Journal Pre-proofs Review A review of the effects of weak interfaces on crack propagation in rock: from phenomenon to mechanism Minghe Ju, Xiaofeng Li, Xing Li, Guanglei Zhang PII: DOI: Reference: S0013-7944(22)00061-3 https://doi.org/10.1016/j.engfracmech.2022.108297 EFM 108297 To appear in: Engineering Fracture Mechanics Received Date: Revised Date: Accepted Date: 2 September 2021 20 January 2022 31 January 2022 Please cite this article as: Ju, M., Li, X., Li, X., Zhang, G., A review of the effects of weak interfaces on crack propagation in rock: from phenomenon to mechanism, Engineering Fracture Mechanics (2022), doi: https:// doi.org/10.1016/j.engfracmech.2022.108297 This is a PDF file of an article that has undergone enhancements after acceptance, such as the addition of a cover page and metadata, and formatting for readability, but it is not yet the definitive version of record. 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A review of the effects of weak interfaces on crack propagation in rock: from phenomenon to mechanism Minghe Jua,b, Xiaofeng Lic* , Xing Lid, Guanglei Zhange aState Key Laboratory for Geomechanics & Deep Underground Engineering, China University of Mining & Technology, Xuzhou 211116, China bDepartment of Civil Engineering, Monash University, Clayton, VIC 3800, Australia cDepartment of Civil and Environmental Engineering, The Hong Kong Polytechnic University, Hongkong, China dSchool of Civil Engineering, Institute of Future Underground Space, Southeast University, Nanjing 211189, China eDepartment of Earth Science and Engineering, Imperial College London, London SW7 2BP, UK Abstract: This article reviews the effect of weak interfaces on crack propagation in rock and some other analogous brittle materials from phenomenon to mechanism. In this review, a variety of fracture patterns (in terms of a propagating crack interacting with a pre-existing interface) are classified, followed by the introduction of some critical influence factors, e.g. strength and toughness of interface, interface angle, interlayer effect, elastic mismatch, dynamic loading, and confining stress. Then, the effects of weak interfaces on the quasi-static and dynamic mechanical behaviors of rock are briefly reviewed. Thereafter, the mechanism of action of weak interfaces on crack propagation in rock is discussed in terms of crack deflection criteria. Finally, some conclusions and outlooks on the research of the effects of weak interfaces on crack propagation in rock are provided. Keywords: Weak interface; crack propagation; heterogeneous rock; dynamic loading; crack deflection criterion * Corresponding author: Xiaofeng Li (Email: xfli@whrsm.ac.cn; Tel: +86 19851538755) 1 / 51 1 Introduction Weak rock structures, e.g. grain boundaries, defects, joints, and faults, are omnipresent in rock at different scales (Fig. 1) [1-8]. As shown in Fig. 1, at the mineral scale, rock is a microscopic heterogeneous material composed of diverse minerals and pre-existing defects (e.g. microcracks, voids, cleavages, and grain boundaries) [7, 9-12]. The granitic rocks present a higher index of heterogeneity than the sedimentary rocks (e.g. sandstone and limestone) at millimeter-scale [7]. With respect to the isotropic characteristics of homogeneous rock, the fracturing behavior of heterogeneous rock is significantly affected by the geometrical features of mineral grains [9-12]. As shown in Fig. 1, the intrusion of dissimilar geomaterials (rock veins, dykes, and sills) is also widely encountered in rock [13, 14]. These dissimilar inclusions could remarkably change the failure pattern of a rock structure. Furthermore, in the exploitation and utilization of underground resources and energy, the path of hydraulic fluid-driven cracks in jointed rock masses may be disturbed by discontinuous geological structures [7, 15-17]. Drilling rig Volcano Not to scale Rock mass Dissimilar inclusion Crack deflection Fault Underground cavern Hydraulic fractures Dyke Magma chamber σv Dynamic load Rock veins Natural fractures Granite 2 mm σh Natural fractures Crack penetration Sill Well Bedding planes Mineral grains Inclusion in granite Rock veins Inclusion in rock mass Hydraulic fracture propagation Blasting in jointed rock Figure 1. Different types of weak rock structures at various scales [5-7, 17]. The trajectory of a propagating crack may be altered when one of the following two scenarios is encountered: (i) a change in loading state, and (ii) the presence of a pre-existing interface and defect [18, 19]. In this review, the term “interface” is used to include different stress and displacement conditions of a rock fracture (a non-welded fracture: stress continuity and displacement discontinuity, and a welded fracture: stress continuity and displacement continuity) [20]. Loading-induced crack kinking occurs commonly in rock materials and rock 2 / 51 engineering, e.g. crack kinking from the tip of an inclined flaw towards the direction of maximum principal stress [21], hydraulic fracture propagation in different in-situ stress states [17, 22]. “Crack kinking/deflection” denotes crack propagation off its original path due to the change in local fracture mode mixity (a mechanical factor) or fracture toughness (a material factor) [19]. In a mixed loading state, cracks tend to propagate along the path of least resistance and kink into a pure Mode-I crack in brittle rock materials [21, 23]. However, pre-existing interfaces may change this sequence on account of their inherent weakness. The manifestation of pre-existing interfaces on crack propagation is more intricate, not only in the elusory fracturing network [3, 24], but the mechanical behavior of materials/structures may also be altered [9, 10]. As with the influences of bedding planes, joints, weak zones etc. in a rock mass (Fig. 1), the originally isotropic rock matrix exhibits significant anisotropic mechanical and physical behaviors [25, 26]. These all are attributed to the disturbance of weak tectonic structures on the rock stress and deformation fields [26, 27]. If subjected to external static/dynamic loads or inner pore pressures, cracks will initiate in the rock mass and interact with such weak structures. In that case, the trajectories of original cracks are distorted into a dispersed fracture network, which can significantly influence the stability of underground structures and efficiency of hydraulic performance [28]. These behaviors are related to the magnitude of the applied loads and pre-existing crack distributions [11, 29]. In this literature review, a variety of fracture patterns (in terms of a propagating crack interacting with a pre-existing interface) are classified, followed by the introduction of some key influence factors, e.g. strength and toughness of interface, interface angle, interlayer effect, elastic mismatch, dynamic loading, and confining stress in Section 2. Thereafter, in Section 3 the effects of weak interfaces on the quasi-static and dynamic mechanical behaviors of rock are reviewed. The mechanism of action of weak interfaces on crack propagation in rock is discussed in terms of crack deflection criteria in Section 4. Finally, some conclusions from, and outlooks for, the research into the effects of weak interfaces on crack propagation in rock are demonstrated in Section 5. This review work gives a detailed summary upon the effects of weak interfaces on crack propagation in rock or rock-like materials/structures, and is of significance for the comprehensive understanding of different fracture patterns influenced by weak interfaces. 2 Effects of weak interface on crack propagation in rock 3 / 51 2.1 Crack propagation pattern The problem of a crack approaching an interface between two dissimilar materials is fundamental to the understanding of the behavior of non-homogeneous materials [30]. For two materials in contact (Materials A and B), when a plane crack initiates under external load in Material B, it propagates and interacts with the pre-existing jointed interface, on account of the relative locations of the propagating crack and pre-existing interface: a series of fracture patterns are classified as shown in Fig. 2. It should be noted that the classifications of different fracture patterns are not limited to rock materials or structures but some other brittle and composite materials and structures are also included due to certain similar fracturing performances. Generally, there are four types of primary positions of the crack relative to the interface: (i) the crack makes close perpendicular contact with the interface; (ii) the crack contacts with the interface directly at an oblique angle; (iii) the crack normal to the interface leaves a ligament between the crack-tip and interface; (iv) the crack is obliquely ahead of the interface. Perpendicular crack (a) B A Crack Interface (b) B Direct penetration Single deflection Double deflection Debonding head Shearing head Penetration head Direct penetration Single deflection Double deflection Curve away Curve toward Mixed cracking A Crack Interface Inclined crack (c) B A Crack Interface (d) B Mixed cracking A Crack Interface Figure 2. A brief summary of crack propagation patterns when approaching a bimaterial interface. (a) and (b) are the types of a propagating crack interacting perpendicularly with a pre-existing weak interface [31-35], while (c) and (d) are scenarios in which an inclined crack propagates to the interface [34, 36, 37]. 4 / 51 The most popular condition is shown in Fig. 2a where the crack interacts perpendicularly with the interface. In the early stages, the T-shaped double deflection of laminated structures was studied as it is common in composite failures [31]. Lu and Erdogan [32] summarized the general cracking patterns of a crack normally contacting an interface, which are direct penetration, double deflection, and mixed double deflection and penetration. These are the widely encountered fracture patterns in brittle materials and structures [33]. Later, He and Hutchinson [34] theoretically found that single deflection is also one of the typical fracture patterns. From their systematic quantifications of double deflection, single deflection, and direct penetration, single deflection was ignored on account of its low possibility of occurrence when the mechanical properties of the two contacting materials are similar. After that, the investigations on crack deflection and penetration at an interface were expanded across broad areas of interest including: fiber reinforced and layered composites [38-40], laminated ceramic composites [41-44], fluid transmission in the geological layered structures [45-49], as well as crack propagation in layered rock structures [3, 50] (with some examples represented in Fig. 3). (a) (b) Sill Dyke (c) (d) Double deflection Single deflection Direct penetration Double deflection Figure 3. Some cases of crack normal interaction with a weak interface/contact. (a) A video record of the process of the deflection of a primary crack at a bi-layer interface in a model system made of brittle rubber blocks [43], (b) different styles of intrusive behavior of dyke and sill formation [45, 51], (c) T-shaped fracture between two stiff limestone layers [50], (d) in situ photographs of direct penetration, double deflection, and single deflection in layered sandstone [3]. 5 / 51 Some researchers proposed that direct contact of the crack with an interface is a critical condition which happens only when the interface is strong enough [35, 52-55]. Normally, if with a weak interface, the interface should first debond when the propagating crack is about to reach it, which is attributed to the specific stress field around the crack-tip. Cook and Gordon [35] primarily explored different debonding patterns of the interface ahead of the crack-tip, with the typical patterns of interface debonding in tension and shear modes shown in Fig. 2b. Leguillon and Martin conducted a series of studies into interface debonding ahead of the crack tip based on the findings in [35] and [34]. They systematically discussed the requirements for each debonding state [52, 53, 56]. In addition of the patterns in [35], they found that penetration in the target matrix ahead of the crack-tip is also possible [56-58]. Moreover, a more complicated pattern of bifurcated penetration ahead of the crack-tip was also detected [40, 59]. Interface debonding ahead of the crack-tip was also observed in some experiments [60] and numerical simulations [59]. These essential findings have been used in rock engineering for the study of the interactions between hydraulic fractures and natural defects [36, 61], dyke and sill formations [62-64], as well as layered and grain-based rock fracturing [3, 65]. The condition of a crack normal to the interface is a particular case which is somewhat ideal in the process of crack propagation. When the propagating crack interacts closely with the interface, at an inclined angle, as illustrated in Fig. 2c, the fracture patterns are slightly different from those in Fig. 2a. The cracking path is no longer symmetrical and the specific profile is related to the material properties [34, 36, 66-68]. These manifestations make the prediction of crack trajectory more difficult but practically meaningful in the investigations of sill formation in conditions affected by pre-existing structures [69-71], injection-induced faulting and earthquakes [69, 72], and crack propagation in a jointed rock mass [73, 74]. The most complicated cases of cracking pattern should be those in Fig. 2d where the inclined straight crack would curve away from, or towards, the interface depending on the relative properties of materials A and B [34, 37]. Many studies have explored this phenomenon as it dominates the failure of grain-based or laminated materials/structures [37, 75-80] where the crack is attracted towards the soft materials while deviated from hard materials. 2.2 Influence factors The cracking network in a structure with massive weak interfaces is the cumulative result of a couple of fracture patterns shown in Fig. 2. Without the weak interfaces, crack propagation in a quasi-homogeneous structure is predicated by the stress state. However, the defined crack paths are disturbed causing the global failure of a structure unclear as the existence of weak 6 / 51 interfaces [81, 82]. Many factors may affect the local fracture pattern when a crack approaches an interface, e.g. strength and toughness of each phase, geometrical properties of each component, as well as the loading state. (1) Strength and toughness The strength or toughness of an interface plays a significant role on the ultimate fracture pattern at an interface or the global failure pattern of a layered or grain-based structure. It has been found in some experiments [83] and simulations [77, 84, 85] that with the increase in strength or toughness of interface, the fracture pattern at an interface may shift from double or single deflection to direct penetration. Not only given changes in the mechanical properties of interface, changing the strength or toughness of substrate material, the fracture manifestation will also be changed. For instance, as the matrix strength decreases, the fracture pattern is changed from penetrating the interface instead of deflecting into the interface [86]. These local changes of fracture pattern would affect the subsequent fracturing performance. As shown in some laboratory tests [87, 88] and numerical simulations [89-91], by increasing the strength or toughness ratio between the interface (or grain boundary) and matrix (or crystalline grain), the percentage of crack deflection decreases and the fracture path becomes better defined (Fig. 4). (a) Crack propagation (b) Figure 4. (a) Intergranular and transgranular cracking performance in a grain-based brittle material with respect to the ratio of fracture energy between the grain boundary and crystalline grain (Rm = ГIG/ГTG). The roughness of the main fracture path is lower at a greater Rm [90], (b) interface strength on crack propagation in laminated structure where the interface strength decreases from left to right [87]. (2) Interface angle and grain size Crack propagation is not only affected by the relative mechanical properties of the interface and substrate material, but the geometrical properties of the interface also exert a significant influence on the ultimate fracture pattern. Numerous experimental and numerical 7 / 51 studies have been conducted on this topic. With respect to the propagating crack normally towards the interface, the inclined crack is likely to deflect into the interface [92]. Generally, the interface debonding length decreases with the increase of interface angle [84, 93-96]. Sometimes, at a certain strength or toughness of the interface, there is a transition of the cracking pattern from single deflection to double deflection [97] or from single deflection to direct penetration with increasing interface angle (with some experimental observations, as shown in Fig. 5a and b) [68, 94, 96, 98-100]. (a) (c) (b) Small grain size 1 μm 1 μm Large grain size Figure 5. Some examples of the effect of interface angle on crack propagation. (a) An experimental study of crack deflection at an interface [68], (b) microscopic observation of crack deflection in a brittle material [98], (c) a phase-field modeling of grain size-effects on crack propagation [101]. The influence of grain size on crack propagation is attributed to the intersection angle between the grain boundary and the propagating crack. This is similar to the effects of weak interfaces in layered structures [101, 102]. As shown in Fig. 5c, when the propagating crack interacts with a large grain, if the direction of the propagating crack is determined, the intersection angle between the grain boundary and the crack is greater than that with a small grain. In addition, the interfacial crack will deflect into the target grain after a certain length of interface debonding. Hence, transgranular cracking is more likely in the grain-based heterogeneous structure with a larger grain size as suggested by the aforementioned two reasons. Such a manifestation is also reflected in laminated structures (Fig. 5a and b) in which interface debonding within a certain distance occurs followed by crack deflection into the substrate. The influence of grain shape on crack propagation is the same (in principle) in terms of the 8 / 51 interaction angle between the crack and the tangent line at the contacting point. The material is vulnerable to crack-penetration through the grain boundary for strip-like grains inclined at a large interface angle [103]. (3) Interphase/interlayer In practice, the interface between two main materials or structures sometimes cannot be clearly identified, instead, a thin interlayer structure is sandwiched between the two main layers. This thin interphase plays a more complicated role in the crack propagation than a single interface [104]. Some typical profiles of the interphase in Fig. 6 indicate that the propagating crack enters the interphase, the original direction of crack propagation is disturbed. Such local disturbance causes the subsequent and global failure of a structure to be erratic. The interphase can be regarded as a thin layer, dissimilar to the substrate, if it is relatively homogeneous (Fig. 6a). Thus, the crack propagation patterns relating to the geometrical and mechanical properties of material as well as loading state can still be found from those in Fig. 2 [92, 104, 105]. On the other hand, crack bifurcation in the interlayer may occur if the weak interlayer is thick and the residual stress (due to the difference of material property between adjacent layers) is significant [44, 106, 107]. Such weak interlayers cause the step-wise failure of the laminated structure and the R-shaped apparent toughness evolution [107, 108]. (a) (b) (c) (d) Figure 6. Different types of interphases in a composite brittle structure. (a) Weak interphase filled with pervasive hard materials, (b) interphase with a layered discontinuous structure, (c) multilayer interphase, and (d) porous interphase [104]. If the interphase is inhomogeneous (Fig. 6b-d), e.g. in a discontinuous structure filled with massive defects and pores analogous to the rock joints or an interphase constituted by a couple 9 / 51 of sub-interlayers, the crack trajectory in the interphase is dispersive [3, 104]. Even so, the local competition between crack deflection and crack penetration at a weak interface is still satisfied but the overall failure is fairly random. In addition, illustrated in Fig. 6, such weak interphase behavior can change the crack path and often trap the propagating crack. This makes it possible to use the interphase to protect certain vulnerable structures [83, 109, 110]. (4) Elastic mismatch The dissimilar elastic properties between two contacting materials exert a significant influence on crack propagation at an interface (Fig. 7). Dundurs [111] proposed two parameters that determine the degree of elastic mismatch between two adjacent materials. Such elastic mismatch manifestation forces the energy distribution around the crack-tip to distort when approaching an interface [4, 112]. The possibility of deflecting into, or penetrating through, the interface is correlated to whether the crack propagates from stiff or compliant material [4, 75, 77], where the crack is likely to deflect into the interface if propagating from a compliant material to a stiff one (EB < EA) [45, 70, 101, 113]. In addition, the fracture patterns of curving towards or curving away from the interface (Fig. 2d) are attributed to the elastic mismatch between two materials if the crack is under Mode-I loading state. Some tests showed that the propagating crack curves to the direction of interface when approaching the interface from a compliant material to a stiff material [75, 114]. On the contrary, the crack directly penetrates the interface if propagating from stiff to compliant materials. Such a difference is also indicated from the stress intensity evolution of the crack-tip from stiff to compliant material as this case is quite different from that in an inverted direction of crack propagation [115]. 10 / 51 (a) 14 (b) 12 Dyke Sill Arrested dyke Dyke-sill hybrid Dyke P0/PfU 10 Limestone Sill 8 6 Marl Interface 4 2 0 0.1 1 (c) Eu/El 10 100 Limestone Eh Em Em Figure 7. Elastic mismatch of two contacted layers on crack propagation. (a) An experiment showing different patterns of dyke and sill formation [45], (b) crack propagation in a layered rock structure with marl sandwiched between two limestone layers (modified from [113]), (c) a phase-field simulation of elastic mismatch of layers on crack propagation [101]. (5) Dynamic loading Crack propagation and interaction with a pre-existing interface under dynamic loading manifest different phenomena from those in quasi-static conditions. If the crack has a low propagation velocity, when it interacts with a weak interface, the propagating crack may form T-shaped double deflection patterns and be trapped within the interface; however, with increasing velocity of crack propagation, the interface debonding length decreases [116] and the fracture pattern may even transform from deflection to penetration [117]. Essentially, fracture pattern transition is the reason for fracture-surface roughness reduction when increased crack-propagation velocity is found in heterogeneous brittle materials [65, 118]. However, experiments by Sundaram and Tippur [119] suggest that a crack can bifurcate at the interface even when given a fast crack-propagation velocity. This is on account of the higher magnitude of tensile stress perpendicular to the interface when the crack is subjected to a greater propagation velocity. Thus, the tensile stress drives the interface to debond and contributes to crack deflection [119, 120]. Similar to those quasi-static conditions, the fracture pattern changes from crack deflection to crack penetration with changing interface angle [18, 121, 122] but multiple cracks may 11 / 51 sometimes form under dynamic loading [123]. Furthermore, a weak interface can restrain the dynamically propagating crack [18, 124] and the crack deflection length generally increases with the reduction of interface strength [120, 121, 125]. The same principles as those governing behavior in quasi-static states should make sense yet the effect of a weak interlayer on crack propagation under dynamic loading is different from those in quasi-static conditions. When two similar materials make close contact, but without adhesion (an open joint), the propagating crack would be arrested within the interface. Nevertheless, the fracture pattern would be converted from deflection to penetration if the interface is an adhesive layer [24]. Furthermore, as the interlayer thickness increases, the penetrating mother-crack would branch into a cluster of daughter-cracks (Fig. 8) [24, 126]. One explanation for this phenomenon is that the reduction of the interlayer stiffness contributes to crack bifurcation at an interface [127]. These phenomena give rise to the idea of using the weak interface or interlayer to enhance the fragmentation intensity of rock. (a) 5 mm (d) 5 mm (b) (c) 5 mm 5 mm (e) 5 mm Figure 8. Crack dynamic propagation through an interface. (a) Monolithic brittle material, (b) interface without adhesion, (c) interface having a near-zero-thick adhesive layer, (d) interface with a 0.13 mm-thick adhesive layer, (e) interface having a 2.5 mm-thick adhesive layer [24]. (6) Confining stress Confining stress is also one of the significant factors affecting crack propagation at a weak interface as both the stress fields around the crack-tip and at the interface are changed [128]. The most typical example in geological engineering work is the fluid-driven crack propagation in jointed rocks, e.g. the interaction between a hydraulic fracture and natural fractures [22, 129, 130], and the formation of dykes and sills in layered rocks [130]. Considering the maximum and minimum principle stresses (σ1 and σ3), the frictional properties of the interface, and the interface angle, Blanton [129] proposed a criterion for determining whether the hydraulic fracture will cross, or be terminated in, the interface based on the hydraulic-fracture 12 / 51 experimental results and this is verified by subsequent experiments and simulations (with some recent typical cases in [17, 82]). In addition, another classical analysis of confining stress on crack deflection at a frictional interface was performed by Renshaw and Pollard [131] where they took the superimposed stress field into consideration (confining stresses and stress field at a random point around the crack-tip). A modified version of their work was exhibited later [132]. These analyses considering the frictional characteristics of the interface can predict the cracking behavior of a hydraulic fracture approaching a natural interface [17, 100, 133]. Generally, in these results, for a given interface angle or coefficient of friction, the fracture pattern may change from crack penetration to crack deflection with decreasing stress difference (σ1-σ3). 3 Effects of crack propagation on mechanical property 3.1 Weak interfaces and their effects on rock fracture toughness Fracture toughness is a quantitative way of expressing the resistance of a material to crack propagation, which proves the ability of a rock structure to bear load or resist deformation in the presence of an initiated crack [134]. Fracture toughness is remarkably related to the rock microstructures, in both of physical and mechanical terms [9, 134-138]. In general, the microcracking types in a grain-based heterogeneous rock are intergranular cracking along the grain boundaries and transgranular cracking through the mineral grains in tension or shear mode [139, 140]. Nasseri et al. undertook a series of experimental investigations of granitic microstructures on fracture toughness. In their studies, granite is under anisotropic conditions due to the differences in mineral composition, e.g. quartz and feldspar, in different directions. Basically, four consequences arise: (i) fracture toughness of granite decreases inversely with the square root of grain size (KIc~Lg-0.5) [134], which is akin to the principle of uniaxial compression tests (σc~Lg-0.5) [135, 141, 142]; (ii) fracture toughness monotonically decreases with pre-existing crack density Dc (KIc~Dc-0.3), crack length Lc (KIc~Lc-0.5), or crack porosity pc (KIc~pc-0.62) [134, 143]; (iii) fracture toughness linearly increases with fracture surface roughness θ*/C (KIc~θ*/C) [9, 144, 145], where θ* and C are the apparent dip angle on the fracture surface and a roughness parameter characterizing the distribution of θ*, respectively [146]; (iv) fracture toughness gradually decreases with the temperature of thermal treatment, which may also be attributed to the difference of thermally-induced pre-existing cracks [147]. Moreover, it was found that the anisotropy index of fracture toughness of Barre granite (ηai~ K -0.06 ) [138, 148], in which ηai is defined as monotonically decreases with loading rate K the ratio of maximal fracture toughness to minimal fracture toughness at a determined loading 13 / 51 rate. The rate-dependent decrease of ηai is not only in the grain-based heterogeneous rocks, but it is also apparent in bedding plane-abundant rocks [149], which is on account of the common mechanism of pattern transition from interfacial cracking to matrix cracking with loading rate. Although a few relationships between fracture toughness and physical properties of grainbased heterogeneous rock in laboratory tests were established, some remain speculative, requiring further clarification. For instance, crack density/porosity and grain size should have a positive correlation [134, 142, 150], which makes the revealed relationship to fracture toughness suspicious. Besides, as shown in Fig. 9, the fracture surface of granite in a higher roughness corresponds to a greater fracture toughness, but the explanation thereof is nonquantitative [9, 144, 145]. Moreover, the widely obtained experimental results of grain size to fracture toughness of grain-based rock are in the form KIc~Lg-λ, where λ is a positive constant dependent on rock microstructure [134, 136, 151, 152]. Nevertheless, Sabri et al. [153] measured the fracture toughness of granite with three different grain sizes and obtained the maximum KIc in rock of medium grain size. These debated consequences should be on account of the differences of dissipated energy of minerals microcracking. An experiment in which higher counts and energies of acoustic emission (AE) events were recorded in specimens of granite with a greater KIc was demonstrated [153]. In view of these different phenomena and findings on rock fracture toughness, the intrinsic sources of high fracture toughness in grainbased heterogeneous rock and the crucial factors on their macro fracture resistance remain to be further investigated. 14 / 51 (b) (a) ~1.8 mm Crack deflection Deflection Deflection Type-1 KIc =1.89 MPa·m1/2 Penetration ~0.6 mm Penetration Crack penetration KIc (MPa·m1/2) 3.0 KIc (Tpye-1) > KIc (Tpye-2) 2.5 2.0 1.5 Deflection dominant 1 mm KIc =1.15 MPa·m1/2 Type-2 1.0 Type-1 Penetration dominant Type-2 Figure 9. (a) Experimental fracture patterns of granite observed via micro CT technique along with the tested macro fracture toughness (modified after [9]), (b) fracture surface profiles of African granodiorite in two microcracking types with the measured KIc arising from use of the notched semi-circular bending method highlighted as well (reproduced from [10]). 3.2 Loading/strain rate effect The anisotropic behavior of transversely isotropic or mineral grain-based heterogeneous rocks under dynamic load has been extensively studied [11, 140, 154, 155]. Generally, the loading method can be categorized into three types. First is the notched semi-circular bending (NSCB) testing method [140, 156-158]. In this method, the nominal Mode-I fracture toughness of the coal and rock materials with different bedding angles was revealed [122, 156, 159]. As summarized in Fig. 10, the difference of fracture toughness with bedding angle is found to gradually decrease with loading rate and the anisotropy index (ηai) exponentially decreases, tending to unity. This tendency also exists in the grain-based heterogeneous rocks under different loading directions [160]. Second are the Brazilian disc (BD) and semi-circular bending (SCB) tensile tests. In these two methods, similar principle was invoked [11, 154, 161-163] wherewith the increased loading rate causes the anisotropic index of bedding-/grain-based rocks to decrease. Another typical scenario is the uniaxial compression (UC) test. As with the influence of weak bedding planes, the minimum uniaxial compression strength was obtained 15 / 51 when the intersection angle between the bedding and the principal loading direction was around 30° at a determined loading rate [164, 165]. These are consistent with the theoretical analysis [25] and numerical simulation [165]. Basically, the difference in bedding angle-dependent dynamic strength decreases at a larger loading rate (or strain rate) [164, 166]. (a) 2.0 P 1/2P Slate Phyllite 1/2P SCB (Black shale) UC UC (Phyllite) (Slate) ηai 1/2P ηai (b) 2.0 P 1.5 1.5 1/2P SCB (Barre granite) P P Bituminous coal 1.0 10 Black shale Barre granite 100 (GPa·m1/2·s-1) P P 1000 1.0 10 100 BD (Barre granite) 1000 (GPa·s-1), ε (s-1) Figure 10. The sensitivity of rock anisotropic index to loading/strain rate. (a) The calculated anisotropic indexes of rocks with loading rate in the NSCB tests [149, 156, 159, 160], (b) anisotropic index with loading rate (or strain rate) of bedding-/grain-based rocks under UC [164], BD [11], SCB [154, 161] tests. In view of the aforementioned studies, even though using different testing methods for the investigation of dynamic fracture of bedding-/grain-based rocks, the rate-dependent toughness or strength is in a similar principle with loading rate (strain rate) for the NSCB [156, 160], BD [11], SCB [154, 161], and UC [164] tests. In some papers, the anisotropic index (ηai), was used to determine the effect of dynamic loading on the toughness/strength behavior. However, there are two main gaps in the existing studies on the loading rate-dependent rock anisotropic behavior: (i) the analysis of essential parameters on the transition of crack trajectory with loading rate is sparse while most reports are limited to the phenomenological description of experimental results; (ii) the fundamental principles of rock anisotropy and the effects of bedding angle and loading rate on crack propagation in the layered rock materials/structures remain to be explored. 4 Mechanism discussion from crack deflection criterion Massive natural materials and structures are included by weak interfaces, exerting anisotropic physical and mechanical performances. The role of crack deflection at an interface was first realized and analyzed about half a century ago by Cook and Gordon [35]. Their 16 / 51 analysis used a strength-based fracture criterion. Later, numerous researchers used linear-elastic fracture mechanics (LEFM) to evaluate crack deflection at an interface from the perspective of energy evolution around the crack-tip [34, 167-171]. 4.1 Strength criterion With the loading perpendicular to the direction of crack propagation, the stress components (σxx, σyy, and τxy) at a random point ahead of the crack-tip were derived by Inglis [172]. If assuming the crack is elliptical where a and b are the semi-axes of the ellipse, one example of the induced stress distributions close to the crack-tip along the major axis is shown in Fig. 11 [35]. Along the x-axis, σyy monotonically decreases from the crack tip where initially it has a high value [σyy ~ (1+2a/b)], while σxx increases from zero and at a distance roughly equal to one crack-tip radius it reaches a maximum value (less than one-fifth of the maximum value of σyy) and then gradually decreases, reaching a stable value approximately equal to the ultimate σyy far from the crack-tip. The shear stress, τxy, around the two shoulders of the cracktip initially at a large negative value and then gradually increases to be positive along the xaxis. With the successive propagation of this tensile crack, the stress field, exhibiting a similar pattern to that shown in Fig. 11, progressively moves forward. σ∞ Crack x Crack 2b Crack y 2a σ∞ σxx σyy τxy Figure 11. Stress contours around the crack-tip under Mode-I tension load [35]. In case of a weak interface ahead of the propagating crack with a ligament of length la, the defined crack trace would be disturbed under the strength difference of each phase in a specific stress field [173, 174]. Cook and Gordon [35] distinguished the failure pattern of an interface into three conditions (Fig. 2b) in terms of the values of σxx and τxy: (i) interface debonding on the x-axis under direct tension and ahead of the main crack; (ii) fracture under shear of the interface at points symmetric about the x-axis and just ahead of the main crack; (iii) penetration of the primary crack through the interface which may or may not break afterwards. In terms of the maximum ratio of the peak value of σxx to σyy, that was taken as 0.2, it was inferred that an interface with a theoretical tensile strength of less than 0.2 times that of the matrix would debond ahead of the main crack leading to the occurrence of crack deflection [174]. Later, 17 / 51 Cook and Erdogan [175] considered the stress intensity factors and the crack opening displacement, and used the Mellin transform in conjunction with the dislocations resulting in a fracture criterion for crack penetration or deflection given the equality of critical stress and material strength of substrate material or interface, respectively. It is noticeable that the power of the singularity in Irwin’s equations [176] for the crack-tip at an interface is no longer that of the homogeneous material (λ = 1/2). For a strong interface, debonding ahead of the growing crack will not occur, so that crack deflection can only occur by changing its direction along the interface [174]. For an interface with higher strength the crack grows straight through the interface into the substrate [177]. Gupta et al. [178] proposed a strength criterion whereby crack deflection is initiated if the strength ratio of the interface ( σ i ) to matrix ( σ m ) is smaller than the maximum stress ratio in the orthotropic directions ( σ x x σ yy ). In this case it was predicted that, for crack deflection to occur, the interface must have a strength of less than about 0.35 of that of the matrix when there is no elastic mismatch [174]. The local stress criterion for crack deflection demands that, under the probing of the crack-tip stress field, the decohesion stress for tensile or for shear separation along the interface is reached before the cohesive strength is reached in the substrate material at the crack tip [173]. The measurements of the stress around the crack indicated that debonding is much more effective than slip at reducing the stress concentration ahead of the crack [179]. For a frictional interface oriented perpendicular to the propagating crack, slip along the interface will occur when τ xy μσ xx , where μ is the coefficient of friction of the interface. Thereafter, a first order analysis of the stresses near a Mode-I crack upon a frictional interface results in a simple criterion for crack deflection ( -σ xx 0.35 0.35 μ ) as shown in Fig. 12 [131]. The σ m σ yy 1.06 shear resistance of the interface plays the key role in development of the penetration scenario [180]. 18 / 51 Crossing stress ratio, -σxx / (σ m-σyy) 10 1 No crossing Partial crossing Complete crossing Theoretical threshold σ T0 m shear capacity threshold 0.1 0 0.2 0.4 0.6 0.8 1 Coefficient of friction, μ Figure 12. The crossing stress ratio criterion. Crossing occurs when stress ratios exceed this theoretical threshold, while interface slip occurs and propagation terminates if the stress ratio is below this threshold [131]. In consideration of the elastic mismatch of the contacted dissimilar phases, the two Dundurs elastic constants α and β should be included [111], α μ A β μ A 1 1 υB μ B 1 υ A 2υB μ B 1 2 υ A μ A 1 μ A υB 1 υB μ B 1 υ A μ B 1 υ A (1a) (1b) where μ and υ are the corresponding shear modulus and Poisson’s ratio of materials, respectively, and indices A and B refer to the corresponding layers. Substituting the shear modulus μ E 2(1+υ) into Eq. (1a), the parameter α can also be denoted as α ( E A* E B* ) / ( E A* E B* ) , where E E (1υ ) is the elastic modulus under plane strain * 2 condition. Stresses near the crack tip that touches the interface are found to be of the following form: σ ij K1 λ f ij θ , where λ defines the intensity of the stress singularity [181]. It was r shown in [175, 182] that λ can be determined as the root of the following characteristic equation: 2 λ 2 α β β 1 α β 1 β 2 2 cos λπ 0 , where the smallest real part is in the range of 0 Re λ 1 . Gupta et al. [173] proposed two dimensionless elastic constants λ and ρ for the determination of desired interface strength required for crack deflection. The stress and deformation fields derived for the anisotropic materials are dependent on material parameters λ and ρ for the two media and on the two Dundurs constants α and β [178]. As shown in Fig. 13a, the effect of β on the stress components is negligible for practical ranges of β between -1/4 and 1/4. The normal stress at the interface, σxx, is most sensitive to the variation in β for α < -0.5. 19 / 51 The transverse component of stress in the bulk material, σyy, shows a strong dependence on β for values of α in the ranges α < -0.5 and α > 0.6. Data for the interdependence of the Dundurs parameters were analyzed by Suga et al. [183] who discovered that β depends only weakly on α in all cases considered, and that the associated changes in β are only approximately one tenth of the change in α. Thus, as shown in Fig. 13a, with ρ1, ρ2, and λ1, λ2 assuming their isotropic values, a choice of arbitrary β provides few compromises in accuracy for most of the relevant components of stress. For a large ligament la, in consideration of the elastic mismatch between two materials, Leguillon et al. [56] derived a strength criterion for crack deflection, respectively, for the weak singularity (EB/EA = 0.1), no contrast (EB/EA = 1), and strong singularity (EB/EA = 10). Interface debonding has two premises: (i) a crack is nucleated at the interface ( σxx σi ), and (ii) substrate material does not fracture ( σ y y σm ) [54]. Thereafter, a consecutive strength criterion based on Cook and Gordon mechanism [35] in consideration of the elastic mismatch was deduced (Fig. 13b) [54]. The domain under the curve thus indicates the conditions under which debonding occurs. Contrarily, in the domain located above the curve, debonding does not occur. (b) 1 (a) 1 ρ1 = ρ2 = λ1 = λ2 = 1 0.8 B 0.8 β=0 0.6 σxx / σyy σ xx σ i β=-1/4 Crack deflection 0.4 σxx / σyy = 0.35 0 -1.0 -0.5 0.6 0.4 Crack penetration σ i / σ mA = 0.45 σ xx / σ yy σ i / σ m σ yy σ m Crack penetration 0.2 Crack Interface β=1/4 σi / σmA σ xx / σ yy σ i / σ m A 0.0 0.5 α = (EA-EB)/(EA+EB) Crack deflection 0.2 0 -1.0 1.0 -0.5 0.0 0.5 α = (EA-EB)/(EA+EB) 1.0 Figure 13. (a) Strength criterion for crack deflection and penetration in bi-materials [173, 178]. (b) Master curve for distinguishing crack penetration and interface debonding derived from the ratio of maximum stress components σxx and σyy (reproduced from [54]). In terms of the strength difference between dissimilar bulk materials, crack tends to deflect as it approaches a hard inclusion while preferentially penetrate a soft inclusion [55]. When the crack approaches an interface from the strong material to the weak material, the crack-tip driving force is amplified as the plastic zone spreads across the interface [184, 185]. Such 20 / 51 plasticity effect determines whether force shielding or amplification is dependent on the distance from the crack-tip to the interface and the magnitude of remote loading. Mohamed and Hansen [77] found that the tensile strength ratio ( σtA σtB ) between two dissimilar materials plays the dominant role in the fracture energy ratio (GfA/GfB) and elastic moduli ratio (EA/EB), and proposed a strength criterion in terms of the relationship between the characteristic length ratio (lchA/lchB) and tensile strength ratio of dissimilar materials where the characteristic length is defined as lch E G f σ t 2 . A brief summary of the existing strength criteria for the determination of crack deflection and penetration is shown in Table 1. Table 1. Strength-based crack deflection criteria. Calendar year Criterion equation σ 1964 σ 1964 & 1996 σ i σ m 0.2 max xx σi , max yy References σm [35] [35, 174] 1982 πEG σmax σmin 2 4 1 υ L 1993 & 2000 σ xx σ i σ yy σm 1995 1999 2000 -σ xx σ t σ yy 1 2 2 sin 2θ sin θ 2μ [129] [56, 178] 0.35 0.35 μ 1.06 l a l m 2.25 σ a σ m [131] 6.0 [77] σ xx σ i σ yy σ m ( E 2 E 1 0.1 , σ i σ m 0.68 ; E 2 E 1 1.0 , σ i σ m 0.99 ; [56] E 2 E 1 10 , σ i σ m 0.79 ) 2004 σrr σi [53] 2007 σ xx x l , l σi σ m max σ yy x l , l 2010 S 0 μ -σ xx 0.35 0.35 μ σ t σ yy 1.06 [54] [132] 4.2 Energy criterion (1) Evolution of energy criterion An alternative approach to determining the critical condition of crack deflection is to use an energy-based analysis to consider interfacial cracking. This was first proposed by Kendall [31] who argued that a deflection criterion based simply on tensile stresses and material strengths is not compatible with the Griffith theory of crack growth [186]. He suggested that, as there was no driving force for the opening of an interface ahead of the main crack, crack 21 / 51 deflection could only occur by the main crack changing its path upon reaching the interface [174]. As shown in Fig. 11, when a pre-existing plane crack occurs under external tensile loading, in the energy criterion, crack advance is governed by the strain energy release rate G at the crack-tip [186, 187]. Crack nucleation occurs when the energy release rate of the cracktip is no less than the fracture energy of the matrix. As the energy release rate is correlated directly to the stress intensity factors, KⅠ and KⅡ, of the crack-tip [176], equivalently, the crack will grow forward if the synthetic stress intensity factor exceeds a critical value for a defined matrix. In elastically homogeneous brittle solids, cracks are generally found to follow a trajectory for which KⅡ = 0. This crack-path criterion is invalid when the crack advances at an interface because, in this case, the relative magnitudes of the fracture energy between the interface and matrix materials should also be considered [188]. If the propagating crack approaches a weak interface, whether the crack is about to deflect into or pass through the interface relies on the relative values of energy release rate of the crack-tip (Gd and Gp) and fracture energy (sometimes denoted by the toughness) of interface and matrix (Гi and Гm) [34]. He and Hutchinson [34] proposed an energy criterion with the help of an asymptotic analysis of the stress field near the tip of a crack contacting an interface in a bimaterial [182], where the propagating crack is likely to deflect into the interface if Γi Γ m Gd Gp . The analysis associated with use of the HH criterion is an asymptotic one in which virtual extensions of a crack ahead in its plane (ηp) or along the interface (ηd) are assumed [34]. The prediction of Gd/Gp is accurate when the length ηd of the kinked crack segment is very small compared to the parent interface itself [189]. This criterion gives a critical Gd/Gp ratio of 0.26 for a doubly deflected crack and 0.25 for a singly deflected crack in the premise of no elastic mismatch. Given crack deflection, the work of fracture should be less along the interface than ahead into the substrate material [173]. Later, Gupta et al. [178] proposed two dimensionless orthotropic parameters λ and ρ for determining the desired level of the interface strength required for crack deflection. After that, an energy criterion for crack deflection at an interface between two aligned, orthotropic media was established by using the method of singular integral equations, which depends on these two parameters and the corresponding Dundurs elastic constants α and β [168]. This criterion is similar to the HH criterion but was modified to be independent of the virtual extensions. In consideration of the crack propagation in two opposite directions from the crack-tips (Fig. 11), when the matrix fracture energy is small enough, H-crack formation is again inevitable. The energy criterion for H-cracking to occur in preference to Mode-I crack penetration was revealed by Tu et al. [190] upon the condition that Гi/Гm < 0.196, which is 22 / 51 analogous to the fundamental crack deflection criterion Гi/Гm < 0.25 in the absence of elastic mismatch. Those energy criteria using a local analysis based on stress intensity factors assume that only what happens within the K-dominant field at the tip of the crack is important and therefore geometrical effects such as crack length, specimen geometry, or loading state can be ignored [174]. However, it was found that the finite length of branch crack and width of the target substrate layer have profound effects on the crack deflection criterion. The deflection prediction derived with the consideration of these two factors is in general more favorable to deflection than the HH criterion [191]. Essentially, there are two limitations of the HH criterion: (i) its uncertainties as to virtual extension length; (ii) it does not consider interface debonding ahead of a primary crack. They lead to the criterion sometimes fail to predict interfacial deflection [192, 193] or interfacial penetration [194]. If the ligament is small enough to be neglected, the HH deflection model offers a satisfactory approximation of the interface debonding mechanism. Nevertheless, the ligament from the crack-tip to the interface and the extension length ratio ηd/ηp are essentially important to the crack deflection [43, 52, 56]. Leguillon et al. [56] established an energy multi-criterion within the framework of two-dimensional linear elasticity by taking the interface debonding ahead into account. They assumed that extension lengths of the cracks should be related to the material and the interface microstructure, and inferred that if assuming ηp = 2ηd can obtain the Leguillon-Sanchez (LS) criterion [195], which is slightly different from the HH criterion where ηp = ηd is assumed. This LS criterion is based on a numerical-analytical approach and can be carried out whatever the value of β and extends without additional complexity to orthotropic substrates. Thereafter, an improved criterion that does not require any assumption concerning the extension length ratio was established by using a quasi-static approximation and assuming that the deflection mechanism occurs under constant loading [196]. Based on a series of their outcomes, the decohesion length at an interface was obtained using an energetic approach and thereafter an interfacial nucleation criterion coupling strength and energetic conditions was proposed [53]. A low toughness interface is not systematically a sufficient condition to promote the initiation of deflection. For the highest values of the interfacial fracture length, the debonding is driven by the energy condition [57]. A summary of these quasi-static energy criteria is illustrated in Fig. 14. The discrepancy between the theory-derived and FEM-derived criteria should be attributed to the differences in the initial assumptions adopted for geometry and loading conditions. The assumption made in HH criterion for computing the ratio Gd/Gp is that the two materials constitute the interface 23 / 51 form two semi-infinite planes that meet at the interface. However, the numerical result shown in Fig. 14 accounts for the finite geometry and the β-effect [188]. Some other typical outcomes of the energy criterion derived later for the determination of crack deflection at an interface are briefly summarized. Based on the results of numerical simulation, a modified version of the HH energy criterion which accounts for the effects of finite reinforcement size, phase volume fractions, phase shape, and phase distribution was developed. The energy criterion for deflection is sensitive to material anisotropy [103, 197]. In addition, the HH criterion was extended to give the closed-form solution for the strain energy release rate of a hydraulic crack with arbitrary angles with respect to the in-situ stress. The critical conditions in which the hydraulic crack deflects into weak interfaces and exhibits a dependence on crack-surface friction and in situ stress anisotropy are given in explicit form [198]. In their results, Mode-II fracture dominates the hydraulic fracturing process and the intersection angle between the hydraulic crack and the weak interface is the determining factor that accounts for crack deflection. Furthermore, the lower friction coefficient between cracked 1.5 HH criterion Martinez and Gupta LS criterion 1 Martin et al. FEM assisted Гi / Гm planes and the greater in situ stress difference can favor hydraulic fracturing [198]. B A Crack Interface Crack penetration 0.5 Crack deflection 0 -1.0 -0.5 0.0 0.5 α = (EA-EB)/(EA+EB) 1.0 Figure 14. A brief summary of quasi-static energy criterion for the determination of crack deflection at an interface [56, 168, 178, 188, 196]. Crack propagation behavior in two-dimensional polycrystals is a function of the fracture toughness of the grain boundary. Whether the crack will pass through the boundary or be deflected into it depends on the impinging angle on the grain boundary, the stress intensity factors at crack tip and fracture toughness of both grain and grain boundary. The crack extends only intergranularly when KICb ≤ 0.4KICg, and the percentage of transgranular fracture increases with increasing KICb [89]. A fracture mechanics model is developed which predicts the 24 / 51 transition between the two fracture modes and provides an energy criterion suitable for the interpretation of experimental fracture results. The proposed criterion determines intergranular fracture occurrence when the ratio of the fracture toughness for intergranular fracture to the fracture toughness for trangranular fracture is no larger than the critical value of 0.5 (KICb ≤ 0.5KICg) [199]. A widely used alterative to simulate the transition from the intergranular to transgranular fracture is the cohesive zone model [101]. Pro et al. [200] embedded cohesive elements throughout the entire mesh in a finite element model (FEM) and derived a kink nucleation criterion non-linearly related to the parameters of the fracture process zone. Moreover, a phase-field model formulated with two-set order parameters describing the crack field and the microstructure field, respectively, is established to study the competition between crack penetration and deflection at an interface. The effect of the applied plastic strain is included, resulting in the finding that the energy criterion based on LEFM is a static and critical case of the present phase-field model [101]. (2) Elastic mismatch A modulus mismatch changes the nature of the stress singularity at the crack tip both for interface cracks [201, 202] and for cracks terminating at an interface [202]. These singularities may have complex components while the resulting stress and displacement fields will have an oscillatory nature [167]. When the crack is normal to the interface, the corresponding criterion for crack deflection at an interface between two elastic materials with similar modulus is approximately Гi/Гm < 0.25 [34]. If the composite structure has an elastic mismatch, as shown in Fig. 14, the critical value for the determination of crack deflection or penetration is not the defined value of 0.25 while it is significantly influenced by the modulus mismatch. For instance, in the case of a weak singularity ( EB EA 0.1), the LS criterion predicts deflection if Γi 0.91Γm. Without contrast between substrates ( EB Γi 0.27Γm. EA 1.0), the prediction of the LS criterion for crack deflection is In the case of a strong singularity ( EB deflection when EA 10), the LS criterion predicts Γi 0.58Γm [56]. The near-tip driving force for fracture is influenced by whether the crack approaches the interfaces from the compliant or stiff material. When a crack subjected to a fixed remote stress approaches a stiffer material, the near-tip stress intensity factor KI decreases, and vice versa [185]. The crack-tip is shielded from remote loads when it approaches the interface from the 25 / 51 compliant material. Crack tip shielding and amplification can be quantified in terms of two contour evaluations of the J-integral where the effective J-integral at the crack tip (Jtip) is greater than the remote J-integral (Japp) when it approaches the interface from the stiffer material [184]. Jtip/Japp < 1 implies crack tip shielding while Jtip/Japp > 1 indicates amplification [4, 184]. In addition, the shielding and amplification effects are dependent on the thickness of the substrate layer, the distance from the crack-tip to the interface, and the remote loading [184]. The influence of the elastic mismatch may possibly be more pronounced for a crack with a cohesive zone growing towards an interface [30]. In composite systems with an elastic mismatch, when EA > EB, cracks tend to deflect to high-stress-concentration sites; conversely, where EA < EB, cracks are expected to be attracted by the soft phase within the stiffer matrix [203]. For an inclined crack versus the existing interface (Fig. 2), when the propagating crack approaches a more compliant material across the interface (α < 0) KII becomes negative. If it is free to curve following a path with KII = 0, the crack will curve toward the interface since the straight crack has KII < 0. Conversely, when the straight crack approaches a stiffer material across the interface (α > 0), KII becomes positive indicating that an actual crack trajectory that satisfies KII = 0 would curve away from the interface [34]. (3) Mode mixity (phase angle) The fracture energy (Г) for a plane crack at an interface is dependent on the relative amount of the tensile (KI) stress field to the shear (KII) stress field at the crack tip [204]. The study in [204] suggested that under mixed-mode loading the critical energy release rate of an interface is a function of KII/KI ratio, depending on the roughness of the interface. It is assumed that the source of shielding is the fact that the crack is trapped, and runs along an interface which is not perfectly smooth. A rougher interfacial surface increases the phase angle, resulting in the growth of interfacial fracture energy [86]. The deflected crack has a higher relative Mode-II contribution. Interface toughness is increased with the ratio increase of shear loading relative to that of tensile loading [188]. The mixity of crack-tip loading mode (characterized by the phase angle, ψ, having a tangent equal to KII/KI) can vary between pure Mode-I (ψ = 0°) and pure Mode-II (ψ = 90°), depending on the loading state as the length of the crack increases and the ratio between the elastic properties of the two materials (Fig. 15) [174, 205]. It was found that, in the case of wedging, the phase angle decreases as the crack grows, remains quasi1 constant in four-point bending but increases in tension [174]. When β = 0, ψ = tan K II K I . 26 / 51 Another finding is such that the stress intensity factors are correlated to the strength constituents and the KI-value is related to the KII-value as follows: K I σ 0 1 2 λβ [181]. K II τ 0 1 2 λβ (b) ГIIC (a) 45° Ψ 0 θ 40 Interface fracture energy, Гi (J·m-2) ГIC Double cantilever beam Ψ ~ 0.5° 90° Four-point bend Ψ ~ 35–60° 2a R Glass/Adhesive Aluminum/Adhesive 30 Mortar/Granite Mortar/Limestone Steel/Epoxy 20 10 0 0 Brazilian disc Ψ ~ 0–90° Composite cylinder Ψ ~ 70–90° Tensioned push-out Ψ ~ 0–90° 15 30 45 60 Phase angle, Ψ (°) 75 90 Figure 15. (a) Schematic illustrations of the dependence of Гi on phase angle ψ where different testing methods for the measurement of Гi involve a wide range of ψ values [188, 205], (b) some experimental results showing variations of Гi with ψ for the adhesive bimaterial structures [86, 188, 204, 206, 207]. The mixed-mode energy release rate at the interface could also be correlated to the phase angle. The total energy release rate associated with an infinitesimal virtual crack extension is written in terms of K as, G= K 2 cosh πε E 2 * , where ε 1 1 β ln . The energetic phase angle 2π 1 β ψ G is defined in a similar term to the stress intensity factors as tan 2 ψG G II Δa , which G I Δa represents a Δ a -dependent measurement of fracture mode mixity. It is noticeable that when β0, ψG ψ K [208]. (4) Toughening Numerous natural materials are composites, with the utilization of crack deflection to provide extra toughness and strength. Planes of weakness may cause toughening in composite materials by deflecting and stopping cracks [35, 209]. One of the methods that has been used to increase the fracture toughness of brittle ceramics is based on the addition of a dispersed 27 / 51 ductile phase [210, 211]. Other methods that have been studied by several researchers rely on transformation toughening [212], fiber reinforcement [213], or microcrack shielding [214]. To achieve toughness in many brittle composites, crack deflection at interfaces is essential [173]. The ability to deflect and channel a crack is an attractive means of enhancing the toughness of brittle polycrystalline materials [97]. To maximize the degree of crack deflection and thereby maximize the toughness of the material, large, hard inclusions should be incorporated at grain boundaries. Toughening mechanisms at grain boundaries are associated with deflecting and directing cracks into predetermined propagation tortuous paths [97]. The fracture toughness loss is relatively small for large-angle intergranular cracks. However, the decrease of fracture toughness of low-angle intergranular fracture and increasing proportion of transgranular fracture in a large-grain-assembled system may result in a better fracture resistance [101]. A proper balance between transgranular and intergranular failure can lead to an optimized fracture toughness. Microstructures with refined grain sizes and balanced bonding strength in grains and grain boundaries can enhance fracture toughness in terms of best promoting the manifestation of more favorable failure mechanism [91]. The toughening effect of the interfaces is significantly increased if partial debonding occurs during bridging. Thus, a limited amount of debonding is advantageous, but too low a bond strength results in complete debonding, which adds only a little toughness to that of the brittle matrix material [97, 209]. In addition, Hsueh et al. [114] found that the elastic mismatch can contribute to fracture toughening in heterogeneous materials, which is attributed to decrease of stress intensity at the crack-tip when a crack is at a compliant-to-stiff interface. To allow crack re-nucleation, the remotely applied load should be increased leading to a greater apparent fracture toughness. Moreover, a compliant interlayer tends to increase the interface toughness by increasing plastic dissipation in the thin layer and developing plastic strains in the interlayer [215]. (5) Residual stress and T-stress The analysis under the HH criterion is asymptotic in which the prediction of Gd/Gp is accurate when the length ηd of the kinked crack segment is very small compared to all other lengths in the problem, including the length of the parent interface crack itself. If there is a stress in the substrate parallel to the interface due to either residual stress caused by thermal expansion misfit or applied loads, then an additional non-dimensional length parameter, not considered in the HH criterion, becomes important [169, 189, 190]. The residual stress, governed by the misfit strain between the two dissimilar bimaterials [216], affects the energy release rates of both the deflected and penetrating cracks [169]. Relatively small values of 28 / 51 residual compression substantially enhance debonding in preference to penetration [190]. Introducing compressive residual stress in the stiffer intact layers of a composite laminate ahead of a growing primary crack would favor crack deflection by allowing advantageous energetic conditions [217]. These residual stresses are expected to become at least partially relaxed during crack advance, thus contributing to the energy balance [205]; however, the residual stress effect is negligible if the intact layer is more compliant than the cracked layer [217]. Another important feature is the T-stress, which acts parallel to the parent Mode-I crack before deflection. This T-stress has an unusually strong influence on the energy release rate at the tip of the deflected crack [218]. The non-singular T-stress affects the shielding and amplification of the stress fields around the crack-tip near a bimaterial interface [184]. Simply using the sign of the T-stress before crack kinking is not sufficient to determine crack growth stability as observed in some experiments. A crack will propagate off its original path due to changes in local fracture mode mixity (a mechanical factor) or fracture toughness (a material factor). The stress intensity factor and the T-stress, have been accepted as a two-parameter fracture criterion in predicting the crack propagation direction and the shape and size of smallscale yield zones [19]. 4.3 Coupled strength-energy criterion Historically, models of crack deflection have been developed using either a strength-based or an energy-based fracture criterion. However, in general, crack propagation depends on both strength and toughness [171]. Gupta et al. [173] defined two dimensionless elastic constants determining the stress and deformation fields in each medium. In that case, the stress criterion established allows determination of the desired interface strength required in the manufacture of a composite to enhance the overall toughness thereof. At the fundamental level, the interface tensile strength and intrinsic toughness are related thus: Γ ~ σ t2 . The interface strength directly controls the plastic dissipation and the roughness-related shielding components, while the overall energy absorption is related to the fracturing process in terms of the energy release rate at the crack-tip [178]. Chen [181] found that, for a mixed-mode crack, the stress intensity factors can be correlated to the strength constituents in terms of the intensity of stress singularity (λ) and Dundurs elastic mismatch parameter β as K I σ t 1 2λβ . K II τ 1 2λβ 29 / 51 (a) 100 (b) 20 E A EB i Eh=1e-6 E A EB Crack penetration 10 15 0.67 10 m i Gi (J·m-2) i 0.33 m Crack deflection 10 Crack penetration 5.0 1 1.0 2.5 1.0 5 Interface decohesion E i i2h 0.01 0.1 0 0.1 1 10 Gm (J·m-2) 100 1000 0 5 10 m i Figure 16. (a) Competition between matrix penetration and interfacial debonding with a coupled strength-energy criterion [57], (b) determination of crack penetration or crack deflection in toughness ratio and strength ratio space [33, 171]. For the crack with a cohesive zone, the critical stress intensity factor is related to the cohesive zone properties as K IC 2 Eσ t ε and the length of the cohesive zone at critical load is lcz π 8 K IC σ t 2 [30]. A strength criterion in terms of the relationship between the characteristic length ratio (lchA/lchB) and tensile strength ratio of dissimilar materials was established where the characteristic length is defined as lch E G f σ t 2 [77]. This characteristic length factor was also used by Martin and Leguillon [53] to estimate the debonding length at an interface. Low toughness and high strength interfaces are associated with low values of the characteristic length while high toughness and low strength interfaces lead to higher values of lch. Thereafter, the competition between the interfacial decohesion and matrix cracking was determined in terms of a normalized energy release rate correlated to the ligament length and interfacial debonding length. Based on the outcomes, an initiation criterion from the perspective of applied strain was developed by Martin et al. [57] by taking both the energy and stress conditions into account, where debonding or penetration condition can be reduced to an energy or a stress condition depending on the relative value of some characteristic fracture lengths of interface and matrix (Fig. 16a). Similarly, Thouless et al. [167] found that occurrence of interfacial debonding is dependent on the stress applied to a bimaterial structure, where σ 1.0 E Γ i a 12 and crack penetrates to the matrix if σ 0.5 E Γ m a . Thereafter, an 12 energy criterion Γi Γm 0.25 for crack deflection is given for two similar substrates. In 30 / 51 addition, the characteristic length is normalized with respect to the pre-existing crack length with the criterion revealed in terms of the relationship between the toughness ratio and strength ratio (Fig. 16b) [171]. Both energy and stress criteria are necessary conditions for the determination of interface fracture but neither one nor the other are sufficient. Thanks to the singularity at a crack-tip, the incremental form of the energy criterion gives a lower bound of admissible crack lengths. On the contrary, the stress criterion leads to an upper bound [219]. Parmigiani and Thouless [171] studied crack deflection by using a cohesive-zone model which incorporates both strength and toughness parameters simultaneously. No matter how tough an interface is, crack deflection can always be induced if the strength of the interface is low enough compared to the strength of the substrate. A low toughness interface is not a sufficient condition to promote the initiation of deflection [167]. There is a lower bound for the ratio of the substrate strength, below which penetration is guaranteed no matter how brittle the interface is. It should be noticed that the effect of modulus mismatch on crack deflection is very sensitive to the mixed-mode fracture criterion for the interface [33, 171, 220]. Moreover, a fracture criterion involving both toughness and tensile strength allows the study of the competition between, on the one hand the crack blunting due to the pores and resulting in an apparent toughness enhancement, and on the other hand the weakening effect caused by an increasing volume fraction of pores [221]. As a summary of above review, a brief statistical analysis of energy criteria pertaining to crack deflection at an interface is shown in Table 2. Table 2. Energy-based crack deflection criteria. Calenda r year 1989 1989 1992 Referenc es Criterion equation Γi 0.25 Γm [167] Γi 0.6 Γm Γi K d Γm Kp [167] [195] 1993 & 1996 Γi G d [89, 205] 1996 d Γi 4 π d c Γm [174] 1996 2 Γ i c E 2 d c E 1E 2 4 π d c E 12 Γm [174] 1996 1 II hm Γ m π EΩ h m 1 I h B Γ B 16 σ A h B 2 [190] 31 / 51 2000 2000 2000 2000 Γ i 0.43Γ m ; Γ i 0.24Γ m Γ i 0.91 Γ m E 1 E 2 0.1 ; Γ i 0.27 Γ m E 1 E 2 1.0 ; Γ i 0 .5 8 Γ m E 1 E 2 1 0 Γ i K d 2ηd Γ m K p ηp [52] [56] 2 λ 1 [222] Γ i μp K μd K 0 Γ m μd K μp K 0 2 λ 1 [56] K p a1p 2 λ G c2 a1p 2λ c 1 2λ 0 G1 l 0 K 1 l 0 2λ K d a1d G ic a1d 2λ c 1 2λ 0 G1 l 0 K 1 l 0 2001 K a Γi d d Γ m K p a p 2004 Γ i Ai l , d Γm Am l 2007 K Ic acr 2 2 β σ sin α 1 σ cos α y x 2018 li ΓR f ψ , cz b l cz 1992 max Gd Gp 0.25 [203] 1992 max Gd Gp 0.4 (Elastic mismatch α=0.57) [203] 1996 Ki≤0.4Km [89] [196] 2010 RL IC [53] [69] 2 i Process zone length ratio: l czb Γi σ b2 [200] Γb σ i l cz LR IC K 0.5K [199] Gd 1 β 2 Gp 1989 K IC A K IC max 1998 Γi Gd Γm Gp 189] [34, 1 α d 2 e 2 R e de c 2 2 [34] B B B δ δ K IC ω A A for A 1 δ δ K IC ω 1 B B δ δ 1 A ω 1 for A 1 δ δ 2 1994 2 2 2 Gd d ηn dg dg ηn g Gp c2 2ηtch η2t h2 1 α [30] 1-2λ ad ap [169] 1/ 4 1994 Gd λ1 H 22 d 2 e 2 2 Re de 2 2 G p 4 cos h πε s 11n 1 c 2000 d Gd max 2 Gp 1 α c 2007 1 2 λ1 d d 2 2 2 2 Gd 1 c11 c 21 2 c11c12 c21c22 η c12 c 22 η ad 2 p [66] 2 2 Gp 1 α b11 b 221 2 b b b b ηp b12 b 222 ηp a [168] 2 [191] 2 11 12 32 / 51 21 22 1 υ1 1 υ2 μ1 μ2 2 Gd K1 K 22 , 4 cosh 2 πε K12 K 22 k12 a 1d 2 λ c h 2 Re ch , 2 2013 2017 1 c 2 1 h 4 Gα Gθ max 2 2α 3cos 2 1 3cos α /16, when sinα>0 3cos2 α 5 3cos α / 8, if sinα 0 2 2017 α Gα cos 4 2 G θ max Gi θ [198] 2 θ α sec 2 0 cos 2 6 cos α 2 s τ 2 sin α s q 2 2 2 2 8 4 sin θ 0 s τ s q 1 cos θ 0 s q 5 3 cos θ 0 s τ Gα G θ max Gb [223] 3iw 1 β iw2 2 e e 1 α 3iw 1 β iw2 e e 2 1 α 2017 2019 2 [198] [198] 2 2 1 θ 3θ θ 3θ 3cos cos sin sin 16 2 2 2 2 [101] 4.4 Effect of dynamic loading A limited amount of work has been done in the analysis of crack deflection in bimaterial structures under dynamic loading. In the framework of LEFM, Xu et al. [121] theoretically analyzed the competition of crack deflection and penetration at an interface between two similar isotropic elastic solids, where a crack propagates forward rapidly to reach the interface from one side of the matrix under an impact load. This energy criterion is derived from the quasistatic LEFM crack deflection criterion in terms of the relationship between energy release rate at the crack-tip and the fracture energy of the material. The quasi-static ratio of two energy release rates depends on the interface angle as, 2 2 Gd θ 1 3θ θ 3θ θ θ 3cos cos sin sin =cos4 . 16 2 2 2 2 Gp 2 (2) In the counterpart of this dynamic analysis, the crack propagation velocities before (v1) and after (v2) deflection are used to evaluate the instantaneous crack-tip energy release rate based on the detailed results in [224]. Thereafter, the ratio of two energy release rates for the deflected interfacial crack and the incident Mode-I crack is given as [121]: 33 / 51 2 2 θ 3θ 3θ θ k v 2 3cos cos αs2kII2 v 2 sin sin 2 α Gd θ,v 2 v 2 D1 2 2 2 2 . 2 Gp v1 16α d1kI v1 v1 D2 2 d2 I (3) The energy criterion for dynamic crack deflection is in a similar form to that in quasi-static conditions [34]: when Gd θ,v 2 Γi v 2 , the dynamically propagating crack deflects into Gp v 1 Γm v1 the interface. The predictions of this dynamic energy criterion are fairly consistent with their experimental tests of brittle materials. This model was later extended to the determination of fracture patterns in ceramic with heterogeneous microstructure [90] and crystalline rocks [65]. When the dynamically propagating Mode-I crack reaches a weak interface, it kinks out of its original trace and shifts to propagate along the weak interface, exhibiting mixed-mode behavior. Xu and Wang [225] performed supplementary analyses of their experiments and theoretical model in [121], where changes in dynamic T-stress values of the incident crack over time were determined and the effect of mode mixity of the interfacial crack was discussed. It is found that the T-stress of the incident crack has a small positive value but exerts a significant influence on the stress fringe pattern of crack-tip in photoelasticity. Moreover, the mode mixity of the kinked crack depends on the kinking angle and the crack-tip velocity. A weak interface will lead to a high Mode-II component and a fast crack-tip velocity of the kinked mixed-mode crack. The effect of elastic mismatch between two neighboring materials in the aforementioned analyses on dynamic criterion of crack deflection is, however, not considered. Huang et al. [117] evaluated the feasibility of the HH criterion in dynamic loading condition based on laboratory tests. From their results, it is found that in dynamic loading, for a determined elastic mismatch, the propagating Mode-I crack is likely to penetrate the interface rather than behaving in accordance with the deflection pattern seen in quasi-static tests. They speculated that the critical curve that determines crack deflection or penetration in quasi-static cases (Fig. 14) should be transferred along the bottom-right direction under dynamic load. Djoković et al. [226] extended the analysis of [121] by considering the elastic mismatch effect in terms of the two Dundurs elastic constants (α, β) [111]. In doing so, the energy release rate at the crack-tip upon deflecting into the interface should be expressed 34 / 51 as Gd H 2 Kd , 2 4cosh επ in which 2 2 1 1 β α d1 1 α s1 α d2 1 α s2 [227] and ε ln H [228]. The Dundurs elastic 2π 1 β μ1 D1 μ 2 D2 parameter β should have a rate-dependent change as indicated in [229]. In view of the number of previous investigations thereof, the effect of α is much greater than that of β [34, 56, 168, 178, 196]. Therefore, the ratio of energy release rate is found to be given by [226, 230]: Gd θ , v 2, α Gp v1 1 Gd θ , v 2 . However, the ultimate format of this criterion looks debatable 1-α Gp v1 as it does not give the specific deriving process and is quite similar to that of [121] with an additional parameter α included. The aforementioned failure/fracture mechanism of inhomogeneous rock and rock-like brittle materials/structures in terms of crack deflection criterion has presented the theoretical development of the effects of weak interfaces on crack propagation. With the comparison of these criteria, it is prominent that: (i) the interaction between a propagating crack and a preexisting weak interface is associated with both the stress and energy aspects in this system; (ii) the energy criterion is more popular in application than the strength criterion for the determination of crack deflection or penetration at an interface as the former considers the properties of the propagating crack. However, coupled strength-energy criteria are elusive and difficult to use as they are sensitive to the change of each parameter therein. In addition, most of the energy criteria apply to the quasi-static state and are mainly used in ceramic composite materials, whereas a small number of applications of such energy criteria are found for the interpretation of inhomogeneous rock fracturing. Moreover, few works on the energy criterion of crack dynamic propagation upon a weak interface has been done, not to mention the deficiencies in these energy criteria. 5 Conclusions and outlook This literature review summarizes the effects of weak interfaces in rock-like materials and structures on crack propagation from phenomenon description to mechanism analysis. Typical fracture patterns in terms of the interaction between a propagating crack and a pre-existing weak interface are elucidated firstly followed by the presentation of their effects on the mechanical property of grain-based and bedding-abundant rocks. Based on the aforementioned review of weak interfaces on the physico-mechanical characteristics of rock-like brittle materials, the intrinsic mechanism is discussed in terms of crack deflection criterion. Overall, some main conclusions are briefly presented below: 35 / 51 (1) Four general types of fracture patterns in terms of a propagating crack interaction with a pre-existing interface are classified. They are the crack directly contacts with an interface perpendicularly, the crack directly contacts with the interface obliquely, debonding or fracturing ahead of the crack when approaching the interface, and the crack curves toward or away from the interface at an inclined angle. (2) A series of factors influence the path of a propagating crack when it goes close to a weak interface. In this work, the key factors, e.g. strength and toughness of interface, interface angle, interlayer effect, elastic mismatch, dynamic loading, and confining stress, are fairly reviewed and summarized. (3) The mechanism of action of weak interfaces on crack propagation in rock is discussed in terms of crack deflection criteria. The evolution and progress of strength criterion, energy criterion, and coupled strength-energy criterion are reviewed as well as the summary of limited work on the effect of dynamic loading. Indeed, the various energy criteria are the favorable ones in the determination of crack propagation at a weak interface. (4) Numerous studies have been conducted upon the effects of weak interfaces on crack propagation; to date, most of the outcomes are derived from tests on composite materials under quasi-static loading. In rock mechanics and rock engineering, these concepts and results have not been widely and popularly used for the investigation of heterogeneous rock fracturing containing weak interfaces, not to mention dynamic load regimes. This review work gives a detailed summary about the effects of weak interfaces on crack propagation in rock or rock-like materials/structures, and is of significance for the comprehensive understanding of different fracture patterns influenced by weak interfaces. To rock mechanics, even though some experimental, numerical and theoretical work on the quasistatic and dynamic fracturing of brittle rocks containing weak interfaces, as reviewed above, have been undertaken, there are some key issues remaining to be addressed: (i) most experimental and theoretical studies are in quasi-static conditions while merely few investigations on the strain rate-dependent rock fracturing containing weak interfaces (beddingplanes or grain/inclusion boundaries); (ii) the existing results mainly sustain discussion of the phenomena of weak interfaces on rock fracturing under tension while the quantitative relationship between dynamic loading and crack propagation in rocks with weak interfaces remains insufficient; (iii) the proposed criteria for the study of quasi-static crack propagation in ceramic and other composite materials can be used and modified in the near future for the 36 / 51 understanding and prediction of rock mass failure during underground resources/energies exploitation; (iv) previous experimental and numerical studies on heterogeneous rock fracturing pay more attention to mineral composition and its effects on the macroscopic failure pattern of rock, while the essential controlling factors and the effect of mineral fracturing on macroscopic mechanical behaviors are rarely discussed; (v) the specific processes of heterogeneous rock dynamic fracturing have not been systematically examined and the intrinsic mechanism in terms of the competition between propagating cracks and rock properties is scarcely implemented for the analysis of heterogeneous rock dynamic fracturing in experiments or simulations. 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Weak interface effects on rock dynamic failure are reviewed and the remaining issues are extracted. 49 / 51 Phenomenon: Weak interface effects on crack propagation Single deflection Double deflection Direct penetration Mechanical feedback: Crack propagation on mechanical property 3.0 Deflection Penetration Deflection Penetration 2.5 2.0 Deflection dominant 1.5 1.0 Type-2 Type-1 Mechanism: Crack deflection criterion 1.5 HH criterion Martinez and Gupta LS criterion 1 Martin et al. FEM assisted Гi / Гm Type-1 KIc (MPa·m1/2) KIc (Tpye-1) > KIc (Tpye-2) B A Crack Interface Crack penetration 0.5 Crack deflection 0 -1.0 -0.5 0.0 0.5 α = (EA-EB)/(EA+EB) 50 / 51 1.0 Penetration dominant Type-2 Declaration of interests ☒ The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper. ☐The authors declare the following financial interests/personal relationships which may be considered as potential competing interests: None. 51 / 51