Acquisition Method Report
Acquisition Method: GCMS SCAN.amx
Path:
D:\CDS Projects\IIT\Results\2022\EXTERNAL\FEBRUARY 2022\LAKSHMI 10022022\LAKSHMI BATCH1.rslt
1 Method Information
Last Saved As:
Created:
Version:
D:\CDS Projects\IIT\Methods\GCMS SCAN.amx Modified:
2021-02-26 17:11:37-08:00 Creator:
2022-0118-1739-28785 Method Status:
2022-01-18 09:39:28-08:00 Modifier:
SYSTEM Description:
Generic
SYSTEM
2 GC
Module Display Name:
Agilent 8890 Module Type:
GC Order:
1
2.1 GC Summary
Run Time:
53.5 min Post Run Time:
0 min
2.2 Oven
Equilibration Time:
Slow Fan:
1 min Max Temperature:
Disabled
350 °C Maximum Temperature Override:
Disabled
2.2.1 Temperature
Setpoint:
Post Run:
On (Initial):
50 °C
75 °C Hold Time:
0.5 min
Program
Rate
Value Hold Time
5 °C/min 180 °C 3 min
5 °C/min 300 °C 5 min
2.3 ALS
ALS Errors:
Pause for user interaction
2.3.1 Back Injector
Syringe Size:
Solvent A Washes (PostInj):
Solvent B Washes (PostInj):
Sample Wash Volume:
Dwell Time (PostInj):
Sample Wash Draw Speed:
Viscosity Delay:
L1 Airgap:
10 μL
3
0
8 μL
0 min
300 μL/min
0 sec
0.2 μL
Injection Volume:
Solvent A Volume:
Solvent B Volume:
Sample Pumps:
Solvent Wash Draw Speed:
Sample Wash Dispense Speed:
Sample Depth:
Solvent Wash Mode:
1 μL
8 μL
8 μL
3
300 μL/min
3000 μL/min
Disabled
A, B
Solvent A Washes (PreInj):
Solvent B Washes (PreInj):
Sample Washes:
Dwell Time (PreInj):
Solvent Wash Dispense Speed:
Injection Dispense Speed:
Injection Type:
3
0
2
0 min
3000 μL/min
6000 μL/min
Standard
2.3.2 Sample Overlap
Mode:
Sample overlap is not enabled
2.4 Front SS Inlet He
Excluded from
Readiness:
***Excluded from Affecting Mode:
GC's Readiness State***
Pressure:
Pre-Run Flow Test:
Split Heater:
Off Total Flow:
Off Liner:
Off
Off Septum Purge Flow:
A Liner has not been selected.
Off
2.5 Back SS Inlet He
Mode:
Total Flow:
Gas Saver:
Liner:
Split Heater:
10.2 mL/min Septum Purge Flow:
Off Split Ratio:
A Liner has not been selected.
On
On 250 °C Pressure:
On 3 mL/min Pre-Run Flow Test:
5 :1 Split Flow:
On
11.367 psi
Off
6 mL/min
2.6 Column
Column Outlet Pressure:
0 psi
2.6.1 Column #1
Column Information:
Agilent
Dimensions:
30 m x 250 μm x 0.25 μm (Uncalibrated)
Out:
MSD
Flow:
1.2 mL/min
D:\CDS Projects\IIT\Report
Templates\Acquisition_Method_Report.rdl
[Rev. 1]
Description:
Column lock:
(Initial):
Average Velocity:
hp_5ms
Unlocked
75 °C
40.402 cm/sec
Temperature Range:
In:
Pressure:
Holdup Time:
Printed: 2022-02-11 12:55:39-08:00
-60 °C—325 °C (350 °C)
Back SS Inlet He
11.367 psi
1.2376 min
Page 1 of 3
Acquisition Method Report
Control Mode:
Constant Flow
2.6.1.1 Flow
Setpoint:
On (Initial):
1.2 mL/min Post Run:
1 mL/min
2.7 Detector Evaluation
Perform Detector Evaluation Test:
Off Signal Selected:
No Signal Selected Checkout Sample:
None
2.8
2.8.1 MSD Transfer Line
2.8.1.1 Temperature
Setpoint:
On (Initial):
280 °C
2.9 Signals
2.9.1 Signal #1: Test Plot
Description:
Dual Injection Assignment:
Test Plot Save:
Front Sample
Off Data Rate:
50 Hz
2.9.2 Signal #2:
Description:
None
2.9.3 Signal #3:
Description:
None
2.9.4 Signal #4:
Description:
None
2.9.5 Signal #5:
Description:
None
2.9.6 Signal #6:
Description:
None
2.9.7 Signal #7:
Description:
None
2.9.8 Signal #8:
Description:
None
3 GC/MS
Module Display Name:
Agilent 5977 MSD Module Type:
GC/MS Order:
1
3.1 Acquisition Method
Tune File:
Quad Temperature:
Stop Time:
Gain Factor:
atune
150 °C
10 min
1
Ion Source:
Fixed Electron Energy:
Solvent Delay:
EM Saver:
EI
70 eV
3.5 min
Off
Source Temperature:
Acquisition Type:
Trace Ion Detection:
EM Saver Limit:
230 °C
Scan
Off
N/A
3.1.1 Scan Time Segments
Scan Time Segments
Time Start Mass End Mass Threshold Scan Speed
3.5 50
600
150
1,562 [N=2]
3.1.2 Real-Time Plots
Total Ion:
Enabled BPC:
Disabled
3.1.3 Jet Clean
Mode:
Not configured
D:\CDS Projects\IIT\Report
Templates\Acquisition_Method_Report.rdl
[Rev. 1]
Printed: 2022-02-11 12:55:39-08:00
Page 2 of 3
Acquisition Method Report
4 Method Properties
Instrument Technique:
Gas Chromatography
5 Schema version
Schema version:
2.3
Method Audit Trail
No method audit trail available
D:\CDS Projects\IIT\Report
Templates\Acquisition_Method_Report.rdl
[Rev. 1]
Printed: 2022-02-11 12:55:39-08:00
Page 3 of 3