Mechanical Engineering Composite Laboratory EXPERIMENT P8: UNIAXIAL TENSILE TEST Department of Mechanical Engineering McMaster University - Hamilton, Ontario Editor: John Colenbrander August 2021 Version Number: 00 Version Date: August 2021 Introduction This lab manual describes the Uniaxial Tensile Test laboratory experiment, which can can be found in the lab locations document on Avenue2Learn. The author of the original lab manual is unknown. It has been updated to this format by the editor in 2021. Several edits have been made for clarity or to better correspond to the current course oering. Typesetting is in LATEX using the refman template. Contents 1 Objective 2 Theory/Background 3 Experimental Apparatus, Procedure and Data Collection 4 Results & Discussion 5 Conclusion Appendices A Property Calculations (Sample Calculations) B Material Data Tables 2 2 8 10 11 12 12 15 1 Objective To familiarize the students with the measurement of mechanical properties (yield strength, ultimate tensile strength, %elongation, ductility) of engineering materials via the uniaxial tensile test. 2 Theory/Background The uniaxial tension test is widely used to provide information on the strength and plastic properties of materials. In this test, a sample of material is elongated by a uniaxial load. The axial load, F, and the change of the sample's length, ∆l, are recorded. The test is performed on a tensile test frame equipped with load and displacement sensors and recording devices. Fig. 1 illustrates a typical, F(∆l ), tensile curve for a ductile material. Figure 1: Tension load - extension curve The actual range of the load and displacement depends on the material and dimensions of the sample. In order to compare dierent materials, the effect of sample dimensions is eliminated by translating load into force per unit cross-sectional areatensile stresses, elongation-tensile strain, σ (ϵ), ϵ. σ, and displacement into relative Fig. 2 illustrates a typical stress-strain curve, for an elastic plastic material. The basic mechanical properties per- taining to the strength and ductility of the material are referred to in terms of stresses and strains. Particularly, so called eective stress and strain utilized in strength analysis, translate any general three-dimensional stressstrain state to values equivalent to the uniaxial tensile test data, σ, and ϵ. The stress strain curve shown in g. 2 contains several characteristic points 2 Experiment P8: Uniaxial Tensile Test usually listed in standard material data sheets. The slope of the initial linear portion of the σ−ϵ curve is referred to as Young's modulus, E, which is the elastic stiness of the material under normal stress. Upon unloading from a stress-strain state within this range of deformation, the sample fully recovers its initial dimensions, i.e., the deformation is purely elastic, ϵel . Some materials may exhibit a non-linear elasticity, i.e., the value of Young's modulus, E, may not be constant, yet there is full elastic shape recovery upon unloading. Figure 2: Stress-strain curve, elastic-plastic material model If, during loading, the strain exceeds a specic limit, upon unloading the initial shape of the sample is not fully recovered and some portion of the total loading strain, ϵ, as plastic strain, becomes permanent. This permanent strain is referred to ϵpl . ϵpl , cannot be induced without ϵel , the stress level at which the referred to as the yield stress, Yo , of the The plastic strain, being preceded by elastic deformation, plastic deformation is initiated is material. Any structural application of a given material should ensure that the maximum value of the eective stress remains below the yield stress, otherwise under expected loading the shape of the structure would become permanently distorted due to plastic deformation. Most materials do not exhibit the presence of a distinct point, without a distinct yield point, Yo , Yo , on the σ − ϵ curve. For materials the yield stress is usually dened as the stress level at which the permanent plastic strain is 0.2%. In the material data sheets this kind of yield stress is referred to as R0.2 . Dierent national standards also list other denitions of the yield stress such as R0.1 , R0.02 , etc., which refer to 0.1% and 0.02% plastic elongation at the yield point. Beyond the yield point the deformation is elastic-plastic. This range of deformation is of primary importance for forming technology applications in which dierent mechanical components are shaped by plastic strains. In the forming technology applications, the plastic strain may become of two or more orders of magnitude greater than the elastic strain. Often, in the analysis of these applications, the elastic properties are neglected, and the material behavior is simplied by the so called rigid-plastic material model, Experiment P8: Uniaxial Tensile Test 3 for which the curve, σ(ϵpl ), begins at the initial yield stress, Yo (ϵ = 0) and ignores the elastic strain, (g. 3). Figure 3: Stress-strain curve, rigid plastic material model In the elastic-plastic range of deformation the level of stress may increase with the magnitude of the strains. hardening. This increase is referred to as strain Strain hardening indicates that the material is gaining strength due to the induced plastic deformation. If a strain hardened material is unloaded from the elastic-plastic range of deformation and reloaded again, the plastic deformation will not resume at the stress level indicated by the initial yield point, σ(ϵpl ), In Yo or R0.2 , but at the stress level near or at the level, reached just before the unloading. [r1 , r2 , r3 ] uniaxial tension test, only one of the principal stress com- ponents is non-zero - the axial stress, σ = σ1 , while the remaining two components associated with the planes orthogonal to the tensile direction are zero, σ = σ2 = σ3 . The elongation of the sample is measured by the ϵ = ϵ1 . However, as the volume of the sample is conserved, its axial strain, cross-sectional area decreases, and therefore, none of the principal strains ϵ1 > 0, ϵ2 < 0andϵ < 0. In the elastic-plastic range a sinσ1 , results in six principal strain components, three strains, [ϵ1 , ϵ2 , ϵ3 ]el , and three plastic strains, [ϵ1 , ϵ2 , ϵ3 ]pl . The axial is zero, i.e., gle stress component, elastic stress and strain are used as the reference but in general the deformation in tensile test has all the same stress and strain characteristics as any other deformation process. The uniaxial tension stress-strain state exists as long as the sample is being deformed uniformly. The initial increase of the tension load, F(Deltal ),shown in g. 1 is due to the strain hardening (monotonic increase of the stress level of the, σ = σ1 , σ(ϵ), curve). However, the axial stresses, are carried by the decreasing cross-section area, A, of the sample. At some point the eect of stress increase on the tension force becomes equal to the eect of the cross-section area decrease. At this point the force reaches a maximum value, Fm ax.. Any further elongation of the sample results in the drop of force and elastic unloading of the previously stressed material with the exception of one zone, which due to micro-structural or dimensional defects has the lowest load carrying capacity. At this stage, the overall extension of the sample length results in localization of the plastic deformation only in the weakest zone referred to as the neck. The stress state in the neck changes to a tri-axial tension, which is caused by the non- 4 Experiment P8: Uniaxial Tensile Test co-linearity of the neck prole with the sample axis. Essentially the stress state in the neck is undened and only the portion of the σ − ϵ curve within the uniform elongation range is considered valid. 2.1 Stress and strain measures There are two basic stress and strain measures used in material data sheets: the engineering and the true measure. The engineering stress and strain measures are obsolete; nevertheless, many national standards still utilize these traditional measures. The engineering stress, ratio of the instantaneous tensile force, of the sample, Fi , σeng , is dened as the to the initial cross-section area Ao , σeng = Fi A0 (1) and the engineering percent strain, e%, as the % ratio of the length increase, ∆l, to the initial length, lo , of the sample: e% = ∆l 100% lo (2) Figure 4: Engineering Stress-strain Curve However, during a tensile test the cross-section area of the sample, A, de- creases due to elongation while each subsequent increase of sample length, dl, takes place over an already elongated sample length, l. It is evident that by neglecting the change in the cross-section area, l, A, and sample length, the engineering measures are not representative of the actual strain and stress state of the material. The stress-stain curve expressed in the engi- neering measures is shown in g. 4. Apparently, based on the engineering stress denition (1) the value of engineering stress decreases past the point marked with the symbol U.T.S. This is misleading; in reality the true stresses continuously increase. Experiment P8: Uniaxial Tensile Test 5 The so-called true stress and true strain measures dene the stress and strain state correctly. The true stress, applied force, Fi , σ , is dened as the ratio of the instantaneous Ai : to the instantaneous cross-section area, σ= and true strain, ϵ, Z li l0 lo , (3) is dened as the product of integration, given by: ε= where, Fi Ai li , is the initial and, dl = ln l li lo (4) is the instantaneous length of the sample. The true strain is also often referred to as the logarithmic strain. 2.2 Strain-strain curve for plastic deformation The relationship, between true stress and strain measures is referred to as the stress-strain curve . For many materials, the experimental, σ − ϵpl , data can be modeled by an exponential function of the form: n σ = K (εo + εpl ) where K , ϵo and n (5) are material constants. These constants are determined by tting a curve expressed by equation (5) between experimental points obtained from a tensile test. Usually the curve-tting algorithm neglects the small elastic deformation. The constant, K , is referred to as ow stress = 1.0 and its value indicates constant. It represents the stress level for ϵo +ϵpl the overall stress level at which the material is deformed plastically. constant, ϵo , The is referred to as initial strain oset. This constant shifts the exponential curve (5) to a position at which for, ϵpl = 0, (the beginning of plastic deformation) the stress level is equal to the initial yield stress, σ = Yo . The constant, n, is referred to as the strain hardening exponent. It indicates the rate of material strain hardening. On a logarithmic scale graph, g. 5, the stress-strain curve, becomes a straight line with slope σ(ϵpl ), represented by equation (5) n, log(σ) = n log (εo + εpl ) + log(K) 6 Experiment P8: (6) Uniaxial Tensile Test Figure 5: Stress-strain curve in logarithmic scale 2.3 Coecient of Anisotropy, r An isotropic material exhibits identical properties in all directions in its volume. In general, an anisotropic material is characterized by dierent values of characteristic properties such as Young's modulus, yield stress, strain hardening etc. depending on the orientation of the loading direction in the material space. Particularly in sheet forming technology applications (for example, forming automotive body panels) a desirable deformation behavior is such that the material resists deformation in its thickness direction but is easily deformable in its plane. This behaviour promotes shaping of the surface over localized thinning and ultimately, splitting, of the sheet during forming. The uniaxial tension test is used to evaluate this property of sheet r, dened as the ratio of ϵ2 = ϵw , measured in the direction of sample's width over ϵ3 = ϵt , measured in the thickness direction: products by means of the coecient of anisotropy, the true strain, the strain, r = εw /εt The coecient of anisotropy, ◦ ◦ r, (7) is determined for three dierent directions ◦ 0 , 45 , 90 in the sheet plane with respect to the rolling direction of the sheet, r0 , r45 , r90 . 2.4 Tensile test data sheet Standard tensile test data sheets provide the following data: Sample dimensions - National standards list several standard dimensions for tensile test samples. They are dierent for at, bar and wire products. The 4:1 gage length/width type sample used in the laboratory comply with the ISO/ASTM recommendations for at (sheet) products with recommended gage length of 60mm (2.25 in) and width 12.5mm (0.5 in), Experiment P8: Young's modulus, Yield stress, Uniaxial Tensile Test Yo or E, R0.2 , - expressed as engineering stresses 7 Ultimate tensile strength U.T.S - expressed as engineering stresses U.T.S = F max /Ao Total Elongation, et % - obtained by putting a fracture sample back together and measuring the % of total length change, ∆lmax /lo . ef % = $ 100% Reduction of area, fractured section q, A.R. or %At - % of the area reduction of the 2.5 Additional data Plastic stress-strain curve parameters Uniform elongation, ϵu or K, ϵo , n, (true measures), %ϵu , - maximum elongation of the material outside the neck expressed in true or engineering strain measures, Coecient of anisotropy, r0 , r45 , r90 (used for at products only). 3 Experimental Apparatus, Procedure and Data Collection 3.1 Apparatus The Instron 4460 test apparatus and it's components are are shown in Figure 6. A test sample is shown with the extensometer installed, mounted in the jaw grippers, in Figure 7. Your TA will provide details of operation of the apparatus. Figure 6: Components of the Instron 4460 Uniaxle Test Apparatus 8 Experiment P8: Uniaxial Tensile Test Figure 7: A test sample installed in the jaws of the Instron. 3.2 Safety The participants of the experiment must wear safety glasses. All participants of this lab experiment must be familiar and follow the Standard Operating Procedure, (SOP), entitled P5 Plastic properties of sheet metal (Instron 1140). The full text of the SOP is available in JHE 207. 3.3 Experimental Procedure The objective of the experiment is to generate a complete material data sheet for a at product. The experiment will be performed on a standard tensile testing machine equipped with load cells, displacement, and strain gages. Prior to the experiment, the students should plan the steps of the experimental procedure. As part of the experimental procedure the students should perform full calibration of all the gages. A set of weights and a device equipped with micrometer screw will be provided to perform the calibration of the load and displacement sensors. Experiment P8: Uniaxial Tensile Test 9 4 Results & Discussion This section in your Full Lab Report will contain the answers to the questions posed to the student in the various lab elements (lab video, Procedure or Results sections, and Live Lab Session ). Of note, the expectation is that the student will not only answer the questions outlined in the Results section of the lab manual, but integrate them into a well-formatted and logical discussion 1 by interpreting the results. The student will link the results to theory presented in the Lab Manual or the literature, and demonstrate an understanding of the physics and engineering implications arising from the lab. The data tables, plots etc. prepared in the Results section and the appropriate information in the Background/Theory should be referred to throughout this section in order to support (or validate, or explain) the interpretation. Students are reminded to properly cite any references they use in their Discussion. The Full Lab Report Rubric and Example Full Lab Report on Avenue provide more details on how to address the Discussion section. After performing the lab, students should prepare the following graphs and address the following questions in the Full Lab Report. Please see the Lab Assignment for data that all students should prepare. 1. Create a graph of true stress/strain and engineering stress/strain for each sample. Plot both graphs on the same gure. 2. Plot the elastic zone for each sample and indicate the properties which can be extracted from the curve. 3. Fit a curve to the plastic region of the true stress/strain graph using the method described and equation (6). Show the logarithmic plots with the sample calculations and plot the empirical curve on the same gure as the engineering stress/strain and true stress/strain curves. What is the purpose of tting a curve to the stress/strain graph? 4. What dierences could be expected by making an extension vs. time graph and a displacement vs. time graph? What signicance would this portray? (Extension data is not provided, do not create the graphs) 5. Complete the property calculations sheets 6. Discuss the following results of the lab. Were the yield strengths of the materials what were expected or this material? Justify your results with information from the literature, or handbooks, remembering to correctly cite all sources. Do these values make sense according to the rolling direction of the samples? Discuss the signicance of the coecient of anisotropy. Which rolling direction would be best suited for high amounts of metalworking? 1 This means that the discussion section should NOT look like an assignment; it should be composed of paragraphs with full sentences and linking of ideas, so that a logical progression through the results/questions is presented. 10 Experiment P8: Uniaxial Tensile Test 7. Describe and discuss at least four sources of error in this lab which could aect the quality of results obtained. 5 Conclusion The student will be asked to draw conclusions concerning the results of their experiments with particular emphasis on the discussion question(s) given. Summarize the major conclusions regarding the experiment. By comparing the σ−ϵ curves of the dierent samples,what inuence does the rolling direction have on tensile properties? Experiment P8: Uniaxial Tensile Test 11 Appendix A Property Calculations (Sample Calculations) Sampled Rolled in 0◦ Directions: Property Formula Calculation Young's Modulus Note: Please indicate on graph also Ultimate Tensile Strength Total Elongation U.T.S = Fmax /Ao et % = (∆lo /lo ) X100% Reduction of Area Flow Stress Constant Strain Hardening Exponent Initial Strain Oset Uniform Elongation Coecient of Anisotropy 12 Experiment P8: Uniaxial Tensile Test Sampled Rolled in 45◦ Directions: Property Formula Calculation Young's Modulus Note: Please indicate on graph also Ultimate Tensile Strength Total Elongation U.T.S = Fmax /Ao et % = (∆lo /lo ) X100% Reduction of Area Flow Stress Constant Strain Hardening Exponent Initial Strain Oset Uniform Elongation Coecient of Anisotropy Experiment P8: Uniaxial Tensile Test 13 Sampled Rolled in 90◦ Directions: Property Formula Calculation Young's Modulus Note: Please indicate on graph also Ultimate Tensile Strength Total Elongation U.T.S = Fmax /Ao et % = (∆lo /lo ) X100% Reduction of Area Flow Stress Constant Strain Hardening Exponent Initial Strain Oset Uniform Elongation Coecient of Anisotropy 14 Experiment P8: Uniaxial Tensile Test B Material Data Tables Sampled Rolled in 0◦ Directions: Parameter Standard Material Data Sheet Value Gage length Initial Sample 25.4mm Gage width Gage thickness Dimensions Final Gage width Gage thickness Sampled Rolled in 45◦ Directions: Parameter Standard Material Data Sheet Value Gage length Initial Sample 25.4mm Gage width Gage thickness Dimensions Final Gage width Gage thickness Sampled Rolled in 90◦ Directions: Parameter Standard Material Data Sheet Value Gage length Initial Sample 25.4mm Gage width Gage thickness Dimensions Final Gage width Gage thickness Experiment P8: Uniaxial Tensile Test 15