an elastic-perfectly plastic response (no strain hardening) for the adhesive. The analyses were simplified by uncoupling the shear and peel stress analyses. Elasto-plasticity was only included in the shear stress formulation, which was based on the shear lag approach outlined by Volkersen (1938) and this was achieved by deriving equations for an elastic inner region and plastic outer region and then applying boundary conditions at the overlap ends and continuity at the inner-outer region boundaries. The peel stress distribution is similar to that of the later Volkersen (1965) analysis, which was elastic. By assuming that joint failure occurs at a critical level of plastic strain, Hart-Smith develops a chart that gives predicted joint strength as a function of a joint geometry parameter and the ratio of failure to initial yield shear strains. The elastic analysis of Bigwood and Crocombe (1989) for an arbitrarily end loaded single overlap was extended to incorporate a full non-linear representation of the adhesive layer where both the peel and shear stresses contribute to adhesive yield, Bigwood and Crocombe (1990). Equations (1.6), (1.7) from the linear analysis have been rewritten expressing the adhesive shear and peel stresses as non-linear functions of strain as Es γ dV1 Es ε dM1 (h1 + η )Es γ dT1 = ; = ; = V1 − 2 dx 2(1 + ν p ) dx (1 + ν p ) dx 4(1 + ν p ) dκ dγ dε = κ; = f1 (M1 , T1 , x); = f2 (M1 , T1 , x) dx dx dx (1.29) Unlike the elastic analyses, here Es is the secant adhesive modulus, determined from a hyperbolic tangent model representing the non-linear adhesive stress strain curve. Eε σ = A tanh (1.30) A In the hyperbolic tangent model the parameter E and A will give the initial modulus and the ultimate stress respectively. These provide a set of 6 first order differential equations in 6 unknowns (T1 (x),V1 (x), M1 (x), ε (x), κ (x) and γ (x)). These governing equations were solved numerically in an incremental manner. Good correlation was found between their analyses and non-linear FE solutions. Figure 1.18 shows the adhesive shear stress distributions arising from a linear (stress lin) and non-linear (stress non-lin) analysis of a typical single lap joint, carrying the same load. The stress-wet curve will be considered later. The high stress regions at the overlap ends in the elastic analysis cannot be sustained as the adhesive yields and thus are significantly reduced. Note however that the adhesive stresses in the middle of the overlap 1 Simple Lap Joint Geometry 80 70 Shear stress, MPa Fig. 1.18 Linear and non-linear adhesive shear stress distribution for a single lap joint 21 60 stress lin stress non-lin stress wet 50 40 30 20 10 0 0.00 6.25 12.50 Dist along overlap, mm are higher for the non-linear analysis as the total area under the shear stress-overlap curves must be the same as the same load is carried by both joints. Crocombe (2007) extended the non-linear analysis of arbitrary end loaded single overlaps (Bigwood and Crocombe, 1990) to consider the effect of environmental degradation. The coupling between the moisture concentration within the joint and the mechanical properties of the adhesive is treated in a similar way to that outlined in the section Design formulae for environmentally degraded single lap joints in Sect. 1.3 on design tools above. However the approach outlined here is not restricted to a limit state and can assess the adhesive joint at any given level of loading. This is a far more useful foundation for the assessment of service life of different joint configurations. Referring again to Fig. 1.14 the two step process is identified. Initially the moisture diffusion within the joint is determined using Fickian moisture uptake laws. Then the effect of the moisture on the constitutive response of the adhesive is modelled as shown schematically in Fig. 1.14. In the analysis this moisture dependent material response is implemented by making the parameters in the hyperbolic tangent model functions of moisture concentration (cm ) i.e. E(cm )ε σ = A(cm ) tanh (1.31) A(cm ) This essentially introduces an infinitely variable non-linear response for the adhesive. Experimental data has shown that it is very reasonable to assume a linear variation of modulus, E(cm ), and ultimate stress, A(cm ) between fully dry and fully saturated values and this has been implemented. However any variation could easily be incorporated. Figure 1.18 also shows the stress distribution in the single lap joint after exposure at 85% RH for 230 days (stress-wet). The moisture concentration at the ends of the overlap was high and has thus degraded the ultimate strength of the adhesive in this region. This is the reason that the stresses in this region are lower than the non-linear dry joint analysis. However, after only 230 days the centre of the joint is still relatively dry, and thus higher stresses, required to transfer the total joint load, can be sustained in this region. 22 Andrew D. Crocombe and Ian A. Ashcroft 1.5 Conclusion A range of analyses relevant to the adhesive lap joint have been presented. The basic mechanics of these joints have been outlined (Sects. 1.2 and 1.3) with a reasonably detailed discussion of some of the classic analyses. In these early analyses the substrates have been considered to carry only tension and bending and the adhesive has been considered as having only 2 stress components (peel and shear) which do not vary across the adhesive thickness. Section 1.3 details some analyses that have been developed to be readily useful in a design context to allow rapid assessment of the adhesive stress distribution. Results are presented in the form of design formulae and more general solutions can be easily implemented on spreadsheets. Much of the later closed form analyses have focused on a better representation of either the substrate and/or the adhesive stress distribution. The effect of these extensions is to increase the complexity of the analyses thus making it more difficult to obtain an analytical rather than numerical solution. Non-linear material behaviour for the adhesive has been discussed separately. A number of different approaches for incorporating this non-linear behaviour have been discussed and the most advanced also incorporates moisture dependency. Very little has been done by way of incorporating failure criteria into these closed form analyses. This is currently being done in FE modelling and it would be reasonable to expect that future developments of closed form analyses might include this capability. The advantage of this is that the simplicity of a closed form approach makes it very suitable for preliminary joint design assessment. References Adams RD and Mallick V (1992) A method for the stress analysis of lap joints. J Adhes 38: 199–217 Bigwood DA and Crocombe AD (1989) Elastic analysis and engineering design formulae for bonded joints. Intl J Adhes Adhes 9: 229–242 Bigwood DA and Crocombe AD (1990) Non linear adhesive bonded joint design analysis. Int J Adhes Adhes 10-1: 31–41 Chen D and Cheng S (1983) An analysis of adhesively bonded single lap joints. J Appl Mech, 50: 109–115 Crocombe AD (1989) Gobal yielding as a failure criteria for bonded joints. Int J Adhes Adhes 9(3): 145–153 Crocombe AD (2008) Incorporating environmental degradation in closed form adhesive joint stress analysis. J Adhes, in press Delale F, Erdogan F and Aydinoglu MN (1981) Stresses in adhesively bonded joints: a closed form solution. J Compos Mater 15: 249–271 Goland M and Reissner E (1944) The stresses in cemented joints. J Appl Mech 66: 17–27 Hart-Smith LJ (1973a) Adhesive bonded single lap joints, NASA report CR112235, Langley Research Centre Hart-Smith LJ (1973b) Adhesive bonded double lap joints. NASA report CR112236, Langley Research Centre 1 Simple Lap Joint Geometry 23 Ojalvo U and Eidinoff HL (1978) Bond thickness effects upon stresses in single-lap joints. AIAA 16(3): 204–211 Oplinger DW (1994) Effects of adherend deflections in single lap joints. Int J Solids Struct 31(18): 2565–2587 Renton WJ and Vinson JR (1977) Analysis of adhesively bonded joints between panels of composite materials. J Appl Mech 44: 101–106 Sawa T, Liu J, Nakano K and Tanaka J (2000) A two-dimensional stress analysis of single lap adhesive joints of dissimilar adherends subjected to tensile loads. J Adhes Sci Tech 14(1): 43–66 Tsai MY and Morton J (1994) An evaluation of analytical and numerical solutions to the single lap joint. Int J Solids Struct 31(18): 2537–2563 Tsai MY, Oplinger DW and Morton J (1998) Improved theoretical solutions for adhesive lap joints. Int J Solids Struct 35(12): 1163–1185 Volkersen O (1938) Die nietkraftverteilung in zugbeanspruchten nietverbindungen mit konstanten laschenquerschnitten. Luftfahrtforschung 15: 41–47 Volkersen O (1965) Recherches sur la theorie des assemblages colles. Construction Metallique 4: 3–13 Chapter 2 Analysis of Cracked Lap Shear (CLS) Joints Liyong Tong and Quantian Luo Abstract This chapter presents analytical models for cracked lap shear joints. Two analytical frameworks are introduced: (1) the overlap is treated as an entire beam to find displacements and force components of the cracked lap shear joints firstly, and then the adherends in the overlap region are treated as individual beams to find adhesive stresses and energy release rates; (2) individual beams are considered only; displacements, force components and adhesive stresses are determined simultaneously by solving the coupled differential equations. Geometrically-nonlinear features of cracked lap shear joints are investigated. Strength of materials and fracture mechanics based failure criteria are discussed. 2.1 Introduction Adhesive bonding technology has been used in aircraft structures over 70 years (Higgins 2000). In modern aeronautical and aerospace industries, this technology is widely employed to join similar and dissimilar materials to form load-bearing structural joints or integrated structures (Adams et al. 1997, Tong and Steven 1999). Adhesive bonding is especially effective to join thin metallic and/or laminated composite sheets. However, structural performance can be dramatically reduced by debonding or interface crack. It is known that debonding is mainly caused by high interface adhesive stresses, which typically exist at a free edge or terminating ends of adhesive layers and also exhibit singularity features. Liyong Tong School of Aerospace, Mechanical and Mechatronic Engineering, J11- Aeronautical Engineering Building, The University of Sydney, NSW 2006, Australia, e-mail: ltong@aeromech.usyd.edu.au Quantian Luo School of Aerospace, Mechanical and Mechatronic Engineering, J11- Aeronautical Engineering Building, The University of Sydney, NSW 2006, Australia, e-mail: qtluo@aeromech.usyd.edu.au L.F.M. da Silva, A. Öchsner (eds.), Modeling of Adhesively Bonded Joints, c Springer-Verlag Berlin Heidelberg 2008 25 26 L. Tong and Q. Luo Fig. 2.1 A cracked lap shear specimen (ASTM round robin) 305 mm 254 mm c Strap adherend P P A a Lap adherend B l Due to the presence of both shear and peel stresses in an adhesive layer, fracture in adhesive or near an adhesive-adherend interface in an adhesive joint is generally a mixed-mode problem. To characterize such adhesive fracture behavior, a number of test specimens have been proposed (Mangalgiri and Johnson 1986, Rao and Acharya 1995, Alif et al. 1997). A cracked lap shear (CLS) specimen in mixedmode condition is one of the specimens that has been widely used for characterizing fracture toughness and studying fracture behavior of adhesively bonded joints. It can also be used to simulate delamination of composite laminate and skin-flange debonding used in practical engineering structures. An ASTM round robin (Johnson 1986) was conducted for calculating energy release rates of the CLS specimen as schematically shown in Fig. 2.1. The CLS specimen is assumed to have a width of 25 mm and a varying debond length a. In general, a CLS specimen subjected to tensile loading can have four possible combinations of support conditions at both ends (Johnson 1986, Lai et al. 1996), namely, (1) clamped-clamped, (2) roller-clamped, (3) roller-roller (similar to single lap joint), and (4) free-fixed. One distinctive feature of the CLS is the eccentric loading path that leads to geometrical nonlinearity (Johnson 1986), and thus large deflections have to be considered in analytical and numerical analyses. 2.2 Background The cracked lap shear specimen was firstly proposed by Brussat et al. (1977) to investigate the mixed mode fracture behavior of shear-loaded adhesive joints. The CLS have been used to study adhesive joint debonding (Brussat et al. 1977, Lin and Liechti 1987, Schmueser and Johnson 1990, Cheuk and Tong 2002) and composite delamination (Mangalgiri and Johnson 1986, Rhee 1994, Rhee and Chi 2001). Johnson (1986) reported the ASTM round robin results conducted by nine groups or laboratories. This work was sponsored by ASTM and all participants were asked to calculate the energy release rate of the CLS specimens with four different debond lengths and two different geometries. It was indicated that, although no generally applicable closed-form solutions exist for the CLS specimen, the nonlinear finite element analysis gives the lab-to-lab consistent predictions with the observed experimental behaviors. 2 Analysis of Cracked Lap Shear (CLS) Joints 27 Analytical analysis for the CLS has attracted much attention in past several decades to sight into its essence. The analytical solutions may be obtained by modeling adherends as beams and the adhesive as a continuous spring with shear and peel stiffness. A spring model for the adhesive is widely used due to the facts that its Young’s modulus is much smaller than that of the isotropic adherends, and it is normally very thin as compared to the adherends. Brussat et al. (1977), Fernlund and Spelt (1991a), Fernlund et al. (1994), and Lai et al. (1996) presented analytical analyses for the CLS specimen using the method developed by Goland and Reissner (1944) for a single lap joint. In this method, the overlap is treated as an entire beam to determine the deflections of the adhesively bonded structure and the force components at the end of the overlap as shown in Fig. 2.2. In the light of the found CLS deflections and the overlap force components, the adhesive stresses and/or energy release rates of the interface crack can then be calculated to predict the CLS failure loads. This method divides analysis into two steps and treats the overlap adherends as an entire or one single beam in the first step and then as two separated sub-beams in the second step (Goland and Reissner 1944). An alternative way is to combine the two steps into one and only the two separated sub-beam model for the overlap adherends is used. This coupled formulation was proposed by Hart-Smith (1973) and has been also widely used for analytical analysis of the CLS specimen. However, the overlap large deflection is not included in this coupled method. Recently, Luo and Tong (2007) presented fully coupled formulations for a single lap joint, in which adherends of the overlap are treated as two individual beams each undergoing large deflections. The adhesive stresses/energy release rates and the force components at the end of the overlap were determined simultaneously. Experimental testing is an essential tool for validating various analyses for the CLS specimen. Not only the analytical results are required to be verified by experiments, but also the experimental test is the unique way to determine the fracture toughness of the adhesive joint to establish the fracture envelope for the CLS specimen. The experimental investigations of the CLS specimen have been conducted by a number of authors, e.g., Fernlund and Spelt (1991b), Papini et al. (1994), Wang l MA F c Outer adherend Overlap MB F RA RB Qk Mk Nk I MB F (t1+t2+ta)/2 I RB Fig. 2.2 Loadings, reaction forces and forces in cross-section I-I 28 L. Tong and Q. Luo et al. (1995), Benzeggaph and Kenane (1996), Rhee and Chi (2001), Rhee et al. (2003), Cheuk and Tong (2002). Both adhesive debonding and composite delamination have been tested in most of these experiments. A noticeable experimental test was conducted by Fernlund and Spelt (1994) as the fracture toughness is obtained for a full range of mode ratios. Dattaguru et al. (1984) initially used geometrically nonlinear finite element analysis (NFEA) to numerically investigate the CLS. In the report presented by Johnson (1986), both linear and nonlinear FEA analyses were conducted. It was concluded that geometrically nonlinear FEA had to be used for the CLS specimen. The FEA modeling of the CLS specimen may be classified into two types: a full 2D (or full 3D) model and a beam (or plate) model with adhesive elements. In the full 2D (or full 3D) model, 2D (or 3D) elements are used to model both adherends and adhesive. A full 3D FEA is an effective tool for the CLS specimen. However, it is well known that it can be computationally expensive and may even encounter numerical difficulty for beam-type and plate/shell-type structures. As concerned about a beam model with adhesive elements, Carpenter (1973, 1980) developed a constant shear and extensional spring element for adhesive idealization. Kuo (1984) developed a continuous spring element with shear stiffness. Luo and Tong (2004) derived a continuous spring element with shear and peel stiffness. These two types of FEA models for adhesive joints can also be combined. Ko et al. (1994) used the weighted adhesive plate element for the CLS specimen, Wu and Crocombe (1996) used beam elements to model the adherends and 2D elements to depict the adhesive. With the development of commercial FEA software, full 2D (or full 3D) models have been widely used (Wu and Crocombe 1996, Cheuk and Tong 2002, Yang et al. 2003, Luo and Tong 2007). When NFEA is used for the CLS analysis, energy release rates (ERR) and/or stress intensity factors are required to be calculated when the fracture mechanics based failure criteria are used. In this case, virtual crack closure technique (VCCT) (Harbert and Hogan 1992, Rhee and Ernst 1993, Panigrahi and Pradhan 2007, Yang et al. 2007) has been widely used. 2.3 Fundamental Formulations In this section, the fundamentals of analytical solutions for the CLS specimen will be discussed. Two theoretical frameworks mentioned in Sect. 2.2 will be discussed in details: (1) the CLS deflections and the force components at the overlap end are determined firstly and then the adhesive stresses and/or energy release rates (ERRs) are calculated, and (2) the CLS displacements, the overlap forces and the adhesive stresses/ERRs are determined simultaneously. In the first analytical framework, analytical analysis for the cracked lap shear consists of two parts: (1) find deflections of the CLS specimen and the force components at the overlap end by taking into account large deflections as shown in Fig. 2.2, and (2) stress analysis and/or ERR calculation for failure prediction. 2 Analysis of Cracked Lap Shear (CLS) Joints 29 The force components at the overlap end include the applied force F, reaction force RB and moment MB and forces in cross-section I-I: axial force Nk , shear force Vk (or Qk ) and bending moment Mk , where Vk is the transverse shear force perpendicular to the deformed beam axis and Qk is that perpendicular to the un-deformed beam axis. The key force component is the edge bending moment Mk at the overlap end as the other components of cross-section I-I may be found by the equilibrium equations or the differential relations of internal forces based on the beam theory. The bending moment at the adhesive edge can be defined as: t2 + ta Mk = kF (2.1) 2 where k is the edge moment factor; t2 and ta are thicknesses of the lap adherend and the adhesive. It is noted that (t2 + ta /2) is the distance of two horizontal forces (see Fig. 2.2), and when t1 = t2 = t, definitions of the edge moment and its factor in Eq. (2.1) are consistent with those of Goland and Reissner (1944) for a single lap joint. The edge moment of a cracked lap shear specimen can be found on the basis of the method proposed by Goland and Reissner (1944), who treated the overlap as an entire Euler beam. In the light of this model, Fernlund et al. (1994) determined the edge moment and the CLS deflections for calculating the value of J-integral. Lai et al. (1996) also used this method to find the overlap force components and then calculated the ERRs for the CLS specimen. After determining the CLS deflections and the overlap force components, the adhesive stresses can be solved based on the formulations developed by Goland and Reissner (1994), and the energy release rates can be calculated by using the J-integration with the mode partition (Fernlund and Spelt 1991a, Fernlund et al. 1994) and the interface crack theory (Suo and Hutchinson 1990, Lai et al. 1996). In the second analytical framework, fully-coupled equations are treated. The edge moment, displacements and the adhesive stresses were solved at the same time. This framework has been used to analyze the CLS with the roller-roller boundary condition (SLJ) by Hart-Smith (1973), Oplinger (1994), and Luo and Tong (2007). In the Hart-Smith model (1973), large deflections of the overlap were not considered. In the Oplinger’s model (1994), large deflections of the overlap coupled with the adhesive shear stress but not peel stress were considered. Luo and Tong (2007) considered large deflections with coupled both shear and peel stresses. The formulation of the second framework can also be extended to the CLS with the other boundary conditions using the same procedure. 2.3.1 Basic Equations for the Outer Adherend and Reaction Forces To find the CLS displacements and the overlap force components, we need to consider the equilibrium, constitutive and continuity conditions of the CLS specimen. 30 L. Tong and Q. Luo The free body diagrams of the CLS specimen and the overlap are shown in Fig. 2.2. The applied force F is the horizontal component of load P. The equilibrium equations of the CLS specimen are: RB + RA = 0 MB − MA + F t2 + ta 2 (2.2) − RA (l + c) = 0 (2.3) In the first framework, deflections of the CLS specimen are schematically illustrated in Fig. 2.3. The bending moment of the outer adherend and the overlap is respectively: M3 (x3 ) = −Fw3 + RA x3 + MA Mo (xo ) = −Fwo − RB xo + MB 0 ≤ x3 ≤ l −c ≤ xo ≤ 0 (2.4) (2.5) The constitutive relations of the outer adherend and the overlap based on the Euler beam are: d 2 w3 d 2 wo (2.6) M3 = −D11 2 ; Mo = −Do 2 dxo dx3 where D11 and Do are bending stiffness of the outer adherend and the overlap. Substituting Eq. (2.6) into Eqs. (2.4) and (2.5) yields: RA MA x3 + F F RB MB wo = B1 sinh βo xo + B2 cosh βo xo − xo + F F w3 = A1 sinh βk x3 + A2 cosh βk x3 + (2.7) (2.8) In Eqs. (2.7) and (2.8), A1 , A2 , B1 and B2 are the unknown integration constants, which are to be determined by using the relevant boundary conditions; and the eigenvalues are: F F βk = ; βo = (2.9) D11 Do It is noted that, in Eqs. (2.7) and (2.8), there are 4 integration constants and 4 reaction force components to be determined. To find the 8 unknowns, we need to have 8 independent equations. By the support conditions at A and B, 4 boundary RA F x3 M3 MA N3 Qo RB F xo z3 Q3 No MB Mo zo Fig. 2.3 Deflections and coordinate systems of the CLS specimen 2 Analysis of Cracked Lap Shear (CLS) Joints 31 equations can be derived; 2 equilibrium equations are given in Eqs. (2.2) and (2.3); the other 2 equations are obtained by the continuity conditions at cross-section I-I. The continuity conditions at cross section I-I can be written as: u3 (l) = uo (−c); w3 (l) = wo (−c); dw3 (l) dwo (−c) = dx3 dxo (2.10) Equation (2.10) is the general requirements of deformation continuity; the axial continuity condition was not used for the formulation based on the method of Goland and Reissner (1944). The 4 integration constants and the 4 unknowns RA , MA , RB and MB can be found by the 4 boundary condition equations that will be discussed in Subsection 2.3.3 and the 4 equations given in Eqs. (2.2), (2.3) and (2.10). Therefore, the CLS deflections are solved and then the edge moment Mk the edge shear force Vk are found by: Mk = −D11 d 2 w3 (l) ; dx32 Vk = dM3 (l) dx3 (2.11) When the CLS deflections and force components of the overlap are solved, adhesive stresses and the ERRs can then be found. 2.3.2 Basic Equations for the Overlap and Adhesive Stresses When upper and lower adherends are identical, or symmetrical adherends, solutions of the shear and peel stresses for the prescribed force boundary conditions of the overlap were presented by Goland and Reissner (1944). For the asymmetrical adherends, solutions of the adhesive stresses can be found in Luo and Tong (2002). In this chapter, we only present adhesive stress analysis for the symmetrical adherends and introduce the following variables: ⎧ ⎪ ⎨2us = u2 + u1 ; 2ws = w2 − w1 ; 2ua = u2 − u1 ; 2wa = w2 + w1 2Ns = N2 + N1 ; 2Qs = Q2 − Q1 ; 2Ms = M2 − M1 ⎪ ⎩ 2Na = N2 − N1 ; 2Qa = Q2 + Q1 ; 2Ma = M2 + M1 (2.12) The variables in Eq. (2.12) have the usual meanings used in the Euler beam theory; subscripts 1 and 2 refer to identical adherends 1 and 2 in the overlap region; the force components are shown in the free body diagrams of the infinitesimal elements, see Fig. 2.4. The equilibrium equations of adherends 1 and 2 in the overlap can be derived from Fig. 2.4, as: 32 L. Tong and Q. Luo Fig. 2.4 Free body diagram for stress analysis of adhesive joints M1 M1+dM1 N1 Adherend 1 Q1 σ z σ τ N1+dN1 Q1+dQ1 τ Adhesive τ τ M2 N2 x M2+dM2 N2+dN2 Adherend 2 Q2 Q2+dQ2 dx ⎧ dN ⎪ ⎪ 1 + τ = 0; ⎨ dx ⎪ ⎪ dN2 ⎩ − τ = 0; dx dQ1 + σ = 0; dx dM1 t1 + τ − Q1 = 0 dx 2 dQ2 − σ = 0; dx dM2 t1 + τ − Q2 = 0 dx 2 (2.13) In Eq. (2.13), τ and σ are the adhesive shear and peel stresses, whose definitions are given by Goland and Reissner (1944): τ= Ga t1 dw1 dw2 + ) ; (u2 − u1 ) + ( ta 2 dx dx σ= Ea (w2 − w1 ) ta (2.14) In Eq. (2.14), Ea and Ga are Young’s and shear moduli of the adhesive. By making use of the variables in Eq. (2.12), Eqs. (2.13) and (2.14) become: ⎧ dNs dQs dMs ⎪ ⎪ − σ = 0; − Qs = 0 ⎨ dx = 0; dx dx ⎪ ⎪ ⎩ dNa − τ = 0; dQa = 0; dMa + t1 τ − Qa = 0 dx dx dx 2 2Ga t1 dwa 2Ea ws τ= ua + ; σ= ta 2 dx ta (2.15) (2.16) The constitutive relations of the Euler beam are: N = A11 du ; dx M = −D11 d2w dx2 (2.17) where A11 is the extensional stiffness of the adherends. It is noted that shear and peel stresses have been decoupled in Eq. (2.15), in which, the 1st and the 2nd row of equations can be used to solve the peel stress and 2 Analysis of Cracked Lap Shear (CLS) Joints 33 shear stress respectively. By substituting Eq. (2.17) into (2.15), and then substituting ua , wa and ws into Eq. (2.16), the governing differential equations for the shear and peel stresses can be obtained as follows: d3τ 2Ga − dx3 A11ta 1+ A11t12 4D11 dτ = 0; dx d4σ 2Ea + σ =0 dx4 D11ta (2.18) The analytical solutions of Eqs. (2.18) are: ⎧ ⎪ ⎨τ = A1 sinh βa x + A2 cosh βa x + A3 σ = B1 sinh βσ x sin βσ x + B2 sinh βσ x cos βσ x ⎪ ⎩ +B3 cosh βσ x sin βσ x + B4 cosh βσ x cos βσ x (2.19) In Eq. (2.19), Ai (i = 1, 2, 3) and B j ( j = 1, 2, 3, 4) are the integration constants, and the eigenvalues are: ⎧ ⎪ 2 2 ⎪ ⎪ ⎨βa = αa βτ ; βτ = ⎪ ⎪ (1 + αk ) ⎪ ⎩αa = ; 4 8Ga ; A11ta √ 2 4 2Ea βσ = 2 D11ta A11t12 αk = 4D11 (2.20) where coefficients αa and αk may reflect influence of the lay-up sequence when the overlap adherends are composite laminates with the symmetrical lay-up. For the isotropic adherends, αa = 1 and αk = 3. The integration constants in Eq. (2.19) can be determined by the prescribed force boundary conditions of the overlap, and the force components of the overlap are dependent on loadings, support conditions and geometrical configurations of the CLS specimen. In this analytical method, large deflections are considered to find the force components of the overlap but not for the adhesive stresses. The entire beam model and the sub-beam model are applied to the overlap force determination and the adhesive stress analysis respectively. Hart-Smith (1973) presented the coupled formulations for a single lap joint. By substituting Eqs. (2.16) and (2.17) into Eq. (2.15), the governing differential equations for adherend displacements can be obtained: d 4 ws 2Ea d 2 us = 0; D11 4 + ws = 0 2 dx dx ta ⎧ 2 d ua 2Ga t1 dwa ⎪ ⎪ − + u =0 ⎪ a ⎨ dx2 A11ta 2 dx ⎪ d 4 wa ⎪ Gat1 dua t1 d 2 wa ⎪ ⎩− + + =0 dx4 D11ta dx 2 dx2 (2.21) (2.22) 34 L. Tong and Q. Luo Equations (2.21) and (2.22) can be analytically solved, whose integration constants are solved by boundary conditions of the overlap. The solved integration constants include unknowns: edge bending moment Mk and rigid body motions. These unknowns should be solved by the continuity conditions at I-I and support conditions of the CLS specimen. It is noted that all the 3 continuity equations given in Eq. (2.10) will be used in this coupled formulations. To use the continuity condition with respect to the axial deformation, the axial displacement of the outer adherend needs to be used. It can be solved by referring to Fig. 2.3 and the constitutive relations, which are given by: F x3 +C1 (2.23) u3 = A11 where C1 is the integration constant. Because large deflections of the overlap are not included in adhesive stress analysis presented in Eq. (2.13) and the solutions given in Eq. (2.19), the analytical solutions of Hart-Smith (1973) do not model the overlap large deflection. By analyzing the Goland and Reissner’s formulation (1944) and the Hart-Smith’s one (1973), the former considered large deflections of the overlap but ignored adhesive deformation, whereas the latter considered shear and peel strains but neglect the overlap large deflections. Recently, Luo and Tong (2007) presented the fully-coupled nonlinear analysis for SLJs, in which, both large deflections and adhesive deformations are modeled. In this method, equilibrium equations of the infinitesimal adherend elements are derived on the basis of the geometrically nonlinear analysis. As shown in Fig. 2.5, the equilibrium equations for the free body diagrams are: ⎧ dw1 dx ⎪ ⎪ dN1 + τ (ds1 ) dx = 0 = 0; dQ1 + σ (dx) + τ ⎪ ⎪ ds1 dx ⎪ ⎪ ⎪ ⎪ ⎪ ⎪ ⎪dM1 + t1 τ (dx) − Q1 dx = −N1 dw1 dx ⎪ ⎨ 2 dx ⎪ dw2 dx ⎪ ⎪ ⎪ ⎪dN2 − τ (ds2 ) ds = 0; dQ2 − σ (dx) − τ dx dx = 0 ⎪ 2 ⎪ ⎪ ⎪ ⎪ ⎪ ⎪ ⎩dM2 + t1 τ (dx) − Q2 dx = −N2 dw2 dx 2 dx (2.24) where, (ds1 )2 = (dx)2 + (dw1 )2 and (ds2 )2 = (dx)2 + (dw2 )2 . By using the variables in Eq. (2.12), the equilibrium equations become: ⎧ dN s ⎪ =0 ⎪ ⎪ ⎪ dx ⎨ dQs dwa ⎪ −σ −τ = 0; ⎪ ⎪ dx dx ⎪ ⎩ dMs dws dwa − Qs = −Ns − Na dx dx dx (2.25) 2 Analysis of Cracked Lap Shear (CLS) Joints Fig. 2.5 Free body diagram for nonlinear analysis of adhesive joints 35 M1 N1 Q1 M1 + dM1 N1 + dN1 Q1 + dQ1 Adherend 1 σ τ z M2 N2 τ τ x dw1/dx Adhesive σ τ M2 + dM2 N2 + dN2 Adherend 2 Q2 Q2 + dQ2 dx ⎧ dNa ⎪ ⎪ ⎪ ⎨ dx − τ = 0 ⎪ ⎪ ⎪ ⎩ dQa − τ dws = 0; dx dx (2.26) dMa t1 dwa dws + τ − Qa = −Ns − Na dx 2 dx dx The nonlinear constitutive relations of the Euler beam are: ⎧ ⎪ d2w du 1 du 2 1 dw 2 ⎪ ⎪ N = A + + − B ⎪ 11 11 ⎪ dx 2 dx 2 dx dx2 ⎨ ⎪ ⎪ d2w du 1 du 2 1 dw 2 ⎪ ⎪ + M = B + − D ⎪ 11 11 ⎩ dx 2 dx 2 dx dx2 (2.27) where the coupling extension and bending stiffness B11 is equal to zero for the symmetrical cross section. In Eqs. (2.16) and (2.25), (2.26), (2.27), 12 equations consists of 12 variables: 6 stress resultants and 4 adherend displacements plus shear and peel stresses. In Eqs. (2.25) and (2.26), differentiating the bending moment equilibrium equations, into which, substituting the shear force equations, and utilizing the axial force equilibrium equations, we have: d 2 ws d 2 wa d 2 Ms − σ = −Ns 2 − Na 2 2 dx dx dx (2.28) d 2 Ma t1 d τ d 2 wa d 2 ws = −N + − N s a dx2 2 dx dx2 dx2 (2.29) When the following higher order nonlinear terms are ignored: dua d 2 ws dx dx2 dua d 2 wa dx dx2 (2.30) 36 L. Tong and Q. Luo The simplified equilibrium equations including effects of the overlap large deflections can be obtained: dNs = 0; dx d 2 Ms F d 2 ws −σ = − 2 dx 2 dx2 dNa − τ = 0; dx (2.31) F d 2 wa d 2 Ma t1 d τ =− + 2 dx 2 dx 2 dx2 (2.32) In Eqs. (2.31) and (2.32), the relation Ns = (N1 + N2 )/2 = F/2 has been used. In the definitions of adhesive shear and peel strains of Eq. (2.14), small strains and rotations of the adherends are assumed. By using this assumption, higher order terms in Eq. (2.27) can be neglected. Utilizing Eq. (2.12), we have: Ni = A11 dui dx Mi = −D11 d 2 wi dx2 (i = s, a) (2.33) By substituting Eqs. (2.16) and (2.33) into Eqs. (2.31) and (2.32), the following governing equations in terms of displacements of adherends in the overlap region of the CLS specimen can be obtained: ⎧ 2 d us ⎪ ⎪ ⎨ dx2 = 0; 4 2 ⎪ ⎪ ⎩D11 d ws − F d ws + 2Ea ws = 0 4 dx 2 dx2 ta (2.34) ⎧ d 2 ua 2Ga t1 dwa ⎪ ⎪ ⎪ A − ua + =0 ⎪ ⎨ 11 dx2 ta 2 dx ⎪ ⎪ d 4 wa Gat1 dua t1 d 2 wa F d 2 wa ⎪ ⎪ + =0 + ⎩−D11 4 + dx ta dx 2 dx2 2 dx2 (2.35) From a mathematical viewpoint, Eqs. (2.34) and (3.35) are linear differential equations for the given axial load F, and can be analytically solved. The closed-form solutions of Eqs. (3.34) and (3.35) are (Luo and Tong 2008): ⎧ ⎪ ⎨us = As1 x + As2 ws = (Bs1 sinh βs1 x + Bs2 cosh βs1 x) sin βs2 x ⎪ ⎩ +(Bs3 sinh βs1 x + Bs4 cosh βs1 x) cos βs2 x ⎧ ua = Aa1 sinh βa1 x + Aa2 cosh βa1 x ⎪ ⎪ ⎪ ⎨ +Aa3 sinh βa2 x + Aa4 cosh βa2 x + Aa5 ⎪wa = Ba1 sinh βa1 x + Ba2 cosh βa1 x ⎪ ⎪ ⎩ +Ba3 sinh βa2 x + Ba4 cosh βa1 x + Ba5 x + Ba6 (2.36) (2.37) 2 Analysis of Cracked Lap Shear (CLS) Joints 37 where, As1 , As2 , Bsi (i = 1, 2, 3, 4), Aa1 and Ba j (i = 1, 2, · · ·, 5; j = 1, 2, · · ·, 6) are the integration constants, which are determined by the boundary conditions. The eigenvalues are respectively (Luo and Tong 2008): βs1 = βσ2 + βk2 , 8 βs2 = βσ2 − βk2 8 (2.38) ⎧ ⎪ βk2 β4 1 1 ⎪ 2 2 2 β 4 + (α − )β 2 β 2 + k ⎪ + β = α β + α a a ⎪ a τ τ τ a1 k ⎪ 2 2 2 4 ⎪ ⎨ ⎪ ⎪ ⎪ βk2 1 1 2 2 βk4 ⎪ ⎪ 2 2 2 4 ⎪ ⎩βa2 = 2 αa βτ + 2 − αa βτ + (αa − 2 )βτ βk + 4 (2.39) For the case of isotropic adherends, Eq. (2.39) degenerates: ⎧ ⎪ βk2 βτ2 βk2 βk4 1 ⎪ 2 2 4 ⎪βa1 = + βτ + + βτ + ⎪ ⎪ 2 2 2 4 ⎪ ⎨ ⎪ ⎪ ⎪ βk2 βτ2 βk2 βk4 1 ⎪ ⎪ 2 2 4 ⎪ ⎩βa2 = 2 βτ + 2 − βτ + 2 + 4 (2.39a) By using the overlap boundary conditions, the integration constants with the unknowns of the edge moment and the rigid body motions can be solved. The unknowns can be solved by the continuity conditions in Eq. (2.10) and the support conditions. It can be seen that, in the second analytical framework of the coupled nonlinear analysis, large deflections of the outer adherend and the overlap, and the adhesive deformations have been considered. The CLS displacements, force components and adhesive stresses can be simultaneously solved. 2.3.3 Boundary Conditions, Loading Cases and Analytical Solution 2.3.3.1 Boundary Conditions To analytically solve the CLS for the 4 possible boundary conditions of the CLS, we first derive the boundary equations in terms of the displacements (Johnson 1986, Lai et al. 1996): (1) Clamped-Clamped w3 (0) = 0; dw3 (0) dwo (0) = 0 and wo (0) = 0; =0 dx3 dxo (2.40) 38 L. Tong and Q. Luo (2) Roller-Clamped w3 (0) = 0; MA = 0 and wo (0) = 0; dwo (0) =0 dxo (2.41) (3) Roller-Roller (equivalent to single lap joint) w3 (0) = 0; MA = 0 and wo (0) = 0; MB = 0 or d 2 wo (0) =0 dxo2 (2.42) (4) Free-Fixed MA = 0; RA = 0 and wo (0) = 0; dwo (0) =0 dxo (2.43) 2.3.3.2 Loading Cases The CLS specimen is subjected to a pair of tensile forces (P) in the experimental test, as shown in Fig. 2.1. The axial force F in Fig. 2.2 is the project of P in the horizontal direction, which is given by: F= (l + c) P (2.44) (l + c)2 + [(t2 + ta )/2]2 The loading cases for the CLS testing specimen are illustrated in Fig. 2.2. In this chapter, we present analytical analysis for the CLS specimen subjected to the tensile force only. For engineering structures with lap shear joints, they may be subjected to transverse forces and bending moments, whose solutions can be found using the similar procedure. 2.3.3.3 The 1st Step Solutions of the 1st Analytical Framework In the 1st analytical framework, solution procedures of the 1st step are to determine the 8 unknowns in Eqs. (2.7) and (2.8) using the 8 equations given in Eqs. (2.2), (2.3), (2.10) and (2.40) or (2.41) or (2.42) or (2.43). Lai et al. (1996) derived force components of the overlap for the boundary conditions of Clamped-Clamped and Roller-Clamped. Goland and Reissner (1944) derived the edge moment for the Roller-Roller boundary conditions and the symmetrical substrates. The consistent formulations for the general CLS with the 4 possible boundary conditions are presented below. (1) Clamped-Clamped: Substituting Eq. (2.40) into Eqs. (2.7) and (2.8) and combining Eqs. (2.2) and (2.3), we have: 2 Analysis of Cracked Lap Shear (CLS) Joints ⎧ MA RA MB RB ⎪ ⎪ ⎨A2 + F = 0; βk A1 + F = 0; B2 + F = 0; βo B1 − F = 0 ⎪ ⎪ ⎩B1 = βk A1 ; B2 = A2 + A1 βk (l + c) + t2 + ta βo 2 39 (2.45) By utilizing Eq. (2.45), Eqs. (2.7) and (2.8) become: w3 = A1 (sinh βk x3 − βk x3 ) + A2 (cosh βk x3 − 1) βk (sinh βo xo − βo xo ) + βk (l + c) (cosh βo xo − 1) βo t2 + ta (cosh βo xo − 1) + A2 (cosh βo xo − 1) + 2 (2.46) wo = A1 (2.47) By substituting Eqs. (2.46) and (2.47) into Eq. (2.10), the following algebraic equations can be obtained: ⎧ A1 [βk βo (l + c) cosh βo c − βk sinh βo c − βo sinh βk l] ⎪ ⎪ ⎪ ⎪ ⎨ +A β (cosh β c − cosh β l) = t2 +ta β (cosh β c − 1) o o o 2 o k 2 ⎪ A1 [βk (cosh βo c − cosh βk l) − βk (l + c) sinh βo c] ⎪ ⎪ ⎪ ⎩ a −A2 (βk sinh βk l + βo sinh βo c) = t2 +t 2 βo sinh βo c (2.48) The integration constants A1 and A2 are readily solved from Eq. (2.48), and then B1 , B2 , RA , RB , MA and MB are obtained by Eq. (2.45). Since deflections and reaction force components are determined, the edge moment is found from Eq. (2.11) (2) Roller-Clamped: Substituting Eq. (2.41) into Eqs. (2.2), (2.3), (2.7) and (2.8) yields: ⎧ RB RA MB ⎪ ⎪ ⎨A2 = 0; B2 + F = 0; F = − F = βo B1 ⎪ ⎪ ⎩ MB = −βo B1 (l + c) − t2 + ta F 2 (2.49) Substituting Eq. (2.49) into Eqs. (2.7) and (2.8), we have: w3 = A1 sinh βk x3 − βo B1 x3 wo = B1 [(sinh βo x0 − βo xo ) + βk (l + c) (cosh βo xo − 1)] t2 + t a + (cosh βo xo − 1) 2 (2.50) (2.51) A set of equations used to determine the integration constants can be obtained by substituting Eqs. (2.50) and (2.51) into Eq. (2.10): 40 L. Tong and Q. Luo ⎧ t2 + ta ⎪ ⎪ ⎨A1 βk cosh βk l + B1 βo [βo (l + c) sinh βo c − cosh βo c] = − 2 βo sinh βo c ⎪ ⎪ ⎩A1 sinh βk l + B1 [sinh βo c − βo (l + c) cosh βo c] = t2 + ta (cosh βo c − 1) 2 (2.52) By solving Eq. (2.52), the integration constants A1 and B1 are determined and then B2 , RA , RB and MB are obtained by Eq. (2.49). The deflections and reaction forces for the CLS are determined. (3) Roller-Roller: Substituting Eq. (2.42) into Eqs. (2.2), (2.3), (2.7) and (2.8), we have: RA = −RB = α F; A2 = 0; B2 = 0 where, α = t2 + ta 2(l + c) (2.53) Equations (2.7) and (2.8) become: w3 = A1 sinh βk x3 + α · x3 (2.54) wo = B1 sinh βo xo + α · xo (2.55) By substituting Eqs. (2.54) and (2.55) into Eq. (2.10), the integration constants A1 and B1 are obtained: ⎧ βo (t2 + ta ) cosh βo c ⎪ ⎪ A =− ⎪ ⎨ 1 2 (βo sinh βk l cosh βo c + βk cosh βk l sinh βo c) (2.56) ⎪ ⎪ βk (t2 + ta ) cosh βk l ⎪ ⎩B1 = − 2 (βo sinh βk l cosh βo c + βk cosh βk l sinh βo c) The edge moment can be found from Eqs. (2.11), (2.54) and (2.56), and the edge moment factor is given by: k= 1 1 = βk Do D11 1 + tanh βo c coth βk l 1+ tanh βk c coth βk l βo D11 Do (2.57) When t1 = t2 = t and ta << t (i.e., D0 = 8D11 ), Eq. (2.57) becomes: k= √ 1 + 2 2 tanh 1 βk c √ coth βk l 2 2 (2.58) Equation (2.58) was recovered from the formulations of Goland and Reissner (1944) by Tsai and Morton (1994). It is noted that the edge moment factor given by Goland and Reissner (1944) is the simplified one for the long outer adherend (βk l >> 1). 2 Analysis of Cracked Lap Shear (CLS) Joints (4) Free-Fixed: Combining Eq. (2.43) with Eqs. (2.2), (2.3), (2.7), (2.8), we have: t2 + ta t2 + ta RB = 0; MB = −F ; B1 = 0; B2 = 2 2 41 (2.59) Equations (2.7) and (2.8) become: w3 = A1 sinh βk x3 + A2 cosh βk x3 wo = t2 + ta (cosh βo xo − 1) 2 (2.60) (2.61) The integration constants A1 and A2 are readily determined By Eqs. (2.10), (2.60) and (2.61): ⎧ βo t2 + ta ⎪ ⎪ sinh βk l (cosh βo c − 1) + cosh βk l sinh βo c ⎪ ⎨A1 = − 2 βk (2.62) ⎪ + t β t ⎪ a o 2 ⎪A2 = cosh βk l (cosh βo c − 1) + sinh βk l sinh βo c ⎩ 2 βk The edge moment factor is: D11 k = − cosh βk c − 1 D0 (2.63) 2.3.3.4 Adhesive Stresses When the CLS deflections and the overlap force components are solved, the adhesive stresses and the energy release rates (ERR) can be calculated. The ERR calculations will be discussed in Sect. 2.5. The large deflections of the overlap are not included for the adhesive stress analysis in the 1st analytical framework based on the method of Goland and Reissner (1944) and the 2nd formulation framework based on the approach of HartSmith (1973). For the prescribed force boundary conditions, the same adhesive stresses are obtained based on the formulations of Goland and Reissner (1944) and Hart-Smith (1973). For the symmetrical CLS with the roller-roller boundary conditions, shear and peel stresses are: ⎧ βτ (Ft1 + 6Mk ) cosh βτ x 3(Ft1 − 2Mk ) ⎪ ⎪ + ⎪τ = ⎨ 8t1 sinh βτ c 8t1 c (2.64) ⎪ 2βσ2 (Bσ 1 sinh βσ x sin βσ x + Bσ 4 cosh βσ x cos βσ x) ⎪ ⎪ ⎩σ = sinh 2βσ c + sin 2βσ c 42 L. Tong and Q. Luo where, ⎧ Vk ⎪ ⎪ ⎨Bσ 1 = Mk (sinh βσ c cos βσ c + cosh βσ c sin βσ c) + βσ sinh βσ c sin βσ c ⎪ ⎪ ⎩Bσ 4 = Mk (sinh βσ c cos βσ c − cosh βσ c sin βσ c) + Vk cosh βσ c cos βσ c βσ (2.65) The maximum shear and peel stresses are: ⎧ 1 ⎪ ⎪ ⎪ ⎨τmax = 8 [(3k1 + 1) βτ coth βτ c + 3 (1 − k1 )] F ⎪ βk ⎪ ⎪ coth βk l βσ2 Mk ⎩σmax = 1 + βσ (2.66) where k1 = (1 + ta )k t1 (2.67) Adhesive stresses shown in Eqs. (2.64) and (2.66) were presented by Goland and Reissner (1944), and then Hart-Smith (1973). Because they are derived on the basis of Fig. 2.4, large deflection effects of the overlap are not included (Tsai and Morton 1994). In the 2nd analytical framework of the fully-coupled nonlinear analysis, the analytical solutions of the CLS specimen are found for the roller-roller boundary conditions (SLJ) and symmetrical adherends in the existing literatures (Luo and Tong 2007). The simplified analytical solutions for the edge moment factor and the maximum adhesive stresses are: βτ c f (βa2 c) − 1 8βτ c(1 + ta /t1 ) k= 1 βτ c f (βa2 c) + 3 + 1 + (βk c) coth βk l + (βk c)2 2βσ c 8βτ c (2.68) ⎧ 1 ⎪ ⎪ ⎪ ⎨τmax = 8 [(3k1 + 1) βa1 coth βa1 c + 3 (1 − k1 ) βa2 coth βa2 c] F ⎪ βk ⎪ ⎪ coth βk l βσ2 Mk ⎩σmax = 1 + βσ (2.69) 1 + (βk c)2 where, f (βa2 c) = βa2 c coth βa2 c − 1 (βa2 c)2 (2.70) The analytical solutions based on the fully-coupled nonlinear formulations can also be applied to the symmetrical CLS specimen with other boundary conditions. 2 Analysis of Cracked Lap Shear (CLS) Joints 43 By comparing the edge moment factor and the maximum adhesive stresses for the analytical framework of Goland and Reissner (1944) with those based on Luo and Tong (2007), differences of the results can be found in the edge moment factor and the shear stress. It is noted that expressions of the maximum peel stress for the two formulations are the same when the same force boundary conditions are prescribed. 2.3.4 Issues for CLS Joints with Composite Adherends When the adherends of the CLS specimen are composite laminates, analytical solutions for the CLS are very complicated. Tsai et al. (1998) indicated that the factors such as the inherent material heterogeneity, residual stresses, free-edge effects and relatively low transverse strength and shear stiffness impose great complexity to bonded composite structures. For the composite laminates widely used in engineering, effects of inherent material heterogeneity, lay-up sequence, lower transverse strength and shear stiffness may be analytically modeled. When the material heterogeneity is considered, the governing equations become the inhomogeneous differential equations, which can also be solved analytically. When the adherends are composite laminates with the symmetrical lay-ups, the formulations presented in this chapter can be extended to the composite CLS specimen; the coefficients αa and αk may reflect influences of the lay-ups. By using the Timoshenko beam or higher order theories, the lower transverse stiffness can be modeled and the analytical analysis can also be conducted. 2.4 Influence of Adherend’s Large Deflections and Adhesive Deformations In this section, numerical results of the analytical solutions are presented and compared with the geometrically nonlinear finite element analysis (NFEA) for edge moment factor, overlap deflections and adhesive stresses. The CLS specimen with the roller-roller boundary conditions and the symmetrical adherends are considered and the input data used in this section are: E1 = 70 GPa, ν1 = 0.34 and t1 = 1.6 mm; Ea /E1 = 0.04, ta /t1 = 0.078, νa = 0.4; c/t1 = 32 and l/c = 1.25. The NFEA results were conducted by Luo and Tong (2007, 2008) using the commercial FEA package MSC/NASTRAN, In the NFEA model, a 4-node isoparametric element was used for both the adhesive and the adherends; 3 and 18 elements were used through the adhesive and adherend thickness in the regions of 0.8c ≤ |x| ≤ c, 1 and 6 elements were used in the other region of the overlap. The geometrically nonlinear FEA with plane strain was implemented. 44 L. Tong and Q. Luo 2.4.1 Edge Moment Factor Figure 2.6 shows the edge moment factor for the CLS with the long overlap. In this figure, NFEA is referred to the NFEA results of MSC/NASTRAN; GR, HS, OP and LT represent the numerical results predicted by Goland and Reissner (1944), HartSmith (1973), Oplinger (1994) and Luo and Tong (2007) analytical formulations. These symbols are used in all relevant figures in this chapter. Figure 2.6 illustrates that the edge moment factor predicted by Hart-Smith (1973) is significantly lower than that predicted by the NFEA, and the predictions of Oplinger (1994), and Goland and Reissner (1944) is obviously higher than the NFEA results. Nevertheless, the edge moment factor predicted by the NFEA and the fully-coupled nonlinear formulation correlates well with each other. It should be noted that Eq. (2.57) is used to calculate k of Goland and Reissner (1944) in Fig. 2.6 for the consistency. More results of comparisons of the fully-coupled nonlinear formulation conducted by Luo and Tong (2007) and the NFEA presented by Tsai and Morton (1994) can be found in Luo and Tong (2007). As the geometrically nonlinear FEA can properly model behaviors of the geometric nonlinearity, the numerical results of Fig. 2.6 indicate large deflections of the outer adherend and the overlap have to be included in the analytical analysis for the CLS specimen. It should be pointed out that, the used data (E1 = 70 GPa and Ea /E1 = 0.04) denote the intermediately flexible adhesive (Tsai and Morton 1994). For the flexible adhesive, the difference between the Goland and Reissner (1994) and the NFEA (Tsai and Morton 1994) is larger (see Luo and Tong 2007). That is, the adhesive deformations should also be taken into account in the analytical analysis for the CLS specimen. 0.6 GR OP LT NFEA HS Edge moment factor k 0.5 0.4 0.3 0.2 0.1 0 0 0.8 1.6 2.4 3.2 4 βk c 4.8 5.6 6.4 7.2 8 Fig. 2.6 Bending factor predicted by the NFEA and the analytical solutions presented by Goland and Reissner (GR), Hart-Smith (HS), Oplinger (OP), and Luo and Tong (LT) for the CLS specimen with the roller-roller boundary condition 2 Analysis of Cracked Lap Shear (CLS) Joints 45 2.4.2 Adherend’s Deflections Figure 2.7 shows the deflection of adherend 1 in the overlap region at βk c = 8 predicted by Goland and Reissner (1944), the NFEA and Luo and Tong (2007). It is noted that deflections of adherends 1 and 2 are the same in the Goland and Reissner formulations. The non-dimensional deflection (wn = w1 /t1 ) and the nondimensional overlap axis (ξ = x/c) were used in Fig. 2.7. Figure 2.7 indicates that the overlap deflection predicted by the fully-coupled nonlinear formulations (Luo and Tong 2007) is almost the same as that of the NFEA, but there exist noteworthy difference between the NFEA and the formulations separated in two steps (Goland and Reissner 1944). It is further evident that the adhesive deformations should be considered in the analytical method for the CLS. 2.4.3 Adhesive Stresses The shear and peel stresses predicted by Goland and Reissner (1994) the NFEA and Luo and Tong (2007) are plotted in Figs. 2.8 and 2.9 respectively. In Figs. 2.8 and 2.9, a beam/adhesive model was used in the analytical analyses. The peak shear and peel stresses occur at the adhesive edge (i.e., crack-tip of the CLS). In the twodimensional analysis using FEA, the peak shear stress occurs very close to the adhesive edges but shear stress is zero at the edge, while peel stresses at the adhesive edge are singular. Therefore, the stress distributions in Figs. 2.8 and 2.9 are plotted in the range of (−1 ≤ ξ ≤ −0.801) for the present analytical solutions and in the range of (−0.999 ≤ ξ ≤ −0.801) for the NFEA. 0.2 Deflection wn1 (= – w1/t1) 0.15 0.1 0.05 0 –0.05 NFEA GR LT –0.1 –0.15 –0.2 –1 –0.8 –0.6 –0.4 –0.2 0 0.2 0.4 0.6 Non-dimensional overlap axis ξ 0.8 1 Fig. 2.7 The overlap deflection predicted by the NFEA, Goland and Reissner (GR), and Luo and Tong (LT) formulations for the CLS with the roller-roller boundary condition 46 L. Tong and Q. Luo 120 Shear stress (MPa) 100 80 GR NFEA LT 60 40 20 0 –1 –0.98 –0.96 –0.94 –0.92 –0.9 –0.88 –0.86 –0.84 –0.82 –0.8 Non-dimensional overlap axis ξ Fig. 2.8 Shear stress predicted by the NFEA, Goland and Reissner (GR), and Luo and Tong (LT) formulations for the CLS with the roller-roller boundary condition The numerical results in Figs. 2.8 and 2.9 are those at βk c = 8, corresponding to a tensile force of 659.6 N/mm. Stresses at the element centre were used in the figures. Figure 2.8 illustrates the shear distribution predicted by Luo and Tong (2007) correlates better with the NFEA results than that of Goland and Reissner (1944). Even for the same edge moment, there still exists difference between the two formulations for the shear stress prediction, which can also be seen from Eqs. (2.66) and (2.69). Figure 2.9 is the peel stresses distribution predicted by Goland and Reissner (1944), the NFEA and Luo and Tong (2007). It can also be seen that, as compared to the NFEA, the fully-coupled nonlinear formulations for the peel stress prediction 140 120 Peel stress (MPa) 100 80 GR NFEA LT 60 40 20 0 –20 –40 –1 –0.98 –0.96 –0.94 –0.92 –0.9 –0.88 –0.86 –0.84 –0.82 –0.8 Non-dimensional overlap axis ξ Fig. 2.9 Peel stress predicted by the NFEA, Goland and Reissner (GR), and Luo and Tong (LT) formulations for the CLS with the roller-roller boundary condition 2 Analysis of Cracked Lap Shear (CLS) Joints 47 are superior to the formulations separated in two steps based on Goland and Reissner (1944). When the same edge moment is applied, the maximum peel stress predicted by the two formulations is the same. In the fully-coupled nonlinear formulations (Luo and Tong 2007, 2008), solutions are found for the displacements. In the formulation process, large extensions, large rotations and deformations (material nonlinearity) are neglected. However, the predicted numerical results of edge moment factor, adhesive stresses, adherend deflections correlate extremely well with those of the NFEA. It indicates that large deflections of adherends are the critical feature of the CLS specimen, which is well represented by the fully-coupled nonlinear formulations. 2.5 Strength Prediction The failure of a CLS specimen may occur in adherend and adhesive and at a bimaterial interface. The failure load may be predicted by the strength-of-material based approach and/or the fracture mechanics based approach (Adams et al. 1997, Tong and Steven 1999), depending on the material properties, adhesive joint configurations and the pre-crack features. A cohesive damage zone model has also attracted attention to predict failure loads of adhesive joints (Sheppard et al. 1998, Yang and Thouless 2001, Blackman et al. 2003, Liljedahl et al. 2006), as there is a cohesive or plastic deformation zone near the crack-tip or the adhesive ends of the CLS specimen generally. 2.5.1 Strength of Material Based Approach The strength of material based approach involves a stress analysis of the CLS specimen, and employment of stress and/or strain based failure criteria. One of the most widely used stress/strain based failure criteria is the von Mises criterion. It has also been considered for the adhesive joints (Kusenko and Tammzs 1981, Czarnocki and Piekarski 1986), in which the failure criteria on the basis of the tensile experimental testing and biaxial experimental testing have been discussed for maximum tensile stress criterion, maximum tensile strain criterion and the modified distortion energy criterion. Crocombe et al. (1990) addressed structural adhesive failures based on strength of materials and fracture mechanics. Because of the stress concentration, complexity of stress analysis and difficulty in experimental testing, the strength of material based criteria for predicting the failure criteria based on strength of materials for adhesive joints have not been well-established (Lee 1991, Yang and Thouless 2001). Also, the CLS specimen is mainly designed to test fracture behaviors of the adhesive joints. Mangalgiri and Johnson (1986) discussed the CLS design to ensure the CLS failure occurred in adhesive and interface. Therefore, most of works on the failure prediction for the CLS has been focused on the fracture mechanics based approach. 48 L. Tong and Q. Luo 2.5.2 Calculation of Energy Release Rates and Failure Prediction The fracture mechanics based approach for the CLS failure prediction includes calculation of the stress intensity factors (SIF) and/or energy release rate (ERR) or J-integral and the experimental testing for the fracture toughness, critical ERRs or J-integral. When the maximum adhesive stresses are found, energy release rates GI and GII can be calculated by (Edde and Verreman 1992, Krenk 1992): GI = ta ta (σmax )2 ; GII = (τmax )2 2Ea 2Ga (2.71) It is noted that both modes I and II are found in Eq. (2.71), which can be directly applied to the CLS with relatively long overlap (Krenk 1992). When the CLS deflections and force components of the overlap are solved, the ERRs and/or the J-integral can be calculated. Lai et al. (1996) calculated the ERRs using the method developed by Hutchinson and Suo (1992) for the bi-material crack. Fernlund and Spelt (1994) calculated J-Integral using the following procedure. As shown in Fig. 2.10, a closed-form expression of the energy release rate can be calculated by using the J-integral: ∂u J= Wn − T dΓ (2.72) ∂τ Γ where W is the strain energy density; n and τ are outward unit normal and tangential vectors to the un-deformed boundary contour; T is the traction vector acting on Γ. When the contour is o–a–b–c–d–e–f–o, no contributions to the J-integral in o–a, b–c, d–e and f–o boundaries as there are no tractions on the crack faces and horizontal boundaries of the upper and lower adherends. The J-integral becomes: J = J(1) + J(2) + J(3) (2.73) where subscripts (1), (2) and (3) represent the boundaries a–b, c–d and e–f respectively. The total energy release rate can be found in light of Eqs. (2.72) and (2.73), which is given by: M32 N32 N22 N12 M12 M22 + + + + − J= 2A(1)11 2D(1)11 2A(2)11 2D(2)11 2A(o)11 2D(o)11 (2.74) where subscripts (1), (2) and (o) represent the upper adherend, lower adherend and the overlap. It is noted that Eqs. (2.72), (2.73), (2.74) can be applied to general adhesive joints. For the CLS specimen as shown in Fig. 2.1, J(2) = 0. It is also worth noting that the shear force effects on ERRs are not included. 2 Analysis of Cracked Lap Shear (CLS) Joints Fig. 2.10 The schematics for J-integral (a) the J-integral boundary (b) force components of the overlap 49 e f a b d o c (a) Q1 M1 N1 M2 N2 Q2 M3 N3 Q3 (b) When the J-integral of the mixed mode is found, the mode should be separated to predict the CLS failure, because the CLS is generally a mixed mode problem. There exist analytical methods for partitioning modes for a cracked homogeneous beam (e.g., Hutchinson and Suo 1992). For the CLS, the NFEA is an effective tool to calculate mode ratios (Johnson 1986). Papini et al. (1994), Fernlund and Spelt (1994) conducted the experimental investigation on the critical energy releases rate for the CLS and presented the critical energy release rate for the 7075-T6/Permabond ESP 310 adhesive system, as shown in Fig. 2.11. When the loading phase angle is found, the critical J-integral Jc can be found from the fracture envelope such as that shown in Fig. 2.11. By comparing the found J-integral Jc with the critical one, the failure loads of the CLS specimens can be predicted. The critical J -integral Jc (J/m2) 6000 5000 4000 3000 2000 1000 0 0 10 20 30 40 50 60 70 80 90 Phase angle =Atan(JII/JI) (Degrees) Fig. 2.11 The critical energy release rate of the 7075-T6/Permabond ESP 310 adhesive system 50 L. Tong and Q. Luo 2.6 Concluding Remarks In this chapter, analytical procedures for stress analysis and failure prediction of the CLS specimen are presented. Because of the complexity, particularly when lap adherend and/or lap adherend of the CLS are composite laminates, closed-form solutions of the CLS are very limited in the existing literatures. Available results show that large deflections of the outer adherend and the overlap must be modeled. The analytical formulation based on Goland and Reissner (1944) are available to calculate the force components at the end of the overlap, both for symmetrical and asymmetrical adherends, but larger errors may appear as the adhesive deformations are not modeled in the formulations, particularly for the cases of long overlaps, thicker and/or soft adhesive, larger applied loadings and composite laminates. The adhesive stresses of general asymmetrical adherends for the prescribed force boundary conditions can be found in Luo and Tong (2002). The analytical solution based on the fully-coupled nonlinear formulations (Luo and Tong 2007) correlate well with the geometrically nonlinear finite element analysis; it can also be applied to the composite laminates. Currently, the analytical solutions are only available for the symmetrical adherends. The analytical solutions for CLS with the clamped-clamped and roller-clamped boundary conditions are yet to be found, and that for the CLS with asymmetrical adherends should be further studied. Acknowledgments The authors are grateful to the continuous support of ARC (Australia) and AOARD/ASOSR (USA). 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Chapter 3 Analytical Models with Stress Functions Toshiyuki Sawa Abstract The interface stress distributions in adhesive butt joints subjected to tensile and cleavage loadings are described using two-dimensional theory of elasticity. Interface stress distributions of adhesive band butt joints are also discussed. In addition, the effects of adhesive Young’s modulus and the adhesive thickness on the interface stress distributions are shown. For adhesive tubular butt joints, the effects on the interface stress distributions are described using axi-symmetrical theory of elasticity. It is shown that singular stresses occur at the edges of the interfaces. It is also observed that the singular stresses decrease as the adhesive Young’s modulus increases and the adhesive thickness decreases. Finally, a method of stress analysis for bonded shrink fitted joints is described and it is demonstrated that the strengths of bonded shrink fitted joints are larger than those of shrink fitted joints. 3.1 Introduction In this chapter, the characteristics of adhesive butt joints of thin plates under tensile [15], and cleavage loadings [20] are described using two-dimensional theory of elasticity. The characteristics of adhesive butt joints of solid cylinders/bars under tensile loadings [14] are also described using axi-symmetrical theory of elasticity. A stress analysis of the tubular (hollow cylinder) butt adhesive joints is also done under tensile [12] and torsional loadings [13]. In designing these adhesive butt joints, it is important to know how to determine the material properties of the adhesive and the adhesive thickness. From the analyses, it is shown how to determine the adhesive properties and the adhesive thickness in the design of adhesive butt joints. In practice, bonded shrink fitted joints are applied using anaerobic adhesive. The effects of some factors are described on the interface stress Toshiyuki Sawa Hiroshima University, 1-4-1, Kagamiyama, Higashihiroshima, Hiroshima, Japan, e-mail: sawa@mec.hiroshima-u.ac.jp L.F.M. da Silva, A. Öchsner (eds.), Modeling of Adhesively Bonded Joints, c Springer-Verlag Berlin Heidelberg 2008 53 54 T. Sawa distributions in the bonded shrink fitted joints [17]. In addition, it is demonstrated that the strengths of bonded shrink fitted joints are larger than those of shrink fitted joints. 3.2 Butt Joints Figure 3.1 shows several types of butt joints. Figure 3.1a shows an adhesive butt joint of thin plates [10, 15, 18, 23, 24]. Figure 3.1b shows a band adhesive joint in which the interfaces are partially bonded [16, 21]. Figure 3.1c shows a butt joint of solid bars/cylinders [4, 7, 8, 11, 14, 25]. Figure 3.1d shows a tubular (hollow cylinder) joint [2, 3, 5, 6, 9, 12, 13, 22, 26]. Figure 3.1e shows butt joints subjected to cleavage loadings [1, 19, 20] as a special case of Fig. 3.1a. Important issues for designers are interface stress distributions and the joint strength. In addition, an important issue is how to determine adhesive material properties, and the adhesive thickness in designing the adhesive joints. 3.2.1 Adhesive Butt Joints of Dissimilar Adherends Subjected to Tensile Loadings Figure 3.2 shows a model for two-dimensional analysis of butt joints under tensile loadings [15]. Two adherends are bonded by an adhesive. Young’s modulus, shear modulus and Poisson’s ratio of the adherends are denoted by E1 , G1 , ν1 , E3 , G3 , ν3 , respectively, where Cartesian coordinates (x, y) are used. The adhesive thickness is denoted by 2h2 . The tensile loading is applied to both ends of the adherends as the stress distribution F(x). The stress distribution F(x) is developed by Fourier series and the two-dimensional theory of elasticity is applied for analyzing the joint under tensile loading F(x). The boundary conditions are described by Eqs. (3.1), (3.2), (3.3), (3.4). (i) on finite strip (I) (adherend) x = ±l; y1 = h1 ; I =0 σxI = τxy ∞ σyI = F(x) = a0 + ∑ as cos I =0 τxy s=1 sπ x l ⎫ ⎪ ⎪ ⎪ ⎬ ⎪ ⎪ ⎪ ⎭ (3.1) (ii) on finite strip (II) (adhesive) x = ±l; II σxII = τxy =0 (3.2) 3 Analytical Models with Stress Functions 55 (a) The adhesive butt joint of thin plates. (b) Band adhesive joints. (c) Butt joint of solid bars/cylinders. (d) Tubular (hollow cylinder) joint. (e) Butt joints subjected to cleavage loadings . Fig. 3.1 Several types of butt joints (iii) on finite strip (III) (adherend) x = ±l; y3 = −h3 ; ⎫ ⎪ sπ ⎪ ⎬ III x σy = G(x) = b0 + ∑ bs cos l ⎪ s=1 ⎪ ⎭ III = 0 τxy III = 0 σxIII = τxy ∞ (3.3) 56 T. Sawa Fig. 3.2 An adhesive butt joint of dissimilar adherends subjected to an external tensile loading [15] (iv) at the interface between finite strips (I) and (II) I σy y =−h = σyII y =h 1 1 2 2 I II τxy y =−h = τxy y =h 1 1 2 2 I II u y =−h = u y =h 1 ∂ vI ∂x 1 2 = y1 =−h1 ∂ v II ∂x ⎫ ⎪ ⎪ ⎪ ⎪ ⎪ ⎪ ⎪ ⎪ ⎬ (3.4) ⎪ ⎪ ⎪ ⎪ ⎪ ⎪ ⎪ ⎪ ⎭ 2 y2 =h2 where, = a0 as = 1 l 1 2l e1 −e1 F(x)dx, sπ x dx, l −e1 (s = 1, 2, 3, · · ·) e1 F(x) cos 1 2l 1 bs = l b0 = e2 −e2 e2 −e2 G(x)dx, G(x) cos sπ x dx, l The numerical calculations were done and the results are shown in Figs. 3.3, 3.4 and 3.5. In the analysis, Airy’s stress functions are used, as in Eq. (3.1). Figure 3.3 shows the effect of Young’s modulus on the stress distributions at the interfaces y2 = h2 and y2 = −h2 , where the ratio E1 /E3 was held constant at 3 and the ratio E1 /E2 was varied as 5, 10, and 100. The abscissa represents the ratio of the distance x to the half length l of the adhesive, and the ordinates indicate the ratio of each stress to the mean normal stress σym at the interface. In Fig. 3.2, it was assumed that the tensile stresses F(x) and G(x) acted uniformly on the upper (y1 = h1 ) and the lower (y3 = −h3 ) surfaces in the region |x| ≤ l[F(x) = G(x)]. From the results, it is seen 3 Analytical Models with Stress Functions 57 Fig. 3.3 Effect of the ratio of Young’s modulus of the adherend to that of the adhesive on the stress distribution. l/h2 = 5.0, h1 /h2 = h3 /h2 = 2.0, E1 /E3 = 3, ν1 /ν2 = ν3 /ν2 = 0.86. F(x) and G(x) are uniform within the region |x| ≤ l [15] that singular stresses occur at the edges of the interfaces and each stress is larger at y2 = h2 than at y2 = −h2 . The absolute values of the stress σy and the shear stress τxy become larger near the edge x/l = 1.0 of the interface with an increase of the ratio E1 /E2 . Figure 3.4 shows the effect of the thickness 2h2 of the adhesive layer, where h1 = h3 ; the value h1 /h2 was 2, 5, and 20; E1 /E3 was 1.5; and E1 /E2 = 3.0. From the results, it is seen that the absolute values of τxy /σym near the edges x/l = 1.0 of the interfaces increase as the ratio h1 /h2 increases. As shown in Figs. 3.3, 3.4 and 3.5, it is found that the singular stresses occur at the edge of the interfaces. It is necessary to examine the value of the singular stresses. 58 T. Sawa Fig. 3.4 Effect of the thickness of the adhesive layer on the stress distribution at the interface. l/h1 = l/h3 = 2.5, E1 /E2 = 3, E1 /E3 = 1.5, ν1 /ν2 = ν3 /ν2 = 1.0. F(x) and G(x) are uniform within the region |x| ≤ l [15] Figure 3.5 shows the relationship between the ratio of the normal stress σy to the mean stress σym and the distance r from the edge in logarithmic scales in order to examine the stress singularity at the edges. This case corresponds to Fig. 3.3. In general, the singular stress is expressed approximately by Eq. (3.5) below, where K is the intensity of the stress singularity and λ is the order of the singularity. The distance from the edge is denoted by r and is expressed by r = (l − x)/l. σy /σym = K/(rλ ) (3.5) The singular stresses are expressed in this form in Fig. 3.5. The distance r is varied between 0.005 and 0.02 mm, because the singular stresses are approximately linear in logarithmic scale in the region of r mentioned above. The parameter λ varies with the ratio of Young’s moduli of the adherend to that of the adhesive. The results show that the difference in Young’s moduli between the two adherends must be small and the rupture occurs at the interface of the adherend with higher Young’s modulus. It is better to increase the value of the adhesive Young’s modulus and decrease the adhesive thickness. When the adherend material is the same, the same trend is obtained. 3 Analytical Models with Stress Functions 59 Fig. 3.5 Singular stress at the edge of the interface. l/h2 = 5.0, h1 /h2 = h3 /h2 = 2.0, E1 /E3 = 3.0, ν1 /ν2 = ν3 /ν2 = 0.86. F(x) and G(x) are uniform within the region |x| ≤ l [15] An issue is how to increase the adhesive Young’s modulus. When the adherend material is metal, the adhesive Young’s modulus is smaller in comparison with that of metal. So, it is important to increase the value of adhesive Young’s modulus by adding fillers with higher Young’s modulus than that of the adhesive. 60 T. Sawa 3.2.2 Adhesive Butt Joints of Similar Adherends Subjected to Cleavage Loadings Figure 3.6 shows a two-dimensional model for analysis of adhesive butt joints subjected to cleavage loadings [20]. The notations are the same as mentioned in Fig. 3.1. The cleavage loadings are important serious conditions for the adhesive butt joints. For analyzing the stress state of the joints under cleavage loadings, the stress distribution of cleavage loading F(x) is developed into Fourier series. In the analysis, Airy’s stress functions are used. They are much more complicated than those in Eqs. (3.1), (3.2). The results of the numerical calculations are shown in Figs. 3.7, 3.8 and 3.9. Figure 3.7 shows the effect of the ratio E1 /E2 of Young’s moduli of adherends to adhesive on the stress distributions at the interface (y2 = h2 ), where E1 /E2 was chosen as 3, 10 and 100. It is assumed that a cleavage load acts uniformly within the region 0.8 < x/l < 1.0. In this figure, σym represents the mean normal stress. The abscissa represents the ratio x/l of the distance x form the centre of the joints to the half length l of adherends and adhesive. It is seen that the distributions of σy , σx , and τxy tend to increase near the edge, x/l = 1.0, and the stress singularity increases with an increase in E1 /E2 . The larger E1 /E2 is, the more uniform the distribution of stress σy becomes. Figure 3.8 shows the effect of adhesive thickness on the stress distribution at the interface. The ratio h1 /h2 of the thickness of the adherend, 2h1 , to that of the adhesive, 2h2 , is varied as 2, 20 and 100. The stress distributions of σy , σx and τxy increase near x/l = 1.0 with an increase in the ratio h1 /h2 . Figure 3.9 shows the effect of the cleavage load distribution F(x) on the stress distribution at the interface. In this case the thickness of the adhesive is held constant and the value of h1 /h2 is set at 5. Numerical calculations were carried out Fig. 3.6 Adhesive butt joint subjected to a cleavage loading [20] 3 Analytical Models with Stress Functions 61 Fig. 3.7 Effect of ratio of Young’s modulus of the adherend to that of the adhesive on the stress distribution at adhesive-adherend interface [20] (y2 = h2 , h1 /l = 0.2, h1 /h2 = 2, ν1 /ν2 = 1 and F(x) is constant over the region 0.8 < x/l < 1.0) 62 T. Sawa Fig. 3.8 Effect of adhesive thickness on the stress distribution at adhesive-adherend interface [20] (y2 = h2 , h1 /l = 0.2, E1 /E2 = 3, ν1 /ν2 = 1 and F(x) is constant over the region 0.8 < x/l < 1.0) 3 Analytical Models with Stress Functions 63 Fig. 3.9 Effect of cleavage stress F(x) distribution on the stress distribution at adhesive-adherend interface [20] (y2 = h2 , h1 /h2 = 5, h2 /l = 0.1, e2 /l = 1, E1 /E2 = 65.6 and ν1 /ν2 = 0.81) 64 T. Sawa in the cases where the uniform load F(x) acts over the regions 0 < x/l < 1.0 and 0.8 < x/l < 1.0. The effect of the load distribution can be seen clearly on the stress distribution at the interface. It is found that the stress singularity near the points x/l = −1.0 and x/l = 1.0 increases in the case where the load distribution F(x) acts over the region 0.8 < x/l < 1.0. This is due to the fact that E1 /E2 and l are large in comparison with h1 and e1 (defined in Fig. 3.9). From the results, it can be concluded that the singular stresses decrease as the Young’s modulus of the adhesive is increased and the adhesive thickness is decreased. In addition, it is found that the singular stress at the edge of the interfaces increases depending on the cleavage distribution. It is also observed that the interface stress σy is compressive at the left region of the interfaces, as shown in Figs. 3.7, 3.8 and 3.9. 3.2.3 Band Adhesive Butt Joints of Dissimilar Adherends Subjected to External Bending Moments Figure 3.10 shows a model for analysis of band adhesive butt joints with dissimilar adherends subjected to external bending moments [21]. The analytical method is the same as the cases of Figs. 3.1 and 3.2 using the two-dimensional theory of elasticity. In the numerical calculations, a stress singularity occurs at the edge (|x1 | = c + l2 , |x1 | = c−l2 ) of the interface (y2 = +h2 , x2 = +l2 ), hence 50 terms in the series were Fig. 3.10 Band adhesive butt joint of dissimilar finite strips subjected to external bending moments [21] 3 Analytical Models with Stress Functions 65 Fig. 3.11 Effect of the ratio of Young’s moduli between the adherends and the adhesive on each stress distribution (σx , σy and τxy ) and on the maximum principal stress distribution (σ1 ) at the interface [21] used to guarantee the convergence of the stresses. Figure 3.11 shows the effect of the ratio of Young’s moduli between the adherends and the adhesive on each stress (σx , σy and τxy ) distribution and on the maximum principal stress σ1 (plane stress) distribution at the interfaces (y2 = +h2 , x2 = +l2 ), where the ratio E1 /E2 was 5, 10 and 60. It is assumed the bending moments act linearly on the upper (y1 = h1 ) and the lower (y3 = −h3 ) surfaces in the region |x1 | ≤ l1 (F(x1 ) = G(x3 )). The abscissa is the ratio of the distance x1 to the half-length l1 of the adherend. In the following analytical results, the stress distributions are analyzed until the point 0.4% inside the length 2l2 from the edge of the adhesive. From the results, it is seen that singular stresses occur at the edge of the unbonded area (x1 /l1 = 0.6) with a decrease of the ratio E1 /E2 and the stress distribution tends to approach the stress distribution F(x1 ) and G(x3 ) with an increase of the ratio E1 /E2 . 66 T. Sawa Fig. 3.12 Effect of the ratio of Young’s moduli between adherends on the maximum principal stress distribution at the interface [21] Figure 3.12 shows the effect of the ratios E1 /E3 of Young’s moduli between adherends on the maximum principal stress σ1 /P distribution. The maximum principal stress at the position x1 /l1 = 1.0 of the interface (y2 = h2 ) increases with an increase of E1 /E3 and increases near the point x1 /l1 = 1.0 of the interface (y2 = −h2 ) with a decrease of the ratio E1 /E3 . From the results, it is predicted that joint strength in the case of dissimilar adherends is smaller than that in the case of similar adherends. Figure 3.13 shows the effect of the thickness 2h2 of the adhesive layer, where the ratio h1 /h2 was 50, 100 and 200. The stress singularity at the edge of the interface (x/l = 0.6, 1.0) increases with an increase of the ratio h1 /h2 . Figure 3.14 shows the effect of the bonding positions on the maximum stress distribution at the interface (y2 = h2 , y2 = −h2 ) in the case of h1 /l1 = 0.2. It is assumed that the stress distributions F(x1 ) = G(x3 ) are linear in the region |x1 | = |x3 | ≤ 0.5l1 and the regions of bonding are 0.2 ≤ |x1 /l1 | ≤ 0.6, 0.4 ≤ |x1 /l1 | ≤ 0.8 and 0.6 ≤ |x1 /l1 | ≤ 1.0. Figure 3.15 shows the maximum principal stress at positions A, B, C and D (positions 0.4% inside from |x1 | = c + l2 , |x1 | = c − l2 ) near the A and edge of adhesive [II] at the interfaces (y2 = h2 , y2 = −h2 ). When positions C are about 0.56l1 , the values of the maximum principal stress at positions A, B, C and D are equal. Figure 3.15b shows the intensity K of the stress singularity at 3 Analytical Models with Stress Functions 67 Fig. 3.13 Effect of the ratio of the adhesive thickness on the maximum principal stress distribution at the interface [21] positions A, B, C and D by using the stress singularity parameters. Generally, the maximum principal stress σ1 /P near the position where stress singularity occurs is expressed approximately by σ1 (r)/P = K/rλ (3.6) where, σ1 (r) : maximum principal stress, r : distance from singularity, K : intensity of stress singularity, λ : order of stress singularity. From the result, when positions A and C are about 0.57l1 , the value K of the intensity of stress singularity at position A becomes equal to that at position C . From 68 T. Sawa Fig. 3.14 Effect of the bonding positions on the maximum principal stress distribution at the interface [21] the above results, it is concluded that the joint strength is maximal when the value c/l1 is between 0.56 and 0.57. Figure 3.16 shows the effect of the bonding area on the maximum principal stress σ1 /P distribution at the interfaces (y2 = h2 , y2 = −h2 ), where F(x1 ) = G(x3 ) = Px1 /l1 (|x1 | ≤ l1 , |x3 | ≤ l1 ) and the ratio 2l2 /l1 is set as 1.0 (bonded completely at the interfaces), 0.6 and 0.4. From the results, it is expected that an increment of singular stress due to an unbonded area is small at both edges (x1 /l1 = +1.0) even if the unbonded area is at the center of the joint. Thus, it is concluded that a band adhesive joint in which the interface is partially bonded efficiently resists external loads if a suitable bonding area is selected. Table 3.1 shows a comparison between the analytical and the experimental results concerning the joint strength. The experiments were performed 30 times. The joint was assumed to fail when the maximum principal stress at position x1 /l1 = 0.996 3 Analytical Models with Stress Functions Fig. 3.15 Effect of bonding positions on the maximum principal stress distribution at the interface [21] Fig. 3.16 Effect of the bonding area on the maximum principal stress distribution at the interface [21] 69 70 T. Sawa Table 3.1 Comparison concerning joint strength of butt joints [21] Adherends St-St (Nm) Al-Al (Nm) St-Al (Nm) Complete Adhesion (2l2 /l1 = 1.0) EXP NUM 123 118 (329) 110 107 (297) 50 48 (134) Band Adhesion (2l2 /l1 = 0.6) EXP NUM 120 116 (299) 108 104 (269) 47 44 (119) equals to the fracture stress of the adhesive. The joint strength prediction was also done by the von Mises criterion and the values are indicated in brackets in Table 3.1. Table 3.1 shows that the predictions based on the maximum principal stress criterion are consistent with the experimental results. The values predicted by the von Mises criterion are larger than the experimental results. It is shown that the joint strength in which the interface is partially bonded is the same as that of a butt joint in which the interface is bonded completely. In addition, it is seen that the joint strength in the case where dissimilar adherends (St-Al) are used is about half that in the case where similar adherends (St-St and Al-Al) are used. In addition, it can be assumed that the residual stress in the band adhesive joint is reduced in bonding process while the strength is the same as a joint with interfaces completely bonded. Thus, it is better for a mechanical engineer to design band adhesive butt joints taking into account the load distribution and the interface length. 3.2.4 Adhesive Butt Joints of Solid Cylinders Subjected to External Tensile Loadings The previous stress analyses are two-dimensional. In this section, a method for axi-symmetrical stress analysis of adhesive butt joints with solid cylinder [14] is described (see Fig. 3.17). Michell’s stress functions are used, where cylindrical coordinates (r, z) are used. The stress singularity at the edge of the interfaces is not taken into consideration. Hence, computations were done varying the number N of terms as 100 and 120 in order to examine the effect of the number N on the stress distributions at the interfaces. It was seen that the difference between both results was less than 3%. Hereafter, computations were done setting the number N of terms as 100. Figure 3.18 shows the effect of the ratio E1 /E2 of Young’s modulus of the adherends to that of the adhesive on the stress distributions at the interface (z2 = h2 ), where the values E1 /E2 were varied as 1, 3, 40, 60 and infinity. In the case where the value E1 /E2 was infinity, that is the adherends were assumed rigid, the analysis was done under the following boundary conditions. ⎫ ⎪ r = a : σr = τrz = 0 ⎪ ⎪ ⎪ ⎪ ⎬ ∂w z2 = ±h2 : u = 0, =0 (3.7) ⎪ ∂r ⎪ ⎪ a a ⎪ ⎭ 2π r(σz )z=h2 dr = 2π rF(r)dr ⎪ 0 0 3 Analytical Models with Stress Functions 71 Fig. 3.17 Adhesive butt joint of solid cylinders subjected to an external tensile loading [14] Fig. 3.18 Effect of the ratio of Young’s modulus of the adherend to that of the adhesive on the stress distributions σz , σr and τrz at the interface [14] (z2 = h2 , h1 /h2 = 10, h1 /a = 0.2, ν1 /ν2 = 1.0. F(r) is constant within the region r ≤ a) In numerical calculations, a tensile load F(r) was assumed to act uniformly within the region r ≤ a on the upper surface of adherend (z1 = h1 ). In Fig. 3.18, σzm represents the mean normal stress. The ordinate represents the ratios σz /σzm , σr /σzm of the normal stresses to the mean normal stress and τzr /σzm the shear stress to the mean normal stress. The abscissa represents the ratio r/a of the distance r from the 72 T. Sawa center to the radius a. It is seen that the distribution of σz tends to be averaged when the value E1 /E2 approaches 1 and the singularity increases with an increase of the value E1 /E2 . It is also seen that the shear stress τzr near the edge r/a = 1.0 increases with an increase of the value E1 /E2 . A difference is not found among the distribution of σz in the cases where E1 /E2 is 40, 60 and infinity, nor in the distribution of τzr . In this model, adherends are assumed to be rigid when the value of E1 /E2 is more than 40. Figure 3.19 shows the effect of the adhesive thickness on the stress distributions σz , σr and τzr at the interface (z2 = h2 ). The thickness 2h1 of the adherends is held constant and the value of h1 /h2 is varied as 5, 10, 20 and 100. There are no differences in the distributions σz and τzr between the cases where h1 /h2 is 20 and 100. The distribution of σz tends to a constant value and the shear stress τzr decreases with an increase of h1 /h2 . Figure 3.20 shows the effect of the load distribution F(r) on the stress distributions σz , σr and τzr at the interface. With the thickness of the adhesive held constant and the value of h1 /h2 set at 5, computations were done in the cases where the uniform load F(r) acts on the region (c/a)2 = 0.1. There is a visible effect of the stress distribution σz but very little effect on the distribution τzr . Figure 3.21 shows a comparison of the analytical results obtained by this study with the results obtained by finite element method (FEM) with respect to the stress distributions in the adhesive. The results obtained by FEM show the stresses at the centroid of the triangle elements. Therefore, the stresses obtained by the analysis were compared with Fig. 3.19 Effect of the adhesive thickness on the stress distributions σz , σr and τrz at the interface [14] (z2 = h2 , h1 /a = 0.2, E1 /E2 = 40, ν1 /ν2 = 1.0. F(r) is constant within the region r ≤ a) 3 Analytical Models with Stress Functions 73 Fig. 3.20 Effect of external load distribution on the stress distribution σz , σr and τrz at the interface [14] (z2 = h2 , h1 /h2 = 5, h2 /a = 0.1, E1 /E2 = 65.6, ν1 /ν2 = 0.81) Fig. 3.21 Comparison of analytical results with results obtained by FEM [14] (h1 /h2 = 10, h1 /a = 1.0, E1 /E2 = 91.0, ν1 /ν2 = 0.91. F(r) is constant within the region r ≤ a) those obtained by FEM at z1 /h2 = 0.92 and 0.17. Both results are in fairly good agreement. From the results, it is found that the singular stresses occur at the edge of the interfaces and they decrease as the adhesive Young’s modulus increases and the adhesive thickness decreases. These points are important in the actual design of joints under static loadings. 74 T. Sawa 3.3 Tubular Joints 3.3.1 Tubular Butt Adhesive Joints Subjected to a Tensile Loading Figure 3.22 shows a tubular (hollow cylinder) butt adhesive joint subjected to a tensile loading [12]. Cylindrical coordinates (r, z) and Michell’s stress functions are used in the analysis. Two adherends are replaced by the hollow cylinders with the same dimensions and material. An external tensile loading is applied by the stress distribution F(r). Young’s modulus and Poisson’s ratio of the adherends and the adhesive are denoted by E1 , ν1 , E2 and ν2 , respectively. The inside diameter of the joints is denoted by 2a, the outside diameter by 2b. The analyses are done using the axi-symmetrical theory of elasticity. The interface stress distribution is important for analyzing the joints. Figure 3.23 shows the effect of Young’s modulus ratio E1 /E2 on the distribution of the stress components σz , σr , τzr at the interfaces. It is seen that each stress component is singular at both edges r = a and r = b. Figure 3.24 shows the effect of the adhesive thickness 2h2 on the interface stress distributions. It is found that the shear stress decreases as the adhesive thickness decreases. Figure 3.25 shows the effect of the tensile loading F(r) distribution on the interface stress distributions. It can be seen that each stress (σz , σr and τzr ) is singular at both the edges (outside and inside radius) of the interfaces. Figure 3.26 shows the effect of the diameter ratio a/b on the stress distributions. It is seen that the shear stress τzr increases near both the edges as the diameter ratio a/b increases while the changes in the stress components σz and σr are smaller. For the tubular (hollow cylinders) adhesive butt joints, the singular stresses occur at the both edge (r = a and r = b) and they decrease as the adhesive Young’s modulus E2 is increased and the adhesive thickness is decreased. Fig. 3.22 Tubular butt adhesive joint subjected to a tensile loading [12] 3 Analytical Models with Stress Functions 75 Fig. 3.23 Effect of the ratio of Young’s modulus of the adherend to that of the adhesive on the stress distributions σz , σr and τrz at the interface [12] (z2 = h2 , a/b = 0.9, (b–a)/2h2 = 10, h1 /h2 = 10, ν1 /ν2 = 1.0. F(r) is uniform within the region a ≤ r ≤ b) 3.3.2 Tubular Butt Adhesive Joints Under Torsional Loading Figure 3.27 shows tubular (hollow cylinder) butt adhesive joints under torsional loadings [13]. The analysis is carried out using the axi-symmetrical theory of elasticity. Cylindrical coordinates (r, θ , z) are used. The shear moduli and Poisson’s ratios for adhesive (I), adherend (II) and (III) are designated by G1 , ν1 , G2 , ν2 , G3 and ν3 , respectively. Numerical computations are carried out in the case where the two adherends (II) and (III) are the same material (G2 = G3 ) and of the same dimensions (c = e, d = f , c/d = 0.5). In order to investigate the effect of the position of the adhesive band on the stress distributions and the displacements, two types of adhesive joints are examined numerically, that is, one is bonded at the outer interface, called type (A) and the other is bonded at the inner interface, called type (B), where the bonded area of each type is the same. Moreover, the effect of the ratio of shear modulus of the adhesive to that of the adherend and the effect of the adhesive thickness are examined in the case of the two types mentioned above. In computations, the number of terms, N, of the series is taken as 200, which is checked to obtain the stresses and the displacements in satisfactory accuracy. Figures 3.28 and 3.29 show the effect of the ratio G1 /G2 of the shear modulus of the adhesive to that of the adherend on the shear stresses and the displacement 76 T. Sawa Fig. 3.24 Effect of the adhesive thickness on the stress distributions σz , σr and τrz at the interface [12] (z2 = h2 , a/b = 0.9, ν2 = 0.3, E1 /E2 = ∞) at the interface between the adhesive and the adherend, respectively, in the case of type (A). Also, these effects in the case of type (B) are shown in Figs. 3.30 and 3.31 From these figures, the maximum stresses become large with an increase of the ratio G1 /G2 at the inner circumference of the interface, i.e. r = a, in the case of type (A) and at the outer circumference of the interface, i.e. r = b, in the case of type (B). On the other hand, the maximum displacements become small with an increase of the ratio G1 /G2 in both cases. Moreover, comparing the results of type (A) with those of type (B), the maximum stresses and the displacements are smaller in the case of type (A), i.e. the case where tubular shafts are bonded at the outer interface of the adherends. Figure 3.32 shows the effect of the thickness of the adhesive on the stress distributions in the case of type (A). From this figure, it is seen that the singularity of the stress becomes larger at the inner circumference, i.e. r = a, with a decrease of the thickness 2h. Figures 3.33 and 3.34 show the effect of the ratio G1 /G2 of shear modulus on the shear stress distributions and on the displacements for two solid shafts bonded at the outer interface (type A). From these figures, it is seen that both the stress and the displacement distributions are similar to the results shown in Figs. 3.28 and 3.29 of the adhesive joint with the tubular shafts. 3 Analytical Models with Stress Functions 77 Fig. 3.25 Effect of the tensile stress F(r) distribution on the stress distributions σz , σr and τrz at the interface [12] (z2 = h2 , a/b = 0.9, (b–a)/2h1 = 0.2, (b–a)/2h2 = 10, E1 /E2 = 65.6, ν1 /ν2 = 0.81) 3.4 Bonded Shrink Fitted Joints Shrink fitting has been used widely for joining cylindrical components of many mechanical structures. At present, shrink fitting in comparison with anaerobic adhesive is used for mechanical joints such as automobile differential gears in order to improve the joint strength and to reduce the assembly weight. Thus, it is important for mechanical design engineers to understand the interface stress distribution and the joint strength of the bonded shrink fitted joints. Furthermore, it is critical to determine the stress distribution and joint strength when an external load is applied to the joints. Figure 3.35 shows a bonded shrink fitted joint subjected to torsion. Prior to assembly, the ring is heated up and is inserted into the shaft on which an anaerobic adhesive is applied. Then the bonded shrink fitted joints are cooled to ambient temperature and left at room temperature. Based on the axi-symmetrical theory of elasticity, the interface stress distribution is analyzed [17]. Figure 3.36 shows the effect of Young’s modulus ratio E3 /E2 on the stress ratio τrθ /σr at the inner surface of the adhesive layer. The stress ratio τrθ /σr at the upper 78 T. Sawa Fig. 3.26 Effect of the ratio of the diameter a/b on the stress distributions σz , σr and τrz at the interface [12] (z2 = h2 , b/2h2 = 100, ν2 = 0.3, E1 /E2 = ∞) end (z/h3 = 1.0) of the adhesive layer decreases as the ratio E3 /E2 increases. It is indicated that the joint strength increases as the rigidity of the ring increases in comparison with that of the adhesive. Figure 3.37 shows the effect of the outer diameter of the rings, 2h3 . It is found that the stress ratio τrθ /σr decreases as the ratio b3 /a2 increases. Thus, it can be assumed that the joint strength increases as the outer diameter 2b3 increases in comparison with the outer diameter of the shafts, 2b1 . Figure 3.38 shows the effect of the engagement length 2h3 . It is found that the effect of the value of h3 /a2 on the stress ratio τrθ /σr near the upper end of the rings (z/h3 = 1.0) is small and that the ratio τrθ /σr inside the edge (z/h3 = 1.0) decreases as the value of h3 /a2 increases. It can be concluded that the joint strength increases as the engagement length 2h3 increases. Figure 3.39 shows an example of the comparison of joint strength between shrink fitted joints and bonded shrink fitted joints. It is shown that the strengths of bonded shrink fitted joints are greater than those of shrink fitted joints. In addition, it is easy to reduce the interference (shrink allowance) for bonded shrink fitted joints in comparison with shrink fitted joints. This is a big benefit for mechanical design engineers. 3 Analytical Models with Stress Functions Fig. 3.27 Tubular adhesive joints subjected to torsional loadings [13] Fig. 3.28 Effects of the ratio of shear modulus of the adhesive to that of the adherend 2 on the shear stress distribution τθ z2 /τn , type (A) (2h/d = 0.1, z = h, a = ((c2 + d 2 )/2)1/2 , c = d/2, b = d) [13] 79 80 T. Sawa Fig. 3.29 Effect of the ratio of shear modulus of the adhesive to that of the adherend 2 on the displacement Vθ 2 /Vn , type (A) (2h/d = 0.1, z = h, a = ((c2 + d 2 )/2)1/2 , c = d/2, b = d) [13] Fig. 3.30 Effect of the ratio of shear modulus of the adhesive to that of the adherend 2 on the shear stress distribution τθ z2 /τn , type (B) (2h/d = 0.1, z = h, a = ((c2 + d 2 )/2)1/2 , c = d/2, b = d) [13] 3.5 Analysis with Stress Functions In this section, the method for analyses are described for adhesive butt joints of thin plates (Fig. 3.2; in the case where the two adherends (II) and (III) are the same material) using two-dimensional theory of elasticity and for adhesive butt joints of solid cylinder (Fig. 3.17) using axi-symmetrical theory of elasticity. 3.5.1 Analysis for Two-Dimensional Problems For analyzing the stress state of a two-dimensional elastic body, Airy’s stress functions are applied. When Airy’s stress functions χ are used, each stress component is described by (3.8) and each displacement is described by (3.9). 3 Analytical Models with Stress Functions 81 Fig. 3.31 Effect of the ratio of shear modulus of the adhesive to that of the adherend 2 on the displacement Vθ 2 /Vn , type (B) (2h/d = 0.1, z = h, a = ((c2 + d 2 )/2)1/2 , c = d/2, b = d) [13] σx = ∂ 2χ , ∂ y2 σy = ∂ 2χ , ∂ x2 τxy = − 1 ∂χ ∂ϕ + · ∂x 1+v ∂y 1 ∂χ ∂ϕ + · 2Gvx = − ∂y 1+v ∂x 2Gux = − ∂ 2χ ∂ x∂ y (3.8) ⎫ ⎪ ⎬ ⎪ ⎭ (3.9) where, G: shear modulus, v: Poisson’s ratio, and χ , ϕ must satisfy the following equations, Fig. 3.32 Effect of the adhesive thickness on the shear stress distribution τθ z2 /τn , type (A) (2h/d = 0.1, z = h, a = ((c2 + d 2 )/2)1/2 , c = d/2, b = d) [13] ∇2 ∇2 χ = 0 (3.10) ∇2 ϕ = 0 (3.11) 82 T. Sawa Fig. 3.33 Effects of the ratio of shear modulus of the adhesive to that of the adherend 2 on the shear stress distribution τθ z2 /τn , type (A) (2h/d = 0.1, z = h, a = ((c2 + d 2 )/2)1/2 , c = d/2, b = d) [13] where, ϕ is obtained from the following equation. ∂ 2ϕ = ∇2 χ , ∂ x∂ y ∇2 = ∂2 ∂2 + 2 2 ∂x ∂y (3.12) In the analysis of a two-dimensional body, for example, rectangular plates, Airy’s stress functions χ must be determined from the bi-harmonic equation described by Eq. (3.12). In the analysis for Fig. 3.2 (in the case where the two adherends (II) and (III) are the same material), the stress functions χ I and χ II are chosen as follows, where I I I I I I I I II II II II AI0 , An , Bs , An , Bs , A n , Bs , An , Bs , An , Bs , An , Bs , (n, s = 1, 2, 3 . . .) are unknown coefficients determined from the boundary conditions. I I I I χ1I = χ1 (AI0 , An , Bs , l, h1 , αnI , βs , Δn , Ωs , x, y1 ) I ∞ AI A I = 0 x2 + ∑ I n αn lch(αnI l) + sh(αnI l) ch(αnI x) − αnI xsh(αnI l)sh(αnI x) cos(αnI y1 ) 2 n=1 Δn αnI2 I ∞ B + ∑ I s {βs h1 ch(βs h1 ) + sh(βs h1 )} ch(βs y1 ) − βs y1 sh(βs h1 )sh(βs y1 ) cos(βs x) n=1 Ωs βs2 (3.13) Fig. 3.34 Effect of the ratio of shear modulus of the adhesive to that of the adherend 2 on the displacement Vθ 2 /Vn , type (A): (2h/d = 0.1, z = h, a = d/(2)1/2 , b = d) [13] 3 Analytical Models with Stress Functions 83 Fig. 3.35 A bonded shrink fitted joint subjected to torsion [17] I I I I χ2I = χ2 (An , Bs , l, h1 , αnI , βs , Δn , Ωs , x, y1 ) I ∞ = An αnI lch(αnI l)+sh(αnI l) ch(αnI x)−αnI xsh(αnI l)sh(αnI x) sin(αnI y1 ) I n=1 Δ α I 2 n n I ∞ Bs {βs h1 sh(βs h1 )+ch(βs h1 )} sh(βs y1 )−βs y1 ch(βs h1 )ch(βs y1 ) cos(βs x) + I n=1 Ω β 2 s s ∑ ∑ (3.14) Fig. 3.36 Effect of Young’s modulus of the rings on the interface stress τrθ /σr distributions [17] (b0 /b1 = 0.71, b1 = a2 , E1 /E3 = 1.0, h1 /b1 = 4.57, h3 /b1 = 0.57, δ = 0.02 mm) 84 Fig. 3.37 Effect of the outer diameter of the rings on the stress τrθ /σr distributions [17] (b0 /b1 = 0.71, b1 = a2 , E1 /E3 = 1.0, h1 /b1 = 4.57, h3 /b1 = 0.57, δ = 0.02 mm) Fig. 3.38 Effect of the engagement length on the interface stress τrθ /σr distributions [17] (b0 /b1 = 0.71, b1 = a2 , E1 /E3 = 1.0, h1 /b1 = 4.57, h3 /b1 = 0.57, δ = 0.02 mm) T. Sawa 3 Analytical Models with Stress Functions 85 Fig. 3.39 Comparison of the joint strength between the shrink fitted joint and the bonded shrink fitted joint [17] (2b1 = 35 mm, 2b3 = 80 mm, 2h3 = 20 mm) In , Ω Is , x, y1 ) In , BIs , l, h1 , αnI , βs , Δ χ3I = χ3 (A ∞ In A I I I I I I α lsh( α l)ch( α x) − α xch( α l)sh( α x) cos(αnI y1 ) =−∑ n n n n n n I I 2 n=1 Δn αn ∞ BIs −∑ β h sh( β h )ch( β y ) − β y ch( β h )sh( β y ) cos(βs x) 1 1 1 1 1 1 s s s s s s I 2 n=1 Ωs βs (3.15) I I I I I χ4I = χ4 (A n , Bs , l, h1 , αn , βs , Δn , Ωs , x, y1 ) I A = − ∑ I n αnI lsh(αnI l)ch(αnI x) − αnI xch(αnI l)sh(αnI x) sin(αnI y1 ) n=1 Δ n αnI2 ∞ I Bs βs h1 ch(βs h1 )sh(βs y1 ) − βs y1 sh(βs h1 )ch(βs y1 ) cos(βs x) −∑ I n=1 Ω s βs 2 (3.16) ∞ II II II II χ1II = χ1 (AII0 , An , Bs , l, h2 , αnII , βs , Δn , Ωs , x, y2 ) (3.17) II , Ω II , x, y2 ) IIn , BIIs , l, h2 , αnII , βs , Δ χ3II = χ3 (A n s (3.18) where, αnI = αn (h1 ) = βs = sπ , l nπ , h1 βs = αnI = αn (h1 ) = (2s − 1)π 2l (2n − 1)π , 2h1 αnII = αn (h2 ), αnII = αn (h2 ), 86 T. Sawa I I = ΔI , Δ n n I = Δn (α I l), Δn = Δ n n I Δn = Δn (αnI l) = sh(αnI l)ch(αnI l) + αnI l, II = Δn (α II l) Δ n n II Δn = ΔIn (αnII l), I Ωs = Ωs (βs h1 ) = sh(βs h1 )ch(βs h1 ) + βs h1 , II Ωs = Ωs (βs h1 ) = sh(βs h1 )ch(βs h1 ) − βs h1 , I = Ωs (β h1 ), Ω s s II Ωs = Ωs (βs h2 ), I = Ω (β h1 ), Ω s s s II Ωs = Ωs (βs h2 ), sh: sinh, ch: cosh (i) For finite strip (I) (adherends) x = ±l; I =0 σxI = τxy y1 = h1 ; σyI = F(x) = a0 + ∑ as cos ∞ sπ l s=1 I =0 τxy ⎫ ⎪ ⎪ ⎪ ⎬ ⎪ x ⎪ ⎪ ⎪ ⎪ ⎭ (3.19) (ii) For finite strip (II) (adhesive) II σxII = τxy =0 x = ±l; (iii) at the interface between finite strips (I) and (II) I σy y =−h = σyII y =h 1 I τxy I u 1 II = τxy y1 =−h1 = uII y1 =−h1 ∂ vI ∂x = y1 =−h1 2 2 y2 =h2 y2 =h2 ∂ vII ∂x (3.20) ⎫ ⎪ ⎪ ⎪ ⎪ ⎪ ⎪ ⎪ ⎪ ⎪ ⎪ ⎬ (3.21) ⎪ ⎪ ⎪ ⎪ ⎪ ⎪ ⎪ ⎪ ⎪ ⎪ ⎭ y2 =h2 where, a0 = 1 2l e1 −e1 F(x)dx, as = 1 l e1 −e1 F(x) cos sπ x dx l (s = 1, 2, 3, · · ·) Substituting Airy’s stress functions χ I and χ II into Eqs. (3.8) and (3.9), the stresses and the displacements for the finite strips [I] and [II] are obtained. By equating them to the boundary conditions, the relations among undetermined coefficients are obtained as follows: 3 Analytical Models with Stress Functions 87 ⎫ ∞ ∞ I ∞ ∞ I I I I I I I I I ⎪ In + ∑ BIs Sns ⎪ B An + ∑ Bs Pns = 0, An − ∑ Bs Pns = 0, A = 0, A + S = 0 ∑ ⎪ n s ns ⎪ ⎪ s=1 s=1 s=1 s=1 ⎪ ⎪ ⎪ ∞ ∞ ∞ ∞ ⎪ I I II I II II I II II II I I ⎪ n + ∑ Bs Sns = 0, ∑ An Qns +Bs − ∑ An Qns + Bs = −as ⎪ ⎪ An + ∑ Bs Pns = 0, A ⎪ ⎪ ⎪ s=1 s=1 n=1 n=1 ⎪ ⎪ ⎪ ∞ ∞ ⎪ I I ⎪ I ⎪ I I I ⎪ A R + B + R + B = 0 A ⎪ ∑ n ns s ∑ n ns s ⎪ ⎪ n=1 n=1 ⎪ ⎪ ⎪ ∞ ∞ ∞ ⎬ I I I I I II I I II ∑ An Qns +Bs + ∑ An Qns − Bs − ∑ An Qns −Bs = 0 ⎪ n=1 n=1 n=1 ⎪ ⎪ ⎪ ⎪ ∞ ∞ ∞ I I ⎪ ⎪ I I I I II II II ⎪ A A R + B − R − B + R + B = 0 A ⎪ ∑ n ns s ∑ n ns s ∑ n ns s ⎪ ⎪ ⎪ n=1 n=1 n=1 ⎪ ⎪ ⎪ ∞ ∞ ∞ ∞ I ⎪ I I I I I I ⎪ I I I I II I II ⎪ ⎪ ∑ AnUns + BsVs + ∑ AnUns + BsVs + ∑ BmWmCms − ∑ BmWm Cms ⎪ ⎪ ⎪ n=1 n=1 m=1 m=1 ⎪ ⎪ ⎪ ∞ ∞ ⎪ II II II II ⎪ II II II II ⎪ − ∑ An Uns − Bs Vs − ∑ BmWm Cms = Ds ⎭ n=1 m=1 (3.22) AI0 = a0 , AII0 = AI0 (3.23) where, 4(−1)n+s α I2 λ sh2 (λ h ) I II s 1 n s I II Pns = Pns αnI , λs , h1 , Ωs = , Pns = Pns αnII , λs , h2 , Ωs I 2 Ωs (αnI + λs2 )2 h1 4(−1)n+s α I2 λ ch2 (λ h ) n s s 1 I I I II II IIs , S = S α , λ , h , Ω Sns = Sns αn , λs , h1 , Ωs = ns 2 ns s n I (α I2 + λ 2 )2 h1 Ω s n s 4(−1)n+s α I λ 2 sh2 α I l I II n s n , QIIns = Qns αnII , λs , l, Δn QIns = Qns αnI , λs , l, Δn = I 2 Δn (αnI + λs2 )2 l 4(−1)n+s αnI λs2 ch2 αnI l I = II , RIIns = Rns αnII , λs , l, Δ RIns = Rns αnI , λs , l, Δ n n 2 I (α I + λ 2 )2 l Δ n n s I I I I I s , QIns = Qns αnI , λs , l, Δn = Pns αnI , λs , h1 , Ωs , Sns = Sns αnI , λs , h1 , Ω Pns I n RIns = Rns αnI , λs , l, Δ I Uns = I Uns (αnI , Δn , G1 , ν1 ) = 2(−1)n+s λs sh2 (αnI l) I 2 αI 1 + 2 n 1 + ν1 αnI + λs2 Δn αnI (αnI + λs2 )G1 l 1 ν1 − 1 I λ h + sh( λ h )ch( λ h ) VsI = Vs (λs , h1 , Ωs , G1 , ν1 ) = s s s 1 1 1 I 1 + ν1 2Ωs λs G1 2 88 T. Sawa I ν1 − 1 1 I Vs = Vs (λs , h1 , Ωs , G1 , ν1 ) = λs h1 − sh(λs h1 )ch(λs h1 ) I 1 + ν1 2Ωs λs G1 2 2 I , E1 ) = 2sh (λs h1 ) I , E1 ) = 2ch (λs h1 ) ,W I = W (λ , h1 , Ω WsI = Ws (λs , h1 , Ω s s s s s I I λ E1 Ω s s λ E1 Ω s s n+s α I ch2 (α I l) 2 − α I2 (−1) ν λ 3 + 1 n n n s I I I Hns = Hns (αn , Δn , G1 , ν1 ) = + In αnI (αnI2 + λs2 )G1 l 1 + ν1 αnI 2 + λs2 Δ I II II I II = Uns (αnI , Δn , G1 , ν1 ),Uns = Uns (αnII , Δn , G2 , ν2 ),VsII = Vs (λs , h2 , Ωs , G2 , ν2 ) Uns I II , E2 ), F I = λs ×Ws (λs , h1 , Ω , E1 ), F I = λs ×Ws (λs , h1 , Ω , E1 ) WsII = Ws (λs , h2 , Ω s s s s s I I II I , G1 , ν1 ), H II = Hns (α II , Δ II , G2 , ν2 ) = Hns (αnI , Δ FsII = λs ×Ws (λs , h2 , Ωs , E2 ), Hns ns n n n I , G1 , ν1 ) I , G1 , ν1 ), J I = λ ×V (λ , h1 , Ω JsI = λs ×Vs (λs , h1 , Ω s s s s s s II II Js = λs ×Vs (λs , h2 , Ωs , G2 , ν2 ) 1 1 1 II Cms = Cms (λm , λs ) = − sin λm + λs l − sin λm − λs l l λm + λs λm − λs 2 E1 E2 ν2 ν1 II = Ems (λm , λs ), DIIs = AI0 (−1)s − , G2 = , G1 = Ems λs E2 E1 2(1 + ν1 ) 2(1 + ν2 ) By solving an infinite set of simultaneous Eq. (3.22), the undetermined coeffiI I IIn and BIIs are determined. From Eq. (3.23), AI and AII are decients An , Bs , . . ., A 0 0 termined. Using the determined coefficients, the stresses and the displacements are obtained. 3.5.2 Analysis for Axi-Symmetrical Elastic Bodies For analyzing the stress states of axi-symmetrical bodies such as solid cylinders (shafts) or hollow cylinders (tubular), Michell’s stress functions are applied. When Michell’s stress functions Φ are used, each stress component σr, σθ , σz, τrz are described as follows. ⎫ ∂ ∂ 2Φ ⎪ 2 ⎪ σr = ν∇ Φ − 2 ⎪ ⎪ ∂z ∂r ⎪ ⎪ ⎪ ⎪ ⎪ ⎪ ∂ 1 ∂Φ ⎪ 2 ⎪ σθ = ν∇ Φ − ⎪ ⎬ ∂z r ∂r (3.24) ∂ ∂ 2Φ ⎪ ⎪ 2 ⎪ σz = (2 − ν )∇ Φ − 2 ⎪ ⎪ ⎪ ∂z ∂z ⎪ ⎪ ⎪ ⎪ 2 ⎪ ⎪ ∂ ∂ Φ 2 ⎭ τrz = (1 − ν )∇ Φ − 2 ⎪ ∂r ∂z 3 Analytical Models with Stress Functions 89 ⎫ ⎪ ⎪ ⎪ ⎬ 1 + ν ∂ 2Φ E ∂ r∂ z ∂ 2Φ 1 ∂ Φ ⎪ 1+ν ⎪ 2 ⎪ ⎭ wz = (1 − 2ν )∇ Φ + 2 + E ∂r r ∂r ur = − (3.25) where, ur is the displacement in the radial direction and wz is the displacement in the z-direction. G is the modulus in shear (G = E / 2(1 + ν )). Michell’s stress function Φ must satisfy the following bi-harmonic equation. ∇2 ∇2 Φ = 0 where, ∇2 = (3.26) 1 ∂2 ∂2 1 ∂ + + ∂ r 2 r ∂ r r 2 ∂ z2 In the analysis for the case of Fig. 3.18, the stress functions ΦI and ΦII are chosen I I I I I I I I II II II II II I , CI , A In , CsI , A as follows, where, A0 , C0 , An , Cs , An , Cs , A n , Cs , A0 , C0 , An , Cs , An , 0 0 II II II II II , C , A n and C (n, s = 1, 2, 3, · · ·) are unknown coefficients determined from Cs , A 0 0 0 the boundary conditions, where Jμ (r) is the first kind of Bessel function of order μ , Iμ (r) is the first kind of modified Bessel function of order μ and λs is the positive root satisfying the equation J1 (λs ) = 0, and Iμ (βn a) is abbreviated as Iμ a , Iμ (βn r) as Iμ r , Iμ (βn a) as I μ a , Iμ (βn r) as Iμ r , and sinh is abbreviated as sh and cosh as ch. I I I I I I ΦI1 = Φ1 (A0 ,C0 , An ,Cs , a, h1 , βnI , γs , Δn , Ωs , ν1 , r, z1 ) 3 I z1 = A0 I z1 r +C0 2 ∞ +∑ I An 3 I 6 2 n=1 βnI Δn × 2(1 − ν1 )I1a + βnI aI0a I0r − βnI rI1a I1r sin(βnI z1 ) (3.27) I Cs ν sh( γ h ) + γ h ch( γ h ) − 2 s s s 1 1 1 1 I s=1 γs3 Ωs × sh(γs z1 ) + γs z1 sh(γs h1 )ch(γs z1 ) J0 (γs r) ∞ +∑ I I I I ΦI2 = Φ2 (An ,Cs , a, h1 , βnI , γs , Δn , Ωs , ν1 , r, z1 ) ∞ =−∑ I An I n=1 β I3 Δ n n 2(1 − ν1 )I1a + βnI aI 0a × I 0r − βnI rI 1a I1r cos(βnI z1 ) I Cs − 2 ν ch( γ h ) + γ h sh( γ h ) s 1 s 1 s 1 1 I s=1 γ 3 Ω s s × ch(γs z1 ) + γs z1 ch(γs h1 )sh(γs z1 ) J0 (γs r) ∞ +∑ (3.28) 90 T. Sawa I In , Ω Is , ν1 , r, z1 ) I0 , C0I , A In , CsI , a, h1 , βn , γs , Δ ΦI3 = Φ3 (A ∞ 3 2 I I0 z1 + C0I z1 r + ∑ An =A I3 I 6 2 n=1 βn Δn × 2(1 − ν1 )I1a + βnI aI0a I0r − βnI rI1a I1r sin(βnI z1 ) (3.29) CsI 2(1 − ν1 )ch(γs h1 ) − γs h1 sh(γs h1 ) 3 I s=1 γs Ωs ×sh(γs z1 ) + γs z1 ch(γs h1 )ch(γs z1 ) J0 (γs r) ∞ +∑ I I I I I ΦI4 = Φ4 (A n , Cs , a, h1 , βn , γs , Δn , Ωs , ν1 , r, z1 ) I A n =−∑ 2(1 − ν1 )I1a + βnI aI0a I0a − βnI rI1a I1r I n=1 β I3 Δ n n ∞ (3.30) I Cs +∑ ν )sh( γ h ) − γ h ch( γ h ) (1 − 2 s s s 1 1 1 1 I s=1 γ 3 Ω s s ×ch(γs z1 ) + γs z1 sh(γs h1 )sh(γs z1 ) J0 (γs r) ∞ II II II II II II ΦII1 = Φ1 (A0 ,C0 , An ,Cs , a, h2 , βnII , γs , Δn , Ωs , ν2 , r, z2 ) IIn , Ω IIs , ν2 , r, z2 ) II0 , C0II , A IIn , CsII , a, h2 , βnII , γs , Δ ΦII3 = Φ3 (A (3.31) (3.32) where, βnI = βn (h1 ) = nπ , h1 βnI = βn (h1 ) = (2n − 1)π II , βn = βn (h2 ), βnII = βn (h2 ) 2h1 I γs = λs /a, Ωs = Ωs (γs h1 ) = sh(γs h1 )ch(γs h1 ) + γs h1 I Ωs = Ωs (γs h1 ) = sh(γs h1 )ch(γs h1 ) − (γs h1 ), I = ΩI , Ω s s I =Ω Ω s s I IIs = ΩIIs Ω 1 Δn = Δn (βnI a, ν1 ) = 2(1 − ν1 ) + (βnI a)2 I21a − (βnI a)I20a /βnI a II Ωs = Ωs (γs h2 ), 1 Δn = Δn (βnI a, ν1 ), I1 Δn = Δn (βnII a, ν2 ), 1 I = Δ , Δ n n I = Δ1 Δ n n IIn = Δn (βnII a, ν2 ) Δ 3.6 Conclusions In this chapter, the interface stress characteristics of adhesive butt joints have been examined. At first, several types of adhesive butt joints are shown and the effects of some factors such as the adhesive Young’s modulus and the adhesive thickness 3 Analytical Models with Stress Functions 91 on the interface stress distributions are described. For adhesive butt joints of thin plates, solid cylinders and hollow cylinders (tubular joints), it was shown that the singular stresses occur at the edges of the interfaces between the adherends and the adhesive and they decrease as the adhesive Young’s modulus increases and the adhesive thickness decreases. It was shown that the bonded area in the band adhesive joints is smaller than that in the adhesive butt joints while the strength of the band adhesive joints is the same approximately as that of the adhesive butt joints. Then, an example of method of analysis for the adhesive butt joints of thin plates and solid cylinders using the stress functions was presented. For two-dimensional problems, Airy’s stress functions were used while for axi-symmetrical problems, Michel’s stress functions were used. For analyzing the singular stresses which occurred at the edges of the interfaces, an analytical method was superior to a computational method such as FEM because the singular stresses depend on the mesh sizes in the FEM. However, the mentioned methods of stress analyses were carried out in the elastic deformation range. In near future, the method should be developed in the elastoplastic region for obtaining more detailed results in estimating the joint strength. Generally, adhesive joints are used under severe conditions and bad environment. In many applications, the joints are subjected to static loadings as well as impact loadings. In near future, adhesive joints will be analyzed under static and impact loading conditions in the elasto-plastic range of the adhesive. References 1. Andersson T. and Biel A. 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(1987) A Stress Analysis of Butt Adhesive Joints Under Torsional Loads. J Adhes 24: 245–258 14. Sawa T., Temma K. and Ishikawa H. (1989) Three-Dimensional Stress Analysis of Adhesive Butt Joints of Solid Cylinders Subjected to External Tensile Loads. J Adhes 31: 33–43 15. Sawa T., Temma K., Nishigaya T. and Ishikawa H. (1995) A Two-Dimensional Stress Analysis of Adhesive Butt Joints of Dissimilar Adherends Subjected to Tensile Loads. J Adhes Sci Technol 9(2): 215–236 16. Sawa T. and Uchida H. (1997) Two-Dimensional Stress Analysis and Strength Evaluation of Band Adhesive Butt Joints Subjected to Tensile Loads. J Adhes Sci Technol 11(6): 811–833 17. Sawa T., Yoneno M. and Motegi Y. (2001) J. Adhes Sci Technol 15(1): 23–42 18. Seo D. W. and Lim J. K. (2005) Tensile, Bending and Shear Strength Distributions of Adhesive-Bonded Butt Joint Specimens. Compos Sci Technol 65: 1421–1427 19. Shahid M. and Hashim S. A. (2002) Effect of Surface Roughness on the Strength of Cleavage Joints. 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(1993) Vicoelastic Analysis of Bonded Tubular Joints Under Torsion. Int J Solids Struct 30(16): 2199–2211 Part II Numerical Modeling Chapter 4 Complex Constitutive Adhesive Models Erol Sancaktar Abstract A complete approach to modeling adhesives and adhesive joints needs to include considerations for: deformation theories, viscoelasticity, singularity methods, bulk adhesive as composite material, adhesively bonded joint as composite and the concept of the “interphase”, damage models, and the effects of cure and processing conditions on the mechanical behavior. The adherend surfaces have distinct topographies, which result in a collection of miniature joints in micron, and even nano scale when bonded adhesively. The methods of continuum mechanics can be applied to this collection of miniature joints by assuming continuous, or a combination of continuous/discontinuous interphase zones. 4.1 Introduction Adhesively bonded joints are complex composite structures with at least one of the constituents, namely the adhesive, most often, being a composite material itself due to the presence of secondary phases such as fillers, carriers, etc. The joint structure possesses a complex state of stress with high stress concentrations, and often, singularities due to the terminating adhesive layer where the substrates may possess sharp corners. Consequently, accurate analysis and modeling of adhesive materials and bonded joints require the use of the methods of composite materials and composite mechanics. The inclusion of the “interphase” region is necessary in this analysis as a distinct continuum. The presence of geometric discontinuities creates stress concentrations and, possibly, singularities adding additional complexity to the topic of adhesively bonded joints. This problem, however, can be alleviated, at least partially, by making the proper changes in the geometry of the bonded joint. Furthermore, since most adhesive materials are polymer-based, their natural viscoelastic Erol Sancaktar Polymer Engineering, Adjunct Professor, Mechanical Engineering, The University of Akron, Akron, OH 44325-0301, e-mail: erol@uakron.edu L.F.M. da Silva, A. Öchsner (eds.), Modeling of Adhesively Bonded Joints, c Springer-Verlag Berlin Heidelberg 2008 95 96 E. Sancaktar behavior usually serves to reduce localized stress concentrations. In those cases where brittle material behavior prevails or, in general, when inherent material flaws such as cracks, voids, disbonds exist, then the use of the methods of fracture mechanics are called for. For continuum behavior, however, the use of damage models is considered appropriate in order to be able to model the progression of localized and non-catastrophic failures. Obviously, a technical person involved in adhesive development and/or applications should keep the above mentioned issues in mind, along with insight into typical joint stress distributions for adhesive joints as well. Stress distributions are relevant from the mechanical adhesion point of view also, since they depend on surface topography, which can be considered a collection of many geometrical forms. Therefore, mechanical adhesion depends on the stress states of different adhesive joint geometries on the scale of the surface topography, which may include many lap, butt and scarf joints in the interphase region. A complete approach to modeling adhesives and adhesive joints, therefore, needs to include considerations for: deformation theories, viscoelasticity, singularity methods, bulk adhesive as composite material, adhesively bonded joint as composite – the concept of the “interphase”, damage models, and the effects of cure and processing conditions on the mechanical behavior. 4.2 Deformation Theories The deformation theory was first introduced by Hencky (1924) as reported by Hill (1956) and Kachanov (1971) in the form: εi j = (σkk /9 K)δi j + ψ Si j (4.1) where, Si j is the deviatoric stress tensor. Equation (4.1) reduces to the elastic stressstrain relations when ψ = 1/2G, where G is the elastic shear modulus. If the scalar function ψ is defined as ψ = (1/2 G) + Ω (4.2) then Eq. (4.1) can be interpreted in the form ε i j = εi j E + εi j V + εi j P (4.3) εi j = (σkk /9 K)δi j + (Si j /2G) + Ω Si j (4.4) εi j P = Ω Si j (4.5) where and, with Ω being a scalar function of the invariants of the stress tensor, and the superscripts E, V and P representing elastic, viscoelastic and plastic behaviors, respectively. 4 Complex Constitutive Adhesive Models 97 Consequently, the relation ε = (σ /E) + Λ σ (4.6) is obtained for uniaxial tension on the basis of Eqs. (4.4) and (4.5) with Λ = 2Ω/3. Ramberg and Osgood (1943) used a special form of Eq. (4.6) with Λ = K σ n−1 to result in: ε = (σ /E) + K σ n (4.7) where, K and r are material constants. They reported that Eq. (4.7) could be used successfully to describe uniaxial tension and compression behavior of various metal alloys. Equation (4.7) was later modified by McLellan (1966, 1969) to accommodate strain rate effects. McLellan interpreted the terms E, K and n of Eq. (4.7) as material functions with the function E representing viscoelastic behavior and functions K and n representing workhardening characteristics. The terms E, K and n were all described as functions of the strain rate (dε /dt) so that rigidity, stress and plastic flow respectively were all affected by variations in the strain rate. Renieri et al. (1976) used a bilinear form of rate dependent Ramberg-Osgood equation to describe the stress-strain behavior of a thermosetting adhesive in the bulk tensile form. The bilinear behavior was obtained when log ε p was plotted against log σ , where ε p represents the second term on the right-hand side of Eq. (4.7). The model adhesive they used was an elastomer modified epoxy adhesive with and without carrier cloth. They made several modifications on the form of the equation previously used by McLellan. First, the plastic strain ε p was assumed to be a function of the over-stress above the elastic limit stress (the development of over-stress approach will be presented subsequently) and second, the stress levels σ ∗ defining the intersection point for the bilinear behavior were found to occur slightly below the stress whitening stress values. The equations they developed in this fashion are given as: ε = σ /E, 0<σ <θ (4.8-1) ε = (σ /E) + K1 [σ − θ ]n1 θ < σ < σ∗ (4.8-2) ε = (σ /E) + K2 [σ − θ ] n2 ∗ σ <σ <Y (4.8-3) where, θ is the elastic limit stress (yield stress) in simple tension, Y is the maximum stress, K1 , K2 , n1 , and n2 are strain rate dependent material functions. Renieri et al. (1976) reported that the adhesive material properties were different before and after stress-whitening due to changes in material behavior and therefore bilinear equations of the form (4.8) were needed to describe such behavior. Brinson et al. (1975) determined that for the adhesive with the carrier cloth the parameter n, Eq. (4.7), varied much less with strain rate in comparison to the adhesive without the carrier cloth. They concluded that the bilinear forms they proposed, Eq. (4.8), accurately predicted the rate dependent behavior of their model adhesive. 98 E. Sancaktar Figures 4.1 and 4.2 show the application of the model described above to the stress-strain and stress whitening behaviors of a bulk thermosetting epoxy film adhesive containing a non-woven nylon mat, as obtained by Sancaktar and Beachtle (1993). In this application, two intersection points are identified by intersecting two pairs of bilinears, each of which containing a common slope line as part of the bilinear sets (Fig. 4.2). This procedure was called “dual bilinear fit” by Sancaktar and Beachtle (1993). These intersection points define upper and lower stress whitening stress limits shown in Fig. 4.1. Ramberg-Osgood type equations were also used to describe shear behavior of structural adhesives. Zabora et al. (1971) used a rate dependent form of the Ramberg-Osgood equation to describe the shear behavior of structural adhesives in the bonded form. Simple power function type relations may be utilized in an empirical fashion to describe nonlinear elastic behavior of structural adhesives in tensile and shear modes when their mechanical behavior is found to be relatively rate insensitive. For example Sancaktar and Schenck (1985-a) used a power function relation given by τ = Kγ r (4.9) where τ and γ are shear stress and strain respectively, to represent the nonlinear elastic shear behavior of a thermoplastic polyimidesulfone adhesive in the bonded form. Sancaktar and Dembosky (1986) showed that when the stress-strain curve has a well defined initial elastic region and a yield point, τy , then a bimodal relation given by Fig. 4.1 A stress-strain diagram identifying upper and lower stress whitening stress limits, σU and σLo ∗ respectively, as well as the visually observed stress whitening stress. The modulus of elasticity, E, and the elastic limit stress, θ for the bulk adhesive tested are 3.3 × 105 and 3.5 × 103 psi, respectively (Sancaktar and Beachtle, 1993) 4 Complex Constitutive Adhesive Models 99 Fig. 4.2 A stress-strain diagram identifying upper and lower stress whitening stress limits, σU and σLo ∗ respectively, as well as the visually observed stress whitening stress. The modulus of elasticity, E, and the elastic limit stress, θ for the bulk adhesive tested are 3.3 × 105 and 3.5 × 103 psi, respectively (Sancaktar and Beachtle, 1993) γ = τ /G, γ = Bτ m τ < τy τ > τy (4.10-1) (4.10-2) can be utilized more appropriately. 4.3 Viscoelasticity Considerations 4.3.1 Linear Viscoelasticity The differential forms of the fundamental constitutive relations are given as: P{Skl } = 2Q{εkl } P {σ } = Q {ε } − Q {AT } (4.11) (4.12) where, A is the thermal expansion function, T is the temperature, Skl and εkl are stress and strain deviators respectively and the differential operators are defined as: u P = ∑ ai (x,t, T )∂ i /dt i (4.13) Q = ∑ bi (x,t, T )∂ i /∂ t i (4.14) i=0 v i=0 100 E. Sancaktar u P = ∑ ai (x,t, T )∂ i /∂ t i (4.15) i=0 v Q = ∑ bi (x,t, T )∂ i /∂ t i (4.16) i=0 v Q = ∑ bi (x,t, T )∂ i /∂ t i (4.17) i=0 T (x,t) Q {AT } = ∫ Q {α (T )}dT (4.18) T0 v i i Q = ∑ b i (x,t, T )∂ /∂ t . (4.19) i=0 In Eqs. (4.13) through (4.19) the terms ai , ai , bi , bi , bi and bi are material properties and the integers u, u , v, v , v and v reflect the complexity of the material behavior, and t represents time. In Eq. (4.18) the quantity α represents the coefficient of thermal expansion. The same constitutive relations can also be represented in integral equation form given by: t t −∞ −∞ σ (x,t) = ∫ EV (x,t,t )[∂ ε (x,t )/∂ t ]dt − ∫ EV T (x,t,t )∂ [AT (x,t )]/∂ t dt and (4.20) t Skl (x,t) = 2 ∫ E(x,t,t )∂ εkl (x,t )/∂ t dt −∞ (4.21) where EV and EV T are the relaxation moduli as functions of time and time and temperature, respectively, and E is the “relaxation memory function”. As shown by Flügge (1975), the assumptions of elastic dilatational behavior or no volume change are frequently used in three dimensional analyses of polymeric materials. As for distortion operations, however, any mechanical model (such as Maxwell, Kelvin, three-parameter solid, etc.) can be used. 4.3.2 Interrelationship Between the Tensile and Shear Properties The constitutive equations proposed for characterization of solid polymer materials in the tensile mode can be reformulated for the case of pure shear. One approach is to replace tensile stress and strain variables by their shear counterparts. It is usually desirable to run a simple bulk tensile test program and subsequently predict (calculate) shear properties from their tensile counterparts. This approach requires a clearly defined relationship between shear and tensile elastic limit and yield variables and material properties. The elastic limit and yield stress values can be related between tensile and shear conditions by using an appropriate failure criterion, 4 Complex Constitutive Adhesive Models 101 such as maximum normal stress, maximum shear stress, distortion energy criteria, etc. A material parameter that needs to be converted in addition to the usual elastic properties is the viscosity coefficient. This can be done by using Tobolsky’s (1960) assumption of equivalent relaxation times in shear and tension. Application of this assumption results in the relation μS = μT /2(l + υ ) (4.22) where μS and μT refer to the viscosity coefficients in shear and tension respectively, and υ is Poisson’s ratio. An application of this procedure for a linear viscoelastic (over-stress) model was shown by Sancaktar and Brinson (1980). 4.3.3 Time-Temperature Superposition The time-temperature superposition principle (TTSP) is used to extend the creep and relaxation data obtained at higher temperatures to values at lower temperatures and longer times in the same strain and stress ranges. Provided that no structural changes occur in the material at high temperatures, TTSP can be used for amorphous and semi-crystalline thermoplastics and thermosets for extrapolation purposes. In order to apply this principle, one should first construct a “master curve,” where the complete compliance-time or relaxation modulus-time behavior is plotted at a constant temperature. For the “master curve” a reference temperature To is chosen. As shown by Ahlonis et al. (1972), the relation for the compliance observed at any time t and temperature To is given in terms of the experimentally observed compliance values at different temperatures T as: D(To ,t) = [ρ (T )T /ρ (To )To ]D(T,t/aT ) (4.23) D(t) = ε (t)/σ (4.24) where and ρ (T ) is the temperature dependent density. An illustration of this procedure is shown in Fig. 4.3, where adjustments for any change in the material density are ignored. A similar relation for the relaxation modulus is given as: E(To ,t) = [ρo (To )To /ρ (T )T ]E(T, aT t) (4.25) E(t) = σ (t)/ε . (4.26) where, The term aT is a time shift factor which can be obtained with the application of the famous Williams-Landel-Ferry (WLF) equation, reported by Ferry (1961). For most polymeric materials the polymer’s glass transition temperature (Tg ) is chosen as the reference temperature for accurate results. Even though Ferry (1961) 102 E. Sancaktar Fig. 4.3 An illustration of time-temperature (t-T ) superposition procedure for shifts in creep compliance, D(t). Adjustments for any change in the material density are ignored reports that the above equations have not been proven to be valid below the Tg , data showing its application for T < Tg is available in the literature. Examples of applications to structural adhesives in the bulk form were given by Renieri et al. (1976) and Keuner et al. (1982). The application of the TTSP can be extended into the nonlinear viscoelastic region, as shown by Darlington and Turner (1978). Examples on the establishment of rate-temperature superposition based on WLF equation as applied to peeling problems have been given by Kaelble (1964, 1969), Hata et al. (1965) and Nonaker (1968). Nakao (1969) and Koizumi et al. (1970) report superposition based on Arrhenius’ equation. 4.3.4 Nonlinear Viscoelasticity Equations (4.11), (4.12) and (4.20), (4.21) can also be used to describe nonlinear material behavior provided that ai , bi , etc. and E, EV are functions of stresses, strains, their derivatives and their invariants in addition to the functional variables shown. On the basis of their observations on polymers, composites and adhesives, Hiel et al. (1983), Rochefert and Brinson (1983), Tuttle and Brinson (1984) and Zhang et al. (1985) report that the extent of nonlinearity is dependent on both the stress level and the time scale. Constitutive relations having the form of Eqs. (4.20) and (4.21) are in agreement with this observation. Schapery (1966, 1969a, b), reports that stress and strain dependent material properties of nonlinear constitutive equations have a thermodynamic origin. For example the one-dimensional constitutive relation t ε = g0 D(0)σ + g1 ∫ ΔD(φ − φ )[d(g2 σ )/d τ ]d τ (4.27) o includes the variables g0 , g1 and g2 which reflect stress dependence of the Gibbs free energy. In Eq. (4.27) D(0) is the initial value of the linear viscoelastic creep compliance, ΔD(φ ) is the transient component and the quantities 4 Complex Constitutive Adhesive Models 103 t φ = φ (t) = ∫ dt /aσ (4.28) o and τ φ = φ (τ ) = ∫ dt /aσ (4.29) o are reduced time parameters and depend on the shift function aσ . “aσ ” is a function of stress and change with entropy production and free energy changes. An equation similar to (4.27) can be written with strain as the independent state variable. In this equation, the strain dependent properties h0 , h1 , h2 and aε reflect the changes in the Helmholtz free energy. Schapery’s Eq. (4.27) was applied extensively by Cartner et al. (1978), Peretz and Weitsman (1982) and by Tuttle and Brinson (1985) in characterization of resin matrix composites. In using nonlinear mechanical models, in addition to utilizing nonlinear elastic and shear thickening or thinning dashpot elements, one can also incorporate nonlinearity by means of a perturbation technique. This is accomplished by adding small perturbation terms which are functions of the current level of elastic strain and strain rate to the elastic and viscous coefficients respectively. This method was originally proposed by Davis (1964) and later applied in material characterization of bulk adhesives by Renieri et al. (1976). Further discussions on nonlinear viscoelastic theory are given by Green and Adkins (1960) and Hilton (1975). 4.3.5 Empirical Description of Creep Behavior The constitutive equations obtained with the use of mechanical models can be solved for the creep condition given by σ (t) = σo H(t) (4.30) with σo and H(t) describing the level of constant stress and the unit step function respectively, to result in a creep equation. In some cases, however, empirical relations describing time dependent strain functions are preferred over this method for practical reasons. Actual creep data can be fitted with such functions to yield accurate analysis in conjunction with equations of the form (4.20), (4.21) or (4.27). A variety of mathematical forms have been proposed to describe the creep behavior of adhesives and polymers in an empirical fashion. The simplest procedure is called the log-log method based on the assumption that the logarithm of the secondary creep rate is linearly related to the logarithm of the stress level at which the creep occurs. This assumption results in a creep relation which is a linear function of time but nonlinear function of stress in the secondary range. An application of this method to polymeric materials was given by Sancaktar et al. (1987-a). 104 E. Sancaktar The creep relation which is most commonly used in the literature is the “powerlaw” compliance given by (4.31) D(t) = D0 + D1 t n where, D0 is the instantaneous compliance, D1 , and n are material constants. Note that Eq. (4.31) allows time reduction by a stress-dependent shift-factor to describe stress enhanced creep. Equations of this form were used by researchers such as Weitsman (1981) and Ravi-Chandar and Knauss (1984) for viscoelastic stress analysis and fracture mechanics considerations (respectively) of adhesives and polymeric materials. Various methods have been proposed to determine the parameters D0 , D1 and n of Eq. (4.31). For example Findley and Peterson (1958) subtract the instantaneous strain from the total strain and plot the transient strain on log-log paper. Other methods were described by researchers such as Boller (1957), Knauss and Enri (1981), Dillard et al. (1982), Dillard and Brinson (1983), Becher (1984) and Henriksen (1984). A comparison and discussion of these methods was given by Dillard and Hiel (1985). As shown by Sancaktar (1991), Figs. 4.4 and 4.5 illustrate the variation of adhesive shear stress at the overlap edges of double lap joints as predicted by linear and nonlinear viscoelastic analyses. In Fig. 4.4, the linear analysis was performed using the Maxwell model with different relaxation times, T , and the nonlinear analysis was performed using Eq. (4.31) with a stress-dependent shift factor. Figure 4.5 illustrates the ability to obtain matching results between the two models by using the Maxwell model with variable relaxation time, T , as given by Sancaktar (1991). Additional methods and discussions on constitutive equations for creep were given by Odquist (1954), Findley and Lai (1967), Gittus (1975) and Findley et al. (1976). 4.3.6 Increases in Joint Strength Due to Rate Dependent Viscoelastic Adhesive Behavior Due to their viscoelastic nature, most adhesives exhibit rate dependent material behavior, which can be modeled, for example, by using mechanical model characterization. In order to describe the rate dependence of limit stress and elastic limit strain for polymeric and adhesive materials in the bulk form, Renieri et al. (1976) and Sancaktar and Brinson (1980) utilized a semi-empirical approach proposed by Ludwik (1909) in the form: dγ dγ τult = τ + τ log (4.32) dt dt where, τult is the ultimate shear stress, d γ /dt is the initial elastic strain rate, and τ , τ , and dγ /dt are material constants. 4 Complex Constitutive Adhesive Models 105 Fig. 4.4 Variation of adhesive shear stress at the overlap edges of double lap joints as predicted by linear and nonlinear viscoelastic analyses. The linear analysis was performed using the Maxwell model with different relaxation times, T , and the nonlinear analysis was performed using Eq. (4.31) with a stress-dependent shift factor. The joint dimensions used in analysis are also shown with δ , L and d representing adhesive thickness, overlap length and the main plate thickness, respectively. Es and Ga represent the Young’s modulus for the substrate and the shear modulus for the adhesive, respectively (Sancaktar, 1991) Renieri et al. (1976) and Sancaktar and Brinson (1980) used the same form of Eq. (4.32) to describe the variation of elastic limit shear stress (τel ) and strains (γel ) with initial elastic strain rates. These expressions may be written as: dγ dγ τel = φ + φ log (4.33) dt dt and, dγ γel = ζ + ζ log dt dγ dt (4.34) where, additional material constants are defined accordingly. Sancaktar et al. (1984, 1985-b) later showed applicability of Eqs. (4.32) through (4.34) for adhesives in the bonded form and also proposed superposition of temperature effects on these equations. As reported by Ward and Hadley (1993), the theoretical basis of Eq. (4.32) can be found in the Eyring Theorem, according to which the mechanical response of an adhesive is a process that has to overcome a potential barrier, (ΔE). The author thinks 106 E. Sancaktar Fig. 4.5 Variation of maximum adhesive shear stress in double lap joints based on nonlinear viscoelastic analysis, using Eq. (4.31) with a stress-dependent shift factor, and linear viscoelastic analysis, using the Maxwell model with variable relaxation time, T (Sancaktar, 1991) that this barrier decreases not only with increasing stress but also with increasing temperature. Based on the Eyring Theorem, the relationship between a limit stress, say τel , and the strain rate can be written as: dγ /dt = A exp[(τelV − ΔE)/RT ] (4.35) where, A is a pre-exponential factor, R is the gas constant, and V is the activation volume. Equation (4.35) can be expressed in logarithmic form as: dγ τel = {ΔE/V } + 2.303 RT log A V. (4.36) dt Sharon et al. (1989) applied Eq. (4.36) to describe rate and temperature dependent variation of four structural adhesives in the bulk form. They used the shift factor [log(1/A)] × 10−3 on the temperature (◦ C) to describe the effect of rate. Another example for bonded joint behavior was given by Chalkley and Chiu (1993). If the energy barrier term ΔE/V of Eq. (4.36) is also affected by temperature then one needs two shift factors in Eqs. (4.32) through (4.34) to describe rate-temperature effects on limit stress-strain equations: dγ dγ τel = {aT 1 }θ + {aT 2 }θ log (4.37) dt dt 4 Complex Constitutive Adhesive Models and, dγ dγ / γel = {bT 1 }ζ + {bT 2 }ζ log dt dt 107 (4.38) where aTi , bTi are shift factors as functions of temperature. Figure 4.6 illustrates an application of Eq. (4.37) by Sancaktar et al. (1984), showing the variation of elastic limit shear stress with initial elastic strain rate and environmental temperature for an epoxy adhesive film with polyester knit fabric carrier cloth. The adhesive was tested in the bonded lap shear mode. In order to analyze the effects of rate and temperature on the interfacial strength of bonded joints, one can initially use a simple energy approach in the following manner: A critical energy level, Wc , is used to represent interfacial failure. In the presence of adhesive, substrate and interphase (a distinct material layer between the substrate and the adhesive layer which transmits the rigid substrate’s energy to the adhesive layer), the combined elastic energy can be written as: 2 2 Eadhesive } +Vip {(1/2)εinterphase Ginterphase } Va {(1/2)εadhesive 2 Esubstrate } = Wc +Vs {(1/2)εsubstrate (4.39) where, Va , Vip and Vs represent volume fractions of the adhesive layer, interphase and the substrate, respectively. Now, if one considers Eq. (4.39) in conjunction with Eq. (4.38) to include rate-temperature effects, then it can be easily deduced that higher Wc levels are obtained at high rate and/or low temperature levels since the proportion of elastic strains increases with increasing elastic limit strains due to high rate and/or low temperature levels. Fig. 4.6 Variation of elastic limit shear stress with initial elastic strain rate and environmental temperature, and comparison with Ludwik’s equation for an epoxy adhesive film with polyester knit fabric carrier cloth. The adhesive was tested in the bonded lap shear mode (Sancaktar et al. 1984) 108 E. Sancaktar 4.3.7 Reductions in Stress Concentration Due to Viscoelastic Adhesive Behavior If the adhesive material exhibits viscoelastic behavior, then the high stress magnitudes observed at the overlap end region of bonded joints are expected to diminish in time due to the creep process. For example Weitsman (1981) utilized the nonlinear viscoelastic “power-law” response, which describes a stress enhanced creep process to illustrate time dependent reductions in shear stress peaks along the adhesive layers of symmetric double lap joints. Sancaktar (1991) later illustrated the applicability of the correspondence principle to the same problem with the use of Maxwell chain to approximate the continuous change in the relaxation time and to coincide with the results calculated using nonlinear viscoelastic theory, as shown in Figs. 4.4 and 4.5. 4.4 Singularity Methods Theoretically, geometrical singularities exist at sharp interface corners. The strength of such singularities depends on the local geometry, including the actual corner radius, and the material properties. Barsoum (1989) considered the cases of elastic adhesive at a rigid corner, and nonlinearly hardening adhesive at a square rigid corner. He showed that for an elastic adhesive the obtuse angle notch gives a much weaker singularity and, hence, a greater failure load. Assuming linear elasticity, Groth (1988) proposed an exact solution for the adhesive stresses at an interface corner in the form of a power series: σi j = ∞ ∑ Kk Hikj (φ )ζ λk + Continuous part (4.40) k=1 where σi j is the stress tensor, ζ = r/h is a non-dimensional radial distance from the singularity, H k i j are functions depending on the geometry angle φ of the corner, Kk constitutes generalized stress intensity factors, and λk defines the strength of singularities governed by the eigenvalues of the λk in the open interval Re (λk ) < 1. Due to restrictions on finite strain energy at the singularity, values of Re (λk ) ≥ 1 are not allowed. Obviously, based on Eq. (4.40), more than one singular term may influence the stress field close to an interface corner. Dempsey (1995) showed that in addition to the power type singularities, i.e. 0(r−λ ) as r → 0, and λ representing the strength of singularity, power-logarithmic type singularities, i.e. 0(r−λ ln r) as r → 0, may occur for homogeneous boundary conditions of composite wedge problems. Stress singularities at butt joint interface corners were discussed Reedy and Guess (1995) and Sawa et al. (1995). 4 Complex Constitutive Adhesive Models 109 4.5 Bulk Adhesive as Composite Material Since most adhesives contain secondary phase materials such as fillers and carrier cloth, they should be treated as composite materials in constitutive modeling. The interesting aspect in such treatment is the fact that such secondary phase constituents form adhesive bonds with the adhesive matrix in small scale. Consequently, localized non-catastrophic failures within the bulk adhesive consisting of interfacial separations are expected to cause constitutive behavior changes for the adhesive bulk. Such behavior can be properly described by using “damage mechanics models” some of which will be described later in this chapter within the context of adhesive materials. It is known that particle size, shape and volume fraction all affect the mechanical behavior of filled polymers. For example, electrically and thermally conductive adhesives which usually contain dispersed metal particles of varying aspect ratios, but usually within the micron size range, require the methods of Eshelby (1957, 1959) for characterization. We note that these types of adhesives sometimes require directional properties. Kerner (1956), Hashin and Shtrikman (1963), Budiansky (1965) and Hill (1965) provided methods for calculation of elastic moduli for isotropic materials filled with spherical particles. Methods for elastic moduli of unidirectional reinforced polymers with infinitely long fibers were given by Hill (1964) and Chow and Hermans (1969). Bulk and shear moduli for disk and needle shaped inclusions were considered by Wu (1966) and Walpole (1969). As reported by Ashton et al. (1969), Halpin and Tsai introduced approximate equations for square fiber reinforcement by reducing Hermans’ solution (1967) using numerical solutions of elasticity theory. Equations for slender rigid inclusions at low concentrations were developed by Russel and Acrivos (1972, 1973). As for effective thermal expansion coefficient of filled polymers, the effects of filler geometry, and constituent material properties have been studied by Kerner (1956). Using the generalized approach of Eshelby, Chow (1977, 1978-a) derived relations for the bulk modulus, transverse and longitudinal Young’s moduli and, the two effective shear moduli, G12 and G13 of the filled polymer containing aligned ellipsoidal particles at finite concentration. Chow (1978-b) also derived relations for the linear and volumetric thermal expansion coefficients for filled polymers containing aligned ellipsoidal inclusions at finite concentration. He concluded that in such filled systems, the volumetric expansion varies only slightly with the aspect ratio of the ellipsoid, while longitudinal and transverse linear expansions show strong dependence on the particle shape. All the modulus calculations developed by Chow are based on the following assumptions: (i) The filler particles are well bonded to the matrix, and consequently, the isostrain condition at the particle/matrix interface can be used to develop the method; (ii) The shapes of particles are uniform ellipsoids with the aspect ratio Cρ , representing the ratio of the major to minor axes; (iii) The particles are distributed with their corresponding axes aligned. Wei (1995) and Sancaktar and Wei (1998) applied the elastic moduli and thermal expansion coefficient relations developed by Chow in describing the material 110 E. Sancaktar behavior of electronically conductive (filled) adhesives in order to be able to determine, accurately, the thermal mismatch stresses which occur between the adhesive and the substrates in the bonded form. Both finite element analysis and closed form solutions were used for stress analysis. We note that the results given by Chow are consistent with the well known rule of mixtures used in long fiber reinforced composites. When the aspect ratio, Cρ , of the particle is Cρ > 50, the moduli are not a function of Cρ . Therefore, for larger Cρ the composite’s behavior is more like that of long fiber reinforced composite. For intermediate aspect ratio cases, i.e. 1 < Cρ < 50, Sancaktar and Wei (1998) proposed an approximation of Chow’s elastic moduli formulas by utilizing the method used for randomly oriented short fibers in predicting the behavior of particle filled adhesives, so that the composite material can be treated as isotropic, as suggested by Agarwal and Broutman (1990). As for the thermal expansion coefficient, the isotropy assumption was accomplished simply by using one-third of the volumetric thermal expansion coefficient, as suggested by Lipatov et al. (1991). We note, however, that in special cases of conductive adhesive applications, directional conduction may be required, in which case the use of non-isotropic, directional material properties would be necessary. The constitutive models cited above for predicting filled polymer behavior all assume perfect adhesive bond between the fillers and the polymer matrix. As such filled polymers are loaded, however, failure of adhesive bonds is expected in proportion to the applied force and the duration of its application. This, in turn, is expected to result in changes in the constitutive properties of the filled polymer adhesive. Lipatov et al. (1991) reported a decrease in the modulus of elasticity of a filled elastomer at separation of filler particles from the binder and described it with the approximate formula (4.41) Ex /E f = exp−4.3 (Vx ) where E f is the initial elastic modulus for the filled polymer with unbroken bonds, Vx is the volume fraction of unbonded filler, and Ex is the composite’s elastic modulus when the fraction, Vx , of the filler particles are no longer bonded to the matrix. Garton et al. (1989) discussed stiff polar molecular additives which interact strongly with the (thermoplastic or thermoset) matrix polymer adhesive, thus decreasing the composite free volume, f , as given by the equation f = V1 f1 +V2 f2 + k V1V2 (4.42) where V1 and V2 are the volume fractions of the polymer matrix and additive, respectively, f1 and f2 are the corresponding fractional free volumes, and k is an interaction parameter. The composite properties: bulk elastic modulus, bulk strength (to a lesser degree) as well as bonded joints properties of strength and stiffness are reported by Garton et al. (1989) to increase with reductions in composite free volume. In another study, Sancaktar and Kumar (1999-a, 2000) obtained increases in the lap joint strength by selectively rubber toughening the high stress concentration regions of the adhesive overlap. This novel approach to increase the lap joint strength by using functionally gradient adhesive introduced a method different from 4 Complex Constitutive Adhesive Models 111 the traditional methods of either increasing the lap joint area or altering the joint geometry. For the different configurations of adhesive arrangements tried, the trends obtained in finite element analysis matched the trends obtained by tensile shear testing. The use of such “functionally gradient” adhesives was later adapted by other researchers such as Pires et al. (2003, 2006), You et al. (2005), and Temiz (2006) under the name “bi-adhesive”, and by Hu and Huang (2005), da Silva and Adams (2006) and Lei et al. (2008) under the names “mixed-adhesive” or “mixed-resin”. 4.6 Adhesively Bonded Joint Composite, the Concept of the Interphase There is strong interrelationship between the properties of the adhesive and the substrates in shaping the final joint behavior. A more accurate prediction of the joint behavior can be obtained by including a distinct “interphase” region in modeling the overall joint behavior. An early discussion of this concept was provided by Sharpe (1972, 1974). This concept becomes especially relevant as efficient methods for inducing mechanically distinct surface topography and chemically distinct interlayers emerge. The use of excimer pulse lasers for surface treatment and topography inducement on metal adherends, shown by Sancaktar et al. (1995-a), cure and post-cure of interphase regions around carbon fibers embedded in epoxy matrix via resistive electric heating by the fiber, shown by Sancaktar and Ma (1992-a), microwave curing of carbon-epoxy composites, which produce “interfacial strengths higher than that achievable in thermally cured system”, as shown by Agrawal and Drzal (1989), and the production of a transcrystalline region in crystalline polymers upon solidifying when in contact with a substrate, as shown by Hata et al. (1994), all provide examples of current methods used to create distinct interphases. Another main reason for the presence of an interphase region is the chemical primer (sizing) applied to the adherend surfaces to improve adhesion. The diffusion of this sizing into the adhesive matrix can create a concentration gradient. There are other possible mechanisms which could lead to an interphase region. Some examples are: possible polymeric diffusion into the substrate during the adhesion process, selective adsorption of one or more of the components in the matrix before curing and the presence of free volume differences between the bulk polymer and the polymer near the substrate-matrix boundary, possibly created by thermal stresses. Figure 4.7 shows different “interphases” between an epoxy-based, approximately 80%wt silver flake filled electrically conductive adhesive and different substrates. Adequate analysis and understanding of the interphase between an adherend and an adhesive is critical for design of efficient bonded structures and composite materials. In adhesion science and technology circles it is a well accepted fact that the mechanical properties of the (polymeric) adhesive material is altered in regions close to the adherend due to the adhesion process. For example, Knollman and Hartog (1985) reported approximately 10% reduction in the adhesive bulk shear modulus, in an interphase region comprising approximately 20% of 112 E. Sancaktar Piezoelectric Device Gold Layer Electrically Conductive Adhesive Stainless Steel Substrate Fig. 4.7 Illustration of different “interphases” between an epoxy-based, approximately 80 %wt silver flake filled electrically conductive adhesive and different substrates. The flake size is approximately 7 μm the bulk adhesive thickness. Consequently, a satisfactory mechanical analysis on the adherend-adhesive interaction should include a finite thickness interphase with its own material properties rather than assuming an interface with unknown properties or very high strength and negligible thickness. Modeling of the adhesive-adherend interphase becomes especially relevant in understanding and design of composite materials with “tailored” interphases which increase the toughness of the composite material. Using the case of a carbon fiber embedded in epoxy matrix, Sancaktar and Zhang (1990) and Sancaktar et al. (1992-b) reported that nonlinear viscoelastic behavior of the matrix and the interphase may have a profound effect on the mechanism of stress transfer. Sancaktar’s analytical model involves a cylindrical interphase surrounding an elastic fiber of finite length. The interphase region has nonlinear viscoelastic material properties. The region surrounding the interphase (which can be assumed to be the bulk of the adhesive matrix) is also assigned nonlinear viscoelastic properties, which are different from those of the interphase. The nonlinear viscoelastic material behavior of the interphase zone and the matrix is represented using a stress enhanced creep. Different interphase diameter values and different material properties for the interphase and the matrix are used to determine their effects on the interfacial shear stress. Results of this analysis reveal that depending on the relative magnitudes of interphase and matrix viscoelastic material properties, it is possible to have stress reductions or increases along the fiber and, hence, the critical fiber length obtained will also vary accordingly, as illustrated in Fig. 4.8. This result reveals that not only the quality of adhesion but also the material properties of the bulk matrix and the interphase, all of which can be affected by cure conditions, can affect the critical fiber length, a concept introduced by Kelly and Tyson (1965) to gage the fiber-matrix interfacial strength. The analytical and experimental results presented so far reveal the possibility for mutual reduction between rate, temperature, and interphase thickness, as shown by Sancaktar et al. (1992-b). If we assume that application of fiber sizing results in thicker interphases, and that the cross-head rate, v, can be related to the shear strain rate, d γ /dt, and the interphase thickness, δ , with the relation: 4 Complex Constitutive Adhesive Models 113 Fig. 4.8 The variation of the maximum shear stress with time and matrix transient creep compliance based on a nonlinear viscoelastic stress analysis of a cylindrical interphase zone for maximum transferred load. The nonlinear analysis was performed using Eq. (4.31) with a stress-dependent shift factor. D0 and D1 are the interphase instantaneous and transient creep compliances, δ is the interphase thickness, and the subscripts m and f indicate matrix and fiber, respectively (Sancaktar and Zhang, 1990) v= f dγ dt g(δ ) (4.43) based on classic shear lag analysis (also based on definition of shear strain), we can then argue that for a fixed strain rate (function) the effect of increased crosshead rate can be induced by increasing the interphase thickness (i.e., application of fiber sizing). Indeed, the experimental results reveal shorter fragment lengths for increased cross-head rate and/or presence of fiber sizing. Based on this premise we can write the following superposition relations for the interfacial strength: τc (T, v, δ ) = τc (To , aT v, δ ) τc (T, v, δ ) = τc (To , v, δ /aT ) (4.44) (4.45) τc (T, v, δ ) = τc (T, v/aδ , δo ) (4.46) and In order to represent the composite behavior of the adhesive/adherend interphase, where the polymeric adhesive is mechanically interlocked to the surface projections 114 E. Sancaktar of a metal adherend, Sancaktar (1996) proposes a “smeared” modulus zone. Although deformation within the bulk adhesive is likely viscoelastic, simple elastic relationships probably suffice, to describe deformation within the topographic surface region. Therefore, simple elastic relationships are used to relate strain gradient within those regions to topography. The equivalent elastic modulus, GIP , for the mechanically interlocked interphase is calculated by assuming an “isostress” condition for the interphase, illustrated in Fig. 4.9. In other words, we assume that the adhesive and the adherend surface (projections) are subjected to the same level of shear stress, τIP , at the interphase, while the composite interfacial shear strain, γIP , is a volumetric weighted average of the adhesive and adherend strains, i.e. γIP = (V f A )(γA ) + (V f S )(γS ) (4.47) In Eq. (4.47) γA and γS are the adhesive and substrate shear strains at the interphase and V f A and V f S are the volume fractions of the adhesive and the substrate surface (projections) at the interphase. Assuming that the adhesive essentially fills the voids, the adhesive volume fraction can be equated to the sum of the void volume fractions of each lamina. With the assumption that the deformations in both the adhesive and the adherend are elastic, we can define the interphase shear modulus as: GIP = τIP /γIP Fig. 4.9 The state of isostress shear at the interphase (4.48) 4 Complex Constitutive Adhesive Models 115 Using Eqs. (4.47) and (4.48) and Hooke’s law to represent adhesive and adherend’s material behavior, we obtain the following expression for the interphase shear modulus: GS GA GS GA = (4.49) GIP = V f A GS + V f S GA V f S (GS − GA ) + GA where GA and GS are the elastic moduli for the adhesive and the adherend, respectively. We now assume that failure at the interphase is more likely with higher strain gradients, dγIP /dz. Of course, in the limit, a strain discontinuity defines failure based on mechanics principles. Based on this premise, we can derive a mathematical expression to gage the possibility of failure using the shear moduli of the adhesive and the adherend along with the adhesive volume fraction, V f A , at the interphase. For this purpose, we first note that differentiation of Eq. (4.48) along the interphase thickness direction (z-direction) results in d γIP dGIP −2 = − τIP γIP (4.50) dz dz An equivalent expression can be obtained by differentiating Eq. (4.49) with respect to z: dV f A dGIP GS GA (GS − GA ) =− (4.51) dz dz [V f A (GS − GA ) + GA ]2 Equating Eqs. (4.50) and (4.51) we can obtain an expression relating the shear strain gradient, dγIP /dz at the interphase to the volume fraction, V f A , and the differential volume fraction dV f A /dz, of the adherend voided during surface preparation. Both parameters are experimentally determinable, as discussed by Sancaktar (1996). Variation in mechanical properties of polymer transition layers was also considered by Silberman et al. (1991). An approach involving macroscopic characterization of the interphase regions in polymer based composite systems by integrated moduli over the thickness is given by Cardon et al. (1993). A three-phase, axisymmetric elasticity solution to predict the sensitivity of the stress state to the interphase material properties and temperature is presented by Sottos et al. (1994). In order to overcome the difficulties arising from the geometrical complexity of bonded joints, a number of studies have been carried out by Adams and Peppiatt (1974), Cooper and Sawer (1979), Hashim et al. (1990), Groth and Nordlund (1991), Dorn and Weiping (1993) and Papini et al. (1994), using the finite element method. Lap and butt joints have been analyzed extensively due to their common usage in engineering applications. Interfaces usually constitute a weak link in the chain of load transfer in bonded joints. Also, the discontinuity of the material properties causes abrupt changes in stress distribution, as well as causing stress singularities at the edges of the interfaces. It is very desirable to optimize the substrate surface topography at the interfaces to maximize the load bearing capacity of bonded joints, and to improve their deformational characteristics. 116 E. Sancaktar During the second half of the twentieth century a considerable amount of research work has been published related to the interface stress distributions, including Bogy (1968, 1970, 1971-a) and Bogy and Wang (1971-b), Renton and Vinson (1977), Mittal and McKenzie (1980), Sih (1980), Okajima and Sinclair (1986), Suhir (1988), Sancaktar (1987-b, 1996), Groth (1988), Adams (1989), Bigwood and Crocombe (1989), Sawa et al. (1989, 1995), Ikegami et al. (1990), Temma et al. (1990, 1991), Nakano et al. (1991), Carpenter (1991), Gao and Mura (1991), Keisler and Lataillade (1995), Apalak et al. (1995), Maugis (1996) and Ganghoffer and Schultz (1996). These studies focused on flat surfaces between two different materials except when the effects of surface roughness were investigated. In general, stress distributions, stress concentrations, singularities, and surface roughness effects were studied. These studies, however, were not extended to the development of a general methodology to include surface topography effects for varying configurations which can be represented by different mathematical functions. An investigation by Sancaktar and Narayan (1999-b) on adhesively bonded scarf joints revealed that the angle between the bonded interface and the loading direction had a significant influence on the stress distributions at the interface. Their analysis revealed that the distributions of stresses became more uniform along the adhesive layer when scarf angles varying from lap joint to butt joint in an increasing order of scarf angle were considered. The transverse and shear stress distributions were in a decreasing order for scarf angle increments of 15◦ between 30◦ and 90◦ , while a reverse trend was observed for the normal stress distributions. The peak normal stress was minimum for the 30◦ scarf joint; on the other hand, the magnitudes of transverse and shear stresses were minimum when a butt joint was used. Uniformly distributed external shear loading on the joints led to higher stresses in lap joints, while 75◦ scarf joint had the lower values. Sancaktar and Narayan (1999-b) stated that an attention to the type of stress (i.e., normal, transverse or shear) provided information relevant to the type of failure (i.e., brittle or ductile type failures). The authors also introduced newly defined design parameters: stress times substrate volume, stress divided by substrate volume, and stress (strain) gradients along and across the adhesive joint, as a general methodology to compare adhesive joints for design optimization. In highly deformable adhesives, most of which are elastomeric in nature, such as those used in pressure sensitive tape and tack applications, a high amount of deformation results in cavitation of the material under dilatation. High dilatation, which is a 3-D concept, may lead to cavitation in localized regions of the adhesive layer starting at a microscopic scale. It is also desirable to know the magnitudes of shear and normal stresses individually since some adhesives are weak in shear loading (ductile adhesives) while others are weak in normal stress loading (brittle adhesives). High levels of stresses result in crack propagation in brittle adhesives and cavitation induced failures in deformable adhesives. Furthermore, not only the magnitudes but also gradients of stresses and strains become an important issue in optimizing the joint strength. Large strain gradients at adhesive-substrate interfaces may result in bond failure. 4 Complex Constitutive Adhesive Models 117 The magnitude of strain gradients depends on the volume fractions of the adhesive and substrate materials within the effective bond region defined by the geometry of the surface topography. The effect of bonded substrate volume, corresponding to the volume of substrate projections beyond a common base-line on the substrate, on the strain gradients across the adhesive layer can be found by relating the volume fraction gradients to the strain gradients. For this purpose, the composite behavior of the adhesive/adherend interphase, where the polymeric adhesive is mechanically interlocked into the surface projections of an adherend can be utilized to determine an equivalent composite modulus, as suggested by Sancaktar (1996) and discussed above. We note that mechanical adhesion depends on surface topography, which can be considered a collection of many geometrical forms. Therefore, mechanical adhesion depends on the stress states of different adhesive joint geometries on the scale of the surface topography, which may include many lap, butt and scarf joints in the “interphase” region. To address this issue, Ma et al. (2001) compared the stress distributions in adhesive joints as functions of varying geometrical interfaces described mathematically in polynomial or other functional forms, as well as the material properties of the adhesive and the adherend or two different substrates joined by an infinitesimally thin adhesive layer. For this purpose, a mathematical procedure was developed to utilize the complementary energy method, by minimization, in order to obtain an approximate analytical solution to the 3-D stress distributions in bonded interfaces of dissimilar materials. In order to incorporate the effects of surface topography, the interface was expressed as a general surface in Cartesian coordinates, i.e., F(x, y, z) = 0, and the results verified by comparison with Finite Element Analysis (FEA). Their methodology involved the following steps: 1. Choose the appropriate stress functions, Φmn , to satisfy stress boundary conditions and utilize equilibrium conditions to relate the stress functions to the stress distribution functions; 2. Use stress interface boundary conditions to reduce the unknown variables in the stress distribution functions obtained; 3. Define a function Π as the sum of compley= f (x,z) mentary energy I and the penalty function R ∑ i=1..3 (ui A − ui B )2 . R is chosen such that it is the largest positive number which causes the total system complementary energy to change by only 0.1%; 4. Use the remaining unknown variables to minimize the function Π formed in step 3, using the Newton quadratic method, and solve all the unknown variables to obtain the complete stress distribution functions. The continuity of displacements was enforced at the interface area, approximately, using the fundamental theorem for surface theory of differential geometry, described by Struik (1950), instead of directly using displacements. This way, the integrations of displacements were avoided, and the stress distributions could be calculated more accurately. For example, for a flat interface (on x-z plane), such as a butt joint, they utilized the following stress functions: ΦAxx = (z2 − 1/4)2 (y − 1/2)2 f1 (x, y, z) (4.52) 118 E. Sancaktar ΦAyy = (z2 − 1/4)2 (x2 − 1/4)2 f2 (x, y, z) ΦAzz ΦAxy ΦAxz ΦAyz ΦBxx ΦByy ΦBzz ΦBxy ΦBxz ΦBzz (4.53) = (x − 1/4) (y − 1/2) f3 (x, y, z) (4.54) = (x − 1/4)(z − 1/4) (y − 1/2) f4 (x, y, z) (4.55) = (x − 1/4)(z − 1/4)(y − 1/2) f5 (x, y, z) (4.56) = (x2 − 1/4)2 (z2 − 1/4)(y − 1/2) f6 (x, y, z) (4.57) = (z − 1/4) (y + 1/2) f7 (x, y, z) (4.58) = (z − 1/4) (x − 1/4) f8 (x, y, z) (4.59) = (x − 1/4) (y + 1/2) f9 (x, y, z) (4.60) = (x − 1/4)(z − 1/4) (y + 1/2) f10 (x, y, z) (4.61) = (x2 − 1/4)(z2 − 1/4)(y + 1/2)2 f11 (x, y, z) (4.62) = (x − 1/4) (z − 1/4)(y + 1/2) f12 (x, y, z). (4.63) 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 Functions fn (x, y, z) are of the type: gn1 sinh(x) sinh(z) + gn2 sinh(x) cosh(z) + gn3 cosh(x) sinh(z)+gn4 cosh(x) cosh(z) where, gni are polynomials of hni1 +hni2 x + hni3 z, and, hni1 , hni2 and hni3 are polynomials of ani j1 + . . . ani jm ym−1 . The selection of sinh x, cosh x, sinh z, cosh z, and y facilitated numerical calculations. A typical distribution for the normal stress, σyy , common to both substrates A and B at the bonded interface of a three-dimensional flat interface between these substrates is shown in Fig. 4.10. This stress is calculated by the novel mathematical procedure based on differential geometry and the penalty function as described by Ma et al. (2001), and summarized above. Figure 4.11 shows the transverse stresses Interface A Y B Z Fig. 4.10 A three-dimensional flat interface between two substrates A and B, loaded as shown and analyzed by FEA with the mesh pattern shown (left). A typical distribution for the normal stress, σyy , common to both substrates A and B at the bonded interface is shown on the right, as calculated by a novel mathematical procedure based on differential geometry and the penalty function (Ma et al., 2001) 4 Complex Constitutive Adhesive Models 119 Fig. 4.11 The transverse stresses σxx , on substrates A (left) and B (right) at the bonded interface, illustrating the discontinuity of this stress across the interface, as sometimes called the “stress jump”, calculated by a novel mathematical procedure based on differential geometry and the penalty function (Ma et al., 2001) σxx , on substrates A and B at the bonded interface, illustrating the discontinuity of this stress across the interface, as sometimes called the “stress jump”. Again, these stresses are calculated by the novel mathematical procedure based on differential geometry and the penalty function as described by Ma et al. (2001), and summarized above. 4.7 Damage Models The incremental theory of plasticity assumes that the strains depend on the entire history of loading. The total increments of deviatoric strain Δεi j is composed of a viscoplastic component (4.64) Δεi j P = d λ Si j where d λ is a variable depending on the loading history, and an elastic component d εi j E = (dSi j /dt)/2G (4.65) d εi j /dt = d εi j E /dt + d εi j P /dt (4.66) so that Obviously, a yield criterion is needed to determine the actual magnitudes of plastic strain increments. This theory was first proposed by Prandtl (1925) and Reuss (1930). Several constitutive forms were proposed to describe the viscoplastic term of Eq. (4.66). Among these Hohenemser et al. (1932), Sokolovsky (1948), Malvern (1951) and Perzyna (1963) proposed essentially the same idea. It involved the assumption that the viscoplastic component be a function of the over-stress above the 120 E. Sancaktar yield point. On the basis of his experimental observations, Sokolovsky determined that the over-stress should be defined above the elastic limit, as a function F(σ − θ ), so that ε = σ /E, ε = (σ /E) + F(σ − θ )/E, σ ≤θ σ > θ. (4.67-1) (4.67-2) The over-stress idea can be incorporated into the viscoelastic mechanical models by means of adding sliding elements to describe yield or termination points. With such an application, equations containing viscosity terms are obtained in a form similar to (4.67). For example Brinson et al. (1975), Renieri et al. (1976), Sancaktar and Brinson (1979, 1980), Sancaktar (1981), Sancaktar and Padgilwar (1982), Sancaktar et al. (1984) and Sancaktar and Schenck (1985-a) used the Modified Bingham model developed by Brinson (1974) to describe the shear and tensile material behavior of structural adhesives in the bulk and bonded forms: σ = Eε d ε /dt = (d σ /dt) + (σ − θ )/μ σ =Y σ ≤θ θ <σ ≤Y σ ≥ Y. (4.68-1) (4.68-2) (4.68-3) The model describes linear elastic behavior below the elastic limit θ , linear viscoelastic behavior between θ , and the maximum stress Y and perfectly plastic behavior above Y . When the sliding element is activated at σ = θ , the model becomes essentially a Maxwell element, as illustrated in Fig. 4.12. A similar application was also reported first by Chase and Goldsmith (1974) and later by Sancaktar (1981), Sancaktar and Padgilwar (1982), Sancaktar et al. (1984), and Sancaktar and Schenck (1985-a), in modifying a three parameter solid model with a sliding element to describe the mechanical behavior of polymeric materials and adhesives. An isothermal theory of separation in (thermoplastic or pressure sensitive) polymer-solid adhering systems based on drawing of filaments is given by Good and Gupta (1988). Ganghoffer and Schultz (1996) stated that the influence of damage on the mechanical behavior is specified through the concept of strain equivalence. They propose that the constitutive law for the damaged material is given by that of the virgin material if the stress tensor σ is replaced by the effective stress tensor σ /(1−d) with the term, d, representing the extent of damage between the virgin state, d = 0 and complete failure, d = 1. The damage parameter is further developed in Chapter 6. Another example of empirical damage modeling in joints bonded using silver flake filled electrically conductive adhesives was given by Gomatam and Sancaktar (2006-a,b), who introduced a comprehensive fatigue life predictive model for single lap joints subjected to variable loading. For the purpose of formulating a fatigue life predictive model, a linear relationship is established first between the maximum cyclic load Pmax (or maximum principal stress, σmax , as suggested by Gomatam, 2002, and Gomatam and Sancaktar, 2004), and the number of cycles N: 4 Complex Constitutive Adhesive Models 121 Stress σ Modified Bingham Model Constant Strain Rate (C.S.R.) σ=Y Plastic V.E. θ= Elastic Limit Stress σ=θ Maxwell behavior: when θ ≤ σ ≤ Y Perfectly Plastic behavior: when σ ≥ Y E Elastic 1 Strain, θ E σ Y µ Stress σ(t) σ=Y Maxwell σ (t) ≤ θ σ ( t) = E ⋅ε Modified Bingham σ=θ Axis Shift for Maxwell Model ( ⎡ σ (t) = θ + μ R⋅ 1 − e ⎢⎣ E ) T⎤ − t− t 0 1 Strain, ⎦⎥ θ< σ (t) ≤ Y Fig. 4.12 The Modified Bingham model and its comparison with the Maxwell model Pmax = C + m N (4.69) where C and m are, respectively, the intercept and slope for this linear relation. For the purpose of the analytical fatigue life predictive model, two separate analytical equations were proposed depending on the intensity (severe or moderate) of the load-ratio first applied, at a maximum cyclic load level. The total fatigue life, NTotal , under severe-to-moderate condition was predicted by the relation, 1 ΔC 1 ns NTotal = ns + − (Cs − P) − 1− (4.70) mM ms mM Ns The total fatigue life under moderate-to-severe condition, on the other hand, was predicted by, nM NTotal = nM + Ns 1 − (4.71) NM In Eqs. (4.70) and (4.71) we have, ΔC = CM −Cs where CM and Cs are the intercepts, and mM and ms are the slopes for the linear relationships between the maximum cyclic load Pmax (or maximum principal stress, σmax ), and the number of cycles N under moderate and severe conditions, 122 E. Sancaktar respectively. nM and ns are the number of cycles applied under moderate and severe conditions, respectively. As illustrated in Fig. 4.13, in going from moderate to severe conditions, we simply add to the number of cycles under moderate conditions (nM ), the predicted remaining life for the sample under the severe condition, Ns [1 − (nM /NM )], based on experimental predictions without making any slope corrections, Eq. (4.71). In going from severe to moderate condition, however, we also make a slope correction, [Cs − P]{(1/ms ) − (1/mM )}[1 − (ns /Ns )], to make the severe and moderate P-N curves parallel, and shift the intercepts to add the remaining life, Δ C/mM , to that already used up under severe condition (i.e. ns ). These particular methodologies were chosen based on experimental observations. Utilizing the above equations, the total fatigue life of the joints subjected to varying loading conditions, namely severe-tomoderate, and moderate-to-severe were computed for a set of test cases, in addition to experimentally determined values, for the purpose of model validation. Comparison between the experimental, and predicted values validated the accuracy, and efficiency of the proposed model. In order to render the model usable with different stress components (σxx , σyy , σzz , τxy , τyz, τxz ) instead of the maximum cyclic load values, Gomatam (2002) utilized the maximum and minimum principal and von Mises stresses obtained from non-linear elasto-plastic finite element analyses to calculate the ratios of peak stress values obtained at corresponding maximum load levels. These stresses were then compared to the intercept ratios obtained from the P-N curves at given environmental conditions. This comparison procedure revealed the maximum principal stress as the appropriate parameter to be used in the form of S-N curves, i.e., σmax = C + mN mm, ms = slopes; nm, ns = number of cycles, under moderate, m, or severe, s, conditions. Cm Δ(C) = Cm – Cs Cs S (4.72) P Δ (C)/m m (M) (S) ns (1 – ns/N s) Ns N 1) Severe to Moderate: NTotal = ns + (Δ(C)/mm) – (Cs–P) ((1/mm)) (1–(ns/Ns)) 2) Moderate to Severe: NTotal = nm + Ns(1–(nm/Nm)) Fig. 4.13 Illustration of the cumulative fatigue damage model (Gomatam and Sancaktar, 2006-a) 4 Complex Constitutive Adhesive Models 123 where C and m are, respectively, the intercept and slope values based on maximum principal stress. The mathematical basis for the maximum principal stress to replace the maximum cyclic load in Eq. (4.69) was illustrated by performing fatigue tests under three different maximum load, Pmax , conditions, and considering the following relations: C3 C3 = (4.73) C1 C1 and C2 C2 = C1 C1 (4.74) where C1 , C2 , C3 relate to Eq. (4.69), and C1 , C2 , C3 relate to Eq. (4.72), as illustrated in Fig. 4.14. In order to account for environmental effects, such as elevated temperature and humidity, a superposition method was applied for fatigue life prediction by shifting the slopes and the intercepts between different environmental conditions. For this purpose, design charts were formulated based on experimental data. These design charts comprise of two parts, one for shifting the slope, and the other for shifting the intercept between different environmental conditions. Once the slopes and the intercepts are determined, Eqs. (4.69) and (4.72) would yield the fatigue life of the joint at the new environmental condition, as illustrated in Fig. 4.15 and shown by Gomatam and Sancaktar (2006-b). The proposed model was also extended to bonded cases with varying stress states. For this purpose, a non-linear elasto-plastic finite element analysis (FEA) for ambient condition, and a non-linear thermo-elasto-plastic FEA for elevated temperature conditions were performed using two different lap joint geometries and boundary conditions to represent two distinct states of stress. Utilizing the FEA results, relations between the stress components, slopes, and intercepts were established. The intercepts were found to be inversely proportional to the maximum stresses, and the slopes directly proportional to a shear stress component. Thus, by using these relations along with a knowledge of the stress states for only two joint configurations, the slope, and intercept for any other lap joint with unknown P-N (σ − N) Pmax = C’ + m’N σmax = C + mN C’3 C1 C’2 C2 PmaxC’1 σmax C 3 (MPa) (N) C’3/C’3 = C3/C1 N N Fig. 4.14 The similarity in P-N and σ − N relations (Gomatam and Sancaktar, 2006-a) 124 E. Sancaktar Hum 90°C 50°C Stress Ratio Hum RT 90°C 50°C RT Stress Ratio Slope Intercept Fig. 4.15 The shifting mechanism implemented for the purpose of predicting fatigue life of joints subject to a stress ratio (R), and maximum cyclic load of Pmax , from one test environment (28◦ C, or 50◦ C, or 90◦ C) to another at the same stress ratio, and maximum cyclic load (Gomatam and Sancaktar, 2006-a) behavior could be computed, from which the fatigue life of the joint could be predicted, as shown by Gomatam and Sancaktar (2006-b). Fatigue and environmental degradation are further discussed in Chaps. 7 and 8. 4.8 The Effects of Cure and Processing Conditions on the Mechanical Behavior Cure and processing conditions have strong effects on the resulting mechanical properties of structural adhesives in the bulk and bonded forms. Variation of various mechanical properties of an epoxy adhesive with or without a carrier cloth as functions of cure temperature, time, and cool down conditions, and their effects on bulk tensile properties were studied by Sancaktar et al. (1983), Jozavi and Sancaktar (1989-a, b, c) and Sancaktar (1995-b), with the work by Jozavi and Sancaktar (1989-c) providing information on the effects of cure conditions on the relaxation behavior of bulk thermosetting adhesives. A comparison of the degree of cure with bulk strength was given by Jozavi and Sancaktar (1988). The effects of the cure parameters on the stress whitening behavior were given by Jozavi and Sancaktar (1989-a, b). The effects on the bonded joint behavior were discussed by Shaw and Tod (1989), Sancaktar and Ma (1992-a) and Turgut and Sancaktar (1992). In general, mechanical properties are improved with increases in cure temperature and time and with slow cool down. Such increases, however, have an upper limit, and further increases in cure parameter magnitudes lead to deterioration in adhesive mechanical properties. Consequently, in general, the variation of mechanical properties with the cure parameters are bell shaped functions. Additional information on the effects of cure conditions were provided by Sinclair (1992). 4 Complex Constitutive Adhesive Models 125 Matsui (1990) provides some empirical relations for the variation of shear modulus and strength of joints bonded using various structural adhesives. In the case of particle filled adhesive systems, such as electrically conductive adhesives, the viscosity, μ , during processing and cure is a function of filler volume fraction, Φ, shear rate, d γ /dt, and resin conversion level, α . The development of viscosity from a chemorheological point of view is important as it relates to the wetting and diffusive characteristics of the adhesive during its cure. These characteristics ultimately determine the viability of the interphase and, therefore, the overall adhesive bond. A comprehensive model may be represented by combining the following models: the power law (shear rate effect), described by Wildemuth and Williams (1985), Castro-Macosko model (conversion effect), described by Castro and Macosko (1980, 1982) and Castro et al. (1984), and Liu model (filler volume fraction effect), described by Liu (2000). Such a combined model takes the form: μ (φ , d γ /dt, α ) = A · (φm − φ )−2 · (d γ /dt) C0 +C1 ·α · αgel αgel − α D+E·α (4.75) where, A, C0 , C1 , D and E are model constants that can be determined by multivariable nonlinear regression analysis of isothermal data. The maximum filler volume fraction, Φm and conversion at gel point, αgel , values are usually known for typical thermosets. Zhou and Sancaktar (2008) incorporated the isothermal temperature effects to obtain a general-form comprehensive model in the form: μ (T, φ , d γ /dt, α ) = A · exp (B/T ) · (φm − φ )−2 · (d γ /dt)C0 +C1 ·α · αgel αgel − α D+E·α (4.76) where, B is the activation temperature and other coefficients are same as in Eq. (4.75). In order to model realistic adhesive processing, usually with a broad temperature range, nonisothermal tests usually need to be undertaken. The comprehensive isothermal chemoviscosity model, based on Eq. (4.76), can then be extended to nonisothermal temperature cure cycle through nonlinear regression analysis of nonisothermal data. In fact, nonisothermal temperature cure is a different process from isothermal cure. The reaction kinetics, total reaction order, and even the reaction energy for epoxy systems may not be constant and same, but process-dependent. Therefore, modifications need to be made to reflect the effects of such a difference. An improvement in the model predictability is expected by allowing parameters D and E in Eq. (4.76) to change with temperature during nonisothermal cure. Furthermore, both of these parameters also show some variation with the volume fraction (Φ) and shear rate (d γ /dt). A modified comprehensive model was thus proposed as follows (Zhou and Sancaktar 2008): μ (T, φ , d γ /dt, α ) = A · exp B T · (φm − φ )−2 · (d γ /dt)C0 +C1 ·α · αgel αgel − α D∗ +E ∗ ·α 126 E. Sancaktar where: D∗ = D0 + D1 · (d γ /dt) + D2 · φ + D3 · T E ∗ = E0 + E1 · (d γ /dt) + E2 · φ + E3 · T (4.77) with Di and Ei values to be determined by data fitting. 4.9 Concluding Remarks Interfaces usually constitute a weak link in the chain of load transfer in bonded joints. Also, the discontinuity of the material properties causes abrupt changes in stress distribution, as well as causing stress singularities at the edges of the interfaces. It is very desirable to optimize the substrate surface topography at the interfaces to maximize the load bearing capacity of bonded joints, and to improve their deformational characteristics. In most engineering joints the adherend surfaces have distinct topographies, which result in a collection of miniature joints in micron, and even nano scale when bonded adhesively. If the interphase is not considered as a discrete collection of individual chemical bonds, the methods of continuum mechanics can still be applied to this collection of miniature joints by assuming continuous, or a combination of continuous/discontinuous interphase zones. Thus, the displacement at the interphase need not be continuous at every location. 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Solids Struct. 2, p 1 You M, Yan ZM, Zheng Y, Xiong WH, Zheng XL, Dai S (2005) Transactions of Nonferrous Metals Soc. China 15 (Sp. Is. 3), p 344 Zabora RF, Clinton WW, Bell JE (1971) Adhesive Property Phenomena and Test Techniques, AFFDL-TR-71-68 Zhang MJ, Straight MR, Brinson HF (1985) Proceedings of the 1985 SEM Spring Conference on Experimental Mechanics, p 205 Zhou J, Sancaktar, E (2008) Chemorheology of Epoxy/Nickel Conductive Adhesives During Processing and Cure, J. Adhes. Sci. Technol. (accepted for publication) Chapter 5 Complex Joint Geometry Andreas Öchsner, Lucas F.M. da Silva and Robert D. Adams Abstract The finite element method is particularly suited to analyse complex joint geometries. Adhesively bonded joints are increasingly being used in engineering applications where the loading mode, the adherends shape and the material behaviour are extremely difficult to simulate with a closed form approach. A detailed description of finite element studies concerning non-conventional adhesive joints is presented in this chapter. Various types of joints, local geometrical features such as the spew fillet and adherend rounding, three dimensional analyses, hybrid joints and repair techniques are discussed. Special techniques to save computer power are also treated. It is shown that the finite element method offers unlimited possibilities for stress analysis but also presents some numerical problems at sharp edges. 5.1 Introduction Stress analysis of bonded joints started 70 years ago with the well known Volkersen shear lag model (Volkersen, 1938). Since, various analytical models have been proposed that include the geometrical non-linearity (Goland and Reissner, 1944), the adhesive plasticity (Hart-Smith, 1973), fibre reinforced plastic adherends (Renton Andreas Öchsner Department of Applied Mechanics, Faculty of Mechanical Engineering, Technical University of Malaysia, 81310 UTM Skudai, Johor, Malaysia; University Centre for Mass and Thermal Transport in Engineering Materials, School of Engineering, The University of Newcastle, Callaghan, NSW, 2308, Australia, e-mail: andreas.oechsner@gmail.com Lucas F.M. da Silva Departamento de Engenharia Mecânica e Gestão Industrial, Faculdade de Engenharia, Universidade do Porto, Rua Dr. Roberto Frias, 4200-465 Porto, Portugal, e-mail: lucas@fe.up.pt Robert D. Adams Department of Mechanical Engineering, University of Bristol, Bristol BS8 1TR, UK, e-mail: R.D.Adams@bristol.ac.uk L.F.M. da Silva, A. Öchsner (eds.), Modeling of Adhesively Bonded Joints, c Springer-Verlag Berlin Heidelberg 2008 131 132 A. Öchsner et al. and Vinson, 1975), etc. However, most of the analytical models are for lap joints of regular shape. Closed form analyses are very useful for an initial estimate of the stress distribution and are generally adequate for design purposes. For adhesive joints of complex shape, numerical techniques such as the finite element (FE) method are preferable. Simple lap joints have been modified because of the nonuniform stress distribution along the overlap. The load transfer and shear stress distribution of various single lap joints (SLJ) are schematically represented in Fig. 5.1. It can be seen that there is a stress concentration at the ends of the overlap for the single lap joint with a square end. Modification of the joint end geometry with a spew fillet or a taper spreads the load transfer over a larger area and give a more uniform shear stress distribution. Adams and co-workers are among the first to have used the FE method for analyzing the stresses in adhesive joints (Adams and Peppiatt, 1974; Crocombe and Adams, 1981; Harris and Adams, 1984; Adams et al., 1986; Adams and Davies, 2002). One of the first reasons for the use of the FE method was to assess the influence of the spew fillet. The joint rotation and the adherends and adhesive plasticity are other aspects that are easier to treat with a FE analysis. The study of Harris and Adams (1984) is one of the first FE analyses taking into account these three aspects. The increasing use of adhesive bonding with composite materials is another typical example of the great advantage of using finite elements (Adams et al., 1986; Adams and Davies, 2002) since the anisotropic behaviour of these materials complicates drastically any analytical approach. But it is when irregular geometries are involved that the FE method is an indispensable tool. Any type of geometry can be modelled, i.e., variations in the adherend shape, local adherend rounding, spew fillet, reinforcements, joints with rivets or bolts, etc. In addition, the simulation gives not only one, two or three stress Fig. 5.1 Load transfer and shear stress distribution in single lap joints 5 Complex Joint Geometry 133 components but all the stress components in all members of the joint. Three dimensional (3D) analyses for assessing width effects is another possibility offered by a FE analysis. As the model gets more complicated in terms of geometry and material behaviour, the computation time also increases. Also, if the user wants to change one geometrical feature, a new model has to be created. For these reasons, parametric studies are more difficult with a FE approach than with a closed form approach. However, special techniques are emerging for solving this problem. All these aspects are discussed in this chapter with a mention to the difficult task of dealing with the singular points present in any type of adhesive joint. 5.2 Types of Joints Adhesive joint studies are generally related to lap joints with flat adherends. The first theoretical analysis of such joints was an analytical model proposed by Volkersen (1938). Since then, many analytical models have been proposed, being the overwhelming majority about lap joints with flat adherends. This is because joints of a more complex geometry are difficult to model using a closed form analysis. Numerical techniques, such as the FE method, can obviously be used for simple geometries such as single or double lap joints with regular flat adherends, but it is for complex geometries that this method of analysis is truly advantageous. Within joints with flat adherends, one can have ‘wavy’ lap joints, ‘reverse bent’ joints, ‘tongue and groove’ joints and scarf joints (see Fig. 5.2). Other types of joints include cylindrical joints, corner joints, T joints and peel joints (see Fig. 5.2). As for analytical models, the majority of the FE analyses are about lap joints with flat adherends. This type of joint is treated in detail in the following sections. However, numerous studies can be found in the literature about other types of joints. Ávila and Bueno (2004) analyzed a new type of single lap joints where the adherends have a ‘wavy’ configuration along the overlap. An FE analysis and experiments show that great strength improvements can be obtained with this technique. Fessel et al. (2007) also studied this type of joint as well as joints with bent substrates along the overlap. An FE analysis and experiments show great joint strength improvements. Dvorak et al. (2001) show with a FE analysis and experimentally that adhesively bonded tongue-and-groove joints between steel and composite plates loaded are stronger than conventional strap joints. Nakagawa and Sawa (2001) studied scarf joints using photoelasticity and a 2D FE model. One of the conclusions is that under a static tensile load, an optimum scarf angle exists where the stress singularity vanishes and the stress distributions become flat near the edge of the interface, but under thermal loads, the optimum scarf angle is not found. Apalak and Davies (1993, 1994) studied different types of corner joints using a linear FE analysis and proposed design guidelines based on the overall static stiffness and stress analysis. Apalak (1999, 2000) developed the previous study taking into account the non-linear geometry. Feih and Shercliff (2005) modelled simple corner joints with composites. 134 A. Öchsner et al. Fig. 5.2 Types of adhesive joints Apalak (2002) studied the geometrical non-linear response of T-joints. Apalak et al. (2003) studied T-joints in terms of thermal and mechanical loads. da Silva and Adams (2002) used the a FE model to predict the joint strength of T-joints based on the plasticity of the adherend. Marcadon et al. (2006) studied T-joint for marine applications and found that both the overlap length and also the distance between the T plywood and the base have an influence on the tearing strength. Kim et al. (1992) studied various configurations of tubular joints (single overlap, double overlap, adherends tapering) and found with a FE analysis and experimentally that the double lap configuration is the strongest joint. Kim and Lee (2001, 2004) used FE models to study the effect of temperature on tubular joints. Kim et al. (1999) modelled composite tubular joints. Oh (2007) used a FE computation to analyze tubular composite adhesive joints under torsion. Good agreement was obtained between the predicted joint strength and the available experimental data. Serrano (2001) used a nonlinear 3D FE model to study glued-in rods for timber structures. The model could simulate experimental behaviour. Peel testing is a very common test for adhesive properties. The problem is highly non-linear in terms of geometry and material and the FE method has been widely used, as for example in the work of Du et al. (2004). 5 Complex Joint Geometry 135 5.3 Adhesive Fillet Various authors have shown that the inclusion of a spew fillet at the ends of the overlap reduces the stress concentrations in the adhesive and the substrate (Adams and Peppiatt, 1974; Crocombe and Adams, 1981; Adams et al., 1986; Adams and Harris, 1987; Dorn and Liu, 1993; Tsai and Morton, 1995; Lang and Mallick, 1998; Belingardi et al., 2002; Apalak and Engin, 2004; Andreassi et al., 2007; da Silva and Adams, 2007a; Deng and Lee, 2007). The adhesive fillet permits a smoother load transfer and decreases the peak stresses. Adams and Peppiatt (1974) found that the inclusion of a 45◦ triangular spew fillet decreases the magnitude of the maximum principal stress by 40% when compared to a square end adhesive fillet. Adams and Harris (1987) tested aluminium/epoxy single lap joints with and without fillet and found an increase of 54% in joint strength for the filleted joint. Adams et al. (1986) tested aluminium/CFRP single lap joints and found that the joint with a fillet is nearly two times stronger than the joint without a fillet. Crocombe and Adams (1981) did similar work but included geometric (overlap length, adhesive thickness and adherend thickness) and material (modulus ratio) parameters. The reduction in peel and shear stresses is greatest for a low modulus ratio (low adhesive modulus), a high adhesive thickness and a low adherend thickness. Dorn and Liu (1993) investigated the influence of the spew fillet in plastic/metal joints. The study includes a FE analysis and experimental tests and they conclude that the spew fillet reduces the peak shear and peel adhesive stresses and decreases stress and strain concentrations in the adherends in the most critical regions. They also studied the influence of different adhesive and different metal adherends. A ductile adhesive and a more balanced joint (aluminium/plastic instead of steel/plastic) give a better stress distribution. Tsai and Morton (1995) studied the influence of a triangular spew fillet in laminated composite single lap joints. The FE analysis and the experimental tests (Moire interferometry) proved that the fillet helps to carry part of the load thus reducing the shear and peel strains. The above analyses are limited to triangular geometry. Lang and Mallick (1998) investigated eight different geometries: full and half triangular, full and half rounded, full rounded with fillet, oval and arc. They showed that shaping the spew to provide a smoother transition in joint geometry significantly reduces the stress concentrations. Full rounded with fillet and arc spew fillets give the highest percent reduction in maximum stresses whereas half rounded fillet gives the less. Furthermore, increasing the size of the spew also reduces the peak stress concentrations. Andreassi et al. (2007) used a two-dimensional computational fluid dynamics model to study spew fillet formation considering the actual adhesive flow produced during joint assembly. This is an interesting approach that allows tuning the adhesive joint strength by changing the adhesive flow parameters. The spew fillet is not beneficial in all situations. In effect, the spew fillet tends to generate more thermal stresses than a square end geometry when used at low temperatures (da Silva and Adams, 2007a). 136 A. Öchsner et al. 5.4 Adherend Rounding Adhesive single lap joints may have several singular (infinite) stresses. The stresses tend to infinite at crack tips and at bi-material junctions. Fracture mechanics can be applied to treat the singular points at crack tips. As regards the bi-material singularities, there can be two or three, depending on the joint geometry (see Fig. 5.3). For both situations, there is an abrupt change in slope giving a sharp corner. The stress field in the vicinity of a sharp corner depends on the mesh used. A stress limit criterion will therefore lead to arbitrary results. The first FE analyses 30 years ago used coarse meshes due to computer memory limitations and therefore did not capture the infinite stress at singular points. The joint strength predictions obtained with stress or strain limit based criteria compared well with the experimental results (Harris and Adams, 1984). With the computer power development, finer meshes can be used which lead to a better stress distribution description but also to stresses that tend to infinite at singular points. The stress or strain limit failure criteria give in this circumstance more conservative predictions and are therefore very arguable. Groth (1988) used a fracture mechanics approach without considering a preexisting crack. He formulated a fracture criterion based on an equivalent generalised stress intensity factor similar to that in classical fracture mechanics. Comparing it to a critical value, joint fracture may be predicted. However, the critical stress intensity factor needs first to be tuned with an experimental test which makes this approach questionable. Another approach for dealing with the singularity points is to use a cohesive zone model (CZM). This approach is associated to interface elements and enables to predict crack initiation and crack growth. It is a combination of a stress limit and fracture mechanics approach and relatively mesh insensitive. Many researchers are using this tool with accurate results (Blackman et al., 2003; de Moura et al., 2006; Liljedahl et al., 2007). However, the parameters associated to the CZM require previous experimental ‘tuning’ and the user needs to know beforehand where the failure is likely to occur. This subject is discussed in detail in Chap. 6. In practical joints the sharp corners are always slightly rounded during manufacture and the singular points will not necessarily exist (see Fig. 5.4). Adams and Harris (1987) studied the influence of the geometry of the corners. Using a simplified model, the effect of rounding on the local stress was investigated. Rounding the corner removes the singularity. Therefore small local changes in geometry have a significant effect. They also performed an elastic-plastic analysis by calculating the Fig. 5.3 Singular points in adhesive joints 5 Complex Joint Geometry 137 Fig. 5.4 Rounding of adhesive and adherend plastic energy density. They found that the stress distribution is more uniform with a maximum some distance from the corner. The reason they give is that as the corner is approached, although the normal stress increases, the rigid adherend restrains the adhesive in the transverse direction. The net hydrostatic component is increased and yield is suppressed so that close to the corner there is a reduction in plastic energy density. It should be born in mind that the effects are local: far away from the corner the stress distribution is unaffected. Apart from the simplified model, Adams and Harris (1987) tested three types of aluminium/rubber-toughened epoxy single lap joints so that local changes at the end of the joint could be assessed. They found excellent agreement between the predicted joint strengths, with the modified models, and the experimental values. 5.5 Adherend Shaping Adherend shaping is a powerful way to decrease the stress concentration at the ends of the overlap. Figure 5.5 presents typical geometries used for that purpose. Some analytical models were proposed to have a more uniform stress distribution along the overlap (Cherry and Harrison, 1970; Adams et al., 1973; Groth and Nordlund, 1991). However, the FE method is more appropriate for the study of adherends shaping. The concentrated load transfer at the ends of the overlap can be more uniformly distributed if the local stiffness of the joint is reduced. This is particularly relevant for adhesive joints with composites due to the low transverse strength of composites. Adams et al. (1986) addressed this problem. They studied various configurations of Fig. 5.5 Adherend shaping 138 A. Öchsner et al. double lap joints where the central adherend is CFRP and the outer adherends are made of steel. They found with FE and experiments that the inclusion of an internal taper and an external fillet can triplicate the joint strength. The same geometry was studied at low temperatures and it was found that the thermal stresses reduce substantially the joint strength (da Silva and Adams, 2007a). Hildebrand (1994) did similar work on SLJs between fibre reinforced plastic and metal adherends. The optimisation of the SLJs was done by modifying the geometry of the joint ends. Different shapes of adhesive fillet, reverse tapering of the adherend, rounding edges and denting were applied in order to increase the joint strength. The results of the numerical predictions suggest that, with a careful joint-end design, the strength of the joints can be increased by 90–150%. The use of internal tapers in adherends in order to minimize the maximum transverse stresses at the ends of bonded joints has also been studied by Towse (1999), Rispler et al. (2000), Guild et al. (2001), Belingardi et al. (2002) and Kaye and Heller (2002). An evolutionary structural optimisation method (EVOLVE) was used by Rispler et al. (2000) to optimise the shape of adhesive fillets. EVOLVE consists of an iterative FE analysis and a progressive removal of elements in the adhesive which are low stressed. Other examples of joint end modifications for joint transverse stress reduction but using external tapers are those of Amijima and Fujii (1989), Sancaktar and Nirantar (2003), Kaye and Heller (2005) and Vallée and Keller (2006). Kaye and Heller (2005) used numerical optimization techniques in order to optimize the shape of the adherends. This is especially relevant in the context of repairs using composite patches bonded to aluminium structures (see Sect. 5.9) due to the highly stressed edges. The FE method is a convenient technique for the determination of the optimum adherend geometry, however the complexity of the geometry achieved is not always possible to realise in practice. 5.6 Other Forms of Geometric Complexity The FE method can be used to study other complex geometrical features such as voids in the bondline, surface roughness, notches in the adherend, etc. (see Fig. 5.6). Nakagawa et al. (1999) studied the effect of voids in butt joints subjected to thermal stresses and found that stresses around defects in the centre of the joint are more significant than those near the free surface of the adhesive. Lang and Mallick (1999), Olia and Rossettos (1996), de Moura et al. (2006) and You et al. (2007) studied the influence of gaps in the adhesive and found that a gap in the middle of the overlap has little effect on joint strength. Kim (2003) proposed an analytical model supported by FE modelling to study the effect of variations of adhesive thickness along the overlap. The author showed that the variations found in practice have little effect on the adhesive stresses along the overlap. 5 Complex Joint Geometry 139 Fig. 5.6 Various forms of geometric complexity Kwon and Lee (2000) studied the influence of surface roughness on the strength tubular joints by modelling the stiffness of the interfacial layer between the adherends and the adhesive as a normal statistical distribution function of the surface roughness of the adherends. The authors found that the optimum surface roughness was dependent on the bond thickness and applied load. Sancaktar and Simmons (2000) investigated the effect of adherend notching on the strength and deformation behavior of single lap joints. The experimental results showed a 29% increase in joint strength with the introduction of the notches, which compared well with the FE analysis results. Yan et al. (2007) studied a similar idea, where the notch is in the middle part of the overlap. A FE analysis showed that a more uniform stress distribution along the overlap can be obtained. 5.7 Three Dimensional Analyses Most of the FE analyses of adhesive joints are two dimensional. Since the width is much larger than the joint thickness, a plane strain analysis is generally acceptable. A generalised plane strain analysis where the joint is allowed to have a uniform strain along two parallel planes in the width direction gives more realistic results. However, for some problems, a two dimensional analysis might lead to erroneous results. Richardson et al. (1993) show that applying the average load on two-dimensional models resulted in errors in the adhesive stresses as high as 20%. The authors propose solutions to limit this problem. Three dimensional effects in the width direction such as lateral straining and the anticlastic bending (see Fig. 5.7) are especially important when analysing composites. Adams and Davies (1996) analysed composite lap joints in three dimensions and showed that the Poisson’s ratio effects are significant in the behavior of composite lap joints. 140 A. Öchsner et al. Fig. 5.7 Three dimensional effects in lap joints The main problem of 3D analyses is the computational time due to the large number of elements. One way of overcoming this problem is to use the submodelling option, where the results from a coarse mesh of the global model are applied as boundary conditions to a much finer mesh of a localised region of particular interest. Bogdanovich and Kizhakkethara (1999) applied this technique to composite double lap joints and concluded that the submodelling approach is an efficient tool although convergence of stresses along certain paths in the joint were not satisfied. They also used the same approach in two dimensions to study the effect of the spew fillet. 5.8 Hybrid Joints Joints with different methods of joining are increasingly being used. The idea is to gather the advantages of the different techniques leaving out their problems. Another possibility is to use more than one adhesive along the overlap or varying the adhesive and/or adherend properties. All theses cases have been grouped here under a section 5 Complex Joint Geometry 141 Fig. 5.8 Hybrid joints called ‘hybrid joints’ (see Fig. 5.8). Such joints are particularly difficult to simulate using analytical models for obvious reasons. The FE method is the preferred tool to investigate the application of such techniques. 5.8.1 Mixed Adhesive Joints Mixed modulus joints have been proposed in the past (Semerdjiev, 1970; Srinivas, 1975; Patrick, 1976) to improve the stress distribution and increase the joint strength 142 A. Öchsner et al. of high modulus adhesives. The stiff, brittle adhesive should be in the middle of the overlap, while a low modulus adhesive is applied at the edges prone to stress concentrations. Sancaktar and Kumar (2000) used rubber particles to toughen the part of the adhesive located at the ends of the overlap and increase the joint strength. The concept was studied with the FE method and proved experimentally. Pires et al. (2003) and Fitton and Broughton (2005) also proved with a FE analysis and experimentally with two different adhesives that the mixed adhesive method gives an improvement in joint performance. Temiz (2006) used a FE analysis to study the influence of two adhesives in double lap joints under bending and found that the technique decreases greatly the stresses at the ends of the overlap. Bouiadjra et al. (2007) used the mixed modulus technique for the repair of an aluminium structure with a composite patch. The use of a more flexible adhesive at the edge of the patch increases the strength performance of the repair. The technique of using multi-modulus adhesives has been extended to solve the problem of adhesive joints that need to withstand low and high temperatures by da Silva and Adams (2007b, 2007c). At high temperatures, a high temperature adhesive in the middle of the joint retains the strength and transfers the entire load while a low temperature adhesive is the load bearing component at low temperatures, making the high temperature adhesive relatively lightly stressed. The authors studied various configurations with the FE method and proved experimentally that the concept works, especially with dissimilar adherends. 5.8.2 Adhesive Joints with Functionally Graded Materials Functionally graded materials are increasingly being used in various applications including adhesive joints. For example, Apalak and Gunes (2007) studied the effect of a functionally gradient layer between a pure ceramic layer (Al2 O3 ) and a pure metal layer (Ni). Gannesh and Choo (2002) studied the effect of spatial grading of adherend elastic modulus on the peak stress and stress distribution in the singlelap bonded joint. The adherends in the overlap length was divided into ten equal regions and material properties assign as a function of the grading. The peak shear stresses could be reduced by 20%. The study previously referred of Sancaktar and Kumar (2000) is effectively a functionally graded adhesive with the use of rubber particles. This is an area that is being intensively studied and where modelling at different scales is essential. 5.8.3 Rivet-Bonded Joints Liu and Sawa (2001) investigated, using a three-dimensional FE analysis, rivetbonded joints and found that for thin substrates bonded, riveted joints, adhesive joints and rivet-bonded joints gave similar strengths whilst for thicker substrates the rivet-bonded joints were stronger. They proved this experimentally. Later, the same 5 Complex Joint Geometry 143 authors (Liu and Sawa, 2003; Liu et al., 2004) proposed another technique similar to rivet-bonded joints: adhesive joints with adhesively bonded columns. Strength improvements are also obtained in this case. The advantage of this technique of that the appearance is the joint is maintained in relation to an adhesive joint. Grassi et al. (2006) studied through-thickness pins for restricting debond failure in joints. The pins were simulated by tractions acting on the fracture surfaces of the debond crack. 5.8.4 Bolted-Bonded Joints Chan and Vedhagiri (2001) studied the response of various configurations of single lap joints, namely bonded, bolted and bonded-bolted joints by three-dimensional FE method and the results were validated experimentally. The authors found that for the bonded-bolted joints, the bolts help to reduce the stresses at the edge of the overlap, especially after the initiation of failure. The same type of study was carried out by Lin and Jen (1999). 5.8.5 Weld-Bonded Joints Al-Samhann and Darwish (2003) demonstrated with the FE method that the stress peaks typical of adhesive joints can be reduced by the inclusion of a weld spot in the middle of the overlap. They studied later the effect of adhesive modulus and thickness (Darwish and Al-Samhann, 2004). Darwish (2004) also investigated weldbonded joints between dissimilar materials. 5.9 Repair Techniques Adhesively bonded repairs are generally associated to complex geometries and the FE method has been extensively used for the optimization of the repair, especially with composites. The literature review of Odi and Friend (2002) about repair techniques illustrates clearly this point. Typical methods and geometries are presented in Fig. 5.9. Among the various techniques available, bonded scarf or stepped repairs are particularly attractive because a flush surface is maintained which permits a good aerodynamic behavior. Odi and Friend (2004) show that an improved 2D plane stress model is sufficient to get reliable joint strength predictions. Gunnion and Herszberg (2006) studied scarf repairs and carried out a FE analysis to asses the effect of various parameters. They found that the adhesive stress is not much influenced by mismatched adherend lay-ups and that there is a huge reduction in peak stresses with the addition of an over-laminate. Campilho et al. (2007) studied scarf repairs of composites with a cohesive damage model and concluded that the strength of the repair increased exponentially with the scarf angle reduction. 144 A. Öchsner et al. Fig. 5.9 Repair techniques Bahei-El-Din and Dvorak (2001) proposed new design concepts for the repair of thick composite laminates. The regular butt-joint with a patch on both sides was modified by the inclusion of pointed inserts or a ‘zigzag’ interface in order to increase the area of contact and improve the joint strength. Soutis and Hu (1997), Okafor et al. (2005) and Sabelkin et al. (2007) studied numerically and experimentally bonded composite patch repairs to repair cracked aircraft aluminum panels. The authors concluded that the bonded patch repair provides a considerable increase in the residual strength. Tong and Sun (2003) developed a pseudo-3D element to perform a simplified analysis of bonded repairs to curved structures. The analysis is supported by a full 3D FE analysis. The authors found that external patches are preferred when the shell is under an internal pressure while internal patches are preferred when under an external pressure. 5.10 Special Techniques in Finite Element Simulation One of the advantages of closed form analyses in relation to the FE method is that parametric studies are much easier to perform. With conventional FE techniques, every time a geometric parameter of the model (adhesive or adherend thicknesses, 5 Complex Joint Geometry 145 angle of the spew fillet, etc.) with a different value is considered, a new model is required which is time consuming. However, recent FE libraries include connections that can be described in a parametric form. Similar families of connections need to be meshed only once and the users need only enter the parameters. Actis and Szabó (2003) have used parametric models for the study of bonded and fastened repairs. These models have associated p-type meshing, where convergence of the solution is achieved by increasing the polynomial order of the element rather than increasing the number of elements in the model (known as h-type meshing). More recently, Kilic et al. (2006) present a finite element technique utilizing a global element coupled with traditional elements. The global element includes the singular behaviour at the junction of dissimilar materials. Other special techniques in FE simulation for the significant reduction of the modelling (mesh generation) and computation time are presented next, which is critical when complex geometries are involved. The main focus is on techniques which do not require any new code at all or are achievable by very simple routines consisting of a few lines of computer code. Advanced topics which require the development of comprehensive new routines, for instance as in the case of new element formulation (e.g. to better approximate singularities), are not considered. The presented techniques are realisable by actual versions of several commercial finite elements codes. The techniques will be applied to the example of a single lap joint problem taken from Zhao (1991) where the influence of different degrees of rounding on the joint strength was experimentally and numerically investigated. The general problem with geometric dimensions and boundary conditions is shown in Fig. 5.10. The adherends were made of 3.2 mm thick aluminium sheets (Young’s modulus: 70 GPa; Poisson’s ratio: 0.33) and the brittle adhesive epoxy resin Ciba MY750 with hardener HY906 (Young’s modulus 2.8 GPa; Poisson’s ratio: 0.4) was used. A 2D plane strain problem was modelled because of the large joint width and the Fig. 5.10 Single lap joint: (a) joint geometry and applied boundary conditions (dimensions in mm); (b) different degrees of rounding (the grey colour represents the adhesive) (Zhao, 1991) 146 A. Öchsner et al. ends of the joints were constrained without any rotation to account for the testing conditions. It should be mentioned here that Zhao (1991) used a two steps approach because of limitations in computer power: A first computation was based on a coarse mesh for the entire specimen, followed by a refined mesh in the corner region with the displacement result from the first analysis as the new boundary condition. The following examples which were realised with the commercial code Marc (MSC Software Corporation, Santa Ana, CA, USA) may be considered as an alternative for such a two step approach. 5.10.1 Consideration of Point Symmetry Commercial finite element codes allow to consider certain types of symmetry conditions. Common examples are symmetry about an axis (so-called reflective symmetry) or cyclic symmetry (structures with a geometry and a loading varying periodically about a symmetry axis). Point symmetry (or origin symmetry, rotational symmetry by 180◦ ) with respect to the origin of the coordinate system occurs for instance in the case of single lap joints under tensile load (cf. Fig. 5.11a). This type of symmetry is not covered by the standard symmetry conditions which are mentioned above. If one can consider the point symmetric deformation behaviour of a single lap joint (cf. Fig. 5.11b), it is obvious that the mesh size and the resulting system of equations can be reduced by 50% which results in a significant reduction of the calculation time. Looking at the deformation of a full single lap specimen (cf. Fig. 5.12) in the centre plane, i.e. x = 0, one can see that a node at a distance +a from the glue line (y = 0) moves under load for the shown arrangement to the negative x and y direction. The movement in the negative y direction is about two orders of magnitude smaller than the displacement in the x direction and difficult to observe in the scale of Fig. 5.12. On the other hand, a node at distance −a from the glue line moves with the same magnitude, however, in the positive coordinate directions. This relationship for a pair of nodes at (0,+ a) and (0,– a) can be expressed by the following constraint condition Fig. 5.11 Deformation of a single lap joint under tensile load: (a) deformed S-shape of the entire specimen; (b) consideration of the S-shape for the half specimen due to appropriate point symmetry condition 5 Complex Joint Geometry 147 Fig. 5.12 Details of a deformed single lap specimens to illustrate node translation in the centre plane x = 0 u v x=0;y=−a = −1.0 0 u · , −1.0 v x=0;y=+a 0 (5.1) where the vector of displacement at node y = −a is referred to as the tied (“slave”) node while the node on the right-hand side is referred to as the retained node (“master”). The connecting matrix is called the constrained matrix. Some commercial finite element codes allow the definition of arbitrary homogeneous constraints between nodal displacements by user subroutines (in the case of MSC Marc: UFORMS routine). When such a routine is supplied, the user is simply replacing the one which exists in the program using appropriate control setup. In the considered case of point symmetry, it must be mentioned that the constraint condition must be defined for each pair of nodes in the centre plane x = 0. 5.10.2 Connecting Dissimilar Meshes Modern adhesives can be applied in films of several micron of thickness while the surrounding adherends may extend to a much larger scale in the range of millimetres, centimetres etc. If accuracy in the adhesive layer is requested, several elements must be introduced over the adhesive thickness and this mesh density must be coarsened in order to limit the total number of elements to account for limitations in computer hardware (in particular the random access memory, RAM). In addition, regions with high stress gradients require a fine and regular mesh if these changes should be evaluated. Such constraints may result in a quite complicated mesh which is difficult to generate and a huge system of equations whose solution is time-consuming. In addition, it might be necessary to introduce transition elements which may have poor performance for specific loading conditions, e.g. bending. As an alternative, the approach of dissimilar meshes (cf. Fig. 5.13) may be introduced. 148 A. Öchsner et al. Fig. 5.13 Example of a finite element model composed of two dissimilar meshes (nodes are not coincident at the interface) The major idea is to generate different types of meshes which are not connected in the classical way, i.e. by common nodes which belong to both touching elements. Regions where high accuracy of the analysis is requested may be composed of a very fine and regular mesh (Fig. 5.13, right part) while other parts can be modelled by coarse and irregular element representations (Fig. 5.13, left part). One method of connecting these dissimilar meshes is to use interface elements (Schiermeier et al., 2001). Nowadays, actual versions of commercial finite element codes allow such an application in the scope of novel contact options, i.e. to “glue” dissimilar contacting meshes without the need for interface elements. In such a case, by specifying that the glue motion is activated, the constraint equations are automatically written between the two meshes and the contact region is not allowed to separate. In the case of the corner rounding influence, a basic single lap joint was meshed with a quite coarse mesh (adherend length: 96.8 mm) and several refined inlays (cf. Fig. 5.10b) were separately generated and successively “glued” to the basic joint. Figure 5.14 shows as an example the refined inlay with the sharp corner which is “glued” at the dissimilar interfaces to the basic joint. Similar meshes for the inlays with different degree of rounding were obtained. To present some numerical results, the normalised von Mises stress along the bond line for the different configurations of corners is shown in Fig. 5.15. It can be clearly seen that the introduction of a rounding decreases the stress peak (as shown in Peppiatt (1974) and Chen (1985)) and thus, results in a higher strength of the adhesive joint. The difference in the peak values are presented in Table 5.1 and compared to experimental findings taken from Zhao (1991). It can be seen that this numerical simulations reveals the same tendency as the experimental values. It must be noted here that the presented numerical results are based on a pure linear elastic analysis and small deformations and an additional consideration of the non-linear material behaviour and appropriate yield conditions of both components can improve the obtained results compared to experimental values. 5 Complex Joint Geometry 149 Fig. 5.14 Dissimilar meshes in the case of the sharp corner: the corner region consists of a much finer mesh Fig. 5.15 von Mises stress k normalised by average shear stress τave along the normalised bond line (y = 0). Stress distributions are obtained or the same external load F Table 5.1 Comparison between joint strength prediction and experiments Corners FE (Strength increase in %) Experiment, Zhao (1991) (Strength increase in %) sharp r = 0.25 r = 1.6 r = 3.2 0 (ref.) 8.54 20.55 24.28 0 (ref.) 16.50 20.00 40.15 150 A. Öchsner et al. 5.11 Conclusions This chapter describes studies that deal with adhesive joints of complex geometry using the FE method. The main conclusions are: 1. The FE method can give the stress distribution in the whole bonded structure and is an efficient tool to identify the stress concentrations. 2. For this reason, the FE method is the most adequate to develop and optimize adhesive joints. 3. FE studies of different complexity were discussed: lap joints with irregular shapes, rounding of adherend ends, spew fillet, hybrid joints and repair techniques. 4. The stress concentrations at sharp corners, where the failure is likely to occur, are difficult to handle using traditional stress-strain approaches because the results are mesh dependent. 5. This problem can be solved, to some extend, rounding the edges, using a strength singularity approach or a cohesive zone model. However, even these methods require some kind of experimental ‘tuning’. 6. The optimization of joint strength by the use of functionally graded adhesives is one the main challenges in adhesive joints modelling. 7. Parametric studies are more difficult to perform with the FE method due to the re-meshing problem and the computation time. However, recent FE programs include routines for automatic re-meshing. Submodelling is another technique for saving computation time and change geometric parameters in an easier way. This has been performed in the present chapter and validated with experimental results. References Actis RL, Szabó BA (2003) Analysis of bonded and fastened repairs by the p-version of the finiteelement method. Comput Math Appl 46: 1–14 Adams RD, Atkins RW, Harris JA, Kinloch AJ (1986) Stress analysis and failure properties of carbon-fibre-reinforced-plastic/steel double-lap joints. J Adhes 20: 29–53 Adams RD, Chambers SH, Del Strother PJA, Peppiatt NA (1973) Rubber model for adhesive lap joints. 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Int J Adhes Adhes 27: 696–702 Zhao X (1991) Stress and failure analysis of adhesively bonded lap joints, PhD thesis, Department of Mechanical Engineering, University of Bristol, UK Chapter 6 Progressive Damage Modelling Marcelo F.S.F de Moura Abstract The application of bonded joints is increasing due to their several advantages to alternative bonding methods. As a result, more efficient predictive tools are necessary to increase the confidence of designers. In this context, cohesive and continuum damage models acquire special relevancy owing to their capacity to simulate damage onset and growth. Both of these methodologies combine strength of materials with fracture mechanics, thus overcoming the limitations of each method. A cohesive mixed-mode damage model based on interface finite elements and accounting for ductile behaviour of adhesives is presented. The cohesive parameters of the constitutive softening law are determined using an inverse method applied to fracture characterization tests under pure modes, I and II. In this context a new data reduction scheme based on crack equivalent concept is developed and applied to fracture characterization tests. Good agreement between the numerical and experimental results was obtained for strength versus overlap length in singlelap joints. A continuum mixed-mode damage model is also presented using a triangular softening law adequate only for brittle or moderately ductile adhesives. In these models the material properties degradation occurs inside of the solid elements, which is advantageous relatively to cohesive methods mainly when damage propagation onset and path are not known a priori. 6.1 Introduction Adhesive joints present several advantages over other conventional bonding methods like mechanically fastened joints. Adhesive joints present less sources of stress concentrations, more uniform load distribution and better fatigue properties. They Marcelo F.S.F de Moura Departamento de Engenharia Mecânica e Gestão Industrial, Faculdade de Engenharia, Universidade do Porto, Rua Dr. Roberto Frias, 4200-465 Porto, Portugal, e-mail: mfmoura@fe.up.pt L.F.M. da Silva, A. Öchsner (eds.), Modeling of Adhesively Bonded Joints, c Springer-Verlag Berlin Heidelberg 2008 155 156 M.F.S.F. de Moura also provide higher flexibility to join different materials, allowing the choice of the better material for each component of a structure. To benefit from these advantages it is crucial to design bonded joints properly. There are two basic approaches: strength of materials and fracture mechanics based methods. These methods are described in more detail below. 6.1.1 Failure Prediction Classical Methods 6.1.1.1 Strength of Materials In the strength of materials approach the maximum stress or strain criteria are the most popular ones. They are based on the assumption that failure occurs when one of the stress or strain tensor components attains the respective strength value. Harris and Adams [19] used with success the maximum principal stress and the maximum principal strain criteria in order to predict the failure of single lap joints. Ikegami et al. [20] used the von Mises stress criterion to predict the failure of scarf joints using metal and composite adherends and Charalambides et al. [4] applied the same criterion to double lap joints. They did not obtain accurate results due to dependence of adhesive behaviour on the hydrostatic stress, which is not accounted for in the von Mises criterion. Several different versions of these criteria were used by other authors. Lee and Lee [28] used the maximum shear strain criterion on single lap tubular joints. Crocombe and Adams [6] proposed the effective plastic strain criterion for peel tests. In these tests the triaxial strain is expressed as an effective one, which is compared to the uniaxial failure strain of bulk specimens. The referred criteria have a main difficulty when applied to the failure prediction of bonded joints. In fact, in bonded joints a problem of stress singularity at the end of overlapping regions arises due to sharp corners. A stress singularity can be defined as a point where, according to linear elastic analysis, an infinite value of stress appears. Evidence of this problem can be detected in finite element analysis, when stresses at the singularity point increase with the mesh refinement and convergence cannot be reached. In conclusion, it can be affirmed that the stress based methods present mesh dependency during numerical analysis due to stress singularities. To overcome this problem the stresses obtained numerically are used in a point stress or average stress criteria [38] in order to evaluate the occurrence of failure. In the point stress criterion the stresses are evaluated at a characteristic distance (Fig. 6.1) whereas in the average stress criterion they are averaged over a distance. The failure occurs when these stress values attain the respective material strength. They can be viewed as semi-empirical criteria as the characteristic distance value is determined from experimental data. Towse et al. [36] used the criterion of critical strain at a given distance to predict failure of double lap joints. In this case, failure is simulated when the strain in the neighbouring region of the singularity reaches the respective limiting value. Although the obtained results agreed with the experimental ones, it should be emphasized that the characteristic distance was experimentally determined, which limits its use in other types of joints. John et al. [22] argues that 6 Progressive Damage Modelling 157 Fig. 6.1 Stress or strain at a characteristic distance from the singularity Position of evaluation point failure occurs when shear stress attains a critical value at a normalized distance from the singularity point in a double lap joint of unidirectional composite. However, this result implies that the critical distance varies as a function of the overlap length which is not physically sound. The average stress criterion applied to failure prediction of bonded joints was used by Zhao [42]. The critical dimension used to evaluate the average of the maximum principal stress was considered as being equal to the adhesive thickness. However, Charalambides et al. [4] demonstrated that for double lap joints the point of maximum stress occurs out of the characteristic region. In summary it can be affirmed that the point and the average stress criteria can provide accurate results but they depend markedly on the previous determination of the characteristic distance, which is usually performed by experimental tests. However, the results can not be easily applied to different types of joints that do not use the same materials and geometry. In fact, the lack of a physical meaning of this characteristic distance renders impossible the establishment of general predictive tools, not depending on a parameter which is a function of type of loading, materials involved and joint geometry. 6.1.1.2 Fracture Mechanics In the strength of materials approach, materials are assumed to be free of defects. Unlike to what happens in strength of materials based approaches, the fracture mechanics approach assumes the presence of an inherent defect in the material, induced during the fabrication process or during work. In this case the objective is to know if the defects can induce catastrophic failure or if, during the predicted structure life, they can propagate stably maintaining their dimensions inferior to the critical size. There are two types of fracture mechanics criteria. The criteria can be based on stress intensity factors or on the energetic concepts. The stress intensity factor is defined as √ (6.1) K = Y σR π a where Y is a non-dimensional factor depending on the geometry and loading distribution, σR the remote applied stress and a the crack length. It is assumed that crack propagation occurs when the stress intensity factor attains its critical value 158 M.F.S.F. de Moura Kc = σu √ πa (6.2) where σu is the strength of the material. The energetic criterion is based on the assumption that crack growth will occur when the energy available at the crack tip (G – strain energy release rate) and due to the applied loading, overcomes the critical strain energy release rate (Gc ), which is a material property. The strain energy release rate is given by G= dW dU − dA dA (6.3) where W is the work realized by external forces, U the internal strain energy and dA the variation of crack surface. It should be noted that G and K are intrinsically related. In fact, Irwin [21], demonstrated that in plane stress G= K2 E (6.4) and in plane strain K 2 (1 − v2 ) (6.5) E where E and ν are the Young’s modulus and Poisson’s ratio, respectively. These relationships are also valid for the respective critical values (Gc and Kc ). Crack growth can take place under three different modes, as it can be seen in Fig. 6.2. The mode I represents an open mode and the others (mode II and mode III) are the shear modes. In the majority of real situations the applied loading originates a combination of modes at the crack tip, which implies that a mixed-mode criterion should be considered in order to better simulate the damage propagation. Several authors applied the fracture mechanics concepts to the failure strength prediction of bonded joints. The majority of the proposed works are based on the concepts of strain energy release rate. It is usually assumed that damage propagation occurs when the strain energy at the crack front is equal to the critical strain energy release rate, which is a material property. Kinloch [24] refers that energetic criterion is advantageous relatively to stress intensity factors approach. First the strain energy release rate has an important physical significance related to the energy absorption. Second, the value of stress intensity factors is not easily determinable, namely when the crack grows at or near to an interface. Ripling et al. [33] also G= Fig. 6.2 Failure modes 6 Progressive Damage Modelling 159 proposed the use of strain energy release rates instead of stress intensity factors recognizing the non-homogeneity of the bonded joints. However, it should be referred that the application of energetic criterion is not absent of some difficulties related to mixed-mode crack propagation. In fact, in homogeneous and isotropic materials cracks tend to propagate under mode I, perpendicularly to the direction of maximum principal stress, independently of the original crack. However, in a bonded joint, the crack growth direction is restricted by the adherends which leads, in most cases, to a mixed-mode crack propagation (I+II). Under these circumstances it is fundamental to use adequate energetic criteria which are generally in the form of GI GIc A + GII GIIc B =1 (6.6) where GIc and GIIc are the critical values in mode I and mode II. The linear energetic criterion (A = B = 1) and the quadratic one (A = B = 2) are the most used. One of the most popular methods based on fracture mechanics concepts is the Virtual Crack Closure Technique (VCCT), which is detailed by Krueger [25]. The method allows obtaining the strain energy release rates and is based on the assumption that, when a crack grows the energy released in this process is equal to the work necessary to close the crack to its initial length before propagation. Figure 6.3 represents a two-dimensional problem where the crack grows from the node l to node i. The method can be applied by two different ways. The first one consists in two steps. In a first run, node l is closed and the forces in the mode I and mode II directions at this node are registered. In a second run, node l is opened originating nodes l1 and l2 and, by applying the same loading, the relative displacements between these nodes in the respective directions are also measured. However, the method can also be applied in a sole run. In this case, it is necessary to use a refined mesh and to assure that self-similar crack propagation exists. The energy necessary to close the crack is obtained by multiplying the loads at node i by the relative displacements between nodes l1 and l2 1 Δ E = (Xi Δ ul +Yi Δ vl ) (6.7) 2 where Xi , Yi represent the loads at the closed node i and Δ ul , Δ vl the difference of displacements between nodes l1 and l2 . The respective strain energy release rates can then be calculated by the product of the relative displacements at the “opened point” (nodes l1 and l2 ) and the loads at the “closed point” (node i) 1 Yi Δ vl 2bΔ a 1 Xi Δ ul GII = 2bΔ a GI = (6.8) being bΔa the area of the new surface created by an increment of crack propagation (see Fig. 6.3). Using the energetic criterion expressed by Eq. (6.6), propagation will occur when the values of GI and GII obtained from Eq. (6.8) satisfy the criterion. It should be 160 Fig. 6.3 The virtual crack closure technique (VCCT) M.F.S.F. de Moura y Elements thickness = b ul2 ul1 vl2 l2 Yi vl1 Xi x i l1 a Δa Δa noted that the method can be easily applied in three-dimensional problems, where mode III can be obtained using the same procedure described for the other modes. It should be referred that the use of fracture mechanics criteria depends on the existence of some kind of defect which is usually simulated as a pre-crack. These initial cracks are artificially introduced and intend to simulate damage or defects originated during the fabrication process or induced in service. Thus, it can be affirmed that fracture mechanics based criteria are more adequate for damage growth instead of its initiation. On the other hand, there are some difficulties associated to this approach. In fact, the initial crack length size and its locus constitute two main difficulties characteristic of the method. 6.1.2 Actual Trends The stress and fracture mechanics based criteria present some disadvantages. The stress based methods present mesh dependency during numerical analysis due to stress singularities. On the other hand, the point/average stress criteria require the definition of a critical dimension which depends on loading, materials and joint geometry, and do not have a physical theoretical foundation. Fracture mechanics approach relies on the definition of an initial flaw or crack length. However, in many structural applications the damage initiation locus is not obvious. On the other hand, the stress-based methods behave well at predicting damage onset, and fracture mechanics has already demonstrated its accuracy in the crack propagation modelling. In order to overcome the referred drawbacks and exploit the usefulness of the described advantages, cohesive damage models and continuum damage mechanics emerge as suitable options. These methodologies combine aspects of stress based analysis to model damage initiation and fracture mechanics to deal with damage propagation. Thus, it is not necessary to take into consideration an initial defect and mesh dependency problems are overcome. Chapters 7 and 8 also deal with this methodology. 6 Progressive Damage Modelling 161 6.2 Cohesive Damage Models The use of cohesive damage models in fracture problems has become frequent in the most recent years. One of the most important advantages of cohesive models is related to their capacity to simulate onset and non-self-similar growth of damage. No initial crack is needed and damage propagation takes place without user intervention. They are usually based on a softening relationship between stresses and relative displacements between crack faces, thus simulating a gradual degradation of material properties. They do not depend on a predefined initial flaw unlike conventional fracture mechanics approaches. Typically, stress based and energetic fracture mechanics criteria are used to simulate damage initiation and growth, respectively. Usually, cohesive damage models are based on spring [7, 26] or interface finite elements [9, 30, 31] connecting plane or three-dimensional solid elements. Those elements are placed at the planes where damage is prone to occur which, in several structural applications, can be difficult to identify a priori. However, an important characteristic of bonded joints is that damage propagation is restricted to well defined planes corresponding to the ones near or at the interfaces between adhesive and adherends or inside the adhesive, thus leading to a typical application of cohesive methods. In the context of adhesive joints, some works considering the cohesive approach have been reported. Gonçalves et al. [18] considered a mixed-mode cohesive damage model to simulate the debonding process of aluminium single-lap joints loaded in tension. A triangular traction-separation law was used. The experimental loaddisplacement curves and failure loads were accurately predicted when the plastic behaviour of the materials was included in the analysis, for the entire range of overlap lengths considered. Blackman et al. [2] used a cohesive zone model (CZM) approach including two parameters, Gc and σmax , to study the fracture of adhesively bonded joints. A polynomial traction-separation law was considered. The main objective was to investigate the physical significance of σmax . Experimental and numerical results were compared using the Tapered Double Cantilever Beam (TDCB) and peel tests under mode I load. It was concluded that the specimen compliance and Gc depend on the value of σmax until a relatively high value of this parameter, when the dependence significantly diminished. A CZM was also employed by Yang et al. [39] to study the coupling between interface fracture and plastic strain of the adherends. For the adhesive, a trapezoidal shape traction-separation law, including plasticity, was used. The model was validated performing T-peel tests on adhesively bonded aluminium joints. The same authors [41] considered a similar traction-separation law for elastic-plastic mode II crack growth modelling. End Notched Flexure (ENF) specimens subjected to a bending load, and undergoing extensive plastic strain prior to failure, were used to validate the model. The main fracture parameters were determined comparing numerical and experimental results for a particular geometry, and then applied to other geometries. Yang and Thouless [40] simulated the mixed-mode fracture of joints bonded with ductile adhesives using a mode-dependent embedded process zone (EPZ) model. Mode I and mode II fracture laws obtained from previous works were combined with a mixed-mode failure criterion to provide quantitative 162 M.F.S.F. de Moura predictions of the deformation and fracture of T-peel specimens and single-lap shear joints. A linear toughness based criterion was used to access complete failure of the EPZ elements and subsequent damage growth. Thouless et al. [35] used a cohesivezone approach to model the mixed-mode fracture of adhesively bonded Glass Fibre Reinforced Plastic single-lap joints. Three and two parameter damage laws were used for mode-I and for mode-II, respectively. The three-parameter (interface cohesive strength, characteristic strength and toughness) mode-I traction–separation law was used in order to simulate interfacial cracking followed by fibre pull-out (experimentally observed for mode-I fracture). On the other hand, mode II tests indicated that only few fibres were pulled out during mode-II fracture. Consequently, a two parameter (interface cohesive strength and toughness) trapezoidal traction–separation law was used to simulate the behaviour of the adhesive layer in mode-II. Experimental and numerical curves revealed excellent agreement, including both the strengths of the joints and the failure mechanisms. Andersson and Stigh [1] used an inverse method to determine the cohesive parameters of a ductile adhesive layer loaded in peel using equilibrium of energetic forces acting on a Double Cantilever Beam (DCB) specimen. This method consists on fitting the load-displacement curves, up to a predefined agreement is achieved, thus defining the used cohesive parameters. They verified that the stress-relative displacement curve can be divided in three parts. Initially the stress increases proportionally to the elongation (linear elastic behaviour of the layer), until a limit stress is achieved. A plateau region is then observed, corresponding to the plastic behaviour of the adhesive. The curve ends with a parabolic softening part. Leffler et al. [29] performed an identical analysis to determine the complete stress versus deformation relation of a thin adhesive layer loaded in shear, using the ENF specimen. The used method included the determination of the energy release rate as a function of the shear deformation at the crack tip, followed by derivation of the traction-separation relation using an inverse method. An approximate trapezoidal relation was obtained. 6.2.1 Cohesive Damage Model Including Plastic Behaviour A cohesive mixed-mode (I+II) damage model was developed in order to simulate damage initiation and growth in bonded joints. The model is implemented via interface finite elements including a constitutive softening law which relates stresses (σ) and relative displacements (δr ) between homologous points. The constitutive law presents a trapezoidal shape to account for the ductile behaviour typical of many adhesives (see Fig. 6.4). It should be noted that the triangular law, which can be used for brittle or moderately ductile adhesives, is a particular case of this trapezoidal one. Before damage starts to grow σ = Eδr (6.9) where E is a diagonal matrix containing the interface stiffnesses (ei , i = I, II). These are defined as the ratio between the Young’s (mode I) or shear modulus (mode II), 6 Progressive Damage Modelling 163 σi Pure-mode model Jic i = I, II σu,i σum,i Mixedmode model Ji δ1m,i δ1,i δ2m,i δum,i δ2,i δu,i δi Fig. 6.4 The trapezoidal constitutive law for pure-mode and mixed-mode and adhesive thickness. The effect of adhesive thickness is then included by this way and it could be neglected in the finite element mesh. In the pure-mode damage model, damage initiates when the relative displacement exceeds δ1,i . From this point up to final failure (δu,i ) a progressive softening is simulated in order to account for the different failure processes occurring in the vicinity of the crack tip. In this region, known as the Fracture Process Zone (FPZ), several damage processes, like plasticity and micro-cracking, take place, which is simulated by this softening law. Damage evolution is implemented through a damage parameter ranging between zero (undamaged) and one (complete failure). The softening relationship can be written as (6.10) σ = (I − D)Eδr where I is the identity matrix and D is a diagonal matrix containing, in the position corresponding to mode i (i = I, II), the damage parameter, d. In the plateau region the damage parameter can be defined as d = 1− δ1,i δi (6.11) where δ1,i (i = I, II) is obtained from the initial stiffness (ei ) and local cohesive strength in each mode σu,i (i = I, II). In the stress softening part of the curve, d = 1− δ1,i (δu,i − δi ) δi (δu,i − δ2,i ) (6.12) The rigorous definition of the second inflexion point (δ2,i ) in pure modes is not necessary since experience has shown that the precise details of the softening slope are generally not very significant. This issue will be discussed in more detail in the following sections. The maximum relative displacement, δu,i , at which complete failure occurs, is obtained by equating the area under the softening curve to Jic , which corresponds to the respective critical fracture energy 164 M.F.S.F. de Moura Jic = σu,i (δ2,i − δ1,i + δu,i ) 2 (6.13) As in the majority of cases, bonded joints are subjected to mixed-mode (I+II) loading, a cohesive mixed-mode damage model, which is an extension of the pure-mode one, is also developed (Fig. 6.4). Damage initiation is predicted using a quadratic stress criterion σI 2 σII 2 + = 1 if σI > 0 (6.14) σu,I σu,II σII = σu,II if σI ≤ 0 where σi and σu,i (i = I, II) represent, respectively, the stresses and local cohesive strengths in each mode. It is assumed that normal compressive stresses do not induce damage. Considering Eq. (6.9), the first Eq. (6.14) can be rewritten as a function of the relative displacements δ1m,I δ1,I 2 + δ1m,II δ1,II 2 =1 (6.15) where δ1m,i (i = I, II) are the relative displacements in each mode corresponding to damage initiation. Defining an equivalent mixed-mode displacement δm = δI 2 + δII 2 (6.16) and a mixed-mode ratio β= δII δI (6.17) the equivalent mixed-mode relative displacement at the onset of the softening process (δ1m ) is obtained combining Eqs. (6.15), (6.16), (6.17) 1+β 2 δ1m = δ1,I δ1,II (6.18) δ1,II 2 + β 2 δ1,I 2 Stress softening onset (δ2m ) is predicted using a relationship between the current relative displacements in each mode and the critical relative displacements, similar to the one considered for the damage initiation point (Eq. 6.15), δ2m,I δ2,I 2 δ2m,II + δ2,II 2 =1 (6.19) Using a procedure similar to the one followed for δ1m , the mixed-mode relative displacement at the onset of the stress softening process (δ2m ) can be obtained 6 Progressive Damage Modelling 165 δ2m = δ2,I δ2,II 1+β 2 δ2,II 2 + β 2 δ2,I 2 (6.20) Crack growth is simulated by the linear fracture energetic criterion JI JII + =1 JIc JIIc (6.21) When Eq. (6.21) is satisfied, damage growth occurs and stresses are completely released, with the exception of normal compressive ones. The energy released in each mode at complete failure can be obtained from the area of the smaller trapezoid of Fig. 6.4 σum,i (δ2m,i − δ1m,i + δum,i ) (6.22) Ji = 2 Combining Eqs. (6.16), (6.17), (6.22) and (6.21) it can be written δum = 2JIc JIIc (1 + β 2 ) − (δ2m − δ1m )δ1m (eI JIIc + β 2 eII JIc ) δ1m (eI JIIc + β 2 eII JIc ) (6.23) which corresponds to the ultimate relative displacement in mixed-mode. The damage parameter can now be evaluated using the critical mixed-mode displacements (Eqs. (6.18), (6.20) and (6.23)) in Eqs. (6.11) and (6.12). 6.3 Evaluation of Cohesive Parameters The accurate evaluation of cohesive parameters of the trapezoidal law is a fundamental task in order to obtain good strength predictions. The properties measured from tests in bulk specimens are not representative because in bonded joints the adhesive is a thin layer and behave differently than in bulk. The solution is to obtain the cohesive properties using specimens where the thickness of the adhesive is similar to the one used in bonded joints. This can be achieved with the Double Cantilever Beam (DCB) and End Notched Flexure (ENF) fracture characterization tests for pure mode I and mode II loading, respectively. The use of these tests to measure the cohesive parameters is described below. 6.3.1 Fracture Energies In the following, the application of the DCB and ENF tests to fracture characterization of adhesives is described. A new data reduction scheme avoiding the inevitable inaccuracies present in the measurement of the crack length during propagation is highlighted. 166 M.F.S.F. de Moura 6.3.1.1 The DCB Test The DCB is a standardized test (ASTM D3433-99) to measure material fracture properties under pure mode I loading. When applied to bonded joints it consists in two beams bonded with the required adhesive thickness with a predefined initial crack length. The load is applied in order to promote pure mode I loading at the crack front (Fig. 6.5). There are two classical data reduction schemes frequently used to obtain the fracture energy in mode I (JIc ). The Compliance Calibration Method (CCM) is based on the Irwin-Kies equation [23] P2 dC (6.24) JIc = 2b da being C the compliance (δ /P). Using this method, the values of load, applied displacement and crack length (P, δ and a) are registered in order to calculate the fracture energy during load history. Alternatively, the Corrected Beam Theory (CBT) is also commonly used [10]. In this case, it is assumed that JIc can be obtained from JIc = 3 Pδ 2b(a + |Δ|) (6.25) where Δ is a correction for crack tip rotation and deflection. Δ is determined from a linear regression analysis of (C)1/3 versus a data. It should be emphasized that both methods depend on crack length measurements during its propagation. This is not easy to perform and remarkable errors can occur, affecting the measured JIc . In order to overcome the referred difficulties, a new data reduction scheme based on crack equivalent concept is proposed. The method does not require crack length measurements and accounts for the energy dissipated at the Fracture Process Zone (FPZ). The FPZ develops ahead of the crack tip in consequence of the nucleation of multiple micro-cracks through the adhesive thickness and plastification. In fact, a quite extensive FPZ exists when ductile adhesives are used. This non negligible FPZ affects the measured toughness as a non negligible amount of energy is dissipated on it. Consequently, its influence should be taken into account, which does not occur when the real crack length is used in a classical data reduction scheme (Fig. 6.6). The proposed method is based on beam theory and depends decisively on the beam compliance. Consequently, it is named Compliance Based Beam Method P b y x h δ P a Fig. 6.5 Schematic representation of the DCB test 6 Progressive Damage Modelling 167 Fig. 6.6 Schematic representation of the FPZ and crack equivalent (ae ) concept (CBBM). Following strength of materials analysis, the strain energy of the specimen due to bending and including shear effects is [14] a 2 a h/2 Mf τ2 dx + U =2 b dy dx (6.26) 0 2E1 I 0 −h/2 2G13 where Mf is the bending moment, I the second moment of area of the specimen, b the specimen width, E1 and G13 the longitudinal and shear elastic properties of a general orthotropic material and 3 P 4 y2 τ= (6.27) 1− 2 2 bh h being y the coordinate along specimen thickness (Fig. 6.5). From Castigliano theorem the displacement δ , can be written as δ= 8 Pa3 ∂U 12 Pa = + 3 ∂P E1 bh 5bhG13 (6.28) This equation constitutes an approach based on beam theory and does not account for all effects influencing the specimen behaviour. For example, it is known that stress concentrations arise around the crack tip, which is not taken into consideration by this approach. To overcome the referred discrepancies, an equivalent flexural modulus can be obtained from Eq. (6.28) and considering two initial conditions taken from the experimental tests: the initial crack length a0 and initial compliance C0 . Moreover, this approach takes into account the variation of the material properties between different specimens at it is based on the experimentally measured C0 . Thus, Ef can be obtained from Eq. (6.28) 12(a0 + |Δ|) −1 8(a0 + |Δ|)3 Ef = C0 − 5bhG13 bh3 (6.29) where Δ is the root rotation correction for the initial crack length (Fig. 6.6). In the beam theory it is assumed that each arm of the DCB specimen is an encastred beam whose length is equal to the crack length a. This parameter (Δ) can be achieved by a linear regression of C1/3 = f(a0 ). The determination of Δ can be performed by slightly loading the specimen with three different initial crack lengths (Fig. 6.7) in order to define the C1/3 = f(a0 ) linear regression (Fig. 6.8). 168 M.F.S.F. de Moura Fig. 6.7 Schematic representation of the compliance calibration as a function of the crack length in the DCB test δ1, P1 δ2, P2 δ3, P3 a03 a02 a01 Alternatively, Wang and Williams [37] proposed another form of determining the root rotation effects by altering the crack length using the parameter ΔI ΔI = h √ 2 Γ Ef Ef E3 3−2 and Γ = 1.18 11G13 1+Γ G13 (6.30) which can be used instead of Δ in Eq. (6.29). Owing to the difficulties inherent to crack monitoring during propagation and to energy dissipation in the FPZ, an equivalent crack length ae (Fig. 6.6) is defined and used instead of the measured crack length. The equivalent crack length is obtained from Eq. (6.28) as a function of the specimen compliance registered during the test and considering ae = a + |Δ| + ΔaFPZ instead of a. The solution of this equation can be found using the mathematical software Matlab and is presented in Appendix. The fracture energy in mode I can be obtained using Eq. (6.24) 6P2 2a2e 1 + (6.31) JIc = 2 b h h2 Ef 5G13 The presented methodology allows obtaining the fracture energy JIc only as function of the P–δ data. For this reason it is designated by Compliance Based Beam Method C1/3 (mm/N)1/3 Fig. 6.8 Schematic representation of the crack length correction due to root rotation in the DCB test Δ a01 a02 a03 a (mm) 6 Progressive Damage Modelling 169 (CBBM). Using this method it is not necessary to measure the crack length during propagation because the calculated equivalent crack length is used instead of the real one. Another advantage is related to the fact that ae includes the effect of the FPZ, which is not taken into account when the real crack length is considered. Moreover, the specimen modulus (Ef ) is not a measured property but rather a computed one (Eq. (6.29)) as a function of the initial compliance, thus accounting for the material variability between different specimens. The only material property required in this approach is the shear modulus G13 . However, from Eq. (6.31) it is straightforwardly concluded that the term containing G13 is negligible relatively to the one of Ef . This means that a typical value of G13 can be used and that it is not necessary to measure it for each specimen. 6.3.1.2 The ENF Test Up to now there is no standardized test to measure the fracture energy of bonded joints under pure mode II loading. The most used are based on interlaminar fracture characterization tests of composite materials. In this context the End Notched Flexure (ENF), End Loaded Split (ELS) and Four-Point End Notched Flexure (4ENF) tests should be emphasized (Fig. 6.9). Fig. 6.9 Schematic representation of the ENF, ELS and 4ENF tests 170 M.F.S.F. de Moura The ELS test presents some difficulties in the measurement of fracture energy related to large displacements effects and to sensibility of the clamping pressure conditions [14]. On the other hand, the 4ENF test requires a quite complex setup and some friction effects on the measured energy were detected [34]. The ENF test is the most simple to execute and consequently is frequently used for materials fracture characterization under pure mode II. There are two main data reduction methods applied to ENF test in order to measure JIIc of bonded joints (Fig. 6.10). The CCM is also based on Eq. (6.24). The compliance calibration can be made by two different ways. One of them consists in performing bending tests using specimens with different initial cracks. This can be achieved using only one specimen by altering its position in the supports. Alternatively, the calibration of C can be reached by measuring the crack length during propagation. A cubic polynomial fitting should be carried out considering C = Co + ma3 (6.32) 3ma2 P2 2b (6.33) which, using Eq. (6.24), leads to JIIc = The Corrected Beam Theory proposed by Wang and Williams [37], can also be applied. The equation is 9P2 (a + |ΔII |)2 JIIc = (6.34) 16b2 E1 h3 where ΔII is a crack length correction to account for shear. The authors showed that ΔII = 0.42 ΔI , ΔI being the correction for mode I obtained for the DCB test (see Eq. (6.30)). It should be emphasized that experimental difficulties in measuring the crack length are higher in mode II fracture characterization tests. In fact, due to applied loading the crack tends to close during propagation which hinders the clear visualization of its tip. On the other hand, the quite large effect of the FPZ size [8] is not accounted for when the real crack length is considered [11]. To overcome these difficulties an equivalent crack procedure, similar to the one used for DCB tests, can be followed to obtain the fracture energy under pure mode II loading using the ENF specimen. As in the DCB test, the method is based on beam compliance and beam theory and, consequently it is also named as CBBM. P P/4 ta b h a0 Fig. 6.10 Schematic representation of the ENF test P/4 P/2 L 2L 6 Progressive Damage Modelling 171 Employing the beam theory and Castigliano theorem, the equation of compliance can be obtained 3L 3a3 + 2L3 (6.35) + C= 3 8E1 bh 10G13 bh The equivalent flexural modulus is obtained using the initial compliance C0 and initial crack length a0 −1 3a30 + 2L3 3L Ef = C0 − 8 bh3 10G13 bh (6.36) This procedure takes into account the variation of the material properties between different specimens and for several effects that are not included in the beam theory, e.g., stress concentration at the crack tip and contact between the two arms at the precrack region. In fact, these effects influence the P–δ curve even in the elastic regime, and their effects are included when the initial compliance is used to determine the Ef . Using Ef (Eq. (6.36)) instead of E1 in Eq. (6.35), an equivalent crack accounting for the FPZ effects is achieved as a function of the beam compliance (C) which varies during propagation Cc 3 2 ae = a + ΔaFPZ = a + C0c 0 3 1/3 Cc − 1 L3 C0c (6.37) where Cc and C0c are given by Cc = C − 3L ; 10G13 bh C0c = C0 − 3L 10G13 bh (6.38) JIIc can now be obtained using the Irwin-Kies relation (Eq. (6.24)) JIIc = 9 P2 a2e 16b2 Ef h3 (6.39) where ae and Ef are given by Eqs. (6.37) and (6.36), respectively. In summary, this data reduction scheme applied to fracture characterization in mode I and in mode II presents several advantages. Using this methodology, crack measurements are unnecessary. Experimentally, it is only necessary to register the values of applied load and displacement. Therefore, the method is designated as Compliance Based Beam Method (CBBM). Using this procedure the FPZ effects, that are pronounced in mode II tests, are included in the fracture energy measurement. Moreover, the flexural modulus is calculated from the initial compliance and crack length, thus avoiding the influence of specimen variability on the results. The unique material property needed in this approach is G13 . However, its effect on the measured fracture energy was found to be negligible [14], which means that a typical value can be used rendering unnecessary to measure it. 172 M.F.S.F. de Moura 6.3.2 Cohesive Critical Displacements P (N) In order to define completely the cohesive damage model it is also necessary to determine the critical displacements corresponding to the inflexion points (δ1,i , δ2,i ). The first one is intrinsically associated to adhesive local strength (σu,i ) and the second one defines the extent of the plateau region (Fig. 6.4). As already referred, these properties do not correspond to that of the adhesive as a bulk material. The definition of the cohesive parameters is performed using an inverse method applied to fracture tests in mode I (DCB) and mode II (ENF). The method consists in three main steps. Initially, the experimental R-curve is obtained from the P–δ curve, applying the CBBM (Fig. 6.11). The plateau region of the R-curve corresponds to the fracture energy of the adhesive. The second step consists in a numerical simulation of the test, using the cohesive damage model to simulate damage initiation and growth. In this simulation the measured fracture energy is an inputted parameter in the numerical approach. The other two cohesive parameters (δ1,i , δ2,i ) can be found by a trial and error procedure. An iterative process should be performed until a good accuracy between the numerical and experimental P–δ curves is obtained, thus defining the cohesive parameters (δ1,i , δ2,i ). This procedure depends on the number of parameters to be fixed. In fact, if the two referred parameters should be accurately determined, a genetic algorithm including an optimisation strategy should be used [16]. However, in some cases only one parameter (δ1,i ) is necessary. This happens when brittle adhesives are used. In 140 120 100 80 60 40 20 0 0 1 2 δ (mm) 3 4 J II (N/mm) 0.8 0.6 0.4 0.2 0 35 37 39 41 a eq (mm) 43 45 Fig. 6.11 A typical P–δ curve of the ENF test (above) and the respective R-curve obtained using the CBBM (below) 6 Progressive Damage Modelling 173 these cases, the trapezoidal law converts into a triangular one. Another case occurs when the model is not sensible to the value of δ2,i . In this situation, this parameter can be arbitrarily defined imposing, for the third part of the softening law, a symmetrical slope relatively to the initial linear part. de Moura et al. [15], performed a parametrical study on single lap joints and verified that even for ductile adhesives, there is a quite large range of values of δ2,i that do not alter the predicted joint strength. The authors concluded that δ2,i can be defined as the point that leads to the third part of the curve being symmetrical relatively to the initial linear part. This choice implies that δ2,i falls in the values range leading to joint maximum strength. When only one cohesive parameter has to be determined, the iterative process can be easily performed. In fact, two or three attempts are usually enough to obtain an acceptable agreement between the numerical and experimental P–δ curves, thus leading to the definition of δ1,i . 6.3.3 Fracture Characterization of Bonded Joints The method described above was applied to fracture characterization of carbonepoxy bonded joints under pure mode I (DCB test) and pure mode II (ENF test). The adherends were unidirectional 0◦ lay-ups with sixteen layers of carbon/epoxy prepreg (TEXIPREG HS 160 RM) with 0.15 mm of ply thickness, whose mechanical properties are presented in Table 6.1 [3]. Curing was achieved in a press during one hour at 130◦ C and 4 bar pressure. The adhesive Araldite 2015 from Huntsmann (Basel, Switzerland) was used (E = 1850 MPa, ν = 0.3) [3]. The bonding process included roughening the surfaces to be bonded with sandpaper and cleaning with acetone to increase the adhesion and avoid adhesive failure, followed by assembly and holding with contact pressure and curing at room temperature. 6.3.3.1 DCB Tests The nominal dimensions of the DCB specimen were 2h = 5 mm, L = 120 mm, b = 15 mm, a0 = 45 mm and adhesive thickness equal to 0.2 mm. The specimens were tested under a tensile loading using an INSTRON testing machine at room temperature under displacement control. The loading rate was kept constant at 2 mm/min. During the test the P–δ curves were registered in order to obtain the respective R-curves using the proposed CBBM. The plateau region of the R-curve defines the Table 6.1 Carbon-epoxy elastic properties [3] E1 = 1.09E + 05 MPa E2 = 8819 MPa E3 = 8819 MPa ν12 = 0.342 ν13 = 0.342 ν23 = 0.380 G12 = 4315 MPa G13 = 4315 MPa G23 = 3200 MPa 174 M.F.S.F. de Moura 80 70 60 P [N] 50 40 Experimental 30 Numerical 20 10 0 0 1 2 3 4 δ [mm] 5 6 7 Fig. 6.12 Comparison between numerical and experimental P–δ curves JIc value which is an inputted parameter of the cohesive damage model. An iterative procedure is followed until a good agreement between numerical and experimental P–δ curves are achieved (Fig. 6.12), thus determining the remaining cohesive properties of the trapezoidal softening law. After some attempts, it was verified that local strength σu,I (or δ1,I ) does not have too much influence and only δ2,I was varied to fit the P–δ curves. σu,I was set equal to 23 MPa. Afterwards, the numerical and experimental R-curves are also compared (Fig. 6.13) in order to check the validity of the proposed model. Generally, good agreement was observed for all tests (Table 6.2) for the inputted and numerically obtained JIc – plateau values corresponding to stable crack propagation. The values of the remaining cohesive parameter are also listed in Table 6.2. 6.3.3.2 ENF Tests JI [N/mm] The nominal dimensions of the ENF specimen are 2h = 5 mm, L = 100 mm, b = 15 mm, a0 = 70 mm and adhesive thickness equal to 0.2 mm. The numerical- 0.55 0.5 0.45 0.4 0.35 0.3 0.25 0.2 0.15 0.1 Experimental Numerical 60 65 70 aeq [mm] 75 80 Fig. 6.13 Comparison between numerical and experimental R-curves 6 Progressive Damage Modelling 175 Table 6.2 Comparison between numerical and experimental JIc and the obtained δ2,I 1 2 3 4 5 6 Average St. Dev. Experimental JIc (N/mm) Numerical JIc (N/mm) δ2,I (mm) 0.484 0.444 0.420 0.333 0.406 0.468 0.425 0.054 0.482 0.441 0.415 0.331 0.404 0.466 0.422 0.055 0.021 0.019 0.018 0.014 0.018 0.020 0.018 0.003 experimental fitting procedures of P–δ curves were more complex in the ENF than in the DCB test. In fact, some sensibility to the two inflexion points (δ1,II , δ2,II ) was observed, which required a larger number of iterations in order to obtain a good agreement between the P–δ curves (Fig. 6.14). The CBBM also provides good agreement between the inputted and measured JIIc (plateau values of the R-curves in Fig. 6.15), which demonstrates the adequacy of the method in order to measure the fracture energy in pure mode II of bonded joints. The values of the cohesive parameters obtained by the inverse method are listed in Table 6.3 for five experimental tests. In summary, it can be affirmed that the numerical model shows that the values of fracture energies obtained by applying the CBBM are in excellent agreement with the ones inputted in the cohesive damage model. This proves that the referred data reduction scheme is able to reproduce the real values of fracture energy of the specimens. Is should be noted that generally the predicted values are a little bit inferior to the inputted ones. This can be explained by the presence of spurious modes at the specimens’ edges. For example, de Moura et al. [13] demonstrated that 1.14% of the total energy available at the specimen edges comes from mode III loading. 800 P [N] 600 Experimental Numerical 400 200 0 0 2 4 6 8 10 12 14 δ [mm] Fig. 6.14 Comparison between numerical and experimental P–δ curves 176 M.F.S.F. de Moura 6 JIIc [N/mm] 5 4 3 Experimental 2 Numerical 1 0 70 75 80 ae [mm] 85 90 Fig. 6.15 Comparison between numerical and experimental R-curves Table 6.3 Comparison between numerical and experimental JIIc and the calculated cohesive parameters (σu,II and δ2,II ) 1 2 3 4 5 Average St. Dev. Experimental JIIc Numerical JIIc (N/mm) (N/mm) σu,II (MPa) δ2,II (mm) 4.88 5.11 4.72 4.36 4.35 4.68 0.33 25.3 23.5 25.6 25.0 20.0 23.9 2.31 0.151 0.169 0.146 0.056 0.153 0.135 0.045 4.85 4.98 4.72 4.24 4.35 4.63 0.32 It should also be emphasized that the average values of cohesive parameters obtained by this inverse method allow defining the constitutive cohesive laws in pure mode I and in pure mode II. These laws can then be used in progressive damage simulations of bonded joints with this type of adherends and adhesive in order to predict their mechanical behaviour and strength. 6.3.4 Application to Bonded Joints In order to verify the performance of the presented cohesive damage model on joint strength prediction, single lap bonded joints were tested experimentally. The adherends had sixteen layers of unidirectional carbon-epoxy (Table 6.1) giving a nominal thickness of 2.5 mm. The remaining nominal dimensions of the joints were 240 mm length, 15 mm width and adhesive thickness of 0.2 mm. Eight different overlap lengths (ranging between 10 and 80 mm) were considered. Five specimens of each case were tested and the maximum load was registered and used to define the joint strength. Cohesive failures were observed in all cases. 6 Progressive Damage Modelling 177 Maximum load (kN) 20 15 10 Experimental 5 Numerical 0 0 20 40 Overlap length (mm) 60 80 Fig. 6.16 Comparison between numerical and experimental single lap joint strengths as a function of overlap length Numerical simulations were also performed considering the average real dimensions of each group of five specimens for each tested case. The average cohesive properties measured under pure mode I and under pure mode II in the previous sections were used as inputted data. The maximum loads obtained from these numerical simulations are compared with the experimental ones in Fig. 6.16. Generally, good agreement was obtained for all overlap lengths. 6.4 Continuum Damage Models The cohesive models require the knowledge of the critical zones where damage is prone to occur in order to place the cohesive elements in these critical regions. Continuum damage models can constitute an appealing alternative when damage propagation onset and path are not known a priori. In these models the material properties degradation occurs inside of the solid elements which avoids the use of special interface elements. The application of continuum damage models in the context of bonded joints can be considered interesting when adhesive thickness should be considered. In fact, it is known that adhesive thickness can influence the mechanical properties of the joint [27]. Another example is related to crack propagation occurring near to one interface due to stress concentration [17]. This non-symmetric propagation can induce local mixed-mode loading which is not captured by cohesive damage models where adhesive thickness is neglected. In these cases the adhesive should be simulated by solid elements with the corresponding properties. The progressive damage is simulated by including the damage onset and propagation criteria in the formulation of solid elements. Usually this is performed by means of a user subroutine in standard software where the material properties are degraded according to the chosen criteria. An approach similar to the one used in the cohesive damage model described in Sect. 6.3 but considering a triangular softening law (see Fig. 6.17), instead of a trapezoidal one, is proposed by several authors [5, 12, 32]. In this case there is a 178 M.F.S.F. de Moura σm σum δ1m δum δm Fig. 6.17 Softening stresses/displacements relationship for the continuum damage model softening relationship between stresses and strains instead of between stresses and relative displacements considered in the cohesive model. Consequently, a characteristic length lc must be introduced to transform the relative displacement into an equivalent strain 1 Jic = σu,i εu,i lc,i (6.40) 2 This parameter is equal to the length of influence of a Gauss point in the given direction and physically can be regarded as the dimension at which the material acts homogeneously. It can be obtained from the coordinates of Gauss points available during simulation. The stress–strain relation can be written considering an equation similar to Eq. (6.10) σ = (I − D)Cε (6.41) being C the stiffness matrix of the undamaged material in the orthotropic directions. Assuming that damage occurs in mixed-mode (I+II) the model described previously can be adopted. For the triangular softening model (Fig. 6.17) the damage parameter is given by d= δum (δm − δ1m ) δm (δum − δ1m ) (6.42) The material properties at a given Gauss point are smoothly degraded according to the assumed criterion, thus simulating the energy releasing at the FPZ. This leads to load redistribution for the neighbouring points, simulating a gradual propagation process and avoiding the stress singularity effects and minimizing the mesh sensitivity effects. As in the cohesive damage model, damage onset and growth are simulated by a quadratic stress criterion and a linear energetic one, respectively, allowing the definition of the critical displacements to be used in Eq. (6.42). More details of the referred model are presented in [15]. 6 Progressive Damage Modelling 179 6.5 Conclusions Adhesive bonded joints are nowadays widely used in structural applications. Consequently, the development of properly design methods is fundamental to increase the confidence of designers in using adhesive bonded joints. Mixed-mode cohesive damage models join the positive arguments of stress based and fracture mechanics criteria overcoming their inherent difficulties. They are presently prominent numerical tools in order to simulate the behaviour of these joints. In this work a cohesive mixed-mode damage model adequate to the simulation of ductile adhesives is presented. The trapezoidal constitutive softening law simulates the adhesive behaviour including its thickness and plastic behaviour. An important issue of the model is related to the determination of the cohesive properties. In fact, it is known that adhesive bulk properties are not exactly the same as the ones of a thin adhesive layer. Therefore, they were determined considering fracture tests (DCB and ENF) where the testing conditions are similar to the ones existing in bonded joints. An inverse method was used to define the cohesive parameters. An iterative procedure was followed in order to fit the numerical and experimental P–δ curves, thus defining the constitutive cohesive laws in the two modes. A new data reduction scheme based on crack equivalent concept was also proposed to measure the fracture energies in the two fracture characterization tests. The method does not require crack monitoring during its propagation and account for the energy dissipated in the fracture process zone which is not negligible, mainly when ductile adhesives are used. The method was validated by experimental tests and numerical simulations. Continuum damage models can be a valuable alternative to cohesive damage models especially when adhesive thickness plays an important role on the behaviour of the joint. In this case the adhesive is simulated by solid elements instead of interface ones. The advantage of this approach is related to damage onset and crack propagation path which are better simulated namely when non-symmetric paths can influence the results. The softening laws are applied to the solid elements degrading the material properties according to the predefined criteria. It should also be noted that continuum damage models are more complicated and can lead to numerical problems related to convergence difficulties. Further developments are necessary in this context. It should be emphasized that the two models can also be used in a bonded joint simulation. In fact, when failure of adherends, for example in composites, is also an issue to be considered, continuum and cohesive damage models can be used to simulate the eventual failure of adherends and adhesive, respectively. The future trends point to the development of a numerical tool incorporating the two kinds of models. The two methods can coexist, although till now there are some unsolved numerical problems. In fact, both models can be implemented via user subroutines in commercial standard software. 180 M.F.S.F. de Moura Acknowledgements The author thanks the Portuguese Foundation for Science and Technology for supporting part of the work here presented, through the research project POCI/EME/56567/ 2004. The author also thanks Dr João Paulo Moreira Gonçalves, Dr José Augusto Gonçalves Chousal and Mr Raul Duarte Salgueiral Gomes Campilho (PhD student) for their valorous collaboration, advices and discussion about the matters included in this chapter. Appendix Equation (6.28) can be expressed as, α a3e + β ae + γ = 0 (6.43) where the coefficients α , β and γ are, respectively α= 8 ; bh3 Ef β= 12 ; 5 bhG13 γ = −C (6.44) Using the Matlab software and only keeping the real solution we have, ae = being 1 2β A− 6α A 13 4β 3 + 27γ 2 α α2 1 − 108γ + 12 3 α (6.45) A= (6.46) References 1. Andersson T, Stigh U (2004), The stress-elongation relation for an adhesive layer loaded in peel using equilibrium of energetic forces, Int J Sol Struct, 41:413–434 2. Blackman BRK, Hadavinia H, Kinloch AJ, Williams JG (2003), The use of a cohesive zone model to study the fracture of fibre composites and adhesively-bonded joints, Int J Fract, 119:25–46 3. 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Irwin GR (1957), Analysis of stress and strains near the end of a crack traversing a plate, ASME J Appl Mech, 24:361–364 22. John SJ, Kinloch AJ, Matthews FL (1991), Measuring and predicting the durability of bonded carbon fibre/epoxy composite joints, Composites, 22:121–127 23. Kanninen MF, Popelar CH (1985), Advanced fracture mechanics, Oxford University Press, Oxford 24. Kinloch AJ (1987), Adhesion and adhesives: science and technology, Chapman & Hall, London 25. Krueger R (2002), The virtual crack closure technique: history, approach and applications, NASA/CR-2002-211628, Icase Report No. 2002-10 26. Lammerant L, Verpoest I (1996), Modelling of the interaction between matrix cracks and delaminations during impact of composite plates, Comp Sci Technol, 56:1171–1178 27. Lee DB, Ikeda T, Miyazaki M, Choi NS, (2004), Effect of bond thickness on the fracture toughness of adhesive joints, J Eng Mat Technol, 126:14–18 28. Lee SJ, Lee DG (1992), Development of a failure model for the adhesively bonded tubular single lap joint. J Adhes, 40:1 29. Leffler K, Alfredsson KS, Stigh U (2007), Shear behaviour of adhesive layers, Int J Sol Struct, 44:530–545 30. Mi Y, Crisfield MA, Davies GAO, Hellweg H-B (1998), Progressive delamination using interface elements, J Comp Mat, 32:1246–1272 31. Petrossian Z, Wisnom MR (1998), Prediction of delamination initiation and growth from discontinuous plies using interface elements, Composites Part A, 29A:503–515 182 M.F.S.F. de Moura 32. Pinho ST, Iannuci L, Robinson P (2006), Physically based failure models and criteria for laminated fibre-reinforced composites with emphasis on fibre kinking. Pat II: FE implementation, Composites Part A, 37:766–777 33. Ripling EJ, Mostovoy S, Patrick RL (1963), Application of fracture mechanics to adhesive joints, in: Adhesion, ASTM STP 360, ASTM, Philadelphia, PA 34. Schuecker C, Davidson BD (2000), Evaluation of the accuracy of the four-point bend endnotched flexure test for mode II delamination toughness determination, Compos Sci Technol, 60: 2137–2146 35. Thouless MD, Waas AM, Schroeder JA, Zavattieri PD (2006), Mixed-mode cohesive-zone models for fracture of an adhesively bonded polymer-matrix composite, Eng Fract Mech, 73:64–78 36. Towse A, Davies RGH, Clarke A, Wisnom MR, Adams RD, Potter KD (1997), The design and analysis of high load intensity adhesively bonded double lap joints. Proceedings of the Fourth International Conference on Deformation and Fracture of composites, Manchester, UK, 479–488 37. Wang Y, Williams JG (1992), Corrections for mode II fracture toughness specimens of composite materials, Comp Sci Technol, 43:251–256 38. Whitney JM, Nuismer RJ (1974), Stress fracture criteria for laminated composites containing stress concentrations, J Comp Mat, 8:253–265 39. Yang QD, Thouless MD, Ward SM (1999), Numerical simulations of adhesively-bonded beams failing with extensive plastic deformation, J Mech Phy Sol, 47:1337–1353 40. Yang QD, Thouless MD (2001), Mixed-mode fracture analyses of plastically deforming adhesive joints, Int J Fract, 110:175–187 41. Yang QD, Thouless MD, Ward SM (2001), Elastic–plastic mode-II fracture of adhesive joints, Int J Sol Struct, 38:3251–3262 42. Zhao X (1991), Stress and failure analysis of adhesively bonded lap joints, PhD thesis, Department of Mechanical Engineering, University of Bristol, UK Chapter 7 Modelling Fatigue in Adhesively Bonded Joints Ian A. Ashcroft and Andrew D. Crocombe Abstract Fatigue is widely recognised as one of the most common causes of mechanical failure and hence the issue of fatigue in bonded joints must be addressed if adhesives are to find wider usage in structural applications. Fatigue failure is difficult to predict accurately and fatigue in bonded joints is complicated by the multi-component nature of bonded joints and by the complex stress distributions and material behaviour. Various methods of modelling the fatigue behaviour of bonded joints have been proposed, varying in complexity, applicability and degree of empiricism. The aims of the models are either to predict the number of load cycles until a certain event occurs (such as macro-crack initiation or complete failure) or to predict the rate of change of crack length (or some other measure of damage) as a function of cycles. In this chapter the main approaches to modelling fatigue in adhesive joints are outlined and examples given of the application of each approach. It is seen that there are many practical modelling routes, the choice being dependent on what is required and the availability of resources, data and expertise. However, it cannot be said at present that there is a generally applicable method of modelling fatigue in bonded joints that is robust, reliable and mechanistically accurate. However, the further development of advanced computational methods, such as finite element analyses incorporating progressive damage, and increased understanding of the mechanisms of fatigue in bonded joints will continue to provide drivers for improved modelling methods. Ian A. Ashcroft Wolfson School of Mechanical and Manufacturing Engineering, Loughborough University, Loughborough, Leicestershire, LE11 3TU, UK, e-mail: i.a.ashcroft@lboro.ac.uk Andrew D. Crocombe Division of Mechanical, Medical and Aerospace Engineering, School of Engineering, University of Surrey, Guildford, GU2 5XH, UK, e-mail: a.crocombe@surrey.ac.uk L.F.M. da Silva, A. Öchsner (eds.), Modeling of Adhesively Bonded Joints, c Springer-Verlag Berlin Heidelberg 2008 183 184 Ian A. Ashcroft, Andrew D. Crocombe 7.1 Introduction Fatigue, in an engineering sense, is the failure of a structure under a repetitive or cyclic loading regime in which the loads involved are considerably lower than those involved in instantaneous, or quasi-static, failure. Fatigue is a significant subject for study for many reasons. Firstly, fatigue loading is seen in nearly all major engineering structures, e.g. aircraft, ships, cars, buildings, bridges, as well as in many nonengineering applications, such as sports equipment and even human parts, such as knees. Secondly, it can result in sudden catastrophic failure after years of apparently safe service. Long periods can be spent in the initiation phase of fatigue damage, in which there may be no outward signs of damage, failure can then quickly accelerate in the final stages. Fatigue damage can be initiated or accelerated by many factors such as accidental impact, over-loading, corrosion, abrasion etc. Thirdly, fatigue failure is notoriously difficult to predict accurately. A problem compounded by the fact that the in-service loading and environment are seldom known to a great degree of accuracy. Hence, it is very difficult to design against fatigue failure without resorting to large safety factors, and hence incurring structural inefficiencies. Monitoring fatigue damage can also be difficult, particularly if initiation is in an inaccessible location or if the critical crack size before rapid fracture is very small. It can be summarised, therefore, that predicting fatigue failure in a structure is both extremely important and rather difficult. The advantages of adhesive bonding compared to other joining techniques are now well recognised and two of the frequently quoted benefits are that stress concentrations are more uniformly distributed than in riveted or bolted joints and that the bonding process does not explicitly weaken the adherends (although there are likely to be stress concentrations in the adherend in the joint area). It might be expected, therefore, that adhesively bonded joints perform well in fatigue, and indeed this is often the case. However, a number of potential problems for adhesive joints subjected to fatigue should also be recognised. Adhesives are, like most materials, susceptible to fatigue and hence if fatigue loading is expected in an application then the fatigue resistance of the adhesive should be investigated. It is well known that adhesives and the interfacial region between adhesive and adherend are sensitive to the environment and this will affect the fatigue resistance of the joint. Adhesives are also susceptible to creep under certain conditions and combined with fatigue this can lead to accelerated failure (Hart-Smith 1981; Harris and Fay 1992; Ashcroft et al. 2001). It should also be remembered that failure in a bonded joint can occur in the adhesive, in the adherend or in the interfacial region between the two and that the relative fatigue resistance of the various components is dependent on many factors, such as geometry, environment and loading, and may vary as damage progresses. For example, in a bonded composite joint subjected to fatigue loads and moisture we have a complex system in which we may have multiple and changing initiation and propagation sites and mechanisms as the dynamic effects of progressive fatigue damage and moisture absorption and desorption occur (Ashcroft et al. 1997, 1999, 2000, 2001a; Abdel Wahab et al. 2001, 2001a). It is not surprising, therefore that many of the initial studies of fatigue in bonded joints were either of a 7 Modelling Fatigue in Adhesively Bonded Joints 185 highly empirical nature or involved simplified systems and it is only in recent years that the fatigue behaviour of bonded joints under loading and environmental conditions more representative of those seen in-service have been explored (Al-Ghamdi et al. 2003; Erpolat et al. 2004; Ashcroft et al. 2005; Nolting et al. 2008). Before discussing the methods of modelling fatigue in bonded joints, it is useful to discuss the reasons why one may wish to do so. Perhaps the obvious reason is to support the design of bonded structures, to ensure that fatigue failure is not likely to occur in service and to aid in the design of efficient fatigue resistant joints; resulting in safer, cheaper and higher performance structures. There is no doubt that modelling can indeed help in these objectives, however, it should also be recognised that the current state of confidence in such modelling means that in most cases the modelling must accompany a complimentary testing programme. Another reason for modelling is to help to understand the mechanisms involved in fatigue failure. This can be achieved through comparing experimental results from carefully designed tests with the predicted results from progressive damage models. Although the micro-mechanisms of damage are rarely an explicit part of the models, they can be used to inform the nature of continuum damage laws incorporated into the model and hence comparison of the experimental and modelling results enables insight into the damage mechanisms and the development of more physically accurate models. A third reason for modelling is to support in-service monitoring and re-lifeing of structures. In this case it is necessary to correlate externally (or internally) measurable parameters with their consequences, in terms of progressive damage of the structure. For example, in recent work (Zhang and Shang 1995; Crocombe et al. 2002, 2005; Graner-Solana et al. 2007; Shenoy et al. 2008) it has been shown that simple back-face strain measurement can be used to monitor the various stages of fatigue damage in a bonded single lap joint and hence continuous monitoring of such a signal can be used to monitor that the joint is performing as predicted and to initiate timely intervention should the measurements indicate a potentially significant change in the structure. It should be recognised that the three activities involving the modelling of bonded joints indicated above are intrinsically linked. Now we have discussed why we should model the fatigue of bonded joints the purpose of the rest of this chapter is to discuss the ways in which this may be done. However, the scope of the chapter should be stated first. Fatigue in bonded joints can be modelled at many different levels and using many fundamentally differing approaches, ranging from modelling events at a molecular level to the analysis of complete structures. In this chapter we will mainly be looking at failure from the view of the mechanical engineer, that is generally in the 10−4 to 100 m scale where fracture mechanics, continuum mechanics and damage mechanics are applicable. The main goals in the modelling of fatigue behaviour are to (i) predict the time (or no. of cycles) for a certain event to occur (such as macro crack formation, critical extent of damage or complete failure) or (ii) to predict the rate of change of a fatigue related parameter such as crack length or ‘damage’. The various methods of doing this are presented in Sect. 7.3 of this chapter and the approach used is to introduce and describe each of the main methods that have been used to date, together with 186 Ian A. Ashcroft, Andrew D. Crocombe one or two examples. In this way the aim is not to attempt to summarise all the work that has been done in this field but rather to give the potential modeller an introduction to the various methods which could be used. However, before the various methods are described it is useful to discuss some of the overarching issues pertinent to modelling fatigue. 7.2 General Considerations 7.2.1 Fatigue Loading Stress It is worth considering in a little more detail what exactly is meant by a fatigue load. The main feature is that the load varies with time and it is useful to characterise the load spectrum in terms of peaks and troughs in the varying load, with a cycle being defined as the time between adjacent peaks (or troughs) and the frequency being the number of cycles in a unit time. The fatigue spectrum can be characterised in terms of the applied load or displacement for simple samples but in more complex structures it is more useful to think in terms of the cyclic stress (or other parameter, such as strain energy release rate) at a point of interest. It is common in laboratory experiments to represent fatigue as a constant amplitude, sinusoidal waveform, as shown in Fig. 7.1. Key fatigue parameters are defined in Table 7.1 (noting that similar parameters can be defined in terms of load, displacement, stress intensity factor etc. rather than stress). Only frequency plus two of the other parameters above in Table 7.1 are needed to characterise a constant amplitude spectrum. Important considerations for adhesively bonded joints are the mean stress and the frequency. As adhesives tend to be viscoelastic/viscoplastic in nature, then a tensile mean load can lead to progressive Sa Smax S Smn Smin Time T Fig. 7.1 Constant amplitude, constant frequency sinusoidal waveform 7 Modelling Fatigue in Adhesively Bonded Joints 187 Table 7.1 Parameters used to describe fatigue spectra Maximum stress Smax Minimum stress Smin Stress amplitude Sa = Period Smax − Smin 2 Smax + Smin Smn = 2 Δ S = Smax − Smin Smin R= Smax T (sec) Frequency f= Mean stress Stress range Stress ratio 1 (Hz) T 1.2 1 1 0.8 0.8 stress stress 1.2 0.6 0.6 0.4 0.4 0.2 0.2 0 0 0 1 2 3 4 5 0 1 2 time (a) 4 5 (b) 1.2 1.2 1 1 0.8 0.8 stress stress 3 time 0.6 0.6 0.4 0.4 0.2 0.2 0 0 0 1 2 3 time (c) 4 5 0 1 2 3 4 5 time (d) Fig. 7.2 Alternative waveforms: (a) square, (b) trapezium, (c) saw-tooth, (d) spike creep of the joint over time. This is exacerbated at low frequencies, where time under load may become as significant as number of cycles in defining failure. However, at high frequencies, hysteretic heating may also lead to premature failure. Most bonded joints are designed for tensile loading and if the joint is subjected to accidental compressive loading then buckling may occur, from which high peel forces arise leading to rapid fracture. 188 Ian A. Ashcroft, Andrew D. Crocombe stress Other idealised forms of fatigue loading that may be used in the laboratory to investigate behaviour under specific conditions are shown in Fig. 7.2. For example an asymmetric saw tooth waveform may be used to investigate the relative importance of the loading and unloading segments of a fatigue cycle. Crack growth tends to occur only in the loading part of the wave, whereas creep can occur whenever a sufficient load is applied, hence, varying loading, unloading and hold segments in a wave can help to investigate the relative importance of creep and fatigue. In real applications it is rare that the idealised types of loading shown in Figs. 7.1 and 7.2 will be experienced. It is more likely that frequency, amplitude, mean and waveform will all vary with time, as illustrated in Fig. 7.3. Moreover, it is likely that there will be different types of loading associated with different events, for example in a car there may be a variable high frequency, low amplitude fatigue load associated with the interaction of the tyres with the road superimposed with lower frequency, higher amplitude fatigue associated with common manoeuvres such as cornering or braking. There are a number of ways to deal with such complex loading. One is to attach a measuring device to a part in-service to characterise typical events and then to create a spectrum from this information to represent, for example, a typical aircraft flight, including take off, in-air manoeuvring and landing etc. The resultant spectrum can then be run repeatedly to look at the effect of multiple such events. The main drawback of this method is that experiments tend to be rather lengthy and may still not be useful if ‘out of the ordinary’ events are not accounted for. It is generally preferable, therefore, to reduce the spectrum. In metals, where the materials are generally rate insensitive, an easy method of accelerating tests is to compress the spectrum and test at high frequency, although any time dependent effects, such as corrosion, will not be represented accurately in such a test. When devising accelerated service simulation tests for adhesive joints, care must be taken when introducing acceleration techniques that any influential time dependent or load sequencing effects are retained in the spectrum. In recent work, modelling of both 1 0.9 0.8 0.7 0.6 0.5 0.4 0.3 0.2 0.1 0 d e c b a f g 0 10 20 time 30 40 Fig. 7.3 Spectrum illustrating various features seen in-service: (a) low rate loading ramp, (b) mean change, (c) amplitude change, (d) frequency change, (e) hold period, (f) high rate unloading ramp, (g) unloaded period 7 Modelling Fatigue in Adhesively Bonded Joints 189 time dependent (Al-Ghamdi et al. 2003; Ashcroft 2005) and load sequencing effects (Erpolat et al. 2004, 2004a; Ashcroft 2004) in bonded joints have been investigated and such modelling is an important complement to any test programme for bonded joints using accelerative techniques. 7.2.2 Fatigue Initiation and Propagation Fatigue is generally divided into initiation and propagation phases. In adhesively bonded joints the differentiation between these two phases, and even if there really are two such phases, is still a contentious issue. However, at the predictive modelling level there is a distinction between how a propagating crack is analysed and how the number of cycles before a macro crack has formed can be predicted and this can be used to differentiate between the initiation and propagation phases. It is clear that fatigue initiation in adhesives is complex and mechanistically different to that in metals. It can also vary with material, geometry and environment. Adhesives themselves tend to be multi-component systems, with filler particles, carrier mats and toughening particles typically added, and failure may involve many mechanisms, including; matrix micro-cracking (initiation, growth and coalescence), filler particle fracture or debonding, cavitation of rubber toughening particles and debonding of carrier mat fibres. An intrinsic part of fatigue failure in a bonded joint may also involve failure, or damage, in the adherend or in the interfacial region between adherend and adhesive, and hence these possible modes of failure should also be considered in any predictive model. An additional difficulty in characterising fatigue failure in bonded joints from a mechanistic approach is that the initial damage tends to be internal and hence detection and experimental characterisation is difficult, especially if this is attempted non-destructively. In terms of in-service inspection, initiation may be linked to the detectability of flaws. In most cases a purely mechanistic definition of the initiation and propagation phases is hence unrealistic and a more pragmatic approach must be taken. In terms of the modeller a useful differentiation is to treat the fatigue damage as an initiation phase until a sufficient crack has formed that further growth can be predicted using fracture mechanics. Mechanistically there is a similar blurring between ‘damage’ and ‘cracking’ as a region considered as damaged rather than cracked may contain micro-cracking. In terms of finite element modelling, damage is often modelled by reducing material properties (the continuum damage mechanics approach), usually stiffness, of the element, and cracking is modelled by detaching element at nodes, after which fracture mechanics methods can be used to model crack propagation. In cohesive zone modelling both damage and crack growth are represented by using specialised elements to join adjacent continuum elements (Loh et al. 2003; Crocombe et al. 2006; Liljedahl et al. 2007, 2007). This topic is described in detail in Chap. 6. 190 Ian A. Ashcroft, Andrew D. Crocombe 7.2.3 Experimental Testing Although this chapter is mainly concerned with how to model fatigue in bonded joints it is impossible to do so without the use of the results from experimental tests. Firstly, tests are required to generate the mechanical properties (and potentially physical and hygro-thermal properties) for each component of the joint. The properties required will depend on the material constitutive model deemed appropriate for each component. A potential difficulty here is that adhesives tend to have rate dependent mechanical properties and the strain rate experienced by an adhesive in a joint will vary significantly both temporally (due both to the cycling and progressive damage) and spatially. Attempting to include this effect in the model may be difficult and usually a compromise value is used. This is likely to be perfectly adequate where the temperature is well below the glass transition point but may be less acceptable at higher temperatures. Experimental testing is also required to provide the parameters associated with the particular fatigue damage model that is to be applied. For example if a crack growth model is to be applied then a fracture mechanics test will have to be carried out to provide the constants relating the chosen fracture mechanics parameter (typically strain energy release rate, G) and the crack propagation rate. Different tests may have to be carried out for failure in the adhesive, in the adherend and at the interface between the two. In addition, it may be necessary to carry out these tests under different environmental conditions. Samples for these tests are similar to those used for determining the fracture parameters in quasi-static loading, e.g. for mode I loading a double cantilever beam (DCB) sample, as shown in Fig. 7.4a is typically used. In these tests it is essential to accurately measure crack growth as a function of cycles during the test and this may be achieved by optical means or the use of crack gauges (e.g. Ashcroft and Shaw 2002; Erpolat et al. 2004a, Ashcroft 2004). It may also be useful to measure displacement at the point of loading if testing is in load control. Another class of tests are those used to validate the fatigue modelling. These tests may also be similar to those used in standard quasi-static testing, such as the single lap joint (SLJ) and double lap joint (DLJ) shown in Fig. 7.4b,c respectively. In these tests the number of cycles to failure may be simply recorded or an attempt may be made to monitor crack (or damage) progression, e.g. though optical or back-face strain measurements (Zhang and Shang 1995; Crocombe et al. 2002, 2005; GranerSolana et al. 2007; Shenoy et al. 2008). In addition to in-situ measurements, damage and crack progression may be investigated in post-failure examination and it is also instructive to examine samples that have only been partially fatigue tested, e.g. by sectioning (Crocombe et al. 2002; Graner-Solana et al. 2007; Shenoy et al. 2008), ultrasonics or x-radiography (Ashcroft et al. 1997, 2003; Ashcroft 2004). If crack propagation rate is to be measured, then a longer overlap length than that used in standard quasi-static tests may be desirable. A common test geometry used to look at fatigue initiation and propagation in adhesively bonded joints is the lap-strap joint (LSJ) shown in Fig. 7.4d (Ashcroft et al. 2001a, 2003, 2008; Johnson 1987; Mangalgiri et al. 1987; Mall and Yun 1987). This tends to be more representative 7 Modelling Fatigue in Adhesively Bonded Joints 191 (a) 25mm 100mm 12.5mm (b) (c) (d) Fig. 7.4 Typical fatigue test samples: (a) DCB, (b) SLJ, (c) DLJ, (d) LSJ 192 Ian A. Ashcroft, Andrew D. Crocombe of applications with long bondlines, such as bonded stiffeners (stringers) in aircraft wings, than the simple lap joints. This differs from the standard fracture mechanics test in that it is often used to look at initiation as well as propagation. Also, fracture is mixed mode and the mode-mixity varies with crack length. Fatigue behaviour in the lap-strap joint can be markedly different from that in simple, short overlap joints, such as the SLJ and DLJ, because, as the strap adherend spans the loading points there is no definitive failure point for the joint and accumulative creep is restricted. The fatigue testing of adhesive lap joints is covered by the standards BS EN ISO 9664:1995 and ASTM D3166-99. In the former it recommends that at least four samples should be tested at three different stress amplitude values for a given stress mean, such that failure occurs between 104 and 106 cycles. This standard also advises on statistical analysis of the data. In general, fatigue data exhibits greater scatter than quasi-static data and this needs to be taken into account when using safety factors with fatigue data. Further advice on the application of statistics to fatigue data is found in BS 3518-5:1966. 7.3 Modelling Methods 7.3.1 Total-Life Methods 7.3.1.1 Stress-Life Approach In the total life approach, the number of cycles to failure (N f ) is plotted as a function of a variable such as stress or strain amplitude. Where the loading is low enough that the deformation is predominantly elastic a stress variable (S) is usually chosen and the resultant plot is termed an S-N curve, or Wöhler plot, and this is known as the stress-life approach. Under these conditions a long fatigue life would be expected and this is termed high cycle fatigue (HCF). The S-N data is either plotted as a loglinear or a log-log plot and a characteristic equation can be obtained by empirical curve fitting, using the forms of equation shown below. S = C + D log N f (7.1) S = AN f α (7.2) The constants in the equations are dependent on many factors, including; material, geometry, surface condition, environment and mean stress. Hence, caution should be used when trying to apply S-N data beyond the samples used to generate the data. The standard stress-life method gives no indication of the progression of damage, although in some cases the onset of cracking is indicated on the plot in addition to the complete failure, hence allowing the initiation and propagation phases to be differentiated. The above factors mean that the S-N curve is of rather limited use in predicting fatigue behaviour, however, it is still useful in fatigue modelling as a 7 Modelling Fatigue in Adhesively Bonded Joints 193 validation tool. Wöhler (1867) noted a stress below which a nominally infinite life is seen, which is termed the fatigue or endurance limit. This concept can potentially be used more widely in predictive modelling, as described further in Sect. 7.3.12. An S-N curve for epoxy/CFRP (carbon fibre reinforced polymer) double lap joints with the geometry shown in Fig. 7.4b can be seen in Fig. 7.5. In this case N f is plotted as a function of the average shear stress amplitude. It should be noted, however, that there is no particular relation between the average shear stress in a joint and failure load, for quasi-static or fatigue failure. For this reason, load rather than stress is often used in total-life plots for bonded joints, to avoid any false conclusions being drawn regarding a relationship between the average shear stress and fatigue life. Three regions can be seen in Fig. 7.5, these can be roughly divided into the low cycle fatigue (LCF) region below approximately 1000 cycles, the high cycle fatigue (HCF) region between approximately 1000 and 100,000 cycles and the endurance limit region above 100,000 cycles. Both the quasi-static strength and fatigue resistance decreases when the temperature is raised from 22 to 90◦ C. The ratio between fatigue limit and quasi-static strength is approximately 0.36 at 22◦ C and 0.26 at 90◦ C, showing that the joints are also proportionally more susceptible to fatigue at 90◦ C. Ashcroft et al. (2001) attributed the accelerated fatigue failure of the joints at 90◦ C to the combined effects of creep and fatigue. As mentioned above, the fatigue life of bonded joints depends not only on the stress amplitude but also on the mean stress. This is illustrated in Fig. 7.6a for a steelepoxy SLJ. The mean level is represented by the R-ratio (min. stress/max. stress), where an increasing value of R indicates an increasing mean for a given amplitude. It can be seen that either increasing the mean or increasing the amplitude results in a reduction of the fatigue life. The relationship between amplitude and mean on the fatigue life can be illustrated in a constant-life diagram in which combinations of mean and amplitude are plotted for a given fatigue life. A constant life diagram plotted from the data in Fig. 7.6a is shown in Fig. 7.6b. 20 22°C Stress amplitude (MPa) 18 90°C 16 22°C (unbroken) 14 90°C (unbroken) 12 10 8 6 4 2 LCF HCF threshold 0 1 10 100 1000 10000 100000 1000000 No. cycles to failure Fig. 7.5 S-N curve for epoxy/CFRP double lap joints (data from Ashcroft et al. 2001) 194 Ian A. Ashcroft, Andrew D. Crocombe 10 R = 0.1 8 Load range, kN Fig. 7.6 (a) Effect of R-ratio on fatigue life, (b) Constant life diagram (data from Crocombe and Richardson 1999) R = 0.5 R = 0.75 6 4 2 0 100 1000 10000 100000 Cycles to failure, Nf 1000000 (a) 6 Load range, kN 5 4 3 2 10000 cycles 1 100000 cycles 0 0 2 4 6 Mean load, kN 8 10 (b) The stress amplitude in the constant-life diagram can be normalised with respect to the stress amplitude for that particular life at R = −1 (Sar ), to produce a normalised amplitude-mean diagram, which tends to consolidate the data at different lives to a single curve. This curve can be fitted to a straight line (Goodman equation) or a curved line, such as a parabola (Gerber equation): Goodman equation : Gerber equation : Sa Sm + =1 Sar Su 2 Sm Sa + =1 Sar Su (7.3) (7.4) These curves are often not accurate for compressive mean stresses, in which case a conservative estimate may be made by assuming that compressive mean stresses provide no benefit, i.e.: 7 Modelling Fatigue in Adhesively Bonded Joints For Sm ≤ 0, 195 Sa =1 Sar (7.5) As was stated earlier, total life methods are completely phenomenological, however, in some cases efforts have been made to differentiate between the initiation and propagation phases (Harris and Fay 1992; Zhang and Shang 1995; Crocombe et al. 2002, 2005; Graner-Solana et al. 2007; Shenoy et al. 2008; Dessureault and Spelt 1997, Quaresimin and Ricotta 2006). Shenoy et al. (2008) used a combination of back-face strain measurements and sectioning of partially fatigued joints to measure damage and crack growth as a function of number of fatigue cycles. It was seen from the sectioned joints that there could be extensive internal damage in the joint without external signs of damage; therefore, determination from external observations alone is likely to overestimate the initiation phase. Shenoy et al. (2008) identified three regions in the fatigue life of an aluminium/epoxy single lap joint. An initiation period (CI) in which damage starts to accumulate, but a macro-crack has not yet formed, a stable crack growth (SCG) region in which a macro-crack has formed and is growing slowly and a fast crack growth region (FCG), which leads to rapid failure of the joint. They found that the percentage of life spent in each region varies with the fatigue load, as shown schematically in Fig. 7.7. At low loads the fatigue life is dominated by crack initiation, whereas crack growth dominates at high loads. The figure also shows the back-face strain signal associated with each phase of fatigue damage and it can be seen how this can be used to monitor damage in a lap joint. Finite element analysis (FEA) can be used to relate the strain signal to simulations of cracking and damage in the joint. Shenoy et al. (2008) observed a curved crack front across the specimen width, necessitating a 3D FEA to accurately represent the evolution of damage/cracking in the joint to compare with the experimental strain, as shown in the mesh in Fig. 7.8. It was further seen, that cracking could occur from (i) one end of the overlap, (ii) approximately equally from both ends of the overlap or (iii) asymmetrically from the two ends. The type of growth No. of cycles to failure Fig. 7.7 Fatigue failure map with superimposed back-face strain (BFS) as a function of number of cycles for bonded single lap joints (Shenoy et al. 2008) BFS plots FCG SCG CI No. of cycles Fatigue load Normalised backface strain Failure curve 196 Ian A. Ashcroft, Andrew D. Crocombe Fig. 7.8 (a) Concave crack front shown schematically, (b) 2D view of the, finite element model showing different sized fillets, (c) 3D view of the joint. Deformed mesh with centre crack (Shenoy et al. 2008) Concave crack front (a) (b) Plane of symmetry (centre of joint width) (c) will affect the back-face strain signals, as shown in Fig. 7.9, and must be represented accurately in the FE model for meaningful comparisons to be made. 7.3.1.2 Fatigue Limit A major limitation of the total life approach is that the crack propagation is highly geometry dependent and hence the data from an S-N curve cannot easily be used to predict the fatigue life for a different sample geometry. However, if a fatigue limit is seen then it may be possible to use the data from one sample to predict the fatigue limit for a different geometry or loading condition. The approach to be used is similar to that for predicting failure under quasi-static multiaxial loading and similar multi-axial failure criteria, e.g. von Mises, Tresca or maximum principal stress, should be used. For example the von Mises effective stress for fatigue limit prediction, σae would be: 7 Modelling Fatigue in Adhesively Bonded Joints 197 SG1 1 mm Loaded substrate Fixed substrate SG2 (a) 80 Backface strain [microstrain] 70 60 50 40 30 SG1 SG2 20 10 0 0 0.2 0.4 0.6 0.8 1 1.2 Crack length [mm] (b) Backface strain [microstrain] 80 70 60 50 40 SG1 30 SG2 20 10 0 0 0.5 1 1.5 2 2.5 Crack length [mm] (c) Fig. 7.9 (a) Location of strain gauges. FEA simulated back faced strain (BFS) plots for. (b) type (i) crack growth, (c) type (ii) crack growth, (d) type (iii) crack growth (Shenoy et al. 2008) 198 Ian A. Ashcroft, Andrew D. Crocombe Backface strain [microstrain] 120 100 80 60 40 20 SG1 FEA SG1 Experimental SG2 FEA SG2 Experimental 0 0 2000 4000 6000 8000 10000 12000 No. of cycles (d) Fig. 7.9 (continued) 1 σae = √ 2 (σa1 − σa2 )2 + (σa2 − σa3 )2 + (σa3 − σa1 )2 (7.6) where σa1 , σa2 and σa3 are the principal stress amplitudes. The method then is to experimentally determine the fatigue limit using calibration samples and then calculate the value of the selected failure parameter at the fatigue limit. The fatigue limit can then be predicted for different geometries for failure in the same material – in theory. However, in practice there are the same difficulties facing those wishing to predict the quasi-static failure load of adhesive joints, i.e. which failure criterion should be chosen and how to deal with the theoretical stress singularities. Abdel Wahab et al. (2001a) predicted the fatigue limit (or fatigue threshold) in the lapstrap joints shown in Fig. 7.4d using a variety of stress and strain based failure criteria, taking the value at a distance of 0.04 mm from the singularity to avoid mesh sensitivity. They also used the plastic zone size as a failure criterion. A summary of the results can be seen in Table 7.2. 7.3.1.3 Cumulative Damage Methods The S-N curve is only directly applicable to constant amplitude fatigue whereas in many cases variable amplitude fatigue spectra are experienced. A simple method to use S-N data to predict variable amplitude fatigue was proposed by Palmgren (1924) and then further developed by Miner (1945). Miner assumed that the total amount of work to cause failure in a sample, W , was a constant, regardless of the amplitude of the fatigue. Therefore if the sample was subjected to a spectrum loading consisting of i blocks, where the work associated with each block was wi , then: ∑ wi = W (7.7) 7 Modelling Fatigue in Adhesively Bonded Joints 199 Table 7.2 Fatigue threshold predictions for lap-strap joints (Abdel Wahab et al. 2001a) Failure load (kN) Experimental Maximum principal strain Von Mises strain Shear stress Peel stress Von Mises stress Maximum principal stress Average principal stress Plastic zone size (0.1%) Plastic zone size (knee) Testing/ageing conditions −50◦ C/50◦ C dry 22◦ C/50◦ C dry 22◦ C/45◦ C, 85%RH 90◦ C/50◦ C dry 11.0 10.89 11.16 11.1 7.83 11.14 10.35 10.26 – – 11.0 11.8 12.2 12.01 8.29 12.03 11.02 11.1 13.5 13.18 9.0 11.8 12.3 11.97 8.82 12.0 10.99 11.04 13.5 12.0 9.0 11.2 11.3 11.4 >15 11.37 14.27 >15 14.0 13.2 He further assumed that the work absorbed in a cycle was proportional to the number of cycles in the block, ni , and hence: wi ni = W Nfi (7.8) Where N f i is the number of cycles to failure at the stress amplitude for that particular block and can be obtained from the S-N curve. Therefore from Eqs. (7.7) and (7.8): ni (7.9) ∑ Nfi = 1 Equation (7.9) is termed Palmgren-Miner’s (P-M) law or the linear damage accumulation model. It can be seen that the fatigue life of a sample in variable amplitude fatigue can be predicted from an S-N curve obtained from constant amplitude fatigue testing of similar samples using Eq. (7.9). However, there are a number of serious limitations to this method. It is assumed that damage accumulation is linear and that there is no load history effect. In many cases these assumptions are not correct. For instance it is assumed that cycles below the fatigue limit will not contribute to the damage accumulation, however, once a crack has formed by the action of stresses above the fatigue limit then it may continue to propagate at stresses below the fatigue limit. In metals it is often seen that an overload induces crack root plasticity which retards crack growth, leading to under-predictions of fatigue life using the P-M rule. Another effect of load sequencing that is neglected is that failure will actually occur when the residual strength of the sample is reduced to the maximum stress in the fatigue spectrum. Hence an overload at the beginning of the spectrum, when little residual strength degradation has occurred may be beneficial, whereas when the residual strength has degraded it may cause quasi-static failure. To account for some of these deficiencies a number of modifications to the P-M rule have been suggested. A number of non-linear damage accumulation models have been proposed (Marco and Starkey 1954; Henry 1955; Leve 1969; Owen and Howe 1972; Bond 1999), as illustrated in Fig. 7.10. Load sequencing events are only accounted for if a different damage parameter is obtained for each stress amplitude 200 Ian A. Ashcroft, Andrew D. Crocombe 1. 1. D = f (n/Nf , S) Damage, D Damage, D D = f (n/Nf ) 1.0 0 S1 S2 S3 1.0 0 n/Nf n/Nf (a) Linear and non-linear, stressindependent damage models (b) Non-linear, stress-dependent damage models Fig. 7.10 Various forms of damage accumulation law seen in the spectrum, as shown in Fig. 7.11a, and to incorporate load interactions further empirical modifications are required, as shown in Fig. 7.11b. Crack growth below the fatigue limit can be accommodated by extending the fatigue curve below the fatigue limit, with either the same (elementary P-M) or a reduced (extended P-M) slope, as illustrated in Fig. 7.12. In the Relative Miner’s law the Miner’s sum, C, on the right hand side of Eq. (7.9) is set to some value other than 1, as shown in Eq. (7.10). ni (7.10) ∑ Nfi = C C is determined experimentally and Schutz and Heuler (1989) suggested that the experimentally determined Miner’s sum can only be applied to other spectra where the peak stresses of the two spectra differ by no more than 20 or 30%. S2 Damage, D 1. Damage, D 1. S2 S1 S1 1.0 0 1.0 0 n/Nf n/Nf (a) (b) Interaction-free, multi-stress level damage accumulation in a nonlinear, stress-dependent model Multi-stress level damage accumulation considering load interaction effects Fig. 7.11 Sequencing and load interaction in stress-dependent damage accumulation models 7 Modelling Fatigue in Adhesively Bonded Joints 201 S Stress level P-M Extended P-M Elementary P-M Number of cycles to failure log(Nf ) Fig. 7.12 Modifications to Palmgren-Miner’s rule The various proposed modifications to the P-M rule can result in better predictions, although at the expense of increased complexity and/or more testing. However, the basic flaw in the method, that it bears no relation to the actual progression of damage in the sample, is still not addressed. Erpolat et al. (2004) used the P-M law and the extended P-M law, shown in Fig. 7.12, to predict failure in an epoxy-CFRP double lap joint subjected to the variable amplitude (VA) fatigue spectrum shown in Fig. 7.13a. The resulting Miner’s sum as a function of maximum load can be seen in Fig. 7.13b. It can be seen that the Miner’s sum is significantly less than 1, varying between 0.04 and 0.3, and decreases with increasing load. This means that the load sequencing is causing damage acceleration, i.e. that the P-M rule is non-conservative, and that the damage acceleration increases with maximum load. It can also be seen in Fig. 7.13b that allowing the cycles below the fatigue limit to contribute to the damage makes little difference. This implies that there is a strong load sequencing effect in the VA fatigue testing of bonded joints and that the P-M rule should not be used as it could lead to in-service failure well below the predicted life. 7.3.1.4 Strain-Life Approach Under high stress amplitudes, plastic deformation occurs and the fatigue life is considerably shortened. This is known as low cycle fatigue (LCF). Under constant stress amplitude fatigue with strain hardening, the strain amplitude decreases after the first cycle, and the subsequent hysteresis loop is repeated a number of times before micro-cracking occurs. In LCF the high loads involved mean that cracks are usually still small when failure occurs. This behaviour leads to a horizontal asymptote to the quasi-static strength in the LCF region, as seen in Fig. 7.5. In constant strain amplitude testing either increasing or decreasing stress amplitude can be seen, depending on whether the material is cyclic strain hardening or softening, although in many cases this stabilises to a constant value after a number of cycles. If there is a positive strain mean then the mean tends to decrease as the sample is fatigued, a phenomenon known as plastic shakedown. This can be compared with the effect of 202 Ian A. Ashcroft, Andrew D. Crocombe Fig. 7.13 (a) VA spectrum for a peak load of 9 kN, (b) Miner’s sum as a function of maximum load (data from Erpolat et al. 2004) 8 Load (kN) 6 4 2 0 2 4 6 10 8 Time (sec) (a) 0.35 P-M 0.3 Extended P-M Miner's Sum, C 0.25 0.2 0.15 0.1 0.05 0 8 9 10 11 Maximum Load (kN) (b) 12 creep in constant stress amplitude testing, which leads to an increase in the mean strain with cycling. Coffin (1954) and Manson (1954) proposed that N f could be related to the plastic strain amplitude, Δε p /2, in the LCF region. β Δε p = B Nf 2 (7.11) This relationship dominates at high loads whereas Eq. (7.1) or (7.2) dominates at low cyclic loads. The total strain amplitude, Δε /2, is comprised of elastic and plastic components: 7 Modelling Fatigue in Adhesively Bonded Joints 203 Δεe Δε p Δε = + (7.12) 2 2 2 Hence from Eqs. (7.2), (7.11) and (7.12) an expression incorporating both HCF and LCF components of the fatigue life can be derived. β Δε A α = Nf + B Nf 2 E (7.13) The strain-life approach is more difficult to implement than the stress-life method, particularly for non-homogenous material systems such as bonded joints. Adhesively bonded joints have stress singularities and a complex stress-strain state throughout the adhesive. Also, structural joints tend to be used in HCF applications and hence the strain-life method has seen little application to adhesively bonded joints. 7.3.2 Strength and Stiffness Wearout Approaches One of the main drawbacks of the total-life methods is that they cannot be used to monitor damage in the sample as only the final failure is characterised. An alternative phenomenological approach is to characterise fatigue damage as a function of the reduction in the strength or stiffness of a sample during its fatigue life. The advantage of this approach is that, unlike the total-life approach, the degradation in the sample prior to failure is characterised. From these models the residual strength or stiffness after a period of loading can be predicted and hence the response to further loading predicted. This makes the method more suitable for predicting the effects of complex loading than the simple total-life models. However, more testing is required than in the total life approach as the residual strength at various percentages of the total life must be determined experimentally at different load or stress amplitudes. 7.3.2.1 Strength Degradation Under Constant Amplitude Loading The residual strength of a joint after a certain number of fatigue cycles, n, is defined as SR (n). This is initially equal to the static strength, Su , but decreases as damage accumulates during the fatigue cycling. Failure occurs when the residual strength equals the maximum stress of the spectrum, i.e. when SR (N f ) = Smax . The rate of strength degradation mainly depends on Su , Smax and R (Smin /Smax ), i.e.: SR (n) = Su − f (Su , Smax , R) nκ (7.14) where κ is a strength degradation parameter. Substitution of the failure criterion (SR (N f ) = Smax ) into Eq. (7.14) gives: f (Su , Smax , R) = Su − Smax N κf (7.15) 204 Ian A. Ashcroft, Andrew D. Crocombe and the residual strength, SR (n), can be defined as: κ n SR (n) = Su − (Su − Smax ) Nf (7.16) 7.3.2.2 Strength Degradation Under Variable Amplitude Loading Schaff and Davidson (1997, 1997a) extended Eq. (7.16) to enable the residual strength degradation of a sample subjected to a variable amplitude loading spectrum to be predicted. j n j + neff , j κ j (7.17) SR ∑ ni = Su − (Su − Smax, j ) Nf, j i=1 j−1 ⎞ κ1 j S − S n ∑ u R i ⎜ ⎟ i=1 ⎟ neff , j = N j ⎜ ⎝ Su − Smax, j ⎠ ⎛ where (7.18) j represents the current stage and n j is the number of cycles elapsed in stage j. However, they noted a crack acceleration effect in the transition from one constant amplitude (CA) block to another, a phenomenon they termed the cycle mix effect, and proposed a cycle mix factor, CM, to account for this. Hence, during the transition: SR (n) → SR (n) −CM CM = Cm Su Δ Smn SR (n) for Δ Smn > 0 (7.19) (Δ Smax /Δ Smn )2 (7.20) where Δ Smn and Δ Smax are the changes in the mean and maximum load values, respectively, during the transition from one stage to another and Cm is the cycle mix constant, which is dependent on material and geometry. Cm can be determined by comparing variable amplitude fatigue lives under different spectra, e.g. two spectra with and without mean stress jumps. Using the cycle mix factor, Eq. (7.18) can be modified to: j−1 ⎞ κ1 j S − S n −CM ∑ u R i j−1→ j ⎜ ⎟ i=1 ⎟ neff , j = N j ⎜ ⎝ ⎠ Su − Smax, j ⎛ (7.21) Where CM j−1→ j is the cycle mix factor for the transition from stage j − 1 to stage j if Δ Smn > 0. Erpolat et al. (2004) assumed a linear damage accumulation for CFRP-epoxy DLJs and formulated their damage law in terms of load/failure load rather than 7 Modelling Fatigue in Adhesively Bonded Joints 205 stress/strength for the reasons stated in Sect. 7.3.1. Residual failure load degradation for each cycle above the fatigue limit, LD, was defined as: LD = Lu − LOL N f ,OL (7.22) where Lu is the quasi-static failure load, LOL is the maximum load of the cycle and N f ,OL is the fatigue life corresponding to this cycle. The residual failure load degradation due to mean load jumps, CM, was then defined as: Δ Lmax CM = α (Δ Lmn )β L peak ( Δ Lmn ) (7.23) where Δ Lmn and Δ Lmax are the changes in the mean and maximum load values during the transition and L peak is the peak load in the spectrum. The parameters α and β are the cycle mix constants, which are dependent on material and geometry. They can be determined by comparing VA fatigue lives under different spectra, e.g. two spectra with and without mean load jumps. Assuming that in each loading block, there are a number of cycles above the fatigue limit (OL1 , OL2 , . . . ) and a number of mean load jumps (CM1 , CM2 , . . .), the failure load degradation during a single block, Δ LRB , can be defined as: ΔL ΔL β L peak Δ LRB = α (Δ Lmn,1 ) max,1 Δ Lmn,1 β L peak + (Δ Lmn,2 ) max,2 Δ Lmn,2 +··· Lu − LOL1 Lu − LOL2 + + ··· N f ,OL1 N f ,OL2 (7.24) Equation (7.24) is illustrated schematically in Fig. 7.14. The number of blocks to failure is given by: Lu − L peak NB = (7.25) Δ LRB Erpolat et al. (2004) termed this the linear cycle mix (LCM) model and showed that it was capable of more accurate predictions of fatigue life for bonded joints under variable amplitude fatigue than Palmgren-Miner’s (P-M) law. Table 7.3 shows a comparison of the predictions using the P-M law and the LCM model for CFRPepoxy DLJs using the VA fatigue spectra shown in Fig. 7.15. It can be seen that, the P-M law significantly over-predicted the fatigue life when there were mean jumps in the fatigue spectrum, whereas, the LCM model produced excellent predictions of the fatigue life. 7.3.2.3 Stiffness Degradation An alternative approach to the strength-based wearout models is to associate damage accumulation with stiffness degradation. Like strength degradation, the stiffness degradation rate can be considered as a power function of the number of load cycles (Dibenedetto and Salee 1979; Yang et al. 1990; Whitworth 1990). This relation was defined by Yang et al. (1990) as: 206 Ian A. Ashcroft, Andrew D. Crocombe (LR -Lpeak )/(Lu -Lpeak ) Residual Failure Load 1 LD1 CM1 LD2 CM2 LD3 0 1 N / Nf Number of Cycles Fig. 7.14 Residual failure load degradation during VA fatigue cycling Table 7.3 Variable amplitude fatigue predictions for epoxy/CFRP DLJs using Palmgren-Miner (P-M) and Linear Cycle Mix (LCM) methods (Erpolat et al. 2004) Spectra 7 (a) 7 (b) 7 (c) 7 (d) 7 (e) Fatigue life (cycles at Lmax = 9kN) Damage sum, C Experimental P-M LCM P-M LCM 200k 180k 80k > 106 > 106 > 106 200k 390k > 106 > 106 200k 200k 62k > 106 > 106 0.18 0.9 0.21 – – 1 0.9 1.28 – – E (n) = E (0) − E (0) (d + a2 B S) na3 +BS d = a1 + a2 a3 (7.26) (7.27) where E(0) is the initial stiffness and S is the stress level, a1, a2, a3 and B are stressindependent parameters. Whitworth (1990) proposed an alternative model: n n a a a E = E (0) − H [E (0) −C] (7.28) Nf Nf where C is a stress-dependent parameter but a and H are independent of the applied stress level. A failure criterion for a stiffness-based wearout models is not as straight forward as that for the strength-based wearout models. One approach is to relate failure stiffness, E(N f ), to stress, e.g.: E(N f ) Smax = E (0) Su (7.29) 7 Modelling Fatigue in Adhesively Bonded Joints 207 Fig. 7.15 Variable amplitude fatigue spectra (Erpolat et al. 2004) which can then be used as a failure criterion for the stiffness-based wearout models. 7.3.3 Fracture Mechanics Based Methods Unlike the stress and strain-life approaches, the fracture mechanics approach only deals with the crack propagation phase. It is assumed that crack initiation occurs during the early stages of the fatigue cycling or a pre-existing crack exists. The 208 Ian A. Ashcroft, Andrew D. Crocombe initial crack size used in the analysis can be measured or an assumed value can be used. The rate of fatigue crack growth, da/dN, is then correlated with an appropriate fracture mechanics parameter, such as Griffith’s (1921) strain energy release rate, G, or Irwin’s (1958) stress intensity factor, K. This relationship can be used to predict fatigue crack growth for different sample geometries. Paris et al. (1961) proposed that da/dN was a function of the stress intensity factor range, Δ K(= Kmax − Kmin ) da = C Δ Km (7.30) dN C and m are empirical constants dependent on the material, fatigue frequency, R-ratio, environment, etc. Various modifications to the Paris crack growth law have been proposed to take R-ratio effects into account. A modified version of the relationship proposed by Forman et al. (1967) is given below. da C (Δ K)m (Δ K − Δ Kth )0.5 = dN (1 − R) Kc − Δ K (7.31) where Kc is the quasi-static fracture toughness and Kth is the fatigue threshold (discussed further below). Although K is the most widely used fracture mechanics parameter for the analysis of metals, it is more complicated to apply to bonded joints, where the constraint effects of the substrates on the adhesive layer make it difficult to define the stress distribution around the crack tip. Therefore, G, is often used as the governing fracture parameter for adhesives if linear elastic fracture mechanics (LEFM) is applicable (i.e. localised plasticity). If an elasto-plastic fracture mechanics (EPFM) parameter is required, because of more widespread plasticity, then Rice’s (1968) J-integral (J) is generally used. The maximum strain energy release rate, Gmax , is often used for the fatigue analysis of bonded joints, in preference to the strain energy release rate range, ΔG, because facial interference of the adhesive on the debonded surfaces may lead to the generation of surface debris, which may prevent the crack from fully closing, thus giving an artificially high value of Gmin (Martin and Murri 1990). Gmax is directly proportional to ΔG, such that: (7.32) ΔG α (1 − R2 ) Gmax Therefore, the Paris law for adhesively bonded joints can be defined as a function of Gmax : da = CP Gnmax (7.33) dN A plot of experimental crack growth rate against the calculated Gmax often exhibits three distinct regions, as shown in Fig. 7.16. Region II is described by Eq. (7.33). Region I is defined by the threshold strain energy release rate, Gth , in which there is little or no crack growth. In Region III there is unstable fast crack growth as Gmax approaches the critical strain energy release rate, Gc . All three regions, which approximate a sigmoidal curve, can be represented by the empirical equation below: 7 Modelling Fatigue in Adhesively Bonded Joints Fig. 7.16 Fatigue crack growth curve 209 REGION I REGION II REGION II (Linear) (Fast) log (da/dN ) [m/cycle] (Threshold) Gc Gth da dN = CP ⋅ G nmax log (Gmax) [J/m2] ⎤n Gth n1 3 1 − ⎢ ⎥ da G max n2 ⎥ = CP Gnmax ⎢ ⎣ ⎦ dN Gmax 1− Gc ⎡ (7.34) The relationship between the fatigue crack propagation rate and the relevant fracture parameter, Γ, is termed the crack growth law and can be represented generically as: da = f (Γ) dN (7.35) This function must be determined and this is usually achieved experimentally using a simple sample geometry, such as the DCB in Fig. 7.4a. For these joints there is often a simple analytical solution for the determination of the fracture parameter, although numerical methods can also be used. Erpolat et al. (2004b) compare a number of different analytical and numerical solutions for the calculation of G and J for DCBs in fatigue. Once the empirical relationship in Eq. (7.35) has been determined then it can be used to predict fatigue crack growth in samples and components of different geometry, as long as the materials and mechanism of failure are the same. The number of cycles to failure is determined from a f Nf = ao da f (Γ) (7.36) Where ao is the initial crack length and a f is the final crack length. Equation (7.36) is often solved numerically, a process known as numerical crack growth integration (NCGI). An initial crack size, ai , is assumed and the fracture parameter Γ calculated. 210 Ian A. Ashcroft, Andrew D. Crocombe The crack propagation rate, dai /dN, is then determined from Eq. (7.35) and the crack size after ni cycles, ai+1 , determined from: ai+1 = ai + ni · dai dN (7.37) This is then repeated until the crack has gone all through the sample or Γ has reached the critical value for quasi-static fracture, in which case failure has occurred, or Γ has reached the threshold value for negligible crack growth. A further consideration is that the mode-mixity is likely to be different in the sample in which fatigue crack growth is being predicted to that used to determine Eq. (7.35) and is also likely to change as the crack grows. Hence a mixed-mode failure criterion must be assumed. The most common mixed mode failure criterion is probably the total strain energy release rate, GT (= GI + GII ), although GI is a possible alternative for brittle materials and many more complex alternatives exist, such as that in Eq. (7.38) (Quaresimin and Ricotta 2006a) Geqv = GI + GII GII GI + GII (7.38) However, Quaresimin and Ricotta (2006b) showed that Geqv and GT provided quite similar predictions of fatigue crack growth in single lap joints. Abdel Wahab et al. (2003, 2004) proposed a general method of predicting crack growth and failure in bonded lap joints incorporating NCGI and FEA. The crack growth law was determined from tests using a DCB sample and this was used to predict the fatigue crack growth in single and double lap joints. Figure 7.17 shows a comparison of the predicted and experimental load-life curves for a single lap joint using both GI and GT as the mixed-mode failure criterion. It has been shown that removing the fillet can 4.5 Maximum load (kN) 4 3.5 3 2.5 2 Experimental (no fillet) Experimental (fillet) nGI nGT 1.5 1 0.5 0 3 3.5 4 4.5 5 5.5 log cycles to failure 6 6.5 Fig. 7.17 Fatigue life predictions using NCGI with total strain energy release rate (nGT) and mode I strain energy release rate (nGI) as failure criteria. Open symbols indicate unfailed samples (data from Abdel Wahab et al. 2004) 7 Modelling Fatigue in Adhesively Bonded Joints 211 reduce or eliminate the initiation phase (Crocombe et al. 2002) and it would be expected that the fatigue life in such samples would be better predicted using a fracture mechanics method than that in samples with the fillets intact, in which the initiation period may be significant. This is demonstrated in Fig. 7.17 where it is seen that the prediction using GT is a good fit to the data from samples with fillets removed but is conservative to the samples with fillets. The good fit between the predictions using GI is thus likely to be coincidence and demonstrates how a combination of two errors (neglecting initiation and incorrect failure criterion) can potentially cancel each other and result in a ‘false’ good prediction. 7.3.3.1 Fatigue Threshold Adhesives and polymer composites tend to have steeper Paris curves than metals such as aluminium, which means that once cracks are of a detectable size, fast fracture can follow quickly. In this case it may be preferable to design for a service life with no crack growth. Abdel Wahab et al. (2001a) proposed the prediction of loading conditions for no crack growth using the fatigue threshold strain energy release rate, Gth , shown in Fig. 7.16. This was validated experimentally using the lap-strap joints shown in Fig. 7.4d. Experiments from samples with unidirectional (UD) CFRP adherends were used to define the threshold value of the fracture parameter and this was then used to predict the fatigue threshold in samples with multidirectional (MD) CFRP adherends. Both elastic (GT ) and elasto-plastic (JT ) fracture parameters were investigated and the crack was placed both in the centre of the adhesive centre line and at the lap-adhesive interface. As well as placement of the crack, prediction of fatigue thresholds using fracture mechanics is also dependent on the initial crack size assumed. Abdel Wahab et al. (2001a) showed that G was very sensitive to crack size at small crack sizes but became less size independent at approximately 0.05 mm and hence this crack size was used in the predictions. The approach of Abdel Wahab et al. (2001a) was extended to samples subjected to environmental ageing by incorporating the method with a coupled transient hygro-mechanical finite element analysis (Ashcroft et al. 2003a). A summary of the results from (Abdel Wahab et al. 2001a) and (Ashcroft et al. 2003a) is presented in Table 7.4. 7.3.3.2 Variable Amplitude Fatigue The numerical integration technique described earlier can easily be adapted to the prediction of fatigue crack growth in variable amplitude (VA) fatigue. In this case the value of Γ in Eq. (7.36) is a function of the varying amplitude fatigue spectrum as well as the crack length and the maximum value of ni in Eq. (7.37) must correspond to the number of cycles that Γ can be assumed constant for a particular loading block. Erpolat et al. (2004a) applied the NCGI technique to the prediction of crack growth in CFRP/epoxy DCB joints subjected to periodic overloads. This method tended to underestimate the experimentally measured crack growth, indicating crack 212 Ian A. Ashcroft, Andrew D. Crocombe Table 7.4 Prediction of fatigue limits in CFRP/Epoxy Lap-strap joints (Abdel Wahab et al. 2001a; Ashcroft et al. 2003a) Ageing conditions Testing conditions Fatigue threshold load, kN Experimental Predicted, GT Predicted, JT 50◦ C −50◦ C 11.0 11.0 9.0 9.0 4.5 6.0 4.5 8.1 8.7 8.2 8.7 2.8 3.7 2.8 11.1 11.6 7.9 11.6 3.8 5.3 3.8 dry 50◦ C dry 50◦ C dry 45◦ C, 85%RH 45◦ C, 85%RH 50◦ C dry 45◦ C, 85%RH dry 22◦ C dry 90◦ C dry 22◦ C, 95%RH 90◦ C, 97%RH 90◦ C, 97%RH 90◦ C dry growth acceleration due to the spectrum loading, as shown in Fig. 7.18a. In addition, an unstable, rapid crack growth regime was seen when high initial values of Gmax were applied, as shown in Fig. 7.18b. This behaviour was attributed to the generation of increased damage in the process zone ahead of the crack tip when the overloads were applied. Ashcroft (2004) presented evidence of these damaged regions through x-radiography and microscopy and proposed a simple extension to the NCGI method to enable these load history affects to be predicted. This was termed the ‘damage shift’ model and is illustrated by Fig. 7.19. In this model it is assumed constant amplitude conditions are represented by plot CA in Fig. 7.19. If an overload is superimposed onto the CA spectrum, then the damage ahead of the crack will increase and the resistance to crack propagation will decrease. It was proposed that this increased damage could be represented by a lateral shift in the FCG curve, as represented by curve OL in the figure, and hence, the effect of the overloads can be represented by a single parameter, ψ . In the initial stages of fatigue damage it is expected that the value of ψ will be dependent on the number and magnitude of the overloads. However, as long as the applied strain energy release rate range, ΔGA , is below a critical value (as discussed later), then as the crack starts to grow through the damage zone an equilibrium position of the FCG curve will be reached that is only dependent on ROL and the ratio of overloads to CA cycles, NR , i.e. At equilibrium : ψE = f (NR , ROL ) (7.39) Δ GCA Δ GOL ψE can easily be determined by comparing the crack growth rates under CA and VA fatigue for a single value of Δ GA . If Δ GA is increased, a critical point will be reached at which Gmax of the overloads is equal to the value of G for the damage shifted FCG curve, Δ GAC in Fig. 7.19. Unstable or quasi-static fracture then occurs. If G increases with crack length then this will lead to catastrophic failure of the joint. However, if G decreases with a, as when testing DCB samples in displacement control, then the crack will eventually stop if the G arrest (Garr ) value is reached before the joint has completely fractured. The value of Δ GA associated with the crack arrest point (Δ Garr ) will now Where: ROL = 7 Modelling Fatigue in Adhesively Bonded Joints 78 Crack Length (mm) Fig. 7.18 Crack growth under VA-loading: (a) low initial G, (b) high initial G 213 76 74 72 70 Prediction 68 Experimental 66 0 0.25 0.5 0.75 1 1.25 Number of cycles * 106 (a) Crack Length (mm) 80 75 70 Prediction 65 Sudden crack growth Experimental 60 0 0.1 0.2 0.3 Number of cycles * 106 Log da/dN (b) OL CA ψE (da/dN)OL (da/dN)CA ΔGA ΔGAC Fig. 7.19 Damage shift model Log ΔG 0.4 0.5 214 Ian A. Ashcroft, Andrew D. Crocombe be much smaller and hence crack growth will be greatly reduced. This model is entirely consistent with the observed crack growth behaviour shown in Fig. 7.18. 7.3.3.3 Creep-Fatigue Ashcroft and Shaw (2002) used Gth from testing DCB joints to predict the 106 cycle endurance limit in lap strap and double lap joints at different temperatures, using GT as the failure criterion. The predictions, shown in Table 7.5, are reasonable, apart from the double lap joint tested at 90◦ C, which fails at a far lower load than predicted. This was attributed to accumulative creep in the double lap joint, which can be seen in plots of displacement against cycles at constant load amplitude, as shown in Fig. 7.20. Creep in fatigue testing of bonded lap joints has also been observed by other authors (Hart-Smith 1981; Harris and Fay 1992). It should be noted, however, that accumulative creep is prevented in the lap-strap joint by the strap adherend. As many adhesives can be considered as visco-elastic/visco-plastic materials over a wide range of their operating environment, it is not surprising that combined effects of creep and fatigue have been seen when bonded joints have been tested in fatigue with a non-zero mean load. The effect of this superimposed creep and fatigue produces a strong frequency and temperature dependency for crack growth when joints are tested in fatigue and also calls into question the applicability of tradiTable 7.5 Fatigue limit predictions from DCB data (Ashcroft and Shaw 2002) Temp. Fatigue limit load, kN Lap-strap joint −50◦ C 22◦ C 90◦ C Double lap joint Expt. Predicted Error (%) Expt. Predicted Error (%) 14 15 14 8 10 11 43 33 21 10.1 10.0 3.3 10.0 12.5 13.0 0 25 294 0.3 90°C RT –50°C Displacement (mm) 0.25 0.2 0.15 0.1 0.05 0 0 2000 4000 6000 8000 N cycles Fig. 7.20 Creep in double lap joints in fatigue 10000 12000 7 Modelling Fatigue in Adhesively Bonded Joints 215 tional elastic and elastic-plastic fracture parameters for characterising crack growth under these conditions. In this case, time dependent fracture mechanics (TDFM) may be preferable. Landes and Begley (1976) and Nikbin et al. (1976) independently proposed a TDFM parameter analogous to Rice’s J-integral. Landes and Begley called this new integral C∗ . As C∗ is only applicable to extensive creep conditions, Saxena (1986) proposed an alternative parameter, Ct , which is also applicable for small-scale and transition creep. This is defined as: Ct = − 1 ∂ Ut∗ (a,t, v̇c ) B ∂a (7.40) Where B is sample width and Ut∗ is an instantaneous stress-power parameter, which is a function of crack length, a, time, t and the load-line deflection rate, v̇c . When analysing creep-fatigue, an average value of Ct , Ct(ave) , can be used. Three methods of predicting creep-fatigue crack growth in bonded joints were proposed by Al-Ghamdi et al. (2004): (i) The empirical crack growth law approach. In this approach a suitable fracture mechanics parameter is selected and plotted against the FCGR or the creep crack growth rate (CCGR = da/dt). A suitable crack growth law is fitted to the experimental data and crack growth law constants are determined at different temperatures and frequencies. Empirical interpolation can be used to determine crack growth law constants at unknown temperatures and frequencies. (ii) The dominant damage approach. This assumes that fatigue and creep are competing mechanisms and that crack growth is determined by whichever is dominant. (iii) The crack growth partitioning approach. This assumes that crack growth can be partitioned into cycle dependent (fatigue) and time dependent (creep) components and that the total crack growth can be determined by summing these components. Method (iii) can be represented by the following equation: da 1 da da = + dN dN fatigue f dt creep (7.41) Al-Ghamdi et al. (2004) used the following form of Eq. (7.41): da mCtq = D(Gmax )n + dN f (7.42) The fatigue crack growth constants D and n were determined from high frequency tests where it was assumed that creep effects were negligible and the creep crack growth constants m and q were determined from constant load crack growth tests. In many cases this method produced an excellent prediction of crack growth, as illustrated in Fig. 7.21a, which illustrates fatigue creep prediction for a DCB joint subjected to variable frequency fatigue. It can be seen that assuming creep or fatigue 216 Ian A. Ashcroft, Andrew D. Crocombe 160 Crack length mm Experimental (Variable frequency) 140 Prediction using G and Ct Prediction using G only 120 Prediction using Ct only 100 80 60 40 20 0 5000 10000 Number of cycles 15000 20000 (a) 160 Experimental (trapezoidal) Prediction in term of fatigue-Creep interaction 140 Crack length mm Prediction in term of G and Ct Prediction in term of G 120 Prediction in term of Ct 100 80 60 40 20 0 5000 10000 number of cycles 15000 20000 (b) Fig. 7.21 Crack growth under: (a) variable frequency fatigue at 90◦ C, (b) trapezoidal fatigue at 90◦ C crack growth alone underestimates the crack growth whereas summation of the two components produces a good fit to the data. In some cases, however, simply adding the fatigue and creep components still underestimates the crack growth. In this case a creep-fatigue interaction term can be introduced, as in the equation below (Ashcroft et al. 2005). da = A(Gmax )n + mCtq +CFint. (7.43) dN Where: CFint. = R pf RycC f c 7 Modelling Fatigue in Adhesively Bonded Joints 217 R f and Rc are scalar factors for the cyclic and time dependent components respectively. Rf = (da/dN) (da/dN) + (da/dt)/ f (7.44) Rc = (da/dt) / f (da/dN) + (da/dt)/ f (7.45) p, y and C f c are empirical constants. Figure 7.21b shows the application of the damage partition method with the interaction term for a test with a trapezoidal waveform. The time parameters used to characterize the trapezoidal waveform were: loading time, tr = 0.1 s, hold time, th = 30 s and unloading time, td = 0.1 s. It can be seen that the prediction including the interaction term is closer than that without. 7.3.4 Fatigue Initiation The fatigue crack growth approach is applicable if the fatigue life is dominated by the fatigue propagation phase. However, if the initiation phase is significant then this approach may considerably underestimate the fatigue life, leading to over-designed and inefficient structures. What is desired then is to predict the number of cycles before the macro-crack forms. This can be done empirically in a similar fashion to the stress-life approach, with the number of cycles to fatigue initiation, Ni , being plotted as a function of a suitable stress (or other) parameter rather than cycles to total failure, N f . This is already demonstrated in Fig. 7.7. Lefebvre and Dillard (1999) argued that as initiation tends to occur near interface corners, where the stress field is singular, a stress singularity parameter would make a suitable fatigue initiation criterion. They showed that under certain defined conditions the singular stress, σkl at point A in Fig. 7.22a could be represented by: σkl = Qkl xλ (7.46) where Qkl is a generalised stress intensity factor, dependent on load, and λ is an eigenvalue that can be related to the order of the singularity and is dependent on the wedge angle, φ , in Fig. 7.22a. It was proposed that Ni could be defined in terms of Δ Q (or Qmax ) and λ in a 3D failure map, as illustrated in Fig. 7.22b. Lefebvre and Dillard (1999a) applied this method to bi-material wedge specimens, with the fatigue initiation point being characterised by back-face strain measurements. Quaresimin and Ricotta (2006a) used a similar generalised stress intensity factor to characterise the number of cycles to fatigue initiation in bonded lap joints and proposed that this could be combined with prediction of the crack propagation life, using the techniques discussed in Sect. 7.3.3, to predict the total fatigue life. 218 Fig. 7.22 (a) Singularities in bonded lap joints, (b) 3D Fatigue initiation map (after Lefebvre and Dillard 1999) Ian A. Ashcroft, Andrew D. Crocombe B A Adherend 1 Adhesive Adherend 2 (a) ΔQ λ Log Ni (b) It should be noted that the approach described above is based on the characterisation of an elastic stress field and hence is not applicable in the case of widespread plasticity or creep. Also, only the singularity at position A in Fig. 7.22a was considered in the works referenced above, whereas, failure at position B is more common in bonded lap joints. 7.3.5 Continuum Damage Mechanics Approach Drawbacks to combining the methods described in Sect. 7.3.3 and 7.3.4 to predict the total fatigue life are that: (i) two separate methods need to be implemented, (ii) progressive damage in the initiation phase is not modelled and (iii) the methods are not mechanistically accurate. The damage mechanics approach addresses some of these problems by allowing progressive degradation and failure to be modelled, thus representing both initiation and propagation phases. Continuum damage mechanics (CDM) requires a damage variable, D, to be defined as a measure of the severity of the material damage (Lemaitre 1984, 1985; Kachanov 1986). It is assumed that D is equal to 0 for undamaged material and D = 1 represents the complete rupture of the material. Between those two extremes, there is another critical 7 Modelling Fatigue in Adhesively Bonded Joints 219 value for the damage variable, Dc which characterises the macro crack initiation and is usually between 0.2 and 0.8. The damage variable, D, is difficult to determine physically, since it is almost impossible to monitor all the micro-cracks and voids in a material. However, a simple estimation is usually made using the stiffness degradation: ED (7.47) D = 1− E where E and ED are the Young’s modulus of the undamaged and damaged material, respectively. Once the damage variable is defined, a damage equivalent effective ∗ , can be defined as: stress, σeff ∗ σeff = σ∗ (1 − D) (7.48) where σ ∗ is the damage equivalent stress which is defined as: σ ∗ = σeq 2 (1 + υ ) + 3 (1 − 2 υ ) 3 σH σeq 2 12 (7.49) where σeq is the von Mises equivalent stress, σH is the hydrostatic stress and ‘u’ ∗ can be used as a quasi-static failure criterion. In order to is the Poisson’s ratio. σeff apply the CDM approach to fatigue, Lemaitre (1984, 1985) derived the following equation for the variation of the damage variable per cycle, δ D/δ N: so σH 2 2 (1 + υ ) + 3 (1 − 2 υ ) 2 B0 3 σeq δD βo +1 βo +1 = σ − σ (7.50) eq,max eq,min δN (βo + 1) (1 − D)βo +1 where so , Bo and βo are material and temperature dependent coefficients, σeq,max and σeq,min are maximum and minimum von Mises equivalent stresses in a CA fatigue loading, respectively. Equation (7.50) can be integrated for constant amplitude fatigue loading. Using the boundary conditions (N = 0 → D = 0) and (N = NR [number of cycles to rupture] → D = 1): βo +1 βo +1 −1 (β0 + 1) σeq,max − σeq,min NR = s σH 2 2 (1 + υ ) + 3 (1 − 2 υ ) 2 (βo + 2) β0 3 σeq (7.51) o Abdel Wahab et al. (2001b) used CDM to predict fatigue thresholds in CFRP/epoxy lap-strap joints and double lap joints. They found that the predictions using CDM compared favourably with those using fracture mechanics. The method was extended to predict fatigue damage in bulk adhesive samples (Hilmy et al. 2006) and aluminium/epoxy single lap joints (Hilmy et al. 2007). 220 Ian A. Ashcroft, Andrew D. Crocombe 7.4 Summary and Future Directions It can be seen that a number of techniques have been used to model fatigue in bonded joints. Although none of these have been proven to be generally applicable to the prediction of fatigue behaviour, all are useful in understanding and/or characterising the fatigue response of bonded joints and it is expected that further developments will continue in all the methods described. For instance, the traditional load-life approach is useful in characterising global fatigue behaviour but is of little use in fatigue life prediction and provides no useful information on damage progression in the joint. However, combined with monitoring techniques, such as back-face strain or embedded sensors, and FEA, the method could potentially form the basis of an extremely powerful in-service damage monitoring technique for industry. The fracture mechanics approach is potentially a more flexible tool than the stress-life approach as it allows the progression of cracking to failure to be modelled and can be transferred to different sample geometries. However, problems with the traditional fracture mechanics approach include: selection of initial crack size and crack path, selection of appropriate failure criteria, load history and creep effects. Also the fracture mechanics approach does not accurately represent the accumulation and progression of damage observed experimentally in many cases. However, recent modifications to the standard fracture mechanics method have seen many of these limitations tackled. In future developments it is expected that fatigue studies of bonded joints will continue to increase our knowledge of how fatigue damage forms and progresses in bonded joints and this will feed into the models being developed. In addition to further developments and extension to the approaches described above it is expected that an area for huge potential advances is in the incorporation of damage growth laws into multi-physics finite element analysis models to develop a more mechanistically accurate representation of fatigue in bonded joint than is currently available. It is also hoped that many of the techniques described above will reach sufficient maturity to form the basis of useful tools for industry, both in the initial design and in-service monitoring of bonded joints in structural applications subjected to cyclic loading. References Abdel Wahab MM, Ashcroft IA, Crocombe AD and Shaw SJ (2001) Diffusion of moisture in adhesively bonded joints. 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J Adhes 49: 23–36 Chapter 8 Environmental Degradation Andrew D. Crocombe, Ian A. Ashcroft and Magd M. Abdel Wahab Abstract Environmental degradation is probably the main on-going concern with regard to the long-term integrity of adhesively bonded structures in-service. This chapter begins by outlining why predictive modelling can make such a valuable contribution in this area and then outlines the steps involved in current state of the art environmental degradation modelling of bonded joints. Essentially, this involves three main steps. The first step is modelling moisture transport through the joint in order to determine the moisture concentration distribution through the joint as a function of time. The second step involves evaluation of the transient mechanical-hygro-thermal stress-strain state resulting from the combined effects of hygro-thermal effects and applied loads. The final step involves incorporation of damage processes in order to model the progressive failure of the joint and hence enable the residual strength or lifetime of a joint to be predicted. The approach adopted here is to outline in summary the key theoretical aspects of each of these steps followed by examples showing how they have been implemented in typical bonded joint finite element (FE) analyses. Andrew D. Crocombe Division of Mechanical, Medical and Aerospace Engineering, School of Engineering, University of Surrey, Guildford, GU2 7XH, UK, e-mail: a.crocombe@surrey.ac.uk Ian A. Ashcroft Wolfson School of Mechanical and Manufacturing Engineering, Loughborough University, Loughborough, Leicestershire, LE11 3TU, UK, e-mail: i.a.ashcroft@lboro.ac.uk Magd M. Abdel Wahab Division of Mechanical, Medical and Aerospace Engineering, School of Engineering, University of Surrey, Guildford, GU2 7XH, UK, e-mail: M.Wahab@surrey.ac.uk L.F.M. da Silva, A. Öchsner (eds.), Modeling of Adhesively Bonded Joints, c Springer-Verlag Berlin Heidelberg 2008 225 226 Andrew D. Crocombe et al. 8.1 Introduction Lifetime prediction has been described as the “Holy Grail” of adhesive bonding. This is an indication both of its importance and difficulty. A number of approaches have been used to address this important problem, including the development of accelerated test methods (Davies and Evrard 2007; Bowditch 1996; Ashcroft et al. 2001), research into the fundamental mechanisms of ageing (Buch and Shanahan 2000; Watts and Castle 1984) and the development of empirical and semi-empirical engineering guidelines (Jumbo et al. 2005; Imielinska and Guillaumat 2004). However, the best route to achieving a practical and generally applicable method, that would be useful to industry, would appear to be one based on the incorporation of empirically quantified degradation mechanisms into a mechanical model of the bonded structure, together with the application of a progressive failure model. There are two main challenges to developing an accurate predictive method along these lines. Firstly, accurate modelling of the various effects of ageing on the mechanical model and, secondly, incorporating a failure model that accurately represents not just the final failure load, but the complete cycle of damage initiation and propagation leading to failure. This is the aim of the work presented in this chapter and a schematic of the approach taken is shown in Fig. 8.1. It is generally agreed that the most common cause of environmental degradation in bonded joints involves the absorption of moisture into the joint. This has a number of effects that must be incorporated into the mechanical model, the most important being: Residual strength or service life Failure criteria Bulk Interface DEGRADATION Stress DIFFUSION Softening Load Bulk Interface Manufacture Joint Fig. 8.1 Lifetime prediction framework Moisture 8 Environmental Degradation 227 a. plasticisation of the adhesive (and adherend in some cases), which will affect mechanical properties and the internal stress distribution (Ashcroft et al. 2003; Loh et al. 2005; Abdel Wahab et al. 2002), b. hygroscopic expansion of the adhesive, which will affect residual stresses in the joint (Yu et al. 2006; Liljedahl et al. 2007; Jumbo 2007), c. weakening of the interface by various mechanisms, which will affect failure (Loh et al. 2002a,b; Crocombe et al. 2006). In order to be able to predict the effects cited above, it is first necessary to be able to quantify moisture transport through the joint. The absorbed moisture will cause swelling as well as degradation of the constituent parts and the interface region. This will affect the stresses in the joint and the residual strength (Abdel Wahab et al. 2002). Once both moisture transport and the subsequent degradation processes have been successfully modelled, there is still the critical issue of predicting the residual strength. Traditionally, strength of materials or fracture mechanics methods have been used to predict the failure of bonded joints (Abdel Wahab et al. 2001b). However, both of these approaches have limitations and neither approach can model the evolving initiation and propagation of damage that is a characteristic of failure in many environmentally degraded joints. Owing to these limitations, progressive damage models are being increasingly used to model the behaviour of advanced materials such as structural adhesives. This chapter outlines the key elements discussed above. The next section focuses on modelling the moisture transport. This is followed by a section that addresses the determination of stress and strain in joints with a varying moisture content. The final part of this chapter then outlines how progressive damage modelling techniques can be used in conjunction with the models of the environmentally degraded joints to determine residual strength. Each section begins with a summary of relevant theory and then concludes with examples showing how this can be implemented. 8.2 Modelling Diffusion 8.2.1 Background Moisture transport in structural adhesives is usually governed by Fickian diffusion (Abdel Wahab et al. 2001a). It can be shown that the 1D moisture concentration (c) at a certain distance from the overlap end (x) within an initially dry (c = 0) joint of overlap length L at a time (t) is given by Eq. (8.1), where co is the saturation moisture uptake of the adhesive and D is the diffusion coefficient. Similar but more complex equations are available for 2D and 3D diffusion. ∞ c(x,t) = co − ∑ 0 4co (2 j + 1)π x −(2 j+1)22 Dπ 2 t L ]e sin[ (2 j + 1)π L (8.1) 228 Andrew D. Crocombe et al. This is exactly analogous to heat transfer in a conducting solid and thus is often implemented in FE using thermal elements, where the diffusion coefficient (D) and moisture concentration (c) are modelled using the thermal conductivity and the temperature respectively. Occasionally transport has been shown to be controlled by anomalous forms of Fickian diffusion and various modifications of the simple Fickian model have been used (Loh et al. 2005; Liljedahl et al. 2005). 8.2.2 Application Transient moisture diffusion in aluminium and carbon fibre reinforced polymer (CFRP) single lap joints (SLJ), bonded with Cytec’s toughened epoxy adhesive FM73, have been analysed using both 2D and 3D finite element analyses (FEA) (Jumbo 2007). Figure 8.2 shows a comparison of predicted moisture concentration in the adhesive layer of an aluminium SLJ using 2D and 3D FEA. The plots shown are for the centre of the adhesive layer in the thickness and width directions. Both analyses give similar results in this case because the overlap is smaller than the sample width and hence ignoring moisture transport in the width direction is not significant with regards to the moisture concentration in the middle of the adhesive layer. Figure 8.3 shows the variation in predicted moisture concentration across the width of the adhesive layer at a position halfway along the overlap. It can be seen that the 2D model cannot predict the expected variation across the width. Close to the edge 1 0.8 0.6 0.4 0.2 0 0 2 2D:1 week 3D:1 week 2D:24 weeks 3D:24 weeks 2D:48 weeks 3D:48 weeks 2D:78 weeks 3D:78 weeks 4 6 8 10 Distance along overlap length, mm 12 14 Fig. 8.2 Predicted moisture concentration along the overlap of an aluminium SLJ aged at 50◦ C/95%R.H. using 2D and 3D FEA (Jumbo 2007) 8 Environmental Degradation 229 1 0.8 0.6 0.4 2D:1 week 2D:24 weeks 2D:48 weeks 2D:78 weeks 0.2 0 0 2 3D:1 week 3D:24 weeks 3D:48 weeks 3D:78 weeks 4 6 8 10 Distance across overlap width, mm 12 14 Fig. 8.3 Predicted moisture concentration across the width of an aluminium SLJ aged at 50◦ C/95%R.H. using 2D and 3D FEA (Jumbo 2007) of the sample it can be seen that the 3D model predicts significantly higher moisture concentrations. The moisture concentration levels for 2D and 3D FEA in the CFRP SLJs follow a similar pattern but saturate more quickly than the aluminium SLJ because of the added effect of moisture transport through the adherend. 8.3 Modelling Stress and Strain 8.3.1 Background Stresses in a bonded joint can be broadly categorised as either mechanical stresses or residual stresses. Mechanical stresses are those arising from mechanical loads whereas residual stresses are those remaining when the mechanical loads are removed. In a bonded joint, three main sources of residual stresses can be identified. These are; changes in temperature, leading to thermal stresses (Yu et al. 2006; Apalak et al. 2007, Jumbo et al. 2007); (see Chapter 9) changes in moisture content, leading to hygroscopic stresses (Yu et al. 2006; Khoshbakht et al. 2006; Jumbo 2007) and changes due to chemical reactions, leading to curing stresses (Zarnik et al. 2004; Macon 2001). The curing stresses in typical adhesively bonded joints are small compared with the thermal and hygroscopic stresses, and in any case can be incorporated into analysis of the thermal stresses once the stress-free temperature has been determined. In bonded joints there may be significant residual thermal stresses 230 Andrew D. Crocombe et al. from the curing operation followed by modification of these stresses as moisture is absorbed. The combined stresses are termed hygro-thermal stresses (Jumbo et al. 2005; Yi and Sze 1998). These residual stresses are generally modelled in a similar way. In fact it is more accurate to refer to this effect as residual strains as this is what is induced by the temperature and the moisture. The stresses are only generated when these strains are not allowed to develop fully. The residual strains are modelled using expressions similar to those in Eqs. (8.2) and (8.3) for thermal and hygroscopic induce strains respectively. εth = αth (ΔT ) (8.2) εhy = αhy (Δc) (8.3) The parameter αhy is known as the swelling coefficient and this has been measured and reported for various adhesive systems (Loh et al. 2005; Liljedahl et al. 2005). These strains can then be incorporated into the adhesive constitutive equations as: [σ ] = [D][ε − εth − εhy ] (8.4) If only one form of residual strain is being modelled then it is possible to use the thermal strain capability that almost all FE codes have. If both forms are to be modelled then some codes (such as ABAQUS) have user routines where coefficients of expansion can be defined. In both cases it will be necessary to run coupled analyses, where the output from one analysis (thermal or moisture) forms the input to another (stress). In addition to these forms of residual stress it may also be necessary to model the change in adhesive material response (plasticisation) caused by the absorbed moisture. This is most easily done by utilising the field dependent material property facility that many FE codes have. Adhesive material properties such as modulus, yield stress and post-yield flow can be defined as a function of a field variable, such as temperature or moisture. Many adhesives exhibit a distinct degradation in these material properties with increasing moisture content (Liljedahl et al. 2006a; Crocombe et al. 2006; Hua et al. 2006). 8.3.2 Application A two step 3D FEA method has been used to model hygro-thermal stresses in the joints discussed in Sect. 8.2 (Jumbo 2007). The first step was a thermal residual stress analysis from the curing temperature to the environmental conditioning temperature (50◦ C) and the second step was a non-linear, coupled stress-diffusion analysis to simulate swelling due to moisture adsorption and the effect of moisture dependent material properties. The effects of moisture ingress in the aluminium SLJ on the hygro-thermal residual stresses are shown in Fig. 8.4. For the stresses at the edge of the joint, shown in Fig. 8.4a, the swelling due to moisture ingress, together 8 Environmental Degradation 231 12 Maximum Principal Stress, MPa 10 8 6 4 Dry 1 week 12 weeks 2 24 weeks 48 weeks 0 0 2 4 6 8 10 Distance along overlap length, mm (a) 12 14 14 Maximum Principal Stress, MPa 12 10 8 Dry 6 1 week 12 weeks 4 24 weeks 2 48 weeks 0 0 2 4 6 8 10 Distance along overlap length, mm (b) 12 14 Fig. 8.4 Hygro-thermal stresses in aluminium SLJ aged at 50◦ C/95%R.H. (a) Sample edge and (b) sample centre (Jumbo 2007) 232 Andrew D. Crocombe et al. with plasticisation of the adhesive, has a significant stress reducing effect during the first week. After this the stresses increase slightly due to further swelling of the adhesive, but remain substantially lower than in the dry adhesive. The stress distribution in the middle of the adhesive is rather different from the edge, as shown in Fig. 8.4b. After 1 week, the stresses at 2–3 mm from the overlap ends are higher than for the dry case. This is because the tensile modulus is higher in this area than at the overlap end, and thus load transfer is shifted from the fillet to the inner region. This trend continues as moisture continues to be absorbed, with the highest stresses in the drier areas in the centre of the joint. As the entire adhesive layer becomes saturated, the stresses become more uniformly distributed, although at a significantly lower level than in the dry adhesive. The effects of mechanical loading on the hygro-thermal stress state was investigated by applying a 6 kN load to the aluminium/FM73 single lap joints. In this case the stresses shown are indicative of those just before significant damage in the joint, which would cause a re-distribution of the stresses. Figure 8.5 shows the von Mises stresses in the adhesive layer at 50◦ C with mechanical, mechanical + thermal and mechanical + hygro-thermal loads at full saturation. It is clear that at the edge and middle of the joint, combined environmental and mechanical loading increases the stress in the adhesive. 8.4 Modelling Damage and Failure 8.4.1 Background Two different forms of progressive damage modelling have generally been used; cohesive zone modelling (CZM), where the failure is localised along a plane (Loh et al. 2003; Liljedahl et al. 2006b) and continuum damage modelling (CDM), where the failure can occur throughout the material (Hua et al. 2007). Potential sites for damage modelling include the adhesive, the interface and the adherend. The CZM approach is more directly applicable to interfacial failure and certain forms of adherend failure whilst the CDM is more relevant to failure in the adhesive. Both are illustrated in Fig. 8.6. The CZM is implemented via a zero volume element where the traction between two nodes follows the curve shown in Fig. 8.6a. Initially, the nodes are held together with minimal separation until the traction reaches a critical value (σU ). Following this, the nodes separate and unload, absorbing energy as they deform. When sufficient CZM elements are used, in conjunction with elastic material properties, a linear fracture mechanics response will be obtained. However the advantage of the CZM approach is that crack formation and propagation will be modelled in a single evolving analysis. The continuum failure model is based on a full non-linear stress strain curve. The onset and development of damage degrades the undamaged non-linear response to a state of complete failure, as can be seen in Fig. 8.6b. It is necessary to define 8 Environmental Degradation 233 40 35 Von Mises Stress, MPa 30 25 20 15 10 6 kN Load 5 6 kN Load + Thermal Load 6 kN Load + HygroThermal Load 0 0 2 4 6 8 10 12 10 12 Distance along the overlap, mm (a) 35 Von Mises Stress, MPa 30 25 20 15 10 6 kN Load 5 6 kN Load + Thermal Load 6 kN Load + HygroThermal Load 0 0 2 4 6 8 Distance along the overlap [mm] (b) Fig. 8.5 Development of hygro-thermo-mechanical stress in aluminium SLJ aged at 50◦ C/95%R.H. (a) Sample edge and (b) sample centre (Jumbo 2007) 234 σu Andrew D. Crocombe et al. σ (MPa) σ d' c b o (kJm–2) δ (mm) δr (a) d a δp (b) Fig. 8.6 (a) Cohesive zone model (CZM) and (b) continuum damage model (CDM) damage in terms of an equivalent plastic displacement in order to achieve mesh independence. To do this a characteristic length is required for each element and this is used in conjunction with the element plastic strain to determine the equivalent plastic displacement. CZM and CDM are treated in detail in Chap. 6. 8.4.2 Application The aluminium and CFRP lap joints discussed above, bonded with either FM73 film adhesive or Hysol’s EA9321 paste adhesive have been aged and tested (Hua et al. 2006; Liljedahl et al. 2007; Jumbo 2007). The testing indicated that the joints bonded with FM73 tended to be controlled by interfacial failure whilst those bonded with EA9321 tended to experience cohesive failure in the adhesive. Thus CZM elements were used with the FM73 joints and CDM was used with the EA9321 joints. The failure parameters for both models were moisture dependent and were determined from independent tests before being applied to either the lap joints (discussed above) or to more complex joints, more representative of those seen in typical aerospace applications. The application of each damage modelling technique is discussed separately below. 8.4.2.1 Continuum Damage Modelling (Adhesive EA9321) Mixed mode flexure (MMF) specimens bonded with EA9321 were aged in various environments to produce three different levels of moisture concentration in the adhesive layer. These joints were tested to failure and the structural response recorded. Finite element analyses incorporating moisture dependent stress-strain data and failure parameters were then undertaken and the failure parameters were chosen by matching with the experimental data. These failure parameters were then used to predict the residual strength of both composite and aluminium single lap joints (SLJ) that had been exposed for various durations in two different ageing environments. Unlike the MMF joints, where the moisture concentration was constant (and 8 Environmental Degradation 235 known) over the entire overlap region, the moisture distribution in the SLJ’s was non-uniform, being largest around the periphery of the joint and smallest in the centre, as illustrated in Figs. 8.2 and 8.3. As shown in Fig. 8.1, the failure modelling is a two-stage process; the first stage determining the moisture distribution and the second implementing the failure analysis using moisture dependent material data and failure parameters. As discussed above, in order to model the moisture diffusing from all edges it is necessary to undertake three-dimensional analyses. Figure 8.7 shows one of the 3D FE models and a typical moisture distribution. When modelling the composite joint the moisture diffusion through the composite, as well as the adhesive, was included. The second stage (failure modelling) of the analysis was then undertaken, using the moisture distribution results from the first stage as part of the input parameters. In the wet joints the failure depends on both the level of strain and the moisture content in the adhesive. The sequence of failure in a typical wet joint is illustrated in consecutive plots in Fig. 8.8. Failure appears to initiate in the fillet region at the corner of the joint where the adhesive has the highest moisture content and experiences large stress and strains, as shown in Fig. 8.8. Failure then progresses through the overlap region with a faster evolution across it (3 directions) than along it (1 direction). This two-stage modelling is repeated for both joints for all exposure times, providing predicted residual strengths. For illustration, the data for the aluminium SLJs are shown in Fig. 8.9, along with the experimental data. The correlation between the two is very good. A more detailed account of this and similar work can be found in Hua et al. (2008). Fig. 8.7 3D FE model and moisture distribution 236 Andrew D. Crocombe et al. Fig. 8.8 Failure propagation through the adhesive (failed elements shown in white and centre of the overlap region is the bottom left corner) 8.4.2.2 Cohesive Zone Modelling (Adhesive FM73) The CZM failure parameters were determined by matching the measured response of mixed mode flexure (MMF) specimens bonded with FM73 and exposed to three levels of moisture concentration. It was necessary to include measured moisture dependent non-linear adhesive stress-strain behaviour with the CZM to be able to match the entire MMF loading response. An excellent match to the entire load response of the MMF specimens can be seen in Fig. 8.10. These same moisture-dependent failure parameters were then used to model failure in the various forms of lap joint bonded with FM73. Coupled stress-diffusion analyses incorporating progressive failure along the interface were undertaken. The progressive failure is illustrated in Fig. 8.11, which shows a partially failed joint. The crack initiated at the embedded substrate corner and propagated into the fillet and then along the overlap. The predicted and measured residual strengths for some of the FM73 lap joints tested are shown in Fig. 8.12 and the excellent correlation between the two is evident. The aluminium joints were aged in a range of ageing environments and this revealed two different degradation mechanisms. Joints exposed in water vapour or by immersion in de-ionised water exhibited a thermodynamic type displacement between the adhesive and aluminium at the interface whilst joints aged in Joint strength, kN 10 8 6 4 Predicted Experimental 2 0 0 10 20 Exposure time, wk 30 Fig. 8.9 Predicted and experimental residual strengths for the aluminium SLJs 8 Environmental Degradation 237 1200 Dry 1000 80%RH Load (N) 800 600 96%RH 400 200 Simulation 0 0 0.5 1 1.5 2 2.5 Displacement (mm) 3 3.5 4 Fig. 8.10 Comparison of measured and predicted environmentally degraded MMF joint response tap water (which had a much higher conductance) exhibited a more rapid degradation, driven by cathodic delamination (Liljedahl et al. 2006a). The predictive modelling described so far has focused on the former whilst modelling of the cathodic delamination is introduced in the context of the “L joints” described in the next section. As a final test of the predictive modelling a series of representative “model” element joints were tested. One of these was an aluminium L joint bonded with FM73 adhesive. The same failure parameters that were determined from the MMF joints and subsequently applied to the lap joints were used in this modelling, thus establishing the universality of the failure parameters and the modelling approach. The predicted and experimental residual strengths are shown in Fig. 8.13. It can be seen Fig. 8.11 Damage propagating through the aluminium single lap joint 238 Andrew D. Crocombe et al. 13 Residual strength, kN Fig. 8.12 Measured and predicted residual strengths for FM73 lap joints CFRP exp CFRP pred Al 95%RH exp Al 95%RH pred AL water exp Al water pred 12 11 10 9 8 7 6 0 5 10 15 20 Exposure, wk 25 30 that the modelling approach based on thermodynamic displacement underestimated the degradation at longer exposure times. Examination of the failed specimens exposed for 32 weeks revealed evidence of the faster cathodic delamination mentioned in the discussion of the lap joints above. In such a process a crack forms on the exposed interface and this accelerates the supply of water to the crack tip. A modelling procedure has also been developed for this mechanism and it can be seen in Fig. 8.13 that the correlation with the experimental data is significantly better. It should be noted that the predictive model correlated closely with not only the residual strength but the entire loading response. This is illustrated in Fig. 8.14a where both predictions and experimental data show a controlled progressive unloading before sudden catastrophic failure. The mismatch in the initial stiffness is because the experimental data includes the displacement in the loading train as well as the L joint. Figure 8.14b,c show clearly that the predicted and experimental crack fronts are curved and more advanced at the centre of the joint. Other work using a similar approach can be found in Loh et al. (2003). Residual strength, kN 2.5 Expt Pred (therm displ) Pred (cath delam) 2 1.5 1 0 5 10 15 20 Exposure, wk 25 30 Fig. 8.13 Measured and predicted FM73 L joint strengths 35 8 Environmental Degradation 239 Prediction Expl 2500 Load (N) 2000 1500 1000 500 0 0.5 1 1.5 Displacement (mm) (a) 2 2.5 centre 0 toe (b) (c) Fig. 8.14 (a) Load-displacement response, (b) measured and (c) predicted crack front shapes 8.5 Summary and Future Directions This chapter has outlined the current state of the art in modelling the environmental degradation in bonded joints. This has been achieved by outlining relevant theory and then illustrating how this can be implemented in the context of aged adhesively bonded joints. The process outlined involves coupling between four different types of analysis; moisture, temperature, stress and damage. It was shown that when used appropriately, good predictions of residual strength following long term exposure can be obtained. At the time of writing, such a modelling approach has only been applied to joints that have been subjected to constant ageing conditions. The next step of the process will be to develop modelling techniques that are applicable to the more realistic 240 Andrew D. Crocombe et al. scenario of ageing under fluctuating conditions. This will involve considering, determining and modelling the reversibility of the ageing processes. A further step from here will be to combine the damage modelling from fluctuating environmental conditions with those from fluctuating loads (constant and variable amplitude fatigue-fatigue). 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Sensor Actuat A-Phys 116: 442–449 Chapter 9 Non-Linear Thermal Stresses in Adhesive Joints Mustafa Kemal K. Apalak Abstract Adhesive joints serve under thermal loads as well as structural loads. The different thermo-mechanical properties of the adhesive and adherend materials cause incompatible thermal strains along the adhesive and adherend interfaces. Consequently, nonuniform thermal stress distributions are observed in the adhesive joints. In case the adhesive joints are constrained, these thermal stresses become more evident even for a uniform temperature distribution. In practice the adhesive joints interact with fluids (air) with different temperature and velocity and experience conductive and convective heat transfers. The variable thermal boundary conditions introduce a new non-linearity in addition to the geometrical and material non-linearities which are observed in adhesive joints. The transient temperature distributions can be obtained by solving the energy equation under the thermal boundary conditions. The corresponding thermal strain and stress distributions can be calculated using the transient temperature distributions. The large displacement and rotations occurring in adhesive joints require the implementation of the small strain-large displacement theory to the elastic stress analysis. This study introduces a simple method for calculating the heat transfer coefficients between the fluid and adhesive joints and explains the implementation of the finite element method to the thermal analysis and the geometrical nonlinear stress analysis. The thermal stresses in the metal-metal adhesive single lap, tubular, metal-metal and composite tee joints were analysed for the variable thermal and specified structural boundary conditions. The variable thermal boundary conditions cause non-uniform temperature distributions through the adhesive lap joints; consequently, non-uniform thermal strain and stress distributions occur. The adherend and adhesive regions in the neighborhood of the adhesive-adherend interfaces were subjected to high stress concentrations. Mustafa Kemal Apalak Department of Mechanical Engineering, Erciyes University, Kayseri 38039, Turkey, e-mail: apalakmk@erciyes.edu.tr L.F.M. da Silva, A. Öchsner (eds.), Modeling of Adhesively Bonded Joints, c Springer-Verlag Berlin Heidelberg 2008 243 244 Mustafa K. Apalak 9.1 Introduction Today’s adhesive agents are suitable to the high static and dynamic loadings in engineering designs. Metal and composite adherends can be joined successfully using the adhesive bonding technique. A reasonable joint strength can be achieved with a suitable adhesive selection and a well-designed adhesive joint for certain loading conditions. In order to understand the adhesion mechanism, the stress and deformation states of the adhesive joints and to predict the mechanical properties of different adhesives the single- or double lap, tubular and butt joints, were widely used as simple test configurations. The present analytical and experimental studies consider only the adhesive layer, or the adhesive and metal or composite adherends as an elastic, elasto-plastic or visco-elastic media. The axial or torsional loadings on the adhesive joints cause stress and strain concentrations around their adhesive free ends due to the geometrical discontinuities and mechanical mismatches of the adhesive layer and adherends. This is known as the edge effect, which can be relieved by modifying the adherend edges [4, 38]. The analytical studies assume the adhesive free ends to be square in order to simplify the mathematical models; however, some amount of adhesive (spew fillet) accumulates around the adhesive free ends due to the pressure applied to the adherends. The shape and sizes of the adhesive spew fillets play an important role in the stress concentrations around the adhesive free ends as well as the rounded adherend corners due to etching process of the adherends [4, 38]. Two types of non-linearities, i.e. geometrical and material, affect stress and deformation states of adhesive joints considerably. The material non-linearity is due to the nonlinear behavior of the adhesive and adherend materials. However, the geometrical non-linearity may arise in case of the joint geometry causing large displacements and rotations when the strains are small. The bending moment occurs due to the load eccentricity and to the adherend deformations of a single lap joint as the load is applied, and the dependence of the moment on the applied load makes the problem geometrically non-linear [53]. Adams [3], and Harris and Adams [30] analyzed the failure modes and loads of single lap joints with adherends and adhesives with different mechanical properties under a tensile load considering the geometrical and material non-linearities. Adams et al. [5] also investigated the shear and transverse tensile stresses in carbon fiber reinforced plastic/steel double lap joints using an elastic-plastic model for the rubber-modified epoxy adhesive. They showed significant increases in the joint strength could be achieved by modifying the local geometry of the critical zones at the edges of the overlap region of the double lap joint. Adams and Harris [6] also investigated the influence of local geometry changes at the adhesive free edges in single lap joints considering material and geometrical non-linearities, and showed that significant increases in the joint strength could be achieved by filleting the adhesive at the free edges of the adhesive layer. Reddy and Roy [49] showed that the large displacement gradients affected the adhesive stresses at the ends of the overlap region of a single lap joint under different loading and boundary conditions. Edlund and Klarbring [28] presented a 3D general analysis method for determining the adhesive and adherend stresses and 9 Non-Linear Thermal Stresses in Adhesive Joints 245 deformations of adhesively bonded joints considering the geometrical nonlinearity. Recently, Andruet et al. [8] developed two and three dimensional finite elements for the geometrical non-linear stress analysis of an adhesively bonded lap joint, and showed that the geometrical non-linearity (the large displacements) affected considerably the peak adhesive stresses. Apalak and Engin [10] applied the small strainlarge displacement theory to an adhesively bonded double containment corner joint using the incremental finite element method, and showed that the small strain-small displacement theory was misleading in predicting the stress and deformation states of adhesive joints for some loading and boundary conditions. Apalak [11, 12, 13, 14] also showed that the geometrical non-linearity had a considerable effect on the stress distributions in the adherends and adhesive layer of different types of corner and tee joints. In practice, adhesive joints also experience thermal loads. A uniform temperature distribution results in a uniform thermal strain distribution in a unconstrained single material; in contrast, a non-uniform temperature distribution causes a single material to have a non-uniform thermal strain distribution. In this case, a single material also experiences thermal stresses due to this non-uniform temperature distribution. The different mechanical and thermal properties of the adhesive and adherends result in a non-uniform temperature distribution. The thermal strains become incompatible along the bi-material interfaces whereas the interfacial total strains are compatible. Therefore, these non-uniform strain distributions are also main reason of non-uniform thermal stress distributions through the adhesive joint and they can peak near the adhesive-adherend interfaces. However, the thermal stress and strain distributions are completely dependent on the thermal boundary conditions of adhesive joints. The present thermal stress analyses of adhesive joints concentrate on (i) the prediction of failure modes of the adhesive layer considering residual stresses induced by fabrication [36, 37, 42, 50], (ii) thermal stress singularities at the adherend corners for wedge angles of a bi-material system [33], (iii) steady state or transient thermal stresses along the peripheries of adhesive defects, i.e. holes or fillers inserted into the adhesive layer or near the adhesive-adherend interfaces [47, 48], (iv) transient thermal stress distributions in the adhesive joints for different thermal expansion coefficients and Young’s modulus ratios of adherends and adhesive [35], and (v) effect of the adhesive surface geometry on the thermal stress fields [1]. The residual thermal stresses induced by fabrication affect failure modes of the adhesive layer in lap joints [42]. Kim and co-workers [36, 37] presented a failure model for the stresses occurring in a tubular lap joint considering the non-linear adhesive properties and thermal residual stresses due to the fabrication. Reedy and Guess [50] showed that the effect of the residual stresses in an adhesive butt joint generated by cooling on the joint strength could be much smaller than would be predicted by a linear analysis. Thus, the peak adhesive stresses in the yield zone at the interface corner could decay significantly when given sufficient time. Ioka et al. [33] studied thermal residual stress distributions at the interface and around the intersections of the interface and the free surfaces of bonded dissimilar materials and found that the thermal stress singularity disappears for a certain range of wedge angles of a pair of materials. Nakano et al. [48] carried out a thermal 246 Mustafa K. Apalak stress analysis of an adhesive butt joint containing circular holes and rigid fillers in its adhesive layer and subjected to a non-uniform temperature field. They showed that the size and location of the circular holes and rigid fillers had an evident effect on the thermal stresses at the interface and at the hole and filler peripheries. Nagakawa et al. [47] investigated thermal stress distributions in an adhesive butt joint containing some hole defects under uniform temperature changes. The thermal stresses around hole defects located near the centre of the adhesive were larger than those around the hole defects located near the free surface of the adhesive. Katsuo et al. [35] carried out transient thermal stress analysis of an adhesive butt joint assuming that the upper and lower end surfaces of the joint were in different temperatures at a certain instant. The thermal expansion coefficient and Young’s modulus ratios of the adhesive and adherends had evident effects on the transient thermal stress distribution. Abedian and Szyszkowski [1] investigated the effects of surface geometry of composites on the thermal stress distributions. The stress state in the composite at and near the free surface was very sensitive to the geometric features of the surface: thus, an ideally flat free surface resulted in large stress concentrations whereas these stresses decreased substantially in case the difference between the fibre and the matrix heights was filled with the matrix material. Anifantis et al. [9] investigated steady state thermal stress and strain concentrations in unidirectional fibre reinforced composites considering the concept of an inhomogeneous interphase between the fibre and matrix phases. In the study the stresses had stronger discontinuities than the strains, exhibiting a high sensitivity to temperature changes and the location of peak stress was independent of the degree of adhesion developed between fibre and matrix while strains were slightly dependent. Inhomogeneous temperature distributions or transient thermal loads might increase these phenomena drastically. Cho et al. [24] studied the effect of curing temperature on the adhesion strength of polyamideimide/copper joints and showed the adhesion strength decreased as the thermal stress increased with the increase of both curing temperature and time. Humfeld and Dillard [32] investigated thermal cycling effects on the residual stresses in viscoelastic polymeric materials bonded to stiff elastic substrates. The residual stresses incrementally shifted over time when subjected to thermal cycling, and damaging tensile axial and peel stresses developed over time due to viscoelastic response to thermal stresses induced in the polymeric layer. In general, these studies assume that a steady-state conductive heat transfer occurred through the adhesive joint under a specific thermal condition; thus, a constant temperature along the outer surfaces of the adhesive joint was imposed. Therefore, a uniform temperature distribution was obtained through the adhesive joint and the residual strain distributions were found around the adhesive free ends as a result of thermal stress analyses based on the small strain-small displacement theory. The effects of the geometrical and material non-linearities, and the presence of the adhesive fillets were not considered. However, in practice the adhesive joints usually interact with a moving fluid at a variable or constant temperature and velocity. As a result, the heat transfer by convection occurs between the fluid and the adherends and adhesive layer whereas it occurs by conduction through the adhesive joint. The heat transfer coefficient between the fluid and adherend or adhesive material, which 9 Non-Linear Thermal Stresses in Adhesive Joints 247 evidently affects the convective heat transfer, is completely dependent on the velocity, temperature-dependent properties, and the flow direction of the fluid with respect to plate or adhesive surface. This is the third type of (thermal) nonlinearity due to variable thermal boundary conditions, which affect considerably thermal strain and stress distributions as well as the temperature distributions in the adhesive joint. Apalak and co-workers [15, 17] investigated thermal stresses in adhesive single lap and tubular lap joints taking into account both the convective and conductive heat transfers, and the large displacement and rotation effects under variable thermal boundary conditions and for different adherend end conditions. They showed that variable thermal boundary conditions caused non-uniform temperature distributions through the adhesive lap joints; consequently, non-uniform thermal strain and stress distributions occurred. The adherend and adhesive regions in the neighborhood of the adhesive-adherend interfaces were subjected to high stress distributions. Finally, a full knowledge of the thermal stress-deformation states of adhesive joints would allow us to design adhesive joints that can withstand the peak adhesive stresses. 9.2 Small Strain-Large Displacement Theory The displacements and their gradients are assumed to be infinitesimal in the small strain-small displacement theory, and the current configuration of a body is compared with its initial state. The components of the unit relative displacement vector are defined as ∂ ui dX j dui = (9.1) dS ∂ X j dS where dX is an arbitrary infinitesimal line vector in the initial position. The small strain tensor is 1 ∂ ui ∂ u j εi j = + (9.2) 2 ∂ x j ∂ xi and the rotation tensor is Ωi j = 1 2 ∂ ui ∂ u j − ∂ x j ∂ xi (9.3) respectively. The large displacement-gradient components make the strain to be characterized from the initial state more difficult than in the small-strain case. Lagrangian formulation allows the finite-strain to be defined based on the material coordinates in the undeformed configuration. The deformation equations for the movement of a particle from its initial position X to the current position x are given as x = x(X,t) or xi = xi (X1 , X2 , X3 ,t) (9.4) An arbitrary infinitesimal material vector dX at X can be associated with a vector dx at x as follows 248 Mustafa K. Apalak dx = F · dX = dX · FT (9.5) using the deformation gradient vector ← F=x∇ (9.6) In terms of the strain tensor the change in the squared length of the material vector dX is given as follows (ds)2 − (dS)2 = 2 dX · E · dX (9.7) (ds)2 − (dS)2 = 2 dXI EIJ dXJ (9.8) or 2 The new squared length (ds) of the element is written in terms of the Green deformation tensor C referred to the undeformed configuration as follows (ds)2 = dX · C · dX (9.9) (ds)2 = dXI CIJ dXJ (9.10) or Comparison of Eqs. (9.7) and (9.9) gives the relationship between the strain tensor E and the Green deformation tensor C 2 E = C−1 (9.11) or 2 EIJ = CIJ − δIJ (9.12) 2 where δIJ is Kronecker delta. The new squared length (ds) of the element is written using the deformation gradient tensor as follows (ds)2 = dx · dx = dX · FT · (F · dX) = dX · FT · F · dX (9.13) Comparison of Eqs. (9.9) and (9.13) shows that the Green deformation tensor C = FT · F or CIJ = (9.14) ∂ xk ∂ xk ∂ XI ∂ XJ (9.15) From Eq. (9.11) the strain tensor becomes E= or 1 EIJ = 2 1 T F ·F−1 2 ∂ xk ∂ xk − δIJ ∂ XI ∂ XJ (9.16) (9.17) 9 Non-Linear Thermal Stresses in Adhesive Joints 249 Using the same reference axes for both xi and Xi , and using lower-case subscripts for both, we have (9.18) xi = Xi + ui with displacement components ui = ui (X1 , X2 , X3 ,t) (9.19) In terms of the displacements, the general expression for Ei j in Eq. (9.17) takes the form 1 ∂ ui ∂ u j ∂ uk ∂ uk Ei j = + + (9.20) 2 ∂ X j ∂ Xi ∂ Xi ∂ X j When Eqs. (9.2) and (9.20) are compared it is evident that the large displacement theory is an extension of the small displacement theory since it includes the squares of the displacement gradients. In case the displacement gradients are not small compared to unity, the large displacement theory should be used in order to consider their non-linear effects on the stress and deformation states of the structures [46, 52]. 9.3 Non-linear Equilibrium Equations In order to establish the non-linear equilibrium equation for the deformed body subjected to the external loads, the virtual internal and external works done on the body are equated. The non-linear equilibrium equation from the virtual-work equation given in terms of the Lagrangian coordinate system is given as [26, 39, 57, 59] δ ET σ dV = ≈ V ρ δ uT q dV + V δ uT qo dA (9.21) A where the external work is due to the virtual displacements δ u acting on the surface tractions, extending over the initial undeformed surface and given by qo = qo1 qo2 qo3 T (9.22) and the body forces per unit mass, acting within the undeformed volume V, given by q = q1 q2 q3 T (9.23) ρ being the density of the undeformed body. The total Lagrangian virtual work Eq. (9.21) can be approximated by the finite element idealization as follows δ pT BT σ dV = δ pT ≈ V V ρ NT q dV + δ pT NT qo dA A (9.24) 250 Mustafa K. Apalak where σ is stress tensor. Since the virtual nodal displacements δ p are arbitrary, ≈ Eq. (9.24) can be written as BT σ dV = ≈ V ρ NT q dV + V NT qo dA (9.25) A where N is a shape function array whose coefficients are functions of the initial position x within the element included in the expression of displacement within an element u=Np (9.26) where the nodal displacement vector p = u1 u2 · · · un T (9.27) and the strain matrix B = B0 + BL (9.28) where B0 is the linear strain matrix being a function of the shape functions only, while BL is the non-linear strain matrix being a function of the shape functions and displacements. The components of Green’s strain vector can be written as 1 E = B0 + BL p (9.29) 2 in terms of the linear and non-linear Green’s strain vectors E0 = B0 p (9.30) and 1 EL = BL p 2 The non-linear equilibrium Eq. (9.25) can be written as ψ (p) = BT σ dV − R = w − R = 0 ≈ (9.31) (9.32) V where R is the right hand side of Eq. (9.25) for convenience and ψ (p) is termed the residual. The Newton-Raphson method is used for the solution of the assembled non-linear equations. The solution is achieved when ψ (p) is reduced to zero or a given convergence criterion is satisfied [26, 39, 57, 59]. In case the body is subjected to initial thermal strains the stress tensor becomes σ = D E − Eth ≈ where D is stiffness matrix and Eth is thermal strain tensor. (9.33) 9 Non-Linear Thermal Stresses in Adhesive Joints 251 9.4 Thermal Model and Finite Element Formulation Application of the first law of thermodynamics to a differential control volume yields ... ∂T T + v ∇T = q + ∇ (D∇T ) ρc (9.34) ∂t with the Fourier’s law q = −D∇T (9.35) where vT = ...vx , vy , vz is the velocity vector for mass transport of heat, q is the heat flux vector, q is the heat generation rate per unit volume, and D is the conductivity matrix. The present problems assume that the adhesive joint is subjected to the specified convection surfaces (Newton’s law of cooling) as q · n = −hm (T∞ − TS ) (9.36) nT D∇T = hm (T∞ − T ) (9.37) where n is the unit outward normal vector, hm is the film coefficient, T∞ is the bulk temperature of the adjacent fluid and TS is the temperature at the surface of the model. Pre-multiplying Eq. (9.34) by a virtual change in temperature δ T , integrating over the volume of the element, and combining with Eq. (9.35) yield ∂T + vT LT + LT δ T (DLT ) dV ρ cδ T ∂t V = δ T hm (T∞ − T ) dS + ... δ T q dV (9.38) V S where LT = ∂ ∂ ∂ ∂x ∂y ∂z (9.39) is a vector operator. The temperature is dependent on both space and time. Therefore, the temperature can be written in terms of element shape functions N and nodal temperature vector Te as (9.40) T = NT Te and the time derivatives of Eq. (9.40) may be written as ∂T ∂ Te = NT = NT Ṫe ∂t ∂t (9.41) δ T and LT also become δ T = {δ Te }T N and LT = BTe (9.42) 252 Mustafa K. Apalak where B = LNT . The variational form of Eq. (9.38) can be written as ρ c {δ Te }T N NT Ṫe dV + V + ρ c {δ Te }T N vT BTe dV V T {δ Te } B DBTe dV = V + {δ Te }T N hm T∞ − NT Te dS T S ... {δ Te } N q dV T (9.43) V If ρ is assumed to remain constant over the volume of the element, and {δ Te }T is dropped, Eq. (9.43) is reduced to the final form as [59] ρ cN NT Ṫe dV + ρ V = S cN vT BTe dV + V T∞ hm N dS − BT DBTe dV V T hm N N Te dS + ... N q dV (9.44) V S 9.5 Thermal Boundary Conditions The previous studies prescribe the final temperature distributions along the boundary of the adhesive joints and in the adhesive joints and then compute the thermal strains using the temperature differences relative to the initial uniform joint temperature [1, 9, 24, 32, 33, 35, 36, 37, 42, 47, 48, 50]. In fact, the materials forming the adhesive joints have different heat conduction/convection capabilities. Therefore, the heat transfer through the adhesive joint members should be analysed in detail for the thermal conditions allowing different heat transfer mechanisms. The heat transfer through the adhesive joint occurs by means of the convection (from fluid to adherends or adhesive), and the conduction (through adherends and adhesive). The heat transfer by convection requires the computation of the heat transfer coefficients between the air and the adherends or the adhesive. Their computations are dependent on how the air flows along the surfaces (vertically or horizontally). Since each surface has different geometry and especially flow conditions, the heat transfer coefficients should be computed for each surface, as follows. In case of a vertical air flow, the heat transfer coefficient is given as [34]; U∞ Deqv 0.731 λair (9.45) hm = 0.205 ν Deqv where U∞ is the air velocity (m/s), Deqv the equivalent diameter (m), ν the kinematic the thermal conductivity of the air (W/m◦ C). In case of a viscosity (m2 /s) and λair horizontal air flow, the heat transfer coefficient is given as [34]: hm = Nu λ L (9.46) 9 Non-Linear Thermal Stresses in Adhesive Joints 253 where λ is the thermal conductivity of the air (kcal/mh◦ C), L is the plate length (m) and Nu Nusselt number defined as Nu = 0.836 · Re1/2 · Pr1/3 (9.47) where Re and Pr are Reynolds and Prandtl numbers, respectively and are described as; U∞ L (9.48) Re = ν cp μ (9.49) Pr = λ where c p is the specific heat (kcal/kg◦ C) and μ the dynamic viscosity (kg/ms). The previous coefficients describing the air properties are values based on an average temperature as follows T∞ + T0 (9.50) Tf = 2 where T∞ and T0 are the air and the plate temperatures, respectively. The thermal coefficients of the air and the heat transfer coefficients are given in [15, 17]. 9.6 Single Lap and Tubular Lap Joints In general the thermal stress and strain distributions in adhesive joints were analysed assuming that the adherends and adhesive layer were subjected to a uniform temperature distribution or the temperature distribution along the boundaries of the adhesive joint was prescribed. The conductive heat transfer through the adhesive joint as well as the convective heat transfer between the adhesive joint and the surrounding fluid were ignored. Therefore, the transient temperature distributions were not considered. Apalak and Gunes investigated the non-linear thermal stresses in an adhesively bonded adhesive single lap joint which is subjected to fluid flows in different temperature and velocity for different adherend edge conditions [15]. They used adherends made of medium carbon steel (1040) with a rubber modified epoxy adhesive and considered the adhesive fillets around the adhesive free edges and the rounded adherend corners (Fig. 9.1) inside the adhesive fillets occurring as a result of etching Fig. 9.1 Mesh details of the finite element model of a single lap joint [15] 254 Mustafa K. Apalak T1 = 120°C 1 • • 10 Upper adherend T0 = 20°C • 9 • 8 • 7 U1 = 1 m /s 2 • 3 • •4 Lower adherend T0 = 20°C 5 • • 6 Y Z X Adhesive, T0 = 20°C T2 = 20°C U2 = 1 m/s Fig. 9.2 Thermal boundary conditions of the single lap joint [15] the adherend surfaces in order to obtain a better bonding surface. The peak adhesive stress and strains occur around these adherend corners. The sharp adherend corners cause stress singularities due to geometrical discontinuities, and the stress levels around the rounded adherend corners are lower than those around the sharp corners [1, 4, 6]. Apalak and Gunes also allowed the heat transfer to occur by conduction throughout the joint and by convection from the joint surfaces to the fluids, or the fluids to the joint surfaces. The convective heat transfer between the fluid and adherend surfaces depends on heat transfer coefficient (see Sect. 9.5). These thermal boundary conditions (Fig. 9.2) make the heat transfer problem of the adhesive joint complex. Since the thermal strain distributions in the adhesive joints are dependent on the temperature distributions, they carried out first the thermal analysis and later the geometrically non-linear stress analysis of the adhesive joint based on the small strain-large displacement theory. They assumed a steady state heat transfer and obtained a non-uniform temperature distribution in the adhesive joint (Fig. 9.3). Due to the thermal boundary conditions the temperature increased from the lower adhesive fillet toward the right upper adhesive fillet and become maximum here. Based on the non-linear stress analysis the adhesive joint exhibited different deformation geometries (large rotations through the overlap region) depending on the edge conditions of the lower and upper adherends (Fig. 9.4), and the thermal and mechanical mismatches of the adhesive and adherends caused high stress concentrations through adhesive regions close to adhesive-adherend interfaces around the adhesive free ends (Fig. 9.5). The peak thermal stresses and strains in the 59.98 61.66 63.34 65.01 66.69 68.37 70.04 71.72 73.39 75.07 Fig. 9.3 Temperature distribution in the single lap joint (in ◦ C) [15] 9 Non-Linear Thermal Stresses in Adhesive Joints 255 (a) (b) (c) Y (d) Z X Fig. 9.4 Deformed geometries (not scaled) for boundary conditions: (a) (BC-I), fixed edgehorizontally free edge, (b) (BC-II), only one corner of both plates fixed, (c) (BC-III), both edges fixed, (d) (BC-IV), fixed edge-vertically free edge [15] (a) BC -I 8.2 9.1 10.1 11.0 12.0 13.0 13.9 14.9 15.8 16.8 9.4 10.6 11.7 12.9 14.1 15.2 16.4 17.5 18.7 19.8 (b) BC -II 23.2 26.4 29.5 32.7 35.9 39.0 42.2 45.4 48.5 51.7 25.3 28.7 32.0 35.3 38.6 41.9 45.2 48.6 51.9 55.2 (c) BC -III 28.2 32.1 36.0 39.9 43.8 47.7 51.6 55.5 59.4 63.4 30.5 34.6 38.7 42.7 46.8 50.9 55.0 59.1 63.2 67.3 (d) BC -IV 11.3 13.5 15.7 17.9 20.1 22.3 24.5 26.7 28.9 31.1 12.6 15.1 17.6 20.1 22.6 25.1 27.6 30.1 32.6 35.1 Fig. 9.5 von Mises stress distributions in the left and right adhesive fillets (All stresses in MPa) [15] 256 Mustafa K. Apalak 1.000 Normalized von Mises stress, (σ eqv / σ max) BC - I 0.950 BC - IV 0.900 0.850 BC - III BC - II 0.800 0.750 0.700 0.08 σmax = 20.00 MPa σmax = 69.54 MPa σmax = 78.61 MPa σmax = 37.49 MPa 0.10 0.12 0.14 0.16 0.18 0.20 0.22 0.24 0.26 0.28 0.30 0.32 0.34 Overlap length - joint length ratio Fig. 9.6 Effect of the overlap length on the von Mises stress σeqv in different critical locations inside the right adhesive fillet for the boundary conditions I–IV [15] adhesive layer occurred at the free ends of the upper adherend-adhesive and the lower adherend-adhesive interfaces, and these thermal strain and stress conditions exceeded yield point for some plate end conditions. The elastic analyses showed that increasing the overlap length is not beneficial in reducing the peak stresses in the critical adhesive (Fig. 9.6) and adherend regions for two adherend end conditions. This study showed that the thermal and material mismatches of the adhesive and adherends result in serious thermal strains along the adhesive-adherend interfaces, especially around the adhesive free ends. In case the variable thermal conditions along the outer surfaces of the adhesive joint exist, non-uniform temperature distribution occurs in the adhesive joint, consequently, non-uniform thermal strain distribution. This makes thermal stress distribution in the adhesive joint more complex. Therefore, actual variable thermal conditions as well as the large rotations and displacements occurring in the joint should be considered in the stress analysis and in the design of adhesive joints. Another adhesive joint used in load transmission of thin-walled structures is the tubular single lap (TSL) joint. Since epoxy adhesives are usually rubber modified in order to obtain higher toughness, they present non-linear behaviour under loads and the exact solutions of the stress and deformation of TSL joints become difficult. The torque transmission capabilities, elastic stress states, the effects of the adhesive thickness and adherend roughness on the torsional static and fatigue strengths of the adhesively bonded tubular lap joints, the failure models, the non-linear properties and the viscoleastic behaviour of the adhesive layer in these joints were investigated in detail for structural loads [2, 7, 25, 29, 31, 41, 43, 56, 58]. In practice, adhesive tubular joints also experience thermal loads as well as structural loads. Since the thermal loads cause different thermal strains in both tubes and adhesive layer, in case the degrees of freedom (translation and rotation) along the free edges of the tubular joint are restrained the thermal strains would cause thermal stresses 9 Non-Linear Thermal Stresses in Adhesive Joints T2 = 20°C 257 U2 = 1 m/s T0 = 20°C T0 = 20°C T1 = 120°C 1• A • 10 B T0 = 20°C 9• 8• • 7 T0 = 20°C T2 = 20°C CL U1 = 1 m/s •2 •3 •4 C T0 = 20°C U2 = 1 m/s •5 •6 θ r z Fig. 9.7 Thermal boundary conditions of a tubular single lap joint (A: Inner tube, B: Adhesive layer, C: Outer tube, T0 : Initial temperature) [17] in the tubular joint. Since the adhesive and tubes have different thermal and mechanical properties they present different deformation states. The strains should be compatible along the adhesive and tube interfaces, therefore the thermal stresses are unavoidable. First, Kukovyakin and Skory considered the effect of the adhesive and adherend thermal expansion coefficients in the thermal elastic stress analysis of a bonded cylindrical joint [40]. Kim et al. investigated the effect of the thermal residual stresses arising in adhesively bonded metal-metal tubular joints [36, 37]. However, these thermal stress analyses assume a uniform temperature distribution, i.e. a constant temperature distribution in all joint regions, or along the geometrical boundaries and do not consider conductive and convective heat transfers through the tubes and adhesive layer, which occur due to variable thermal boundary conditions. Apalak et al. carried out a geometrically non-linear thermal stress analysis of an adhesively bonded (steel) tubular lap joint subjected to air flows in different temperature and velocity over its inner and outer surfaces (Fig. 9.7, see Sect. 9.5) [17]. Based on the thermal analysis they obtained a nonuniform temperature distribution in the tubular joint. The temperature is minimal in the inner adhesive fillet and increases nonuniformly toward the outer adhesive fillet and then becomes maximal here (Fig. 9.8). As a result of the non-uniform temperature distribution and different CL r max min Left free edge Right free edge 55.6 57.2 58.8 60.4 61.9 63.6 65.2 66.7 68.3 69.9 Fig. 9.8 Temperature distributions in the left and right free edges of overlap region in the tubular single lap joint (all temperatures in ◦ C) [17] 258 Mustafa K. Apalak CL (a) r (b) (c) Fig. 9.9 Deformed geometries (not scaled) for boundary conditions: (a) (BC-I), only one corner of two tubes fixed, (b) (BC-II), the free ends of two tubes fixed, and (c) (BC-III), the free edge of the inner tube fixed and the right free edge of the outer tube free only in the axial direction [17] material properties, the thermal strains at the different locations of the adhesive joint, even in zones with similar material properties, become nonuniform. Consequently, the deformation geometries of the tubular joint were affected considerably for different tube edge conditions (Fig. 9.9). The stress concentrations were observed inside both inner and outer adhesive fillets around the adhesive free edges (Fig. 9.10). The (a) (b) (c) – 45.8 – 40.9 – 36.1 – 31.2 – 26.4 – 21.5 – 16.7 – 11.8 – 6.94 – 2.09 – 35.8 – 32.2 – 28.6 – 24.9 – 21.3 – 17.7 – 14.0 – 10.4 – 6.78 – 3.15 – 68.2 – 61.3 – 54.4 – 47.4 – 40.5 – 33.6 – 26.6 – 19.7 – 12.8 – 5.84 – 68.5 – 61.4 – 54.4 – 47.3 – 40.2 – 33.1 – 26.1 – 19.0 – 11.9 – 4.83 – 25.6 – 23.7 – 21.9 – 20.0 – 18.2 – 16.3 – 14.5 – 12.6 – 10.8 – 8.90 – 26.8 – 24.6 – 22.4 – 20.2 – 18.0 – 15.8 – 13.6 – 11.4 – 9.18 – 6.98 Fig. 9.10 (a) radial σrr , (b) normal σzz , and (c) shear σrθ stress variations inside the left and right adhesive fillets for the BC-II (stresses in MPa) [17] 9 Non-Linear Thermal Stresses in Adhesive Joints 259 1.00 Normalized von Mises stress, ( eqv / max) BC - III 0.90 max= 63.29 MPa 74.36 MPa max= 19.10 MPa max= 0.80 0.70 0.60 BC - II BC - I 0.50 0.09 0.15 0.20 0.28 0.33 Overlap length - joint length ratio Fig. 9.11 Effect of the overlap length on the von Mises stress σeqv in different critical locations inside the right adhesive fillet for the boundary conditions I–III [17] most critical stress states appeared in cases the tube edges are fully constrained. The radial and circumferential stresses were compressive. The peak adhesive and tube stresses occurred at the free ends of the adhesive-inner and outer tube interfaces, and the lowest stresses at the adhesive fillets neighboring the tube edges. In addition, the adhesive stress distributions around the rounded tube corners were smooth. Increasing the overlap length had an important reducing effect in the peak adhesive stresses (Fig. 9.11) and tube stresses in case the tube edges were fixed. 9.7 Adhesively Bonded Tee Joints In structural adhesive joints, another category is tee joints, in which the joint members are bonded at a right angle or at some other angle. Generally, the joints are subjected to loadings either in the plane of the plate or transverse to it. The analysis and design of tee joints are more complicated than for lap joints or tubular joints. Adams and Wake showed some possibilities of tee joints which may be encountered in practice [4]. Shenoi and Violette used adhesively bonded composite tee joints in small boats and investigated the influence of joint geometry on the ability transfer out-of-plane loads [54]. However, the stresses in tee joints, especially in the adhesive layer, and the effect of joint geometry on the adhesive stresses and on the joint stiffness have not been investigated. Apalak et al. presented a design of a tee joint with a double support [22] or with a single support plus angled reinforcement [23] and showed that the peak adhesive stresses occurred around the adhesive free ends and around the lower corners of the vertical plate, and that the side loading was the most critical among the loading conditions used for the tee joint. They also investigated 260 Mustafa K. Apalak the effects of support lengths on the peak adhesive stresses and the overall joint stiffness for various loading and boundary conditions, and gave the appropriate joint dimensions based on the analyses. Li et al. also presented similar results related to tee joints [44, 45]. da Silva and Adams developed simple mathematical models for predicting the strength of different tee joints [27]. Apalak investigated the effect of geometrical non-linearity on the stress states of adhesive tee joint with double support [16] and with single support plus angled reinforcement [13], and showed that the stresses in the critical joint regions, especially in adhesive fillets, were overestimated with the linear elasticity theory. Apalak et al. studied the thermal behaviour of adhesively bonded tee joint with a single support plus angled reinforcement [18]. They considered the tee joint configurations bonded to a rigid base and a flexible plate (Fig. 9.12) and applied the fluid flows in different temperatures and velocities along the outer surfaces of the plates, supports and adhesive layer (Fig. 9.13) and allowed the convective heat transfer between the outer surfaces and air as well as the conductive heat transfer through the tee joint members. The thermal analysis showed that non-uniform temperature distributions occurred in both tee joint configurations. The temperature distributions inside the adhesive fillets were different depending on the rigid base (Fig. 9.14) or the flexible plate configurations. The air flow along the lower surface of the horizontal flexible plate caused a reduction of the temperature levels and the temperature contours to be parallel to the horizontal plate. The tee joint bonded to an elastic plate can translate and rotate more in comparison with the tee joint bonded to a rigid base (Fig. 9.12). This large rotation and displacements can be evaluated easily based on the small strain-large displacement theory. The peak adhesive stresses occurred inside the adhesive fillets (Fig. 9.15). Consequently, the thermal stresses in the adhesive fillets in the tee joint bonded to a rigid base were higher (Fig. 9.16). The stress concentrations were observed around the rounded corners of the left support and the angled reinforcement and reached peak levels at the adhesive interface-rounded adherend corners. As a result, the variable thermal boundary conditions cause a non-uniform temperature distributions; thus, a third type of (thermal) non-linearity in the thermal stress analysis of adhesive joints 1 10 1 To = 20°C U∞= 1 m / s Ta =120 °C U∞ = 1 m / s Ta = 120 °C U∞ = 1 m / s Ta = 20 °C 4 a) U∞ = 1 m/s Ta = 20 °C 2 4 3 8 9 5 6 2 3 b) 5 To = 20 °C 7 10 7 To = 20 °C 11 12 13 14 15 18 6 11 12 13 14 15 8 9 19 16 17 U∞ = 0.5 m / s Ta = 60 °C Fig. 9.12 Thermal boundary conditions of a tee joint with single support plus angled reinforcement bonded to (a) a rigid base, and (b) a flexible plate [18] 9 Non-Linear Thermal Stresses in Adhesive Joints 261 Y Z X b) a) Fig. 9.13 Boundary conditions and deformed geometries of a tee joint with single support plus angled reinforcement bonded to (a) a rigid base (BC-I), and (b) a flexible plate (BC-II) [18] appears in addition to the geometrical and material non-linearities. The edge conditions of the adherends or bonding the adhesive joint to a rigid or flexible base affect considerably the stress and deformation states of the adherends and adhesive layer, especially inside the adhesive fillets. In addition Apalak et al. investigated the effect of the support length on the peak thermal stresses inside the adhesive fillets and in the adherends [18]. In the case of the tee joint bonded to rigid base, increasing the support length reduced (by 50–60%) the peak stresses inside the left and right horizontal fillets whereas it causes an increase of 35% in the peak stresses inside the vertical adhesive fillet which is most critical region. Apalak et al. also investigated thermal stresses occurring in adhesively bonded tee joints with double support [19]. The tee joint configurations were bonded to a flexible plate or a rigid base (Fig. 9.17) and subjected to the fluid flows parallel or tangential to the outer surfaces of the steel adherends and adhesive layer (Fig. 9.18). They considered the conductive and convective heat transfers through all members of the adhesive joint and presented a simple calculation method for the heat transfer coefficients between the adherend surfaces and the fluids (see Sect. 9.5). First, the steady-state heat transfer analysis of the adhesively bonded tee joint was carried out for each of the two joint configurations. They obtained temperature distributions in the adhesive fillets for the tee joint bonded to a rigid base (Fig. 9.19). Due to the ther- A B C D E F G H a) = = = = = = = = 88 90 91 93 95 96 98 99 A B C D E F G H b) = = = = = = = = 45 48 50 52 54 56 58 60 A B C D E F G H = = = = = = = = 68 70 73 75 77 79 82 84 c) Fig. 9.14 Temperature distributions in critical regions of a tee joint with single support plus angled reinforcement bonded to a rigid base (BC-I): (a) left horizontal adhesive fillet, (b) right horizontal adhesive fillet, and (c) vertical adhesive fillet (all temperatures in ◦ C) [18] 262 A B C D E F G H I Mustafa K. Apalak = = = = = = = = = 25 31 38 44 50 56 63 69 75 a) A B C D E F G H I = = = = = = = = = 15 18 22 25 29 32 36 40 43 A B C D E F G H I b) = = = = = = = = = 14 20 25 30 35 40 45 50 55 c) Fig. 9.15 von Mises stress σeqv distributions in critical regions of a tee joint with single support plus angled reinforcement bonded to a rigid base (BC-I): (a) vertical adhesive fillet, (b) left horizontal adhesive fillet, and (c) right horizontal adhesive fillet (all stresses in MPa) [18] mal boundary conditions, the left lower and left vertical adhesive fillets experienced higher temperatures than the adhesive fillets on the right-hand side of the adhesive tee joints. Thus, temperatures decrease uniformly from surfaces interacting with the air at high temperature to ones interacting with the air at low temperature. The temperature differences through the adhesive fillets are between 3 and 9◦ C. This temperature difference is large enough to cause the thermal strains causing the thermal stresses in the adhesive joints. In the adhesive tee joint bonded to a flexible plate Normalized von Mises stress, ( eqv / max ) 1.10 1.00 0.90 (a) (b) (c) 0.80 0.70 max = 102.0 MPa 82.9 MPa max = 73.3 MPa max = 0.60 0.50 0.40 0.04 0.06 0.08 0.10 0.12 0.14 0.16 Support length - joint length ratio 0.18 0.20 0.22 Fig. 9.16 Effect of the support length on the normalized von Mises σeqv /σmax stresses in the critical adhesive locations: (a) vertical adhesive fillet, (b) left horizontal adhesive fillet, and (c) right horizontal adhesive fillet (Rigid base, BC-I) [18] 9 Non-Linear Thermal Stresses in Adhesive Joints 263 Y Z a) X b) Fig. 9.17 Boundary conditions and deformed geometries of a tee joint with double support bonded to (a) a rigid base (BC-I) and (b) a flexible plate (BC-II) [19] the joint regions interacting with the fluid with high-temperature also experience a higher temperature than other regions. Similar temperature distributions are also observed in the adhesive fillets. The variable thermal boundary conditions (air streams with different temperature and velocity) along the outer surfaces of the adhesive joint resulted in a non-uniform temperature distribution through the adhesive layer and other joint members. As a result, a non-uniform thermal strain distribution occurred. The geometrical non-linear thermal stress analysis showed that large rotations occurred in the bonding region of the adhesive tee joint and the free regions of the vertical and horizontal plates deformed considerably (Fig. 9.17). In addition, the free edges of the adhesive layers experience stress concentrations and the von Mises stresses peak at the rounded corners inside the adhesive fillets. The adhesive fillets interacting the fluids with higher temperatures, such as the left lower and vertical adhesive fillets, contain considerable stress concentrations (Fig. 9.20). Both adherend and adhesive stresses in the tee joint bonded to a flexible plate were smaller than those in the joint bonded to a rigid base. The flexible horizontal plate allows the 1 10 2 11 3 12 U∞ = 1 m/s Ta = 50 °C 4 a) 5 7 8 9 6 13 U ∞ = 1 m/s U ∞ = 1 m/s Ta = 20 °C Ta = 50 °C 15 4 5 7 16 17 18 21 10 2 3 11 U∞ = 1 m/s b) 14 1 6 12 Ta = 20 °C 13 14 15 16 17 18 8 9 22 19 20 U∞ = 1 m /s , Ta = 30 °C Fig. 9.18 Thermal boundary conditions of a tee joint with double support bonded to (a) a rigid base, and (b) a flexible plate [19] 264 Mustafa K. Apalak A B C D E F G H A B C D E F G H = = = = = = = = = = = = = = = = 35.2 35.9 36.5 37.1 37.8 38.4 39.0 39.7 40.8 41.3 41.8 42.3 42.8 43.3 43.8 44.2 A B C D E F G H b) a) = = = = = = = = 30.1 30.7 31.4 31.9 32.6 33.2 33.9 34.5 A B C D E F G H c) = = = = = = = = 25.6 26.1 26.5 27.0 27.5 27.9 28.5 28.9 d) Fig. 9.19 Temperature distributions in the critical regions of an adhesively bonded tee joint with double support bonded to a rigid base: (a) left horizontal adhesive fillet, (b) left vertical adhesive fillet, (c) right vertical adhesive fillet, and (d) right horizontal adhesive fillet (all temperatures in ◦ C) [19] tee joint to deform in the transverse direction; therefore, the internal load distribution reduce partly. Thus, the rigid adhesive joints experience serious stress levels. The variable thermal boundary conditions and the thermal-mechanical mismatches of the adhesive and adherends result in a non-uniform temperature distribution in the adhesive joint; consequently a non-uniform thermal strain and stress distributions. These stress concentrations around the adhesive free ends of A B C D E F G H I = = = = = = = = = a) 7.81 9.53 11.2 13.0 14.7 16.4 18.1 19.8 21.5 A B C D E F G H I = = = = = = = = = A B C D E F G H I 4.78 6.32 7.87 9.41 11.0 12.5 14.0 15.6 17.1 b) c) = = = = = = = = = 4.05 4.95 5.84 6.74 7.64 8.53 9.43 10.3 11.2 A B C D E F G H I = = = = = = = = = 3.70 4.87 6.04 7.21 8.38 9.54 10.7 11.9 13.1 d) Fig. 9.20 von Mises stress σeqv distributions in the critical regions of an adhesively bonded tee joint with double support bonded to a rigid base: (a) left horizontal adhesive fillet, (b) left vertical adhesive fillet, (c) right vertical adhesive fillet, and (d) right horizontal adhesive fillet (All stresses in MPa) [19] 9 Non-Linear Thermal Stresses in Adhesive Joints 265 the adhesive joints subjected to structural loads can be reduced by increasing the bonding surface (overlap length) or tapering the adherend edges [4]. Therefore, the effect of the support length on the peak stresses inside the adhesive fillets and at the critical plate regions was investigated for the adhesive tee joints bonded to a rigid base and a flexible plate. Increasing the support length results in increases in the normalised equivalent stresses at the critical adhesive locations (Fig. 9.21). The detailed analysis of the stress components showed that the normal stress σxx is compressive and dominant among all stress components at the critical adhesive locations whereas the normal stress σyy is compressive and dominant in the critical vertical plate locations (not shown). However, the compressive state of the normal stresses may be advantageous in cases the adhesive tee joint experiences tensile loading conditions since the tensile stress levels can be reduced. The stress components and equivalent stress are increased as the support length is increased. Thus, the vertical plate tends to buckle as a result of thermal strains and its one fixed end. The bending moment occurring at the left free end of the horizontal adhesive layer increases since the vertical plate buckles. However, the equivalent stress at only the left horizontal adhesive fillet increases 1.27 times. The adhesively bonded tee joint was analysed for two specific boundary conditions causing buckling in the vertical and horizontal plates. Increasing the support length makes the joint region relatively stiffer. However, the extensional thermal elongations are restrained. In this case most of the load is transferred to the support via the adhesive fillets. Since the normal stresses inside the adhesive fillets are compressive, in case the tee joint experiences an additional tensile load this would be advantageous in order to reduce the total stresses. max) 0.92 Normalized von Mises stress, ( 0.96 eqv / 1.00 0.88 0.84 0.80 max= 29.30 MPa 20.80 MPa max= 13.75 MPa max= 14.73 MPa (a) (b) (c) (d) 0.76 0.72 max= 0.68 20 30 40 50 60 70 80 Support length (mm) Fig. 9.21 Effect of the support length on the normalized von Mises σeqv /σmax stresses in the critical adhesive locations: (a) left horizontal adhesive fillet, (b) left vertical adhesive fillet, (c) right vertical adhesive fillet, and (d) right horizontal adhesive fillet (Rigid base, BC-I) [19] 266 Mustafa K. Apalak 9.8 Micromechanics of Composite Materials The engineering constants of unidirectional fiber-reinforced lamina can be computed by using the micro-mechanics approach based on the engineering constants of fiber reinforcement ( f ) and matrix (m) in the material coordinates (x1 , x2 , x3 ) as [51] E1 = E f V f + EmVm (9.51) E f Em E f Vm + EmV f (9.52) υ12 = υ f V f + υmVm (9.53) G f Gm G f Vm + GmV f (9.54) E2 = G12 = where Vm and V f are the volume fractions of the matrix and fibre, E1 is the longitudinal modulus, E2 is the transverse modulus, υ12 is the major Poisson’s ratio, G12 is the shear modulus, and the shear moduli of the fiber and the matrix Ef Gf = 2 1+υf (9.55) Em 2 (1 + υm ) (9.56) Gm = respectively. The following reciprocal relations also exist υ21 υ12 = , E2 E1 υ31 υ13 = , E3 E1 υ32 υ23 = E3 E2 or υi j υ ji = Ei Ej (9.57) In case of a transversely isotropic material with the 2 − 3 plane as the plane of isotropy E2 = E3 , G12 = G13 and υ12 = υ13 (9.58) The generalized Hooke’s law for an anisotropic material under isothermal conditions is given by σi j = Ci jkl εkl (9.59) or in contracted notation [51] σi = Ci j ε j (9.60) If the coordinate planes are chosen parallel to the three orthogonal planes of material symmetry, Eq. (9.60) can be written in matrix form in the material coordinates (x1 , x2 , x3 ) as 9 Non-Linear Thermal Stresses in Adhesive Joints ⎡ ⎤ ⎡ C11 C12 σ1 ⎢ σ2 ⎥ ⎢ C21 C22 ⎢ ⎥ ⎢ ⎢ σ3 ⎥ ⎢ ⎢ ⎥ = ⎢ C31 C32 ⎢ σ4 ⎥ ⎢ 0 0 ⎢ ⎥ ⎢ ⎣ σ5 ⎦ ⎣ 0 0 σ6 m 0 0 C13 C23 C33 0 0 0 0 0 0 C44 0 0 267 0 0 0 0 C55 0 ⎤⎡ ⎤ 0 ε1 ⎢ ε2 ⎥ 0 ⎥ ⎥⎢ ⎥ ⎢ ⎥ 0 ⎥ ⎥ ⎢ ε3 ⎥ ⎢ ⎥ 0 ⎥ ⎥ ⎢ ε4 ⎥ 0 ⎦ ⎣ ε5 ⎦ ε6 m C66 (9.61) The substitution of the engineering constants into the inverse relation of Eq. (9.61) gives ⎡ 1 ⎤ υ31 υ21 ⎡ ⎤ 0 0 ⎡ ⎤ E1 − E2 − E3 0 ε1 ⎢ υ12 1 ⎥ σ1 υ ⎢ − E1 E2 − E323 0 0 0 ⎥ ⎢ σ2 ⎥ ⎢ ε2 ⎥ ⎢ υ13 υ23 1 ⎥⎢ ⎥ ⎢ ⎥ ⎢ ⎥⎢ ⎥ ⎢ ε3 ⎥ ⎢ ⎥ = ⎢ − E1 − E2 E3 01 0 0 ⎥ ⎢ σ3 ⎥ (9.62) ⎢ ⎥ ⎢ 0 ⎢ ε4 ⎥ 0 0 G23 0 0 ⎥ ⎢ ⎥ ⎢ σ4 ⎥ ⎢ ⎥ ⎢ ⎥ ⎣ ε5 ⎦ 0 0 0 G113 0 ⎦ ⎣ σ5 ⎦ ⎣ 0 ε6 m σ6 m 0 0 0 0 0 G112 or {ε }m = [S]m {σ }m (9.63) In order to determine the strain-stress relations of a laminate, it is necessary to convert strain components referred to the material (lamina) coordinate system (x1 , x2 , x3 ) to those referred to the problem (laminate) coordinate system (x, y, z) as ⎡ ⎤ ⎤⎡ ⎤ ⎡ 2 m n2 0 0 0 −mn εxx ε1 ⎢ εyy ⎥ ⎢ n2 m2 0 0 0 mn ⎥ ⎢ ε2 ⎥ ⎢ ⎥ ⎥⎢ ⎥ ⎢ ⎢ ⎥ ⎢ εzz ⎥ ⎢ 0 1 0 0 0 ⎥ ⎢ ⎥ =⎢ 0 ⎥ ⎢ ε3 ⎥ (9.64) ⎢ 2εyz ⎥ ⎥ ⎢ ε4 ⎥ ⎢ 0 0 0 m n 0 ⎢ ⎥ ⎥⎢ ⎥ ⎢ ⎣ 2εxz ⎦ ⎣ 0 0 0 −n m 0 ⎦ ⎣ ε5 ⎦ 2εxy p ε6 m 2mn −2mn 0 0 0 m2 − n2 where m = cos θ , n = sin θ , and similarly {ε } p = [R]T {ε }m (9.65) {σ } p = [R]T {σ }m (9.66) In order to relate compliance coefficients in the two coordinate systems, Eqs. (9.63) and (9.65) are substituted into Eq. (9.66) as {ε } p = [R]T {ε }m = [R]T ([S]m {σ }m ) = [R]T [S]m [R] {σ } p (9.67) {ε } p = [S] p {σ } p (9.68) S = [R]T [S] [R] (9.69) where [S] p ≡ S and [S]m ≡ [S] 268 Mustafa K. Apalak The thermal expansion coefficients αi j are also transformed (α12 = α13 = α23 = 0) as αxx = α11 m2 + α22 n2 (9.70) αyy = α11 n2 + α22 m2 (9.71) 2αxy = 2 (α11 − α22 ) mn (9.72) 2αxz = 0, 2αyz = 0, αzz = 0 (9.73) 9.9 Adhesively Bonded Composite Tee Joints Adhesive bonding technique is used successfully for joining carbon fibre reinforced plastics to metals or composite structures. A good design with either simple or more complex geometry requires stress and deformation states to be known for different boundary conditions. In case the adhesive joint is subjected to thermal loads, the thermal and mechanical mismatches of the adhesive and adherends cause thermal stresses. The plate-end conditions may also result in the adhesive joint to undergo large displacements and rotations whereas the adhesive and adherends deform elastically (small strain). Apalak et al. carried out thermal and geometrically non-linear stress analyses of an adhesively bonded composite tee joint with single support plus an angled reinforcement made of unidirectional CFRPs using the non-linear finite element method [20]. In the stress analysis, they considered the effects of the large displacements using the small displacement-large displacement theory and investigated the stress states in the plates and the adhesive layer of the tee joint configurations bonded to a rigid base and a composite plate (Fig. 9.22). An initial uniform temperature distribution was attributed to the adhesive joint for a stress free state, and then variable thermal boundary conditions, i.e. air flows with different velocity and temperature were specified along the outer surfaces of the tee joints (Fig. 9.12). Since the adhesive tee joints consist of adhesive layer and adherends having different Y Z a) X b) Fig. 9.22 Boundary conditions and deformed geometries of a composite tee joint with single support plus angled reinforcement bonded to (a) a rigid base (BC-I), and (b) a flexible plate (BC-II) [20] 9 Non-Linear Thermal Stresses in Adhesive Joints A B C D E F G H a) = = = = = = = = 63.2 64.1 64.9 65.9 66.7 67.6 68.5 69.4 A B C D E F G H b) = = = = = = = = 40.6 42.4 44.2 45.9 47.7 49.5 51.3 53.1 269 A B C D E F G H = = = = = = = = 53.1 54.2 55.4 56.6 57.7 58.9 60.0 61.2 c) Fig. 9.23 Temperature distributions in critical regions of a composite tee joint with single support plus angled reinforcement bonded to a rigid base: (a) left horizontal adhesive fillet, (b) right horizontal adhesive fillet, and (c) vertical adhesive fillet (all temperatures in ◦ C) [20] mechanical and thermal properties, non-uniform temperature distributions occurred in the adhesive tee joints, and consequently, non-uniform thermal strain distributions (Fig. 9.23). In addition, the edges of the horizontal plate and vertical plate were restrained partly or completely (Fig. 9.22), and then the thermal stress distributions of two adhesive tee joints were determined based on their non-uniform thermal strain distributions using the small strain-large displacement theory. In case of the rigid base, the vertical plate of the adhesive tee joint buckled and the upper free end of the vertical adhesive layer experienced large displacements. The tee joint with flexible base had similar deformations for the vertical plate and the free ends of the vertical adhesive layer; moreover, its horizontal plate was deformed (buckled) considerably. Thus, the left and right free ends of the horizontal adhesive layer and the middle region of the horizontal plate had evident deformations. High normal stresses occurred in the horizontal and vertical sections of the joint regions of both tee joints. Furthermore, the horizontal and vertical adhesive fillets were subjected to high stress concentrations in both rigid (Fig. 9.24) and flexible bases. In general, the stress levels reached a maximum at the free ends of the horizontal plate or vertical plate-adhesive interfaces and distributed uniformly through adhesive fillets towards the rounded corners of the support and the angled reinforcement member. However, the most critical adhesive regions were the left horizontal and vertical adhesive fillets. In case of the adhesive tee joint with a rigid base, the support length has an effect of decreasing the peak stresses in the right horizontal adhesive fillet whereas its effect on the peak stresses in the vertical adhesive fillet and at the vertical plate (Table 9.1). The support length had an effect of decreasing the peak stresses at the critical locations inside the left horizontal and vertical adhesive fillets, and in the horizontal plate whereas its effect on the peak stresses in the vertical adhesive fillet and in the vertical plate is insignificant. Apalak et al. also presented a practical outline of how to carry out the thermal analysis and stress analysis of adhesively bonded joints subjected to variable thermal boundary conditions requiring the heat transfer to take place by conduction throughout the joint members and convection between fluid and adherend surfaces [21]. They investigated the temperature and stress states of an adhesively bonded composite tee joint with 270 A B C D E F G H I b) Mustafa K. Apalak = = = = = = = = = 8.51 10.4 12.3 14.2 16.0 17.9 19.8 21.7 23.6 A B C D E F G H I a) = = = = = = = = = 7.96 9.06 10.2 11.3 12.4 13.5 14.5 15.6 16.7 A B C D E F G H I = = = = = = = = = 5.66 6.42 7.19 7.95 8.71 9.48 10.2 11.0 11.8 c) Fig. 9.24 von Mises stress σeqv distributions in critical regions of a composite tee joint with single support plus angled reinforcement bonded to a rigid base (BC-I): (a) left horizontal adhesive fillet, (b) vertical adhesive fillet, and (c) right horizontal adhesive fillet (all stresses in MPa) [20] double support by applying variable thermal boundary conditions to its outer surfaces. Air streams with different velocity and temperature are specified parallel and perpendicular to the outer surfaces of the joint members (Fig. 9.18). The thermal analyses of the tee joints bonded to rigid and flexible bases showed that the temperature distributions were non-uniform through the adhesive joint. The temperature distributions were also non-uniform in the adhesive fillets at the adhesive free edges for both rigid and flexible bases (Figs. 9.25 and 9.26). In addition, the geometrical non-linear analysis based on the small strain-large displacement theory predicted that non-uniform temperature distributions caused non-uniform thermal strain and stress distributions and considerable deformations in the tee joints (Fig. 9.17). The critical adhesive and plate regions appear as the adhesive free ends as well as the middle section of the horizontal and vertical plates, respectively. Due to the plate edge conditions, the vertical and flexible horizontal plates are forced to buckle; especially, the horizontal plate is deformed considerably undergoing large displacement and rotations (Fig. 9.17). The left horizontal and vertical adhesive fillets are the most critical adhesive regions where the von Mises stresses achieve significant levels (Figs. 9.27 and 9.28). The normal stresses σxx and σyy are dominant in the stress states of the tee joints rather than the shear stress σxy . The normal stresses are usually compressive in the critical adhesive fillets; consequently, these stress states in the adhesive fillets would contribute to joint strength in cases where the tee joint is subjected to the loading conditions which cause tensile stresses in these regions. The joint failure can be expected along the composite plates surfaces as well as inside the adhesive fillets in cases where toughened adhesives are used [55]. In case of tee joints made of adherends, which may yield, the adherend yielding causes the free ends of the adhesive layer to undergo higher deformations; therefore, the adhesive 9 Non-Linear Thermal Stresses in Adhesive Joints 271 Table 9.1 Effect of the support and angled reinforcement length (a) on the peak stress components (in MPa) at the critical adhesive and plate locations of the adhesively bonded composite tee joint with a rigid base (PV: Percentage variation) [20] a σxx PV σyy PV σxy PV Left horizontal adhesive fillet 20 30 40 50 60 −21.20 0.00 −20.90 −1.42 −20.70 −2.36 −22.30 5.19 −20.80 −1.89 Right horizontal adhesive fillet −17.60 −15.70 −14.90 −13.40 −14.50 0.00 −10.80 −15.34 −23.86 −17.61 −13.60 −13.00 −12.80 −13.10 −12.60 0.00 −4.41 −5.88 −3.68 −7.35 20 30 40 50 60 −11.80 −11.20 −11.10 −11.10 −11.20 Vertical adhesive fillet 0.00 −12.70 0.00 −5.08 −11.40 −10.24 −5.93 −10.80 −14.96 −5.93 −9.46 −25.51 −5.08 −10.60 −16.54 −7.06 0.00 −6.76 −4.25 −6.60 −6.52 −6.72 −4.82 −6.56 −7.08 20 30 40 50 60 −12.30 −12.40 −12.30 −11.10 −12.10 Bottom adhesive layer 0.00 −14.50 0.81 −14.70 0.00 −14.70 −9.76 −15.50 −1.63 −14.60 0.00 1.38 1.38 6.90 0.69 −9.14 −9.20 −9.21 −9.45 −9.15 0.00 0.66 0.77 3.39 0.11 20 30 40 50 60 −15.30 −15.40 −15.50 −15.50 −15.50 Vertical plate 0.00 0.65 1.31 1.31 1.31 −15.10 −15.20 −15.20 −15.20 −15.10 0.00 0.66 0.66 0.66 0.00 −4.41 −4.24 −4.17 −4.13 −4.11 0.00 −3.85 −5.44 −6.35 −6.80 20 30 40 50 60 −4.47 −4.49 −4.49 −4.40 −4.48 0.00 0.45 0.45 −1.57 0.22 −33.80 −34.00 −34.30 −35.10 −34.90 0.00 0.59 1.48 3.85 3.25 −3.79 −3.81 −3.82 −3.76 −3.82 0.00 0.53 0.79 −0.79 0.79 failure is more probable rather than the adherend failure. For that reason, bonding an additional composite sheet along the most deformed section of the plates can reinforce the buckled plates of the tee joints. In addition, increasing the bonding area could relieve the peak adhesive stresses at the adhesive free ends. However, the thermal non-linear elastic stress analyses of two tee joints for different supports showed that increasing the support length do not have the same reducing effect of normal and shear stresses, it could reduce the von Mises stresses only by 10–15% in the most critical adhesive and plate locations. Also, it results in decreases of up to 35% in the von Mises stresses in the less critical adhesive and plate regions. Modifying the edge geometry of the composite plates would be more effective in reducing the 272 Mustafa K. Apalak A B C D E F G H A B C D E F G H = = = = = = = = = = = = = = = = A B C D E F G H 50.1 51.3 52.6 53.8 55.0 56.3 57.5 58.7 60.9 61.9 62.9 63.9 64.9 65.9 66.9 67.9 b) = = = = = = = = 40.4 41.6 42.8 43.9 45.2 46.4 47.8 48.8 A B C D E F G H c) a) = = = = = = = = 31.4 32.4 33.4 34.3 35.3 36.3 37.3 38.3 d) Fig. 9.25 Temperature distributions in the critical regions of an adhesively bonded tee joint with double support bonded to a rigid base: (a) left horizontal adhesive fillet, (b) left vertical adhesive fillet, (c) right vertical adhesive fillet, and (d) right horizontal adhesive fillet (all temperatures in ◦ C) [21] A B C D E F G H A B C D E F G H a) = = = = = = = = 50.7 51.4 52.2 52.9 53.7 54.4 55.1 55.9 = = = = = = = = 48.9 49.9 50.8 51.7 52.7 53.6 54.5 55.5 A B C D E F G H c) b) = = = = = = = = 41.0 42.0 43. 43.9 44.9 45.9 46.9 47.9 A B C D E F G H = = = = = = = = 39.4 39.9 40.3 40.8 41.3 41.8 42.3 42.8 d) Fig. 9.26 Temperature distributions in the critical regions of an adhesively bonded tee joint with double support bonded to a flexible base: (a) left horizontal adhesive fillet, (b) left vertical adhesive fillet, (c) right vertical adhesive fillet, and (d) right horizontal adhesive fillet (all temperatures in ◦ C) [21] 9 Non-Linear Thermal Stresses in Adhesive Joints A B C D E F G H A B C D E F G H = = = = = = = = 7.93 10.0 12.1 14.2 16.2 18.3 20.4 22.5 = = = = = = = = 273 A B C D E F G H 7.31 8.48 9.65 10.8 12.0 13.2 14.3 15.5 4.55 5.78 7.00 8.22 9.45 10.7 11.9 13.1 A B C D E F G H c) b) a) = = = = = = = = = = = = = = = = 2.85 3.45 4.06 4.66 5.27 5.87 6.48 7.08 d) Fig. 9.27 von Mises stress σeqv distributions in the critical regions of an adhesively bonded tee joint with double support bonded to a rigid base: (a) left horizontal adhesive fillet, (b) left vertical adhesive fillet, (c) right vertical adhesive fillet, and (d) right horizontal adhesive fillet (All stresses in MPa) [21] peak stresses rather than increasing the support length for these thermal and structural boundary conditions. Finally, the thermal loads may result in non-uniform temperature distributions in the adhesive joints due to the different thermal properties of the adhesive and composite plates, consequently non-uniform thermal strain distributions arise. In A B C D E F G H A B C D E F G H a) = = = = = = = = 6.93 8.16 9.40 10.6 11.9 13.1 14.3 15.6 = = = = = = = = 6.86 7.91 8.95 10.0 11.0 12.1 13.1 14.2 A B C D E F G H b) c) = = = = = = = = 4.65 5.73 6.81 7.89 8.97 10.1 11.1 12.2 A B C D E F G H = = = = = = = = 4.18 5.11 6.05 6.98 7.91 8.85 9.78 10.7 d) Fig. 9.28 von Mises stress σeqv distributions in the critical regions of an adhesively bonded tee joint with double support bonded to a flexible base: (a) left horizontal adhesive fillet, (b) left vertical adhesive fillet, (c) right vertical adhesive fillet, and (d) right horizontal adhesive fillet (All stresses in MPa) [21] 274 Mustafa K. Apalak case some additional structural constraints are imposed to adhesive joints, they may experience considerable high stress and strain distributions. In case large displacements and displacement gradients are observed, the small strain-large displacement theory would predict reasonably accurate stress and deformation states of the adhesive joints providing that the adhesive and composite adherends have small strains. 9.10 Conclusions In case adhesive joints are subjected to the thermal loads, the different thermal and mechanical properties of the adhesive layer and adherends cause incompatible thermal strains along the adhesive-adherend interfaces. Consequently, the non-uniform thermal stress distributions around these regions occur even if the temperature distribution is uniform and the adhesive joint is not constrained. The variable thermal boundary conditions cause a third non-linearity affecting the stress and strain distributions in the adhesive joints. The interaction of the adhesive joint with a fluid having a specific velocity and temperature results in heat transfer to take place by convection between the fluid-adherends or adhesive layer, and by conduction through the adhesive joint. After the transient temperature distribution in the adhesive joint was determined for the thermal boundary conditions, the corresponding thermal strain and stress distributions can be found. The adhesive joints, especially the bonding region, experience large displacements and rotations; thus, deform considerably. In order to consider the effects of the large displacements on the stress and deformation states of the adhesive joints, the small strain-large displacement theory should be implemented to the thermal stress problem since the small strain-small displacement theory overestimates the stresses as well as the displacements. Based on the thermal stress analyses of adhesively bonded single lap, tubular lap and tee joints with metal or composite adherends under variable thermal boundary conditions, non-uniform temperature distributions, and consequently, non-uniform thermal strain and stress distributions were observed. The peak stresses occurred around the adherend corners inside the adhesive fillets or along the adherend-adhesive interfaces depending on the structural boundary conditions. Increasing the overlap area did not reduce these peak adhesive stresses for all boundary conditions, on contrary, caused the peak stresses to increase. References 1. Abedian A, Szyszkowski W (1999) Effects of surface geometry of composites on thermal stress distribution – a numerical study. Compos Sci Technol 59(1):41–54 2. Adams RD, Peppiatt NA (1977) Stress analysis of adhesive bonded tubular lap joints. J Adhes 9:1–18 3. 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Zienkiewicz OC, Taylor RC (1991) The finite element method (solid and fluid mechanics, dynamics and non-linearity), vol. 2, McGraw-Hill Company, UK Chapter 10 Impact Chiaki Sato Abstract This chapter treats mechanical aspects of adhesively bonded joints subjected to impact loads. Fundamentals of impact mechanics of solids are introduced in Sect. 10.2, where stress wave phenomena are explained. A simple formulation of lap joints subjected to an impact stress, which is based on the Volkersen model, is given and calculated numerically with the discrete element finite difference method in Sect. 10.3. Fundamentals of the finite element method for dynamic problems are introduced in Sect. 10.4, where two types of methods: implicit and explicit schemes are explained. In Sect. 10.5, a calculation result of a single lap joint with the finite element method is shown as an example. Experimental methods for evaluating the impact strength are discussed in Sect. 10.6. Stress distributions and their variation as a function of time for joints subjected to impact loads are given by calculations based on analytical models and the finite element method. 10.1 Introduction Adhesively bonded joints in actual products may be sometimes subjected to impact loading. For example, passenger cars can be subjected to impact loading in case of crash. Recent car structures of steel have many adhesively bonded parts such as door panels, engine bonnets, and in addition, main structures in some cases. Almost all the inner panel and the outer panel of a door are joined together with the combination of adhesion and metal plastic working, which is called hemming technique. The engine bonnet has an outer skin and an inner stiffener that are joined with an adhesive and spot welding. The technique is called weld bonding, and it can also be applied to the main structures of recent expensive cars instead of using spot welding only. Even for the joints with plastic parts including bumper, adhesion is employed Chiaki Sato Precision and Intelligence Laboratory, Tokyo Institute of Technology, 4259 Nagatsuta, Midori-ku, Yokohama 226-8503, Japan, e-mail: csato@pi.titech.ac.jp L.F.M. da Silva, A. Öchsner (eds.), Modeling of Adhesively Bonded Joints, c Springer-Verlag Berlin Heidelberg 2008 279 280 C. Sato quite often. In order to prove the crashworthiness of the structures, the evaluation and estimation of the impact strength of such joints are indispensable for appropriate design. Particularly, when the joints are used in critical parts, passenger safety depends strongly on their design. Therefore, adhesively bonded joints have become very important recently, and automobile engineers have aimed at establishing design rules. Mobile electronic devices such as mobile phones or pocket PCs are the other typical case, and they have many joints bonded with adhesives or pressure sensitive adhesives. They are also subjected to impact loading in case of drop, and the situation is not rare as almost all users have experienced such a case. It is, therefore, necessary to ensure the impact durability of the joints in the design process. Despite the facts, much research on impact phenomena of adhesively bonded joints has not been conducted so far due to various difficulties. Impact phenomena of materials are different from static ones from two points of view. One of them is the change of material properties because of high strain rate. The other is the presence of stress waves that propagate in elastic bodies as if waves would do on the surface of water. The former needs complicated experimental setups to assess material properties under high rate loading. The latter requires difficult analysis to determine the stress distribution and its variation with respect to time. Both are not present in the case of static investigation, and they make dynamic investigation more difficult. Many procedures to assess the impact performance of materials have been devised because of interest in a wide variety of applications and some of them have been adopted as standard. The methods using a pendulum hammer, like the Charpy or Izod tests, are the most usual techniques for impacts of relatively low velocity. The ASTM Block Impact Test (ASTM D950-78) is a modification of such pendulum hammer methods to be suitable for the evaluation of adhesive joints, and it is the most usual and popular. Energy consumed to break the specimen can be determined by the method. Though it is useful only to compare quantitatively the performance of adhesives, those methods cannot be applied directly to obtain mechanical properties of materials such as Young’s modulus, Poisson’s ratio and strength of the adhesive and adherends. In addition, the variation of the material constants with respect to strain rate is also unknown from the methods. Thus, more sophisticated methods are required to evaluate the material properties or the impact strength of joints, even though they tend to be more difficult and more expensive than static tests. Although dynamic stress analysis of adhesively bonded joints is possible with a closed-form approach, the governing equations are difficult to solve because they involve partial differential equations. Therefore, numerical calculation is essential even for the closed-form approach. Finite Element Method (FEM) simulations are more versatile to calculate stress states in bodies of complicated shape. However, dynamic FEM is more difficult than static FEM, and know-how is necessary to carry out it properly. As another inherent difficulty of adhesively bonded joints, the stress singularity is to be treated even in case of dynamic analysis. This chapter shows how to estimate stress distribution in adhesively bonded joints subjected to impact loading or high-rate loading, and how to assess the impact 10 Impact 281 strength of the joints. At first, fundamentals of impact dynamics on elastic bodies and adhesively bonded joints will be introduced briefly. Next, a simple formulation of single lap joints and the calculated results will be shown. The theory of numerical dynamic analysis using FEM will be discussed and a result of stress calculation for a single lap joint will be shown as an example. Finally, impact strength evaluation of joints will be shown, where experimental methods and a failure criterion will be considered. 10.2 Fundamentals of Impact Dynamics of Elastic Bodies Stress analysis of solid bodies subjected to impact loads is different from the static case in terms of the time variation of the stress distribution. Stress in a solid body subjected to an impact is not only variable in time at a point, but also the stress translates in the body as a wave propagates in a media. The phenomenon is called “stress wave propagation”. The stress wave occurs because of the combination of body mass, in other words, density distribution, and the elasticity of the body. The dominant stress waves are the dilatational and the shear waves. There are similar kinds of stress waves such as the longitudinal wave in narrow rods or the deflection wave in flexural beams. Another type of waves is the surface acoustic wave (SAW) including Rayleigh waves occurring on the surface of bodies. The dilatational and the shear waves are most influential for the stress distribution in bulk materials, and the longitudinal and the deflection waves are influential only in narrow rods or flexural beams. The surface waves do not affect much the stress state in a body. Thus, the dilatational and the shear waves are discussed firstly, and the longitudinal and the deflection waves are discussed later in the section. The kinetic equation of solids can be written: ρ ∂ σ ji Dvi =∑ + Ki Dt j ∂xj (10.1) where ρ , v, σ and K indicate density, particle velocity, stress and body force per volume of a point in the solid respectively, and suffixes i and j denote the directions in Cartesian space. Since v is a vector and σ is a tensor, v has a suffix and σ has two suffixes. The symbol D/Dt denotes the operator of Lagrangian derivative. The particle velocity can be expressed with displacement as follows: vi = ∂ ui ∂ ui Dui = + vj Dt ∂t ∑ ∂ xj j (10.2) To obtain a linear equation, trivial terms in Eq. (10.2) are neglected. That is equal to regarding the operator of Lagrangian derivative as partial derivative. D ∼ ∂ = Dt ∂t (10.3) 282 C. Sato Then, Eq. (10.1) can be approximated as ρ ∂ σ ji ∂ 2 ui =∑ + Ki 2 ∂t j ∂xj (10.4) The constitutive equation of a linear elastic solid can be given by: σi j = λ ∑ εkk δi j + 2Gεi j (10.5) k where λ and G are the Lamé constant and the shear modulus of the solid respectively. In Eq. (10.5), ∑ εkk indicates the summation of εxx , εyy and εzz , where εi j is k the strain tensor which can be defined as the following: 1 ∂ u j ∂ ui εi j = + 2 ∂ xi ∂ x j (10.6) Now, combining Eqs. (10.4), (10.5) and (10.6), the kinetic equation of a linear elastic solid, which is called the Navier equation, is obtained. ρ ∂ 2u j ∂ 2 ui ∂ 2 ui = (λ + G) ∑ +G∑ + Ki 2 ∂t j ∂ xi ∂ x j j ∂ x j∂ x j (10.7) Equation (10.7) can also be expressed using symbols of vector analysis as follows: ρ ∂ 2u = (λ + G) ∇ (∇ · u) + G∇2 u + K ∂ t2 (10.8) Now, we neglect the body force K to simplify the situation. Using the relation ∇ × (∇ × A) = ∇(∇ · A) − ∇2 A, where A is an arbitrary vector, the following equation is obtained. ∂ 2u ρ 2 = (λ + 2G) ∇ (∇ · u) − G∇ × (∇ × u) (10.9) ∂t The displacement vector field u can be described with scalar potential φ (x,t) and vector potential ψ (x,t) as u = ∇φ + ∇ × ψ . Therefore, Eq. (10.9) can be written as: 2 ∂ 2φ ∂ ψ 2 2 ψ =0 ∇ ρ 2 − (λ + 2G) ∇ φ + ∇ × ρ 2 − G∇ ∂t ∂t (10.10) Since Eq. (10.10) is an identical equation, we obtain two important results: ρ ∂ 2φ = (λ + 2G) ∇2 φ ∂ t2 (10.11) ∂ 2ψ = G∇2 ψ ∂ t2 (10.12) ρ 10 Impact 283 Since Eqs. (10.11) and (10.12) are wave equations, they can be expressed with sound velocities c1 and c2 as: ∂ 2φ = c1 2 ∇2 φ (10.13) ∂ t2 ∂ 2ψ = c2 2 ∇2 ψ (10.14) ∂ t2 where c1 is (λ + 2G)/ρ , c2 is G/ρ , φ is the field of dilatational waves, and ψ is the field of shear waves. A one-dimensional dilatational wave propagating in a quasi-infinite solid media of one-dimension such as a very long bar is treated next because three dimensional wave propagation is too difficult to solve mathematically. Such a stress wave is called a longitudinal wave. Dilatational waves are spherical waves and longitudinal waves are plane waves. Therefore, the velocity c1 is different from the velocity c0 of longitudinal waves. In other words, no wave propagation in transversal directions to the axis is assumed. The longitudinal wave velocity c0 is given by E/ρ , where E is the Young’s modulus of the solid. Here, the influence of Poisson’s ratio can be neglected. Thus, the governing equation of a longitudinal stress wave translating in the x-direction can be obtained as follows: ∂ 2u 1 ∂ 2u = ∂ x2 c0 2 ∂ t 2 (10.15) where u is the displacement in the x-direction. The wave equation can be solved mathematically and the so called d’Alembert’s solution is obtained, given by u(x,t) = η (x − c0t) + ξ (x + c0t), where η ( ) and ξ ( ) are arbitrary functions indicating wave forms. The solution implies that a displacement field consists of two components: a “progressive wave” η (x − c0t) and a “retrograde wave” ξ (x + c0t), as shown in Fig. 10.1, and the superposition law is applicable. Fig. 10.1 Schematic diagram of a progressive wave and a retrograde wave 284 C. Sato If the one-dimensional media has an end, stress waves reflect there. There are two sorts of special ends in terms of reflection: “free ends” and “fixed ends”. Now consider the situation in which a positive progressive wave propagates along the media to the end. If it is a free end, the stress value must be zero there, and a negative retrograde wave must occur so that the positive progressive wave could be canceled, as shown in Fig. 10.2. In the case of a fixed end, the displacement of the end must be zero, and a positive retrograde wave is generated to compensate the virtual displacement that could occur if the media had no end and were continuous, as shown in Fig. 10.2. Such “free end reflection” and “fixed end reflection” can be described as “negative reflection” and “positive reflection” respectively. However, such perfectly free or fixed ends are extreme cases, and ordinary ends have intermediate properties. Stress wave reflection may also occur at an interface between dissimilar materials having different acoustic impedances, which are given by ρ c0 . The deflection wave can propagate along a flexural beam. The kinetics of a beam part can be written as follows: ρ Adx ∂ 2w ∂ F dx = ∂ t2 ∂x (10.16) where A and w indicate the cross section and the deflection of a beam, and F is the shear force applied to the cross section of the part, as shown in Fig. 10.3. The relation between bending moments M and cross sectional shear loads F is given by: ∂M +F = 0 (10.17) ∂x Assuming the deflection w is small, the well known following relation is obtained: Fig. 10.2 Free end reflection (top) and fixed end reflection (bottom) 10 Impact 285 Fig. 10.3 Shear force and bending moment applied to a part of a beam ∂ 2w M = ∂ x2 EI (10.18) where E and I are the Young’s modulus and the area moment of inertia of the beam respectively. From Eqs. (10.16), (10.17) and (10.18), the governing equation is obtained and it can be written as: ρA ∂ 2w ∂ 4w + EI =0 ∂ t2 ∂ x4 (10.19) This formulation is called the Bernoulli-Euler beam theory, but the equation is not an ordinary wave equation. The velocity of waves derived from Eq. (10.19) depends on wavenumber. The phenomenon is called “dispersion”. However, such dispersion phenomenon does not occur in actual beams. The mistake is caused because the shear deformation is not taken into account. Another formulation, which is so called the Timoshenko beam theory, can explain the proper motion of any beam with consideration of the shear deformation of the beam. 10.3 Simple Kinetic Model of Lap Joints Subjected to Impact Loads Correct stress analysis is necessary to estimate the strength of adhesively bonded joints. Much research on the stress distribution in joints has been carried out since the first theory emerged: Volkersen’s shear lag model [14]. Since the stress distribution in joints depends on dimensions, types of materials and particularly configuration, suitable designs to reduce stress concentration has been pursued. Stress analysis using FEM has a history of over 30 years and almost all joint configurations have been investigated already with the method. For instance, Adams and Peppiatt [2] conducted FEM analysis of lap joints and compared them with the closed forms of Goland-Reissner models [6]. Other researches treated the joints considering the elasto-plastic or visco-elastic properties of adherends and adhesives. However, dynamic analyses of the joints are still rare because they are more difficult than static ones. The difficulty is due to the fact that dynamic analysis needs repeated calculations and consumes much of computer resources. A simple kinetic model of a single lap joint subjected to impact loading is shown next in order to calculate dynamic response of stress distribution in the adhesive 286 C. Sato layer [11]. The Volkersen model, which is the simplest one for lap joints, is used here. As shown in Fig. 10.4, the condition of force equilibrium, the compatibility of deformation and the constitutive relations of the materials of each element can be expressed as the following: t1 W ∂ σ1 +W τA = 0, ∂x ε1 = ∂ u1 , ∂x E1 ε1 = σ1 , ε2 = t2 W ∂ u2 , ∂x E2 ε2 = σ2 , ∂ σ2 −W τA = 0 ∂x (10.20) u2 − u1 tA (10.21) GA γA = τA (10.22) γA = where t1 , t2 and tA are the thickness of adherend 1, adherend 2 and adhesive layer, u1 , u2 and W indicate the particle displacements of adherend 1, adherend 2 and the width of the joint. The other symbols, ε , σ , γ , τ , E and G denote normal strain, normal stress, shear strain, shear stress, Young’s modulus and shear modulus respectively, and the suffixes, 1, 2 and A indicate adherend 1, adherend 2 and adhesive layer, respectively. Here, the shear strain is engineering strain. From these equations, the Volkersen’s equation is obtained as follows: ∂ 2 γA 2GA − γA = 0 ∂ x2 EtstA (10.23) Here, to simplify the equation, it is assumed that the adherends have the same thickness, Young’s modulus and density, and they are denoted as ts , E and ρ respectively. Equation (10.20) can be modified into a dynamic model adding the inertia force for each element as follows: Fig. 10.4 Load balance in a single lap joint 10 Impact 287 t1 W ∂ σ1 ∂ 2 u1 +W τA = t1W ρ1 2 ∂x ∂t t2 W ∂ σ2 ∂ 2 u2 −W τA = t2W ρ2 2 ∂x ∂t (10.24) where ρ1 and ρ2 are the density of adherend 1 and adherend 2 respectively. The following governing equation is obtained, which can be called the dynamic Volkersen model: ∂ 2 γA 2GA ρ ∂ 2 γA − γA = (10.25) 2 ∂x EtstA E ∂ t2 This can be written by stress as follows: ∂ 2 τA 2GA ρ ∂ 2 τA − τ = A ∂ x2 EtstA E ∂ t2 (10.26) Equations (10.25) and (10.26) are a type of partial differential equation called “telegraph equation” and they can be solved fully analytically in some cases of simple boundary and initial conditions. Unfortunately, single lap joints have quite complicated boundary conditions, and it is difficult to solve the equations analytically. Now, a numerical approach is applied to the equation assuming a case of single lap joints. Equations (10.25) and (10.26) are inconvenient to define proper boundary conditions for single lap joints. Therefore, Eqs. (10.24) are used as the governing equation. The equations can be simplified as follows: ∂ 2 u1 ρ1 ∂ 2 u1 GA + (u − u ) = 2 1 ∂ x2 E1t1tA E1 ∂ t 2 ∂ 2 u2 ρ2 ∂ 2 u2 GA − (u − u ) = 2 1 ∂ x2 E2t2tA E2 ∂ t 2 (10.27) It is assumed that a stress wave having a step wave form propagates in adherend 1 from the left to the right as shown in Fig. 10.4. The boundary conditions of the joint are quite complicated because reflection of stress waves occurs at the overlap edges. They can be written as: t t σ U(λ ) ∂ u1 (x, λ ) u1 |x=− L = −2 cs1 d λ + cs1 dλ 2 E1 ∂ x x=− L 0 0 2 ∂ u2 =0 ∂ x x=− L 2 ∂ u1 =0 ∂ x x= L 2 t ∂ u2 (x, λ ) dλ (10.28) u2 |x= L = − cs2 2 ∂ x x= L 0 2 288 C. Sato where σ is the amplitude of stress wave, U(t) is the unit step function, cs1 and cs2 are the longitudinal stress wave velocities of adherend 1 and 2 respectively defined as cs1 = E1 /ρ1 and cs2 = E2 /ρ2 . Equations (10.27) can be transformed to discrete equations using the central difference for space and the backward difference for time shown as: 2 u1 (xn+1 ,tn ) cs1 u1 (xn−1 ,tn ) − + k + + k1 u2 (xn ,tn ) u1 (xn ,tn ) + 1 2 2 2 (Δx) (Δx) (Δt) (Δx)2 cs1 = (−2u1 (xn ,tn−1 ) + u1 (xn ,tn−2 )) (Δt)2 2 u2 (xn+1 ,tn ) cs2 u2 (xn−1 ,tn ) − + k2 + + k2 u1 (xn ,tn ) u2 (xn ,tn ) + (Δx)2 (Δx)2 (Δt)2 (Δx)2 cs2 = (−2u2 (xn ,tn−1 ) + u2 (xn ,tn−2 )) (10.29) (Δt)2 where k1 = GA /(E1t1tA ) and k2 = GA /(E2t2tA ). Stepwise time integration of Eqs. (10.29) gives displacement vectors u1 and u2 at each time step. Based on the results, distribution of shear stress τA can be calculated. An example of MATLAB program to solve this problem is shown in Appendix. Figure 10.5 shows a calculated result of shear stress distribution in the adhesive layer of a single lap joint subjected to a step load of 1 MPa in amplitude. Here, the single lap joint is 40 mm in lap length, 4 mm in thickness of the adherends, which Fig. 10.5 Shear stress distribution and variation along bondline of a single lap joint calculated based on the dynamic Volkersen model (see Appendix) 10 Impact 289 are made of aluminum alloy having a tensile modulus of 72 GPa and the density of 2.8 × 103 kg/m3 . The thickness and the shear modulus of the adhesive layer are 0.1 mm and 1.0 GPa respectively. It is shown in Fig. 10.5 that the stress near the load input side (Position = −L/2) increases initially and the stress at the opposite side (Position = L/2) increases with a delay, which is due to the duration of stress wave propagation between the sides. At the load input side, there is stress oscillation, but it decays soon. In case of static loading, the maximum shear stress at the both sides of the joint, denoted as τAmax , can be calculated from the static Volkersen model: τAmax = GA kL σ coth( ) EtA k 2 (10.30) where k = 2GA /(EtstA ). The value of τAmax is 0.527 MPa when a static load σ of 1 MPa is applied to the joint, and this is smaller than the maximum stress value of 1 MPa in Fig. 10.5. Therefore, the dynamic stress concentration factors of the joint are greater than those in static condition. In Fig. 10.5, the shear stress values at both edges decrease gradually, and converge to τAmax after enough time. 10.4 Theory of Numerical Dynamic Analysis by FEM 10.4.1 Static Analysis The finite element method for solids is based on the principle of virtual work, and it is given by: ∑ ∑ σi j δ εi j dV = V i j S q · δ udS+ V b · δ udV (10.31) where σi j and δ εi j indicate stress tensor and virtual variation of strain tensor, and q, b and δ u are surface force, body force applied to the solid and virtual displacement occurring in the solid respectively. The subscripts V and S indicate total volume and total surface of the solid respectively. Other suffixes i and j denote the direction of x, y and z axes. The principle of virtual work has the same meaning as the equilibrium equation which is one of the fundamental relations in solid mechanics. The stress and strain vectors are expressed as: ⎞ ⎛ ⎞ σx εx ⎜ σy ⎟ ⎜ εy ⎟ ⎜ ⎟ ⎜ ⎟ ⎜ σz ⎟ ⎜ εz ⎟ ⎟ ⎟ ⎜ σ = ⎜ ⎟ and ε = ⎜ ⎜ γxy ⎟ τ ⎜ xy ⎟ ⎜ ⎟ ⎝ τyz ⎠ ⎝ γyz ⎠ τzx γzx ⎛ (10.32) 290 C. Sato Note that the components of strain vector are not tensor strains but engineering strains. Though stress and strain are tensor quantities, the vector notation is convenient to calculate virtual work. Equation (10.31) can be simplified by inner product of vector, and it is shown as follows: V σ · δ ε dV = S q · δ udS + V b · δ udV (10.33) A displacement vector u in a finite element is associated with the nodal displacement vector a of the element via the shape function matrix N of the element as follows: u = Naa (10.34) The strain vector ε in the finite element is also associated with the nodal displacement vector a via the strain-displacement relation matrix B of the element as follows: ε = Ba (10.35) Therefore, Eq. (10.33) can be approximated by the following: ∑V σ · Bδ aΔV = ∑S q · Nδ aΔS + ∑V b · Nδ aΔV (10.36) Since Eq. (10.36) is an identical equation which is independent on δ a, the equation can be modified as follows: ∑V BT σ ΔV = ∑S NT qΔS + ∑V NT bΔV (10.37) When the constitutive relation of the solid is linear elastic, stress vector σ is given by: σ = Dε = DBa (10.38) where D is the local stiffness matrix. In case of isotropic materials, it can be expressed as: D= E (1 − ν ) (1 + ν ) (1 − 2ν ) ⎡ 1 ν /(1 − ν ) ν /(1 − ν ) ⎢ ⎢ ×⎢ ⎢ ⎣ 1 sym. 0 ν /(1 − ν ) 0 1 0 (1 − 2ν )/2 (1 − ν ) 0 0 0 0 (1 − 2ν )/2 (1 − ν ) ⎤ 0 0 ⎥ ⎥ 0 ⎥ ⎥ 0 ⎦ 0 (1 − 2ν )/2 (1 − ν ) (10.39) where, E is Young’s modulus and ν is Poisson’s ratio. Equation (10.37) can be modified using matrix D and is shown as follows: ∑V BT DBaΔV = ∑S NT qΔS + ∑V NT bΔV (10.40) 10 Impact 291 The left term in Eq. (10.40) includes nodal displacement vector a, and it can be extracted from summation. Thus, we obtain the final form of the equation for the finite element method: (10.41) Ka = F + B where K = ∑V BT DBΔV , F = ∑ S NT qΔS, B = ∑V NT bΔV , and a is the total nodal displacement vector of the whole structure, and it is the sum of local displacement vectors a defined in each element. Solving Eq. (10.41) gives a , and then ε is calculated using Eq. (10.35). The stress σ is obtained using Eq. (10.38). 10.4.2 Dynamic Analysis with Implicit Solver In case of dynamic conditions, few modifications of the static equation are necessary. That can be done by adding the term of inertia force to the equation following d’Alembert’s principle. Equation (10.31) is modified to the following: ∑ ∑ σi j δ εi j dV = V i j S q · δ udS + V b · δ udV − V ρ ü · δ udV (10.42) where ü is acceleration vector. Therefore, Eq. (10.31) becomes: Ka = F + B − Mä (10.43) where M = ∑V NT ρ NΔV , and is called the mass matrix. To solve Eq. (10.43), the integration in time space has to be carried out. For the purpose, many schemes for time integration have been presented. Implicit schemes use futures status of a that is extrapolated by functions such as Taylor expansion. The simplest extrapolation in implicit schemes is to use a difference quotient of ä given by: a − 2an + an−1 ä n+1 = n+1 (10.44) (Δt)2 where an+1 is the future status because the present time step is n, and än+1 is nothing but an approximation at this step. Substituting ä in Eq. (10.43) with Eq. (10.44), the following is obtained: −1 Fn+1 + Bn+1 + M(2an − an−1 )Δt 2 an+1 = M/(Δt)2 , +K (10.45) and an+1 , i.e., a of the next time step can be calculated. Although this scheme is simpler than other sophisticated implicit ones, it shows common characteristics of implicit schemes. The biggest problem of implicit schemes is that the inverse matrix calculation has to be done in each time step. If the time step Δt needs to be changed during calculation, not only backward substitution, but also forward elimination has to be carried out. Therefore, implicit schemes are less efficient than explicit methods. The other problem is the huge amount of memory consumption 292 C. Sato because the matrix M/(Δt)2 + K has to be stored in memory. The memory should be solid-state to reduce calculation time. Use of hard disk or virtual storage is not recommended. Therefore, the memory consuming nature of the schemes is very expensive. On the other hand, implicit schemes are very stable, so that longer time steps than explicit schemes can be selected with reasonable results. Actual implicit schemes used for practical application are more complicated than those mentioned above. One popular scheme is the Newmark-β method, which uses Taylor expansion for extrapolation. The method is given by: an+1 = an + Δt ȧn + where, (Δt)2 än + β (Δt)2 än+1 − än 2 ȧ n+1 = ȧ n + Δt γ ä n+1 + (1 − γ ) ä n (10.46) (10.47) −1 ä n+1 = M + (1 + α ) β (Δt)2 K 1 2 K ȧa n − (1 + α ) − β (Δt) K ä n × Fn+1 + Bn+1 − Kan − (1 + α ) ΔtK 2 (10.48) α = 0, β = 0.25 and γ can take different values, determining the stability of the scheme. The parameters are selectable to tune up the compromise of stability and response. For instance, in the Hilber-Hughes-Tailor method, which is more stable with shorter time steps, has the parameters α = −0.1, β = 0.3025 and γ = 0.6 [9]. 10.4.3 Dynamic Analysis with Explicit Solver Explicit schemes are more efficient than implicit ones and their use is increasing in many applications such as crash analysis of car bodies in the last two decades. The equation of explicit schemes is given by: (10.49) ä n = M−1 Fn + Bn − Kan To obtain an+1 , additional calculations have to be carried out using the central difference as follows: (10.50) ȧ n+0.5 = ȧ n−0.5 + Δtn ä n an+1 = an + Δtn+0.5 ȧ n+0.5 (10.51) where Δtn+0.5 = tn+1 − tn and Δtn = tn+0.5 − tn−0.5 . As seen in Eq. (10.49), if a lumped weight matrix for M is used, inverse matrix calculation can be omitted. In addition, there is no need to store the entire matrix K −1 which includes many fill-ins or zeros after the forward elimination, and calculation of only Kan is a less 10 Impact 293 memory consuming process. Because of such advantages, explicit schemes have recently become the only choice to treat huge scale applications. As a matter of fact, crash analysis of whole car structures, which is one of the biggest calculation these days, can be completed using only a PC of high performance within few weeks. Many packages of explicit finite element analysis are commercially available now. LS-DYNA (LSTC, Livermore, U.S.A.), which is derived from previous DYNA3D (Lawrence Livermore National Laboratory, Livermore, U.S.A.), PAMCRASH (ESI, Paris, France), RADIOSS (Altair Engineering, Troy, U.S.A.) and DYTRAN (MSC, Santa Ana, U.S.A.) are famous explicit programs. Though these programs aim at car design mainly, they can be applied to other purposes. A famous implicit program: ABAQUS (SIMULIA, Providence, U.S.A.) has also developed an explicit solver recently. Such programs are made based on the Lagrange method. Therefore, they are also suitable for large deformation problems. The disadvantage of explicit scheme is the necessity of using a lumped matrix for M. Using a lumped matrix decreases the accuracy of results, and the use of high-order elements is also ineffective. Finer meshes are more suitable for explicit schemes than high-order elements. 10.5 Numerical Modeling of Simple Lap Joints The result shown in Sect. 10.3 is based on the dynamic Volkersen model which neglects the adherend deflection caused by the bending moment due to the offset of the adherends. The deformation is considerable if thin adherends are used. Another model of lap joints was presented by Goland and Reissner [6]. The adherend bending was considered in the model. However, it is hard to obtain a closed form solution of a dynamic Goland-Reissner model, and even a numerical solution by the discrete element finite difference method is too complex. Direct simulation using the finite element method is easier to perform. Sato and Ikegami investigated the deformation and stress distribution of single lap joints, taper lap joints and scarf joints subjected to impact loads using the finite element method [13]. In the analysis, the adhesive layer was treated as a viscoelastic material and the impact load was a step function. In the calculated results, sharp and impulsive stress concentrations occur at the edge of the load input side as shown in Fig. 10.6. After the transient process, stresses at both overlap edges increase gradually, although the applied stress wave is a step function and the amplitude is constant. The phenomenon occurs due to the bending moment caused by the stress wave propagation through the “cranked path” in the offset bonded joint. Higuchi et al. conducted a dynamic analysis of butt joints of cylindrical steel rods subjected to tensile impact loads using the three dimensional finite element method and showed the stress variation in the adhesive layer with respect to time and the presence of a stress singularity at the circumferential edge of the adhesive layer [8]. Figure 10.7 shows the calculated results by FEM of impact deformation of a single lap joint. This is a three-dimensional elastic analysis using the explicit solver 294 C. Sato Fig. 10.6 Stress distribution and variation with respect to time of a single lap joint subjected to impact step load calculated by the dynamic finite element method Fig. 10.7 Stress distribution and deformation of a single lap joint subjected to a impact step load calculated by PAM-CRASH 10 Impact 295 PAM-CRASH (ESI, Paris, France). The adherends of the joint are 100 mm long, 25 mm wide and 4 mm thick. The overlap length is 12.5 mm and the adhesive thickness is 0.1 mm. The material constants are the same as the joint treated with the dynamic Volkersen model in Sect. 10.3. In addition, the Poisson’s ratios νs , νA of the adherend and the adhesive layer are 0.3 and 0.4 respectively. A tensile stress of 1 MPa step function is applied to the left edge of the specimen in Fig. 10.7, and the right edge is fixed perfectly. The front of a stress wave reaches the overlap at 0.02 ms, so that there is no stress in the overlap at 0.01 ms as shown in Fig. 10.7. After 0.02 ms, the stress wave propagates in the overlap and the joint begins bending. Although the applied stress is constant, the deflection of the joint continues to increase due to dynamic effects. 10.6 Impact Strength Evaluation of Adhesively Bonded Joints Not only are analytical methods, but also experimental methods very important to investigate the properties of materials used for adhesively bonded joints and the strength of the joints. In this section, trends in experimental methods are discussed. In addition, impact strengths of several adhesives are shown based on the results presented in previous papers. 10.6.1 Pendulum Test As mentioned in the introduction, the block impact test (ASTM D950-78) has been the only standard used to test adhesively bonded joints under impact loading for long time. In the test, a small block is bonded to a larger block which is fixed to the base of the testing machine and an impact load is applied to the small block due to the collision of a pendulum hammer, as shown in Fig. 10.8. At impact, the joint is Fig. 10.8 ASTM block impact test (D950-78) 296 C. Sato subjected to a high rate shear loading and is fractured. After the pendulum hammer hits the specimen, its velocity decreases. The impact energy absorbed by the joint specimen can be calculated from the difference of the pendulum height between the initial position before the test and the maximum height that is subsequently reached after the collision. If the pendulum is instrumented, a load-displacement curve can be obtained. In the technique, a load sensor and a displacement sensor are installed in the pendulum tester. The load sensor, which is usually a piezo-electric loadcell, is inserted between the pendulum and the tooth of the hammer. The displacement sensor, which is often rotational and angular, is attached to the axis of the pendulum. The instrumented technique gives important data, such as maximum loads applied to the specimen, maximum displacement of the small block by which maximum shear strain of the adhesive layer can be calculated, and a more precise absorbed energy determined. Adams and Harris calculated the stress distribution in the specimen of the block impact test using the finite element method [1]. Unfortunately, the stress distribution in the adhesive layer highly depends on the position at which the tip of the impactor hits the specimen. The position deviates occasionally from the objective point because of misalignment of the experimental setup. Thus, it is concluded that this test only gives a quantitative information of the ability of adhesives to withstand high loading rate and cannot be used for design purpose. Nevertheless, the results of the test are convenient for estimating approximately the maximum stress occurring in the joints. In the experiments, strength assessment of adhesives was carried out using four different types of epoxy adhesives, MY750 (Ciba-Geigy, Switzerland) which consisted of a diglycidyl ether of bisphenol A with anhydride hardener HY906 and a tertiary amine catalyst DY062, AY103 (Ciba-Geigy, Switzerland) plasticised with an amine hardener HY956, ESP105 (Permabond, Winchester, UK) which is a single part toughened epoxy, and toughened MY750 modified with CTBN, i.e. a synthetic rubber carboxyl-terminated butadiene-acrylonitrile. The brittle unmodified MY750 presented the lowest absorbed energy. The plasticised epoxy AY103 also showed low absorbed energy, but greater than that of unmodified MY750. The rubber modified epoxy and the single part toughened epoxy ESP105 showed much higher absorbed energy compared with unmodified MY750 and AY103. Thus, the results show the importance of adhesives ductility in order to withstand impact loading. Pendulum testers are available not only for impact blocks but also for other types of specimens including lap joints. Harris and Adams carried out impact tests on single lap joints having aluminium alloy adherends bonded with epoxy adhesives [7]. Recently, another kind of pendulum test using a wedge was adopted as a standard: Impact Wedge-Peel (WP) test which is shown in Fig. 10.9. An impact load is applied to the specimen through the wedge. The method can be thought of a modified version of the Boeing wedge test for impact loading. Blackman et al. carried out precise experiments of the IWP test using a fast hydraulic testing machine and a piezoelectric loadcell [4]. 10 Impact 297 Fig. 10.9 Configuration of the impact wedge-peel (IWP) specimen ISO 11343 10.6.2 Split Hopkinson Bar (Kolsky bar) The pendulum tests described above are easy to use, but a high strain rate cannot be realized. A strain rate of up to about 102 s−1 can be obtained. When a higher strain rate is necessary, the split Hopkinson bar technique is often used because a strain rate of 102 s−1 – 103 s−1 can be realized easily and using special experimental setups strain rates as high as 104 s−1 can be obtained. A typical Hopkinson bar equipment is used for impact compression tests, and it has two steel bars (input bar and output bar) between which a specimen is inserted, as shown in Fig. 10.10. Fig. 10.10 Basic configuration of split Hopkinson bar apparatus for compressive (top) and tensile (bottom) impact tests of materials 298 C. Sato A striker, which is usually accelerated with a gas gun, collides with the end of the input bar to cause a stress wave that transmits to the specimen as an impact load. The applied load and its variation with respect to time are measured with strain gauges bonded on the opposite surfaces of the input bar. Deformation of the specimen can also be calculated from the velocities of the edges of the input bar and the output bar that can be measured form the gauge data. Since a relatively higher strain rate can be realized easily and the deformation of specimens can be measured without any additional displacement sensors, the Hopkinson bar method is the most used technique for impact tests. The ingenious apparatus was first introduced by Kolsky, and is also called the Kolsky bar [10]. For the strength evaluation of adhesively bonded joints subjected to impact loads, an aspect of Hopkinson bar – that it is suitable only for compression tests – is sometimes an obstacle because tensile impact tests are very often required. Therefore, compression loads should be transformed into tensile loads by any means. Yokoyama used the split Hopkinson bar technique shown in Fig. 10.10 to apply a tensile load to butt joints bonded with a cyano-acrylic adhesive [15]. In the experiment, the tensile stress wave was caused by the collision of a tubular impactor against a loading block, fixed at the end of an input bar. The tensile wave was applied to the specimen as a tensile impact load. Yokoyama and Shimizu also conducted impact shear tests of adhesive joints using a compressive setup of split Hopkinson bar and pin-and–collar joint specimens [16]. The same configuration of specimens was also used by Bezemer et al. [3]. 10.6.3 Other Special Methods Since the adhesive layer in practical joints is usually subjected to a combination of shear and tensile stresses even under impact loading, tests for combined high rate loading are important to obtain a strength criterion, but are not easy to carry out. Sato and Ikegami measured the strength of butt joints of steel tubes, bonded with an epoxy adhesive Scotch Weld 1838 (Sumitomo 3M, Tokyo, Japan) hardened with a polyamide resin, when subjected to a combination of tensile and torsional impact loads using a clamped Hopkinson bar equipment [12]. The strength of the butt joints under combined impact loading is shown in Fig. 10.11 with approximation curves fitted with von Mises law and 2nd polynomials. The curve of 2nd polynomials shows better fitting than that of von Mises law. The tensile strength of the joints, which is equal to the peel strength of the joints, is approximately 80 MPa, and it is larger than the shear strength that is about 50 MPa. The strength of the joints measured under impact loading was much higher and approximately twice than the static strength as shown in Fig. 10.11. However, the shapes of failure locus were similar in both cases. Therefore, the same type of failure criterion, in this case a quadratic criterion, can be used for static and impact loadings 10 Impact 299 Fig. 10.11 Comparison between impact strengths and static strength of tubular butt joints obtained from combined impact tests and approximation curves fitted by von Mises law and a quadratic criterion Cayssials and Lataillade used an inertia wheel equipment to carry out impact tests of lap shear specimens which consisted of galvanized steel sheet bonded with two kinds of epoxy adhesive: an unmodified DGEBA hardened with dicyandiamide and its modified version with a block copolymer and fillers [5]. 10.7 Conclusion The stress state in adhesively bonded joints is complicated even they are subjected to static loads. When impact loads are applied to them, the stress analysis becomes too difficult with a closed-form approach because the stress state changes from a field distribution to a wave translation. The partial differential equations found in dynamic models are difficult to solve analytically. In addition, the effect of wave reflection and boundary conditions needs to be evaluated. Ignorance on actual impact loads applied to structures is another problem. It will not be solved so soon even if the other problems can be solved. Instead of a closed-form approach, using a finite element analysis is more adequate to impact applications. As seen in the present chapter, finite element codes have become more powerful and more affordable recently. However, some difficulties such as the presence of stress singularities, impact properties of materials, and also deficient experimental methods still exist. Therefore, it is very hard to predict impact strength of adhesively bonded joints still now. Since few papers have treated the subject previously, there is no good result yet. Some of the problems under impact are also present in static conditions. Thus, further progress in adhesion science is required. Not only the development of new adhesives, but also the progress of impact mechanics of adhesively bonded joints is indispensable. 300 C. Sato 10.8 Appendix %------------------------------------------------% Dynamic Volkersen model solution for lap joints % This is a m-file for MATLAB(c) 5.0 or later. % by Chiaki Sato, 2/10/2008 % CAUTION! POSITION AXI is inverted. % 0.04 m and 0 m indicate -L/2 and L/2 respectively. clear; EN = 41; TT = 30e-6; DT = 0.05e-6; PT = 0.3e-6; E1 = 72e9; E2 = 72e9; GA = 1e9; RHO1 = 2.8e3; RHO2 = 2.8e3; T1 = 4e-3; T2 = 4e-3; TA = 0.1e-3; LL = 40e-3; ASTRS = 1e6; %Element number + 1 %Total time (s) %Time step (s) %Display print time step (s) %Young’s modulus of adherend 1 (Pa) %Young’s modulus of adherend 2 (Pa) %Shear modulus of adhesive (Pa) %Density of adherend 1 (Kg/mˆ3) %Density of adherend 2 (Kg/mˆ3) %Thickness of adherend 1 (m) %Thickness of adherend 2 (m) %Thickness of adhesive (m) %Lap length (m) %Applied stress to adherend 1 (Pa) DX = LL/(EN - 1); %x step (m) Cs1 = sqrt(E1/RHO1); %Stress wave velocity in adherend 1 Cs2 = sqrt(E2/RHO2); %Stress wave velocity in adherend 2 %k1,k2,k3,k4,k5 are elements of total K matrix. K1 = 1.0/DXˆ2; K2 = -2.0/DXˆ2 - GA/(E1*T1*TA) - 1.0/(Cs1ˆ2*DTˆ2); K3 = GA/(E1*T1*TA); K4 = GA/(E2*T2*TA); K5 = -2.0/DXˆ2 - GA/(E2*T2*TA) - 1.0/(Cs2ˆ2*DTˆ2); %Generating total K matrix TK(1,1) = 0.0; TK(1,2) = 0.0; TK(1,4) = 0.0; TK(1,5) = 0.0; TK(2,1) = 0.0; TK(2,2) = 0.0; TK(2,4) = -1.0; TK(2,5) = 0.0; TK(1,3) TK(1,6) TK(2,3) TK(2,6) = = = = 1.0; 0.0; 0.0; 1.0; 10 Impact 301 for I=3:2:2*EN+1 TK(I,I-2) =K1; TK(I,I+1) =K3; TK(I+1,I-2)=0.0; TK(I+1,I+1)=K5; end I = 2*EN+3; TK(I,I-4) TK(I,I-1) TK(I+1,I-4) TK(I+1,I-1) = = = = -1.0; 0.0; 0.0; 1.0; TK(I,I-1) =0.0; TK(I,I+2) =K1; TK(I+1,I-1)=K1; TK(I+1,I+2)=0.0; TK(I,I-3) TK(I,I) TK(I+1,I-3) TK(I+1,I) = = = = TK(I,I) =K2; TK(I,I+3) =0.0; TK(I+1,I) =K4; TK(I+1,I+3)=K1; 0.0; 0.0; 0.0; 0.0; TK(I,I-2) TK(I,I+1) TK(I+1,I-2) TK(I+1,I+1) = = = = %Transforming the TK matrix to a sparse matrix sparse(TK); %Initializing valiables %DISP1 and 2 are displacements of adherend edges. %U, Ut and Utt are displacement vectors, %where t indicates delay of one step in time. %F is a nodal force vector. %STRESS is a container of results DISP1 = 0.0; DISP2 = 0.0; U = zeros(2*EN+4,1); Ut = zeros(2*EN+4,1); Utt = zeros(2*EN+4,1); F = zeros(2*EN+4,1); STRESS = zeros(1,EN); %Time integration loop for I=0:DT:TT %setting displacement of adherends edges DISP1 = DISP1 - 2.0 * Cs1* ASTRS / E1 *DT ... + Cs1 *(Ut(5)-Ut(3))/DX*DT; DISP2 = DISP2 - Cs2 *(Ut(2*EN+2)-Ut(2*EN))/DX*DT; %setting boundary condition F(1) = DISP1; F(2) = 0.0; F(2*EN+3) = 0.0; F(2*EN+4) = DISP2; for J=3:2:2*EN+1 F(J) = (-2.0*Ut(J)+Utt(J))/(Cs1ˆ2*DTˆ2); 1.0; 0.0; 0.0; 0.0; 302 C. Sato F(J+1) = (-2.0*Ut(J+1)+Utt(J+1))/(Cs2ˆ2*DTˆ2); end %Inverse matrix calculation U = TKˆF; %calculating shear stress tau for J=1:1:EN TAUA(J)= GA*(U(2*J+2)-U(2*J+1))/TA; end %Storing displacement vectors to previous ones Utt=Ut; Ut=U; %Thinning out result data if mod(I,PT)==0 STRESS = [STRESS;TAUA]; end end %Graphic output as a 3D figure STRESS = fliplr(STRESS); [X,Y]=meshgrid(0:PT:TT+PT,0:DX:(EN-1)*DX); surf(X,Y,STRESS’); xlabel(’TIME (sec)’); ylabel(’POSITION (m)’); zlabel(’SHEAR STRESS (Pa)’); %Figure modification [row,col]=size(STRESS); [val,num]=max(reshape(STRESS,1,row*col)); xlim([0,TT]); ylim([0,(EN-1)*DX]); zlim([0,val*1.2]); colormap(ones(32,3)) %------------------------------------------------- References 1. Adams RD, Harris JA (1996) A critical assessment of the block test for measuring the impact strength of adhesive bonds. Int. J. Adhes. Adhes. 16: 61–71 2. Adams RD, Peppiatt NA (1974) Stress analysis of adhesively-bonded lap joints. J. Strain. Anal. 9: 185–196 3. Bezemer AA, Guyt CB, Volt A (1998) New impact specimen for adhesive: optimization of high-speed-loaded adhesive joints. Int. J. Adhes. Adhes. 18: 255–260 4. Blackman BRK, Kinloch AJ, Taylor AC, Wang Y (2000) The impact wedge-peel performance of structural adhesives. J. Mater. Sci. 35: 1867–1884 5. Cayssials F, Lataillade JL (1996) Effect of the secondary transition on the behaviour of epoxy adhesive joints at high rates of loading. J. Adhes. 58: 281–298 6. Goland M, Reissner E (1947) Stresses in cemented joint. ASME J. Appl. Mech. 11: A17–27 10 Impact 303 7. Harris JA and Adams RD (1985) An assessment of the impact performance of bonded joints for use in high energy absorbing structures. Proc. Instn. Mech. Engrs. 199: C2, 121–131 8. Higuchi I, Sawa T, Okuno H (1999) Three-dimensional finite element analysis of stress response in adhesive butt joints subjected to impact tensile loads. J. Adhes. 69: 59–82 9. Hilber HM, Hughes TJR, Taylor RL (1977) Improved numerical dissipation for time integration algorithms in structural dynamics. Earth Eng. Struct. Dyn. 5: 283–292 10. Kolsky H (1949) An investigation of the mechanical properties of materials at very high rates of loading. Proc. Phys. Soc. Series B 62: 676–700 11. Sato C (2005) Impact behaviour of adhesively bonded joints. In Adams RD (ed) Adhesive bonding, Science, technology and applications. Woodhead Publishing, Cambridge, pp. 164–187 12. Sato C, Ikegami K (1999) Strength of adhesively-bonded butt joints of tubes subjected to combined high-rate loads. J. Adhes. 70: 57–73 13. Sato C, Ikegami K (2000) Dynamic deformation of lap joints and scarf joints under impact loads. Int. J. Adhes. Adhes. 20: 17–25 14. Volkersen O (1938) Die niet kraft vertelung in zug bean spruchten. Luftfahrt forschung 15: 41–47 15. Yokoyama T (2003) Experimental determination of impact tensile properties of adhesive butt joints with the split Hopkinson bar. J. Strain Anal. 38: 233–245 16. Yokoyama T, Shimizu H (1998) Evaluation of impact shear strength of adhesive joints with the split Hopkinson bar. JSME Int. J. Series A 41: 503–509 Chapter 11 Stress Analysis of Bonded Joints by Boundary Element Method Madhukar Vable Abstract Boundary element method (BEM) has proven to have very good resolution of large stress gradients such as in front of cracks and in regions of stress concentration, yet its application in analysis of bonded joints is practically non-existent even though large stress gradients exist in the bonded region and bonded joints are one of the critical technology in modern design. This is because application of BEM to bonded joints is not simple or straight forward. This chapter describes the commonality and differences between BEM and other approximate methods, advantages of BEM application to bonded joints, the research challenges, BEM formulation, the discretization process and the sources of errors, the mesh refinement techniques, and some numerical results. 11.1 Introduction Finite Element Method (FEM), Finite Difference Method (FDM), and Boundary Element Method (BEM) are the three major numerical methods for solving partial differential equations in science and engineering. Unlike FEM and FDM, which are very versatile and general, BEM is a more specialized numerical tool that can yield significant advantages for a class of problems such as bonded joints. There are three features of BEM that makes it attractive for analysis of stresses in bonded joints: (i) It has proven to have very good resolution of stress gradients such as those that appear in front of cracks or in regions of stress concentrations and thus possibly will do the same with strong stress gradients in bonded joints; Madhukar Vable Mechanical Engineering – Engineering Mechanics, Michigan Technological University, Houghton, MI 49931, USA, e-mail: mavable@mtu.edu L.F.M. da Silva, A. Öchsner (eds.), Modeling of Adhesively Bonded Joints, c Springer-Verlag Berlin Heidelberg 2008 305 306 M. Vable (ii) It requires discretization only of the boundary which makes remeshing easy in shape optimisation or parametric study such as in rounding, tapering or shaping of the adherend or adhesive fillet; (iii) It implicitly satisfies the conditions at infinity, thus potentially eliminate the discretization of large segment of adherends. Given the above potential advantages, one would expect a pervasive use of BEM in the analysis of bonded joints. This is not so. Search of several data bases reveal there is a paucity of papers in which BEM is used in conjunction with analysis of bonded joints. The review paper of Adams [4] while describing several modeling techniques for analysis of bonded joints has no mention of BEM. This is because application of BEM to bonded joints is not simple or straight forward. This chapter describes the commonality and differences between BEM and other approximate methods, advantages of BEM application to bonded joints, the research challenges, BEM formulation, the discretization process and the sources of errors, the mesh refinement techniques, and some numerical results. 11.2 Advantages of BEM Application to Bonded Joints We first consider the commonalities and differences between various approximate methods to elaborate the potential advantages of BEM in application to bonded joints. Nearly all approximate methods convert a boundary value problem into a set of algebraic equations. This is usually accomplished by representing the field variable u (for example displacement or temperature) by a series n u= ∑ c jφ j (11.1) j=1 where c j are the constants to be determined, and φ j are an independent and a complete set of n approximating functions. If there are no additional conditions on φ j , then we will generate three types of error: — error in the differential equation (ed ) that is distributed in the domain Ω shown in Fig. 11.1; — error in natural boundary conditions (en ) distributed on the boundary (Γn ) where natural boundary conditions (conditions on traction, heat flux, etc.) are imposed; — error in essential boundary conditions (ee ) distributed on the boundary (Γe ) where essential boundary conditions (conditions on displacements, temperature etc.) are imposed. Clearly we have an analytical solution if all three errors ed , en , and ee are zero. Thus, in approximate methods at least one of the error is not zero. This non-zero error is minimized in some manner. The most general minimizing principle is the weighted residue in which the error is made orthogonal to a weighting function and can be written in the general form 11 Stress Analysis of Bonded Joints 307 Γe Fig. 11.1 Homogenous body Γn Ω (d) ψi ed dxdy + Γe Ω (d) (e) (n) (e) ψi ee ds+ (n) ψi en ds = 0 (11.2) Γe where ψi , ψi , and ψi are the weighting functions, chosen by some criteria that depends upon the approximate method. Generally speaking, these weighting functions are related to the approximating function φ j through the operators of the differential equation or boundary conditions. On substituting the errors ed , en , and ee into Eq. (11.2) we obtain a linear system of algebraic equations in the unknown constants c j , whose coefficients are the integrals such as shown in Eq. (11.2). In the domain methods such as FEM and FDM the functions φ j are chosen such that the error en or ee is forced to be zero. For example, ee is forced to zero in the stiffness version of FEM and en is forced to zero in the flexibility version of FEM. In either case we are left with the evaluation of integral over Ω requiring discretization of the domain. However in boundary methods, such as BEM, the functions φ j are chosen such that error ed is forced to zero, leaving evaluation of integrals only over the boundary. Hence, in BEM only the boundary needs to be discretized. Meshing and remeshing is significantly simpler in BEM than in FEM (and other domain methods) for problems of shape optimisation or parametric study (rounding, tapering or shaping of the adherend or adhesive fillet) in which the boundary shape changes. The discretization process converts the integrals in Eq. (11.2) to a sum of integrals over the elements. Thus, in FEM and domain methods when we set the domain integral over the element to zero in Eq. (11.2), we imply that the differential equation is satisfied in an average sense over the element. But in BEM it is satisfied exactly as ed is forced to zero. If there are stress gradients in the direction of the domain interior, then BEM can potentially yield better resolution by choosing points of stress evaluation very close to each other, while in domain methods the resolution is dictated by the size of the elements. For this reason BEM has proven to have very good resolution of stress gradients for problems of stress concentration and fracture mechanics. Thus, BEM can potentially give good resolution of stress gradients in the thickness direction of the adherend and the adhesive. However, if the stress gradients are along the boundary, as is the case on the adherend-adhesive interface, then BEM like FEM requires a good graded mesh. One research challenge in application of BEM to bonded joints is the development of a mesh refinement scheme for the interface problems. In BEM, the functions φ j are the fundamental solutions of the differential equations, hence implicitly satisfy the zero stress conditions at infinity. If there is a 308 M. Vable uniform stress at infinity then we simply add its value to the integral equations. Thus in BEM we need only discretize boundary of a hole in an infinite medium and do not have to discretize the exterior as is the case in domain methods. However joints have boundaries that start at the adhesive end and extends to infinity. Such boundaries will need specialized infinite boundary elements. The above discussion shows that BEM has the potential of high accuracies in resolution of stress gradients in bonded joints but there are also some research challenges. To further elaborate the difficulties and the on going research it is necessary to discuss BEM formulation and discretization process. The initial discussion is for homogenous materials which is then extended to multiple materials. 11.3 BEM Formulation for Homogenous Materials There are several versions of BEM and variety of approaches for formulating the integral equations of BEM. Cheng and Cheng [16] gives a description of the history of BEM, along with various means of formulating the problem. We will confine our discussion to the two most used versions: the Indirect and the Direct BEM. The displacement ui and the stress σi j at any point in the body can be represented [6, 8] by the integral representation shown in Eqs. (11.3) and (11.4). This representation will be used to describe two versions of Indirect BEM and Direct BEM. ui = (uF)ik tki − tko ds + (uc)ik uik − uok ds + (u∞ )i Γ σi j = Γ (σF)i jk tki − tko ds + (11.3) Γ (σc)i jk uik − uok ds + (σ∞ )i j (11.4) Γ where, — tk and uk represent traction and displacement in the k direction, and the superscripts i and o represent the values of these variables just inside and just outside the boundary Γ of the body which is considered inscribed in an infinite body; — (σ∞ )i j are the uniform stress components applied at infinity; — (u∞ )i is the displacement field associated with the uniform stress at infinity; — the influence functions (uF)ik and (σF)i jk relate the displacement ui and stress σi j at any field point in the body to the force singularity Fk applied at a source point on the boundary Γ; — the influence functions (uc)ik and (σc)i jk relate the displacement ui and stress σi j at any field point in the body to the displacement singularity ck applied at a source point on the boundary Γ; — a repeated index implies summation. Assuming linear-elastic-isotropic-homogenous material, the following relationships between the influence functions can be established [6, 8]. 11 Stress Analysis of Bonded Joints 309 (σF)i jk = μ (uF)ik, j + (uF) jk,i + λδi j (uF)mk,m (11.5) (σc)i jk = μ (uc)ik, j + (uc) jk,i + λδi j (uc)mk,m (11.6) (uc)ik = − (σF)i jk n j (11.7) where, — μ and λ are the modulus of rigidity and Lame’s constant for the material; — δi j represents Kronecker’s delta; — n j are the direction cosines of the unit normal at the source point on the boundary Γ; — a comma implies differentiation with respect to the field point. Equations (11.3) and (11.4) have two displacements and two tractions on the inside and the outside of Γ as variables, resulting in a total of 8 variables. Two of the variables are known and two can be determined from the boundary conditions. Thus four variables must be eliminated from these two equations. We consider three possibilities of eliminating the additional variables. Indirect Force Singularity BEM: In this formulation, as one moves from the inside of the body to the outside (infinite), continuity of displacements uo k = ui k across the boundary Γ is enforced. The traction jump across the boundary Fk = t i k − t o k is the unknown density function that is determined from the boundary conditions. Indirect Displacement Singularity BEM: Also known as Displacement Discontinuity [17] formulation. In this formulation, as one moves from the inside of the body to the outside (infinite), continuity of traction t o k = t i k across the boundary Γ is enforced. The displacement jump ck = ui k − uo k is the unknown density function that is determined from the boundary conditions. Direct BEM: Also known as Rizzo’s Method [32]. In this formulation, it is assumed the outside (infinite) body is undeformed, i.e., uo k = 0 and t o k = 0. Only Eq. (11.3) is used in determining the unknown. If displacements ui k are specified then traction t i k are the unknown density functions and if traction t i k are specified then ui k are the unknown density functions. There are other formulations such as Dual BEM [27], or Direct BEM in which tangential derivatives of the displacements are the unknowns [19]. Many more are possible, particularly for the Indirect BEM [21]. Which particular formulation for which particular situation would lead to the smallest error, that is, require the least number of unknowns for a specified error? Answer to this question is not currently available in the literature. But with regard to the above three formulations, the results presented in [7, 8, 42] provide some answers that are discussed below. For smooth boundaries, the Indirect BEM with force singularity has been shown to have the fastest convergence. For boundaries with corners, the Direct BEM has the fastest convergence. For boundaries that represent cracks in the interior of the materials, the indirect BEM with displacement discontinuity has the fastest convergence. 310 M. Vable 11.4 Discretization and Sources of Errors The integrals in Eqs. (11.3) and (11.4) are reduced to algebraic expressions through a discretization process. The discretization process is an approximation of the actual geometry and the behavior of known and unknown density functions (displacements and tractions). Thus, the discretization process is the process by which numerical errors are introduced into the methodology. This section briefly describes the discretization and the associated errors. For additional details see [45]. A single integral in Eq. (11.3) is considered below to briefly describe the discretization process. Point Q is the point where a quantity is being evaluated and S is the integrating point on the boundary. Ii (Q) = (uc)ik (Q, S) uk (S) ds (S) (11.8) Γ The boundary Γ is sub-divided into NE elements and the integral is replaced by a summation of integrals over each element as shown below: NE Ii (Q) = ∑ (uc)ik (Q, S) uk (S) ds (S) (11.9) n=1 Γn where Γn is the boundary of the nth element. 11.4.1 Interpolation Error On each element the density functions (tk and uk ) are represented by interpolation functions (Nq ). The constants of the interpolation functions are the nodal values of the density functions (Tkq ). The result is an algebraic expression in (Tkq ) as shown below: ⎡ ⎤ Ii (Q) = NE Kn n=1 q=0 ∑ ⎣ ∑ Tkq (uc)ik (Q, S) Nq (S) ds (S)⎦ (11.10) Γn where Kn is the order of polynomial (interpolation function) in the nth element. Two errors are introduced at this stage: mesh error discussed in Sect. 11.4.6 and an error due to the location of the nodes (collocation points) where the nodal values of the density function are prescribed or to be found. If the density functions are discontinuous at both ends of the element, then the optimum location of collocation points are the roots of the Chebyshev polynomial of the second kind [23]. Traditionally in BEM, corners, or points at which boundary condition values jumps, or points where boundary condition changes from essential to natural or vice versa, are points where density functions are permitted to be discontinuous during mesh creation. In [43, 44] an algorithm is described for determining the optimum location of the collocation 11 Stress Analysis of Bonded Joints 311 points for different types of interpolation functions. These interpolation functions could be up to fifteenth order polynomials that could be discontinuous at the element end or have continuity up to the seventh derivative of the density function. The optimum locations of the collocation points were presented in tables for use by other researchers. Based on the study in [43, 44], the recommendations for selecting interpolation functions are the following: (i) For elements that are continuous at both ends, it is better to increase the polynomial order by increasing the continuity order rather than by adding additional nodes inside the element. (ii) For elements that are discontinuous at one end, it is better to increase the polynomial order by adding nodes inside the element rather that by increasing continuity at the other end of the element. 11.4.2 Integration Error The integration error arises from the evaluation of integrals in Eq. (11.10). These integrals can be evaluated numerically or semi-analytically as described below. In numerical integration, the integrand is approximated by known functions, usually polynomials such as in Gauss Quadrature. The singular nature of the influence functions require, the singularity in the element be extracted analytically if possible, or the integrand be made smooth by processing the integrand in some manner. Reference [35] documents the many approaches to the numerical integration error. The strength of numerical integration is in its generality – that is, the algorithms are not specific to the functions in the integrand. The integration error is from the approximation of the integrand but the shape of the integration path (boundary) does not affect the integration error. In semi-analytical integration schemes [2, 3, 9, 39], the integration path is usually approximated by a series of straight lines. Analytical expressions of the integrals over the straight line segment can be obtained. Thus, if the original boundary is made up of straight line segments, then no integration error is introduced into the analysis. If the boundary is curved then it leads to integration error. The creation of corners where two straight line segment join has a particularly deleterious effect on the integration error when the field point approaches the corner. The study in [9] showed that: (i) Large integration errors are obtained when the field point is within one segment length from the boundary. (ii) Increasing the number of tangent points (number of line segments) decreases the magnitude of the error. (iii) The integration errors rapidly decrease with distance from the boundary and are nearly negligible at two segment lengths. (iv) The error decreases as one moves towards the tangent points and away from the corners. 312 M. Vable Based on these observations an algorithm is described in [9] that creates an integration path of straight line segments to reduce the integration error dramatically. The advantages of the semi-analytical scheme for bonded joints are: (i) For straight boundaries, which are most of the boundaries in bonded joints, there is no integration error. (ii) The singular nature of the influence function does not pose any additional difficulties when the stresses are evaluated at the interface or close to it as in the middle of the adhesive. 11.4.3 Continuity Error For quantities of interest, stresses and displacements, to be bounded on the boundary, the density functions (tk and uk ) must satisfy certain continuity conditions at the element ends which depend upon the order of singularity in the influence functions used in formulating the integral equations. If the influence function varies as (1/rn ), where r is the radial distance from the singularity then n is the order of singularity. The influence function (uF)ik has a zero order singularity and thus imposes no continuity requirement on the density function. The influence functions (σF)i jk and (uc)ik have a first order singularity, hence requires the density function to be continuous on smooth boundary points. The influence (σc)i jk has a second order singularity, hence requires the density function and its derivative to be continues on smooth boundary points. Quite often the continuity conditions, particularly on the derivatives of the density functions, are relaxed at the element ends for the sake of simplicity in approximating the unknown density functions. This can impact at two points in the BEM analysis: (i) All requisite continuity conditions are not met during enforcement of the boundary conditions. This can lead to errors in the density function, resulting in large errors in the analysis as discussed in the next section. (ii) Assuming no continuity error during enforcement of boundary conditions, then a large spike in error will be seen in stresses close to the point where continuity is violated and this error propagates inwards up to one element length as shown in [8]. 11.4.4 Collocation Error The boundary conditions can be satisfied in a collocation sense or in Galerkin sense. In collocation schemes the boundary conditions are satisfied at finite number of discrete points. The decision on the location of these points affects the error in the analysis and is referred to as the collocation error. Galerkin schemes minimize the collocation error by integrating the boundary condition over the elements, but this 11 Stress Analysis of Bonded Joints 313 increases the computation cost significantly as two integrals have to be evaluated and the complexity of these integrals usually results in numerical integration schemes and the associated integration error. The location of the boundary conditions collocation points has three effects: (i) it affects the distribution of the error over the body. (ii) it affects the matrix conditioning of the algebraic equations and hence the matrix conditioning error discussed Sect. 11.4.5. (iii) it couples with the continuity error to produce extremely large error in the analysis. In this work, the collocation points are chosen as the same points as those that minimized the interpolation error. When the boundary conditions and interface conditions are satisfied in a collocation sense, the algebraic expressions of the type in Eq. (11.10) result in algebraic equations which can be symbolically represented as [A] {w} = {r} (11.11) where, {w} and {r} are the unknown and known nodal values of the density function, respectively, and [A] is a known matrix with coefficients that are summations of integrals of the type shown in Eq. (11.10). The solution of Eq. (11.11) gives the displacements and tractions on the boundary. In a lap joint this implies that we know both the peel stress and the shear stress on the interfaces of the adhesive and the adherends. The equivalent algebraic form of Eqs. (11.3) and (11.4) are used to determine the stresses and displacements at any point Q in the interior of the materials. 11.4.5 Matrix Conditioning Error The sensitivity of the solution of Eq. (11.11) to the errors in the right hand side vector, depends upon the conditioning of the matrix in the algebraic equation. The amplification of the error in the input data due to the matrix conditioning [13, 40, 41] is referred to as the matrix conditioning error. A measure of matrix conditioning is defined below: Matrix Condition Number = A × A−1 (11.12) where A and A−1 are the norm of the matrix and its inverse respectively. The norm of the matrix is defined as A = max ∑ Ai j i j=1 (11.13) 314 M. Vable The conditioning of the matrix can be improved by using the equilibrium equations [13, 40, 41]. 11.4.6 Mesh Error Mesh error refers to the error in the analysis that is generated by the choice of number of elements, the size of elements, end location of the elements, and the choice of the order of polynomial in the elements. This error is addressed by mesh refinement techniques. There are several mesh refinement schemes in BEM. In the h-method [29, 31] the order of polynomial is kept fixed and an element is subdivided to improve accuracy. However, the total number of unknowns can become very large. In the pmethod [30, 37, 38] the element size is kept fixed, while the polynomial order of the interpolation function is increased in order to improve the accuracy. Though the convergence rate for the p-method is better than the h-method for smooth functions, the method may not converge [36] near a singularity. The hp-method [11, 28, 30] is a combination of the h-method and the p-method that overcomes some of the convergence problems of the p-method near the singularity, but the location of the singularity has to be specified and several parameters have to be specified or evaluated to determine the neighborhood of the singularity. Furthermore the p-method and the hp-method are usually used in conjunction with the Galerkin method due to the difficulty posed in selecting new collocation points as the order of polynomial increases. In the r-method [14, 15, 22, 24] the total number of elements and the order of polynomial are kept fixed, but the spacing of the elements is adjusted to minimize error. If the initial mesh does not have sufficient degrees of freedom then the desired accuracy may not be obtained with r-method [33]. The hr-method [10, 33, 34] is a combination of the h-method and the r-method in which the polynomial order is fixed. The number of unknowns in the hr-method can become large near a singularity. Now it is known [20] that a graded mesh in which the polynomial order increase away from singularity has a higher convergence rate than a graded mesh with a uniform polynomial order. Such hpr-method exist in FEM but none to date has been published for BEM. The above discussion highlight that mesh refinements schemes do well for smooth density functions but have difficulties when density functions have singularities, particularly when the location of singularities are not known. Successful application of BEM for fracture mechanics problem is primarily due to the fact that the stress singularity is in front of the crack, a region that is not discretized in BEM. However, problems such as lap joints contain strong gradients in the density function along the interface and the location of the maximum value cannot be prescribed during mesh construction. Thus developing an hpr-method for BEM that is applicable to bonded joints is one of the research challenge that has to be met. 11 Stress Analysis of Bonded Joints 315 11.5 Multiple Materials Bonded joints have corners, thus the Direct BEM is the appropriate formulation and will be the only one described in this paper for multiple materials. Figure 11.2 shows a general bi-material problem. Ω1 and Ω2 refer to material 1 and material 2, respectively. Γ1 and Γ2 are the non-interface boundaries of Ω1 and Ω2 , respectively and Γint is the interface boundary between the two materials. The integration on the interface in each material is in opposite direction as shown in Fig. 11.2. The boundary integral equations for displacements and stresses at point Q that are written for a homogenous material can be written for the mth material [18, 46] as: (m) ui = (uF)ik tk ds + Γm Γint + (m) Γm + (m) (uc)ik uk ds + (u∞ )i (11.14) Γint (σ F)i jk tk ds + = (uc)ik uk ds + Γm σi j (uF)ik tk ds (σ F)i jk tk ds Γint (σ c)i jk uk ds + Γm (m) (σ c)i jk uk ds + (σ∞ )i j (11.15) Γint The boundary conditions in the local normal and tangential (n, t) coordinate system can be written as: (m) tk (m) (m) = tk or (m) uk (m) = uk k = n,t on Γm (11.16) (m) where, tk and uk are the specified tractions and displacements in the local normal and tangential directions on the non-interface boundaries of each material. Γ2 Ω1 Fig. 11.2 Bi-material geometry Γ1 Ω2 Γint Γint 316 M. Vable Theoretically speaking, there are 7 possible interface conditions [46] that describe the jump in tractions or displacements across the interface in each direction. In this paper we consider only perfectly bonded interface conditions that requires a continuity of displacements and tractions in the local normal and tangential coordinates at the interface as shown below. (1) (2) tk = tk (1) (2) uk + uk = 0 k = n,t on Γint (11.17) In Eqs. (11.14) and (11.15) the integration is on the boundary of mth material and the density functions tk and uk that affect the stresses and displacements inside the mth material are those that are defined on the boundary of that particular mth material. The values of tk and uk of the other material boundaries do not appear in the expressions of stresses and displacements in Eqs. (11.14) and (11.15). Thus, once the density functions are known, the accuracy of results inside a material is determined by the accuracy with which the density function on the boundary (interface or non-interface) is determined. The incorporation of the stress at infinity in the Eqs. (11.14) and (11.15) work effectively [25, 48] when an inclusion is embedded in a different infinite material subjected to the uniform stresses at infinity. In bonded joints however the boundary of the adherend starts at the adhesive end and extends to infinity, thus requires use of infinite boundary elements. Reference [12] describes an infinite boundary element that can be used with numerical integration schemes. Research is on going to develop an infinite boundary element that can be used with semi-analytical integration schemes. 11.6 Numerical Results If not the only one, [47] is one of the very few papers in which BEM is used for analysis of bonded joints. Some of the results from [47] are presented here. The results were generated using program BEAMUP that has been developed by the author and his students. Details of the program can be found on the webpage http://www.me.mtu.edu/%7Emavable/BEAMUP/index.html. Figure 11.3 shows a lap joint with various variables used in the numerical problems. The angle θ is the spew angle. The far field roller supported boundary with stress has to be modelled because the infinite boundary elements for analytical integration scheme used here are still being developed. The dimensions and material properties of the lap joint used by Pickett and Hollaway [26] is used as the basic geometry. Pickett and Hollaway did not consider any spew, that is θ = 90◦ . The remaining geometric parameters are: L1 = L2 = 12.7 mm h1 = 0.15 mm L = 76.2 mm h2 = 1.6 mm (11.18) The stresses were non-dimensionalized with respect to the far field stress σ . The material properties of adherend and the adhesive are shown in Table 11.1. In 11 Stress Analysis of Bonded Joints 317 y 0.5 L I L2 h1 C A σ x J θ B H G E F D K σ h2 L1 L Fig. 11.3 Lap joint geometry the analysis, the material parameters were non-dimensionalized with respect to the modulus of elasticity of the adhesive. 11.6.1 Discretization of Joint Boundaries into Sub-Boundaries A corner is a point where tractions are usually discontinuous and the modelling of density function must account for this discontinuity. Similarly one must provide for the possibility that the density function may become discontinuous at a point where the nature of boundary condition changes. To permit modelling of discontinuities in the density function, the boundary of each region is assumed to be made up of sub-boundaries. The end points of sub-boundary are corners and points where the nature (type) of boundary condition changes. These points in Fig. 11.3 are identified by the letters C through K. Continuity of density function is assumed at all points on the sub-boundary except the end points where the density function is permitted to be discontinuous. The last element on the sub-boundary is thus a discontinuous element [44] discussed in Sect. 11.4.1. The boundaries of bottom and top adherend of a lap joint are modelled as seven sub-boundaries: CD, DE, EF, FG, GH, HI, and IC as shown in Fig. 11.3. Each side of the adhesive boundary is modelled as a sub-boundary. 11.6.2 Graded Mesh for BEM In [47] a study was conducted to establish the importance of graded mesh along the interface for FEM as well as BEM. As the authors had only hr-mesh refinement scheme [10] for homogenous material, they described a procedure of constructing the graded mesh on the interface that is not discussed here. Stresses were evaluated Table 11.1 Material properties Adhesive Adherend Modulus of elasticity (GPa) Poisson’s ratio 3 69 0.36 0.32 318 M. Vable along line AB in both adherends to ensure that symmetry of results were not lost due to graded mesh construction. Figure 11.4 shows the graded mesh of quadratic elements on each sub-boundary of the adherend and the adhesive. The numbers of elements on each sub-boundary are shown in brackets in Fig. 11.4. The coordinate along each sub-boundary is non-dimensionalized with respect to the sub-boundary length in order to show the relative mesh distribution on all sub-boundary simultaneously. The sub-boundary meshes show a very fine mesh in the regions of large stress gradients (near point D along CD). In adherend, gradation of mesh is also seen near points H and E. Stress results close to the line HE show that there is a variation of stress due to bending that is being perturbed by the discontinuity of traction at these points. As these points have little impact on the stresses in the adhesive, it may be possible to eliminate this gradation by decreasing the number of elements for modeling the unknowns in the future. Note that the presence of bending stresses cause the mesh gradation to be different along sub-boundaries EF and GH. The mesh gradation in the adhesive sub-boundaries KD and CJ in Fig. 11.4 is small but influenced by the proximity of the maximum shear and peel stress. The differences in mesh gradation for sub-boundaries KD and CJ is a consequence of the procedure used in creating the graded mesh in [47]. Given the mesh is not very fine on these sub-boundaries, it is unlikely these differences, which are an artifact of the procedure of [47], has significant overall impact on the stress values, but is yet (a) (5) I C (20) H I (10) G H (5) F G (10) E F (10) D E (30) C D 0.00 0.20 0.40 0.60 0.80 Non-dimensionalized boundary length 1.00 (b) K D (5) J K (30) C J (5) D C (30) 0.00 0.20 0.40 0.60 0.80 Non-dimensionalized boundary length 1.00 Fig. 11.4 Mesh of quadratic elements. (a) Adherend. (b) Adhesive boundary 11 Stress Analysis of Bonded Joints 319 another reason for the development of mesh refinement scheme for multiple materials. The total number of unknowns for modelling the lap joint are 1075. Results are also included for some cases for a uniform BEM mesh having the same number of elements on each sub-boundary as shown in Fig. 11.4. A graded mesh of 240 four noded quadrilateral elements is used for FEM results for comparison. The graded mesh was produced by starting from the free edges of the bonded region and increasing the length of successive elements by a factor of 1.25. The results were obtained using the commercial finite element package ABAQUS [1]. Stresses were calculated through the center of the adhesive. Plots were made of peel stress (σyy ) and shear stress (τxy ) for each case. Note the stress results will be for the non-dimensionalized stresses with respect to the far field stress σ . As both FEM and BEM are highly susceptible to the gradation in the meshes, the results should be viewed with caution in deducing conclusions about relative merits of either methodology. The purpose of comparing results of FEM and BEM is only to establish viability of BEM as an alternative in the analysis of bonded joints. 11.6.3 Single Lap Joint with No Spew Figure 11.5 shows the results for shear and peel stress through the middle of the adhesive obtained by FEM and BEM with uniform and graded mesh. The results show very similar trends. The BEM graded mesh has a better stress gradient resolution than the BEM uniform mesh. The peak values for stresses by FEM are higher than the BEM uniform and BEM graded mesh. Neither FEM nor BEM have optimum meshes, hence too much should not be read into the relative merits of the two methodology based on the results shown in Fig. 11.5. The only conclusive observations that can be read from the results of Fig. 11.5 are: (i) BEM is a viable analysis technique for lap joints; (ii) research is needed for developing a mesh refinement scheme to produce optimum meshes for multiple material problems. 11.6.4 Double Lap Joint with No Spew From analysis perspective, the primary difference between a single lap joint and double lap joint is the boundary condition imposed on the sub-boundary of the lower adherend shown in Fig. 11.3. In the input of the computer program the boundary condition was changed from a free boundary to a roller boundary with zero normal displacement and zero tangential traction. The stress results are shown in Fig. 11.6. Once more the FEM and BEM results show similar trends. Again it must be emphasized that neither BEM nor FEM has optimum graded meshes and the differences in 320 M. Vable 1.00 0.87 Normal Stress 0.73 FEM 0.60 0.47 BEM graded 0.33 0.20 BEM uniform 0.07 –0.07 –0.20 –7.00 –5.25 –3.50 –1.75 0.00 1.75 3.50 5.25 7.00 3.50 5.25 7.00 x-coordinate in mm 0.60 0.51 Shear Stress 0.42 FEM BEM graded 0.33 0.24 BEM uniform 0.16 0.07 –0.02 –0.11 –0.20 –7.00 –5.25 –3.50 –1.75 0.00 1.75 x-coordinate in mm Fig. 11.5 Results for single lap joint with no spew results can be an outcome of the gradation rather than something intrinsic to either methodology. 11.6.5 Single Lap Joint with Spew The lap joint with two spew angles of θ = 30◦ and θ = 45◦ were solved. The mesh on the adherend was not changed from that shown in Fig. 11.4a. The differences in mesh gradation for sub-boundaries KD and CJ is once more an artifact of the procedure used for creating graded mesh in [47]. The graded meshes are shown in Fig. 11.7. Figures 11.8 and 11.9 shows the stress results for various spew angles of θ = 30◦, θ = 45◦ and θ = 90◦ . The maximum peel stress and shear stress decrease significantly from no spew (θ = 90◦ ) to a spew with an angle of 45◦ . But the change in maximum stress is negligible when the spew angle is changed from θ = 45◦ to θ = 30◦ . 11 Stress Analysis of Bonded Joints 321 0.30 0.25 Normal Stress 0.20 FEM 0.15 0.10 0.05 0.00 –0.05 BEM –0.10 –0.15 –7.00 –5.25 –3.50 –1.75 0.00 1.75 3.50 x-coordinate in mm 5.25 7.00 5.25 7.00 0.30 0.26 BEM Shear Stress 0.21 0.17 0.12 0.08 FEM 0.03 –0.01 –0.06 –0.10 –7.00 –5.25 –3.50 –1.75 0.00 1.75 3.50 x-coordinate in mm Fig. 11.6 Results for double lap joint with no spew (a) K D (30) J K C J (30) D C (5) (5) 0.00 (b) 1.00 0.20 0.40 0.60 0.80 Non-dimensionalized boundary length K D (5) J K (30) C J (5) D C (30) 0.00 0.20 0.40 0.60 0.80 1.00 Non-dimensionalized boundary length Fig. 11.7 Adhesive meshes for spew angle of (a) θ = 30◦ (b) θ = 45◦ 322 (a) M. Vable 0.70 0.60 Normal Stress 0.50 0.40 θ = 90° θ = 45° 0.30 0.20 0.10 θ = 30° –0.00 –0.10 –0.20 –7.00 –5.25 –3.50 –1.75 0.00 1.75 3.50 x-coordinate in mm 5.25 7.00 (b) 0.70 0.63 θ = 90° Normal Stress 0.57 0.50 θ = 45° 0.43 0.37 0.30 θ = 30° 0.23 0.17 0.10 –6.50 –6.44 –6.38 –6.31 –6.25 –6.19 –6.12 –6.06 –6.00 x-coordinate in mm Fig. 11.8 Normal stress results for spew angles. (a) Over entire bond. (b) Magnified near the end of bond In Fig. 11.7, notice that the impact of spew angle on mesh gradation on boundaries KD and CJ is negligible. In other words, modelling of spew poses no additional complexity in BEM, which is certainly not true for FEM where the entire domain needs to be discretized with a fine mesh in the corners. The ease of modelling changing boundary shapes is a demonstrable reason for considering BEM in analysis of bonded joints. With similar ease, the rounding of adherend corners can be accommodated. 11.7 Research on the Horizon at Time of Publication The results in this chapter show that BEM is a viable technique for stress analysis of bonded joints. It has the potential of producing good resolution of stress gradients and is robust enough for parametric study of joint parameters. Further improvements in the resolution of stress gradients requires development of an hpr-mesh refinement scheme for material interfaces and development of infinite boundary elements for use with semi-analytical integration schemes. The hpr-mesh refinement scheme for material multiple materials [25] has been developed and its application to bonded 11 Stress Analysis of Bonded Joints (a) 0.50 0.40 Shear stress 323 0.30 θ = 90° θ = 45° θ = 30° 0.20 0.10 –0.00 –0.10 –7.00 –5.25 –3.50 –1.75 0.00 1.75 3.50 x-coordinate in mm 5.25 7.00 (b) 0.50 θ = 45° Shear stress 0.40 0.30 0.20 θ = 30° θ = 90° 0.10 –0.00 –0.10 –6.50 –6.44 –6.38 –6.31 –6.25 –6.19 –6.12 -6.06 –6.00 x-coordinate in mm Fig. 11.9 Shear stress results for spew angles. (a) Over entire bond. (b) Magnified near the end of bond joints is expected in the near future. Research is ongoing in the development of infinite boundary elements. The design of mechanically fastened joints is facilitated by stress concentration factor curves which are drawn as a function of various geometric parameters. 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Int J Adhes Adhes 20:145–154 Index A Acceleration vector, 291 Accelerative techniques (fatigue), 189 Accelerated test methods, 226 Activation temperature, 125 Adherend-adhesive interaction, 112 Adherend rounding, 131, 136–137, 148, 150, 244, 253, 254, 256–260, 263, 269, 306–307, 322 Adherend shaping, 135, 137–138, 306–307 Adherend thickness, 135, 144 Adherend yielding, 270 Adhesion, 111–112, 126 Adhesive thickness, 14, 19, 53, 58, 135, 138, 163, 177, 228 Adhesive thickness (effect), 57–58, 60, 62, 65–66, 72–76, 80, 90 Ageing, 226 Airy’s stress functions, 16, 56, 60, 80, 82, 86, 91 Aluminium adherend, 135, 137, 142, 145, 161, 211, 219, 228–237, 289, 296 Anaerobic adhesive, 77 Anticlastic bending, 139 Arrhenius’ equation, 102 Average shear stress, 149, 193 Average stress criterion, 156–157, 160 Axi-symmetrical stress analysis, 70, 74–75, 91 B Back-face strain measurement, 185, 190, 195–196, 217, 220 Backward substitution, 291 Band adhesive (butt joint), 64–70, 91 Beam model, 33 Beam theory, 29, 166–167, 170 Bending moment (butt joint), 64–70 Bending moment factor, 9–12, 29, 35–38, 44 Bending moment, 9, 29–30, 38, 167, 244, 265, 284–285, 293 Bent substrates, 133 Bessel function, 89 Bilinear behavior, 97–98 Bi-material interface, 245, 315 Bi-material wedge, 217, 245 Block impact test, 280, 295 Boeing wedge test, 296 Bolted-bonded joints, 128, 143 Bolted joints, 184 Bonded shrink fitted joints, 77–78 Bonding position (effect), 66, 68–69 Bonding area (effect), 68–69 Boundary element method, 305–323 Boundary element method (formulation), 305–306 Brittle adhesives, 116, 142, 145, 162, 172, 296 Brittle failure, 116 Buckling, 187, 265, 269–271 Bulk adhesive, 91, 95–96, 98–100, 102, 109–111, 112, 114, 124, 156, 165, 179, 219 Butt joints, 53–74, 108, 115–117, 138, 144, 244, 246, 293, 298–299 C Carbon fibre reinforced plastic, 109–110, 138, 193, 201, 204–205, 211, 219, 228–229, 234, 244, 268 Carrier, 95, 97, 107, 109, 124, 189 Castigliano theorem, 167, 171 Castro-Macosko model (conversion effect), 125 Cathodic delamination, 237–238 Cavitation, 116, 189 327 328 Characteristic length (continuum damage model), 178 Charpy test, 280 Chemical reactions, 229 Chemorheology, 125 Circumferential stresses, 259 Clamped-clamped, 37–38 Cleavage loading (butt joint), 60–64 Coarse meshes, 136, 140, 146, 148 Coefficient of thermal expansion, 99, 109–110, 245–246, 257 Coffin and Manson law, 202 Cohesive parameters, 158, 165–176 Cohesive strength, 162–164 Cohesive zone model, 47, 143, 150, 155, 161, 162, 189, 232, 234, 236 Collocation error, 312 Complementary energy method, 117 Compliance (creep), 101–102, 113 Compliance (fracture mechanics), 161, 166, 170 Compliance based beam method, 166, 167–169, 171–172 Compliance calibration method, 166, 170 Composite delamination, 26, 28 Composite laminates, 33, 43, 50, 135, 144, 263 Composite materials, 14, 15, 23, 95–96, 109–112, 111, 132–133, 134–135, 139–140, 156–157, 169, 179, 184, 211, 234, 243–244, 246, 259, 266–268 Computation memory, 147, 291–292 Computation time, 133, 140, 145, 150 Conductive adhesives, 109, 120, 125 Constant-life diagram, 193–194 Constitutive equation of a linear elastic solid, 282 Constitutive models (adherend), 29, 30, 34, 285 Constitutive models (adhesive), 95–126, 230, 290 Constrained matrix, 147 Continuity conditions, 29, 34, 117, 309, 312 Continuity error, 312 Continuum damage model, 155, 160, 177–179, 189, 218–219, 232, 234–236 Corner joints, 133, 245 Corner radius, 108 Corrected beam theory, 166 Coupled analyses (environmental degradation), 230, 235, 239 Crack acceleration effect (fatigue), 204, 214 Crack arrest point (fatigue), 212 Crack equivalent concept, 166–167 Crack front, 158, 238–239 Index Crack growth rate, 190, 208–209 Crack growth, 136, 158–159, 161–162, 164–167, 170, 181, 183, 186, 192, 195, 203, 206–207, 209–213, 228 Crack initiation, 136, 183, 236 Crack length correction, 165, 168, 170 Crack path, 220 Crack root plasticity (overload), 199 Cracked lap shear (CLS) joints, 25–50 Cracking, 189 Crash analysis, 292–293 Creep, 101, 103–104, 108, 112, 184, 187, 187–188, 202, 214–215, 218 Creep-fatigue, 214–216 Critical dimension (failure prediction), 157 Cross-head rate, 112–113 Crystalline polymers, 111 Cumulative fatigue damage model, 122, 190, 195, 203, 219 Cure, 95–96, 124–125 Curing stresses, 229 Cyano-acrylic adhesive, 298 Cycle mix method, 204–205 Cyclic strain hardening, 201 Cyclic strain softening, 201 Cyclic symmetry, 146 Cylindrical joint, 257, 293 D D’Alembert’s solution, 283, 291 Damage, 189 Damage equivalent stress, 219 Damage growth, 155, 160, 161–162, 165, 172, 178, 189, 195, 220 Damage initiation, 151, 160, 162, 164, 172, 184–185, 226–227 Damage mechanics models, 95–96, 109, 120, 155–179, 185 Damage parameter, 120, 163, 217 Damage partition method, 215, 217 Damage shift model (fatigue), 212 Data reduction scheme (fracture energy), 165–166, 169–170, 171, 175 Debond length, 26 Debonding (adhesive), 25, 28, 161 Debonding (filler), 189 Deflection wave, 281 Deformation gradient, 248 Deformation gradient tensor, 248 Deformation theory, 96–99 De-ionised water, 236 Delamination, 26 Density, 101 Index Density functions (boundary element method), 309, 310–311, 312–313 Deviatoric strain, 119 Deviatoric stress tensor, 96 Diagonal matrix, 162–163 Diameter of the rings (effect), 78, 84 Diameter ratio (effect), 74, 78 Differential geometry (surface theory), 117–119 Diffusion, 111, 227–228 Diffusion coefficient, 227–228 Dilatational waves, 281, 283 Direct boundary element method, 308–309, 315 Discretization, 305–306, 310–314, 317 Displacement vector, 247, 290 Distortion energy criterion, 101 Dissimilar adherends, 142, 156, 245 Dissimilar meshes, 147–149 Double cantilever beam, 162, 166–168, 173–174, 179, 190–191, 209–212, 214–215 Double lap joint, 19, 20, 104–106, 108, 133–134, 138, 140, 142, 156–157, 190, 193, 201, 204–205, 210, 219, 244, 319, 321 Dual bilinear fit, 98 Dual boundary element method, 309 Ductile adhesives, 116, 155, 161–162, 173, 179 Ductile failure, 116 Dynamic analysis, 280–281, 285, 289, 291, 292 Dynamic loadings, 244 Dynamic stress concentration, 289 Dynamic Volkersen model, 287–288, 293, 295 E Edge moment, 29, 38–39, 44–45 Edge shear force, 31 Effective plastic strain criterion, 156 Effective stress tensor, 120 Elastic limit strain, 104, 107 Elastic limit stress, 97–98, 105, 107, 121 Elastomer modified epoxy adhesive, 97 Elasto-plastic fracture mechanics, 208, 211 Embedded process zone, 161 End loaded split, 169–170 End notched flexure, 161–162, 165, 169–175, 179 Energetic criterion, 158, 159 Energy barrier (viscoelasticity), 106 Engagement length (effect), 78, 84 Entropy, 103 329 Environmental degradation, 11, 21, 179, 218, 225–240 Epoxy adhesive, 97, 107, 124, 135, 137, 145, 193, 195, 204–205, 211, 219, 244, 253, 256, 296, 298–299 Equilibrium equations, 29 Equivalent composite modulus, 117 Equivalent crack length, 168–169, 183 Equivalent elastic modulus, 114 Equivalent mixed-mode displacement, 164 Equivalent plastic displacement (damage model), 234 Error (numerical), 305–306, 307 Euler beam theory, 30–32, 35, 285 Excimer pulse lasers, 111 Explicit solver (dynamic analysis), 279, 292–293 Eyring theorem, 105–106 F Failure criterion, 22, 28, 47, 100 Failure criterion (stress/strain based), 47, 136, 156, 161–162, 179, 196 Failure criterion (fracture mechanics), 48, 157–160, 179 Fatigue crack growth curve, 209, 211 Fatigue failure, 184–185 Fatigue initiation, 184, 189–190, 192, 195, 207, 217–218 Fatigue life (limit), 120–124, 155, 192, 196–198, 205–206, 210–211, 218, 256 Fatigue loading, 186–189 Fatigue (modelling), 183–220 Fatigue propagation, 184, 189, 190, 192, 195, 217–218 Fatigue spectrum, 186, 199 Fatigue threshold, 208, 211–212 Fibre pull-out, 162 Fickian diffusion, 14, 21, 227–228 Filler, 95, 109, 125, 189, 245–246 Fine meshes, 136, 140, 145, 293, 318, 322 Finite difference method, 293, 305 Finite element analysis, 18, 19 Finite element method (butt joint), 72–73 Finite element method (equation), 289 First law of thermodynamics, 251 Flexible adhesive, 44 Fluid dynamics, 135 Forward elimination, 291 Fourier series, 18, 54, 60 Fourier’s law, 251 Four-Point End Notched Flexure, 169–170 330 Fracture mechanics, 28, 96, 104, 136, 155, 157–160, 185, 189–190, 192, 207–217, 227, 307, 314 Fracture process zone, 163, 166–167, 168, 169, 178 Fracture toughness, 26–27, 48, 208 Free end reflection (stress wave), 284 Fixed end reflection (stress wave), 284 Free-fixed, 38, 41 Free surface, 16–17, 138, 245–247, 252–254, 256–257, 260–263, 268, 270 Free volume, 110–111 Frequency (fatigue), 186 Functionally gradient joints, 110–111, 142 G Gaps (adhesive), 138, 244 Gas constant, 106 Gauss point, 178 Gauss quadrature, 311 Generalised plane strain analysis, 139 Generalized stress intensity factors, 108, 136, 217 Genetic algorithm, 172 Gerber equation, 194 Gibbs free energy, 102 Glass fibre reinforced plastic, 162 Glass transition temperature, 101, 190 Global yielding, 14 Goland and Reissner, 8, 27, 42–44, 47, 131, 293 Goodman equation, 194 Green deformation tensor, 248 Griffith, 208 H Heat transfer, 228, 243 Heat transfer coefficients, 243, 246, 252–253, 261 Heat transfer (conductive), 243, 246–247, 253, 257, 260, 261 Heat transfer (convective), 243, 246–247, 253, 254, 257, 260, 261 Helmholtz free energy, 103 Hemming technique, 279 High cycle fatigue, 192–193, 203 High strain rate, 280, 297, 298 High stress amplitudes, 201–202 Higher order theories, 43 Highly deformable adhesives, 116 Hilber-Hughes-Tailor method, 292 Hooke’s law, 115, 266 h-type meshing, 145, 314 hp -type meshing, 314 Index hpr -type meshing, 314, 322 hr -type meshing, 314, 317 Humidity (effect), 123 Hybrid joints, 140–141 Hydrostatic component, 137, 156 Hygro-mechanical finite element analysis, 211 Hygroscopic expansion, 227 Hygroscopic strains, 229 Hygroscopic stresses, 229 Hygro-thermal stresses, 230–232 Hygro-thermo-mechanical stress, 233 Hyperbolic tangent model, 20–21 I Identity matrix, 163 Impact dynamics (fundamentals), 281–285 Impact energy, 296 Impact modeling, 279–299 Impact strength, 279–281, 295, 299 Impact wedge-peel, 296–297 Implicit solver (dynamic analysis), 280, 291–292 Incremental finite element method, 245 Incremental theory of plasticity, 119 Indirect boundary element method, 308–309 Inertia force, 291 Inertia wheel test, 299 Initial elastic modulus, 110 Initial stiffness, 163 Instantaneous compliance (creep), 104 Instantaneous strain (creep), 104 Integration error, 311–312 Interface (displacement), 75–76, 80–82 Interface (failure), 58, 161–162, 177, 190, 232, 236, 238 Interface stiffnesses (cohesive zone model), 162 Interface (stress), 25, 57–59, 64–86, 90, 115–116, 133, 256–257, 260, 269, 274, 307, 313–314 Interface (traction), 18 Interface crack theory, 29 Interface crack, 25 Interface elements, 148, 161–162, 177 Interfacial strength, 107, 111–113 Interface (stress wave reflection), 284 Interlaminar fracture, 169 Internal strain energy, 158 Interphase, 95–96, 111–117, 125–126, 246 Interpolation error, 310–311 Inverse method, 162, 172, 175, 176 Irwin-Kies equation, 166, 171 Isostress condition (interphase), 114 Isothermal chemoviscosity model, 125 Index Isothermal theory of separation, 120 Iterative finite element analysis, 138 Izod test, 280 J J-integral, 29, 48–49, 208, 215 Joint design, 13–14, 116, 133, 185, 240, 244, 247, 259, 280, 296, 305, 323 Joint rotation, 10, 132 Joint strength, 4, 14, 20, 66, 68, 77–78, 85, 91, 104, 110, 116, 133–137, 138–139, 141–142, 143–144, 173, 244, 270 K Kelvin model, 100 Kinetic equation of solids, 281–282 Kinetic model (impact loads), 285–286 Kolsky bar, 297–298 L Lagrangian formulation, 247, 293 Lamé constant, 309 Lap joints, 3–22, 116, 120, 132, 133, 137, 192, 217, 245, 279, 296, 314–315 Lap-strap joint, 190–191, 199, 212, 219 Large deflection (overlap), 33, 34 Lifetime prediction, 226 Linear elastic fracture mechanics, 208, 215, 232 Linear fracture energetic criterion, 165, 175 Liu model (filler volume fraction effect), 125 L-joint, 234 Load eccentricity, 244 Load distribution (effect), 72–73, 77 Loading history, 119, 220 Load sequencing effects (fatigue), 188–189, 201 Log-log method (creep), 103–104 Longitudinal stress (adhesive), 14, 16–17 Longitudinal wave, 281, 283, 288 Low cycle fatigue, 193, 201–203 Ludwik’s equation, 107 Lumped weight matrix, 292 M Mass matrix (dynamic analysis), 291 Master curve, 101 Mat, 98 Matrix (composite material), 266 Matrix conditioning error, 313–314 Maximum cyclic load, 120–123, 124 Maximum peel stress (adhesive), 41–43, 45, 320 331 Maximum shear stress (adhesive), 43, 104, 113, 289, 320 Maximum stress, 97, 120 Maximum strain criterion, 47, 156 Maximum stress criterion, 47, 70, 97, 156–157 Maximum principal stress (adhesive), 135 Maxwell model, 96, 104, 106, 120–121 Mean stress (fatigue), 186, 192–193 Mean stress jumps (fatigue), 204 Mechanical adhesion, 117 Mechanical interlocking, 113, 117 Mechanical-hygro-thermal stress-strain state, 225 Mechanical stresses, 229 Mesh dependency, 150, 156, 160 Mesh insensitive, 136 Mesh convergence, 156 Mesh error, 314 Mesh refinement, 156, 305, 306, 314, 319 Metal adherend, 94, 111, 135, 138, 156, 211, 243–244, 268 Michell’s stress functions, 70, 74, 88–89, 91 Micro-cracking, 163, 189 Micromechanics (composite materials), 266–268 Microscopy measurement (crack), 212 Miner’s law, 198–203, 205 Mixed-adhesive joint, 111, 141–142 Mixed-mode, 155, 158–159, 161, 177–179, 210 Mixed mode flexure, 234, 236 Mixed-mode ratio, 164 Mixed-resin joint, 111 Mode I, 46, 158–159, 161, 165, 166, 168, 170, 172–173, 190 Mode II, 46, 158–159, 161, 162, 169–175, 177 Mode III, 158, 160, 175 Modified Bingham model, 120–121 Modified distortion energy criterion, 47 Moire interferometry, 135 Moisture, 13, 21, 184, 230, 234–235, 239 Moisture absorption, 226, 228, 230 Moisture concentration, 225, 227–229, 234 Moisture transport, 225, 227–229 Mixed-mode (loading), 26, 49 Multi-physics finite element analysis, 220 Multivariable nonlinear regression analysis, 125 N Navier equation, 282 Newmark-β method, 292 Newton quadratic method, 117 Newton’s law of cooling, 251 332 Newton-Raphson method, 250 Nodal displacement vector, 250, 290–291 Nodal temperature vector, 251 Non-destructive inspection, 189 Non-linearity (geometry), 26, 34, 44, 47, 102–103, 127, 131, 243, 244–245, 259, 260, 260–261, 268, 271, 274 Non-linearity (adhesive), 20–21, 98, 131, 230, 236, 243, 244, 260 Non-linearity (thermal), 243–274 Non-self-similar crack growth, 159 Non-uniform temperature distributions, 239, 243, 245, 254, 256, 257, 263–264, 269–270, 273–274 Normal stress (adhesive), 116 Notches (adherend), 138 Number of cycles to failure, 209 Number of cycles to fatigue initiation, 217 Numerical crack growth integration, 209–210 Nusselt number, 253 O Optical measurement (crack), 190 Origin symmetry, 146 Orthotropic material, 167 Overlap length, 5, 10, 13, 48, 134–135, 155, 176–177, 190, 256, 259, 265, 295 Overload (fatigue), 212 Over-stress, 119–120 P Parametric studies, 133, 144, 150, 306–307, 322 Particles, 109, 125, 142, 189 Patches, 138, 142, 144 Parameters (fatigue spectrum), 186 Paris’ law, 208, 211 Peak stress (adhesive), 7, 12, 15, 44, 122, 135, 142, 143, 200, 246, 255–257, 256, 259, 261, 265, 269, 271, 273–274, 316 Peel joint, 133, 156 Peel stress (adhesive), 6, 9, 11, 14–19, 29, 31–33, 35, 41, 42–43, 135, 319 Penalty function, 117–119 Pendulum hammer, 280, 295–296 Pendulum test, 295–297 Perturbation technique (nonlinear viscoelasticity), 103 Photoelasticity, 133 Piezo-electric loadcell, 296 Pin-and–collar joint, 298 Plane strain problem, 145 Plastic adherend, 131 Plastic energy density, 137 Index Plastic shakedown (fatigue), 201 Plastic strain, 97 Plastic strain amplitude, 202 Plasticisation, 227 Plasticity (adherend), 134, 285 Plasticity (adhesive), 92, 131–132, 134, 161, 179, 198, 199, 281 Point symmetry, 146–147 Poisson’s ratio effects, 139–140 Post-failure examination, 190 Potential barrier (viscoelasticity), 105 Power-law response (nonlinear viscoelasticity), 108, 125 Prandtl number, 253 Pre-crack, 153, 160, 171, 207 Pressure sensitive tape, 116, 120, 280 Primer, 111 Principal of virtual work, 249, 289 Processing conditions, 95–96, 124–126 Progressive wave, 283–284 p-type meshing, 145, 314 P –δ curve, 171–175, 179 Q Quadratic stress criterion, 164, 178, 298–299 R Radial stresses, 258 Ramberg and Osgood equation, 97 Random access memory, 147 Randomly oriented short fibers, 110 Rapid fracture (fatigue), 187, 187, 195, 207 Rate dependent material behaviour, 97, 98, 102–103, 108, 189 Ratio between fatigue limit and quasi-static strength, 193 Rayleigh waves, 281 R-curve, 172, 173–174 R-ratio (fatigue), 193–194, 208 Reflective symmetry, 146 Reinforcement (joint), 259–260, 268, 270 Reinforcement (composite material), 266 Relaxation modulus, 101–102 Relaxation time, 108 Repairs, 138, 142 Residual, 250 Residual failure load (fatigue), 205–206 Residual strains, 230, 246 Residual strength, 144, 199, 203, 225, 227, 234–238 Residual stress, 70, 229–230, 245–246, 257 Retained (“master”) node, 147 Retrograde wave, 283–284 Reversibility of the ageing processes, 240 Index Reverse bent joints, 133 Reynolds number, 253 Rice, J.R., 208, 215 Rivet-bonded joints, 132, 142–143 Riveted joints, 184 Rizzo’s method (boundary element method), 309 Roller-clamped, 38–39 Roller-roller, 38–39, 41–46 Rotational symmetry, 146 R-type meshing, 314 Rule of mixtures, 110 S Safety factor (fatigue), 192 Sandwich (joint), 8 Saw tooth waveform (fatigue), 187–188 Scarf joint, 4, 116–117, 133, 143, 293 Secondary creep rate, 103 Secondary phase materials, 109 Shape function, 250–251, 290 Shear modulus (adhesive), 111, 125, 289 Shear modulus (effect), 75–76, 79–80, 82 Shear modulus (interphase), 114–115 Shear stress (adhesive), 3–4, 5, 12–13, 15–19, 29, 31–33, 35, 41, 43, 45–46, 100–101, 112, 131, 132, 284, 318 Shear stress (substrate), 15–17 Shear-lag analysis, 6, 12, 113, 131, 285 Shear waves, 281, 283 Shift factor (creep), 104–107, 113 Single lap joint, 4–22, 31, 120, 132–133, 136–137, 139, 143, 145, 146, 161–162, 173, 177, 185, 190, 210, 219, 228–231, 232–234, 235–236, 244, 253–254, 279, 285–287, 293–294, 296, 319 Singularity, 18, 43, 58–60, 64, 66–67, 70, 72, 76, 95, 96, 108, 115–116, 126, 133, 136, 145, 156–157, 160, 178, 198, 199, 217–218, 245, 254, 280, 293, 299, 308 Sinusoidal waveform (fatigue), 186 Sliding elements (viscoelasticity), 120 Small strain-large displacement theory, 243, 247–249, 254, 260, 269–270, 274 S-N curves, 122, 192–193, 196, 198 Soft adhesive, 50 Softening law (stress-displacement), 162–163, 173, 177–178 Solid cylinders (butt joint), 70–71, 88–91 Specific heat, 253 Spew fillet, 131, 132, 135, 140, 145, 150, 210–211, 232, 235, 244, 253–262, 263–265, 269–270, 272–274, 306–307, 312–313, 316, 319–320 333 Spike waveform (fatigue), 187 Split Hopkinson bar, 297–298 Spring element, 28 Spring model, 27 Square waveform (fatigue), 187 Statistical analysis of the data (fatigue), 192 Steel adherend, 133, 138, 189, 240, 253, 257, 261, 293, 299 Stepped joint, 4, 143 Stiffeners, 192 Stiffness degradation approach (fatigue), 205 Stiffness matrix (continuum damage model), 178 Stiffness matrix (finite element method), 250, 290 Strain-displacement relation matrix, 290 Strain equivalence (damage), 120 Strain energy release rate, 26–29, 41, 48–49, 158–159, 190, 208, 210, 212 Strain-life approach (fatigue), 201–203 Strain matrix, 250 Strain rate, 97, 105, 112 Strain tensor, 247, 282, 289–290 Strap joints, 133 Strength degradation approach (fatigue), 203–204 Strength of materials, 156–157, 227 Strength of singularities, 108 Strength prediction, 47–49, 136, 143, 158, 165, 176, 299 Stress amplitude, 193–194, 201–203 Stress concentration, 95–96, 108, 116, 132, 135, 137, 142, 143, 150, 155, 167, 171, 184, 243, 244, 246, 254, 258, 263–264, 269, 285, 293, 305, 307, 323 Stress concentration factor curves, 323 Stress-free temperature, 229 Stress functions, 80–91, 117 Stress intensity factor, 28, 48, 157, 158, 208, 323 Stress jump (interface), 119 Stress-life approach (fatigue), 192–203, 220 Stress ratio, 124 Stress tensor, 250, 289–290 Stress wave, 279–280, 283–284, 287–288, 293, 295, 298 Stress wave propagation, 281, 289 Stress whitening, 97–99, 124 Stress-strain curve, 97 Submodelling, 140, 150 Superposition method (fatigue life), 123 Support (joint), 259–265, 268, 269–273 Surface acoustic wave, 281 Surface (adherend), 95 334 Surface roughness, 116, 138, 139, 256 Surface topography, 12, 96, 111, 115–117 Surface treatment, 111 Superposition law (stress waves), 283 Swelling, 227, 232 Swelling coefficient, 230 Symmetrical lay-ups (composites), 43 T Tailored interphases, 112 Taper, 132, 134, 138, 293, 306 Tap water (environmental degradation), 237 Taylor expansion, 291–292 Telegraph equation (dynamic Volkersen model), 287 Temperature (effect), 99–100, 101–102, 112, 123, 124, 134, 135, 138, 214, 228, 229–230, 239, 245 Tensile loading (butt joint of solid cylinder), 70–71 Tensile loading (butt joint of thin plates), 54–55 Tensile loading (tubular joint), 74–75 Theory of elasticity, 54 Thermal analysis, 243, 245–246, 257, 260–269, 270 Thermal boundary conditions, 243, 245, 247, 252–253, 257, 263–264, 268–269, 270 Thermal conductivity, 228, 252–253 Thermal cycling, 246 Thermal loads, 133, 243, 245–246 Thermal model, 251–252 Thermal strains, 230, 243, 245, 250, 252, 254, 256, 258, 262, 263–264, 269–270, 273 Thermal strain tensor, 250 Thermal stresses, 19, 111–112, 135, 138, 229, 243–274 Thermodynamic type displacement (environmental degradation), 236–238 Thermoplastic polyimidesulfone, 98 Thermoplastics, 98, 110, 120 Thermosets, 97, 98, 110, 124 Thin plates (butt joint), 53–70, 80, 91 Three dimensional finite element analysis, 28, 123, 134, 140, 144, 195, 228–229, 230, 244 Three dimensional failure map (fatigue), 217–218 Three-parameter solid model, 100, 120 Tied (“slave”) node, 146 Time (effect), 100 Time dependent fracture mechanics, 215 Time shift factor, 101 Index Time-temperature superposition principle, 101–102 Timoshenko beam, 43, 285 T-joints, 2, 134, 243, 259–274 Tongue and groove joints, 133 Torsional loading (tubular joint), 75–77, 79–80 Total-life methods (fatigue), 192–203 T-peel joint, 161–162 Traction-separation law, 161–162, 165, 173, 179 Transient strain (creep), 104 Transient temperature distribution, 243, 253 Transition elements, 147 Transverse stiffness (composites), 43 Transverse strength of composites, 137 Transverse stress (adhesive), 118 Trapezium waveform (fatigue), 187, 216–217 Tubular joints, 74–91, 134, 139, 156, 244, 245, 247, 256–259, 270, 299 U Ultrasonics, 190 Unidirectional reinforced polymers, 109, 246 Uniform temperature distribution, 243–245, 253, 268 V Variable amplitude fatigue, 211–214, 240 Variable frequency fatigue, 215–216 Variational principle, 19 Varying loading conditions, 122 Virtual crack closure technique, 28, 159–160 Viscoelasticity, 95–96, 99–101, 102, 113–114, 214, 252, 285, 293 Viscosity, 125 Viscosity coefficient, 101 Viscoelasticity (nonlinear), 99–102, 104, 108 Void, 96, 114, 138 Volkersen, 6, 13, 133, 279, 285, 287 Volume fractions, 109, 114, 125 Von Mises criterion, 47, 70, 156, 298–299 W Wavy lap joints, 133 Weakening of the interface, 227 Weighted residue, 306 Weld-bonded joints, 143, 279 Wet joints, 235 Wetting, 125 Width effects, 133, 139–140 Williams-Landel-Ferry (WLF) equation, 101 Wöhler, 192 Work hardening, 97, 108 Index X x-radiography, 190, 212 Y Yield criterion, 119 Yield point, 120 Yield stress, 97, 100 Young’s modulus (adhesive), 59, 91, 105 335 Young’s modulus (effect), 54–56, 57–58, 65–66, 70–71, 74–75, 83, 90, 91, 145, 245–246 Z Zero adhesive shear stress, 19, 45 Zero volume element, 232 Zigzag joint, 144