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MYRRH COLOPHONY

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MYRRH
Gum Myrrh, Bol, Myrrha
B.Source
oleo-gum-resin obtained
from Commiphoramolmol
and other Commiphora
species.Burseraceae.
G.Source
N E Africa and S Arabia.
One of the characteristics
of the Burseraceae family
plants possess oleoresinous canals in their
conducting tissues.
The plants are small shrubs
or trees about 3 m in
height.
exude yellowish coloured
resin when the incisions are
made in the bark of the
tree.
Gradually hardens and
becomes dark or reddishbrown in colour.
This coagulated mass is
collected in goat skins by
the native tribals and sent
to the market.
Description
Colour-Externally, it is
reddish-brown, internally,
brown.
Odour and Taste-Aromatic
and agreeable.
Size-About 1.5 to 3.0 cm in
diameter.
Shape-lt is tound in the
form of rounded or
irregular tears.
Extra Features
The fractured surface of the
drug is somewhat granular.
It is brittle and shows
translucent surface.
Whitish spots on broken
pieces are also seen.
Chemical Constituents
l0 % of yellowish thick
volatile oil;
60 % of gum;
25 to 40% of resin, and
bitter principle ( 3 - 4 %).
Several impurities 5 %.
Resin contains ether
soluble resin acids, a, B
andy
commiphoric acid and
3 heerabomyrrholic acids
are ether-insoluble acids
present.
Volatile oil contains
terpenes, cuminic
aldehyde, eugenol, etc.
The gum- oxidase enzyme.
It yields nsot more than 70
% of alcohol insoluble
matter.
Identification
1. 0.1 g substance and
0.5g of sand are triturated
with solvent ether, filtered
and allowed to evaporate,
the thin him formed gives
violet colour on contact
with bromine vapours.
2 triturated with water, it
forms yellowish-brown
emulsion.
Odour-Faint and
terebinthinate.
Taste-It occurs in the foIm
of an8ular, translucent
masses ot various
sizes.
Uses
stimulant and an antseptic.
protective.
Astringent to the mucous
membrane - tincture mouth washes and gargles.
Standardas
MP - 75C to 85°
Acid value - 130 to 180
Saponiication value - 188
to 192
Ash value - Not more than
0. 125%
5. Specific gravity - 1.08
Adulteration
several species like
Arabian myrrh, Yemen
myrrh, etc. Both of
them are less fragrant and
less aromatic. In India,
myrrh is substituted by
Balsamodendron
ukul, Known as Indian
bdellium
COLOPHONY
Synonyms
Rosin; Kosina;
Colophoniunm; Kesin;
Amber-resin, Gum rosin,
pine-Tesin.
Biological Source
Colophony is the residue
left after the distillation of
the oil of turpentine from
the crude-oleo-resin
obtained from various
specIes of Pinus belong to
tamilyPinaceae.
Geographical Source
Prepared in North America,
Northern Europe, Pak and
India.
Description
Colour-pale yellOw to
yellowish brown or amber
colour.
Extra Features
brittle and readily fusible
with glossy appearance.
Solubility
insoluble in water but
soluble in alcohol, carbon
disulphide, chloroform,
ether, many
fixed and volatile oils,
glacial acetic acid and in
light petroleum.
Chemical Constituents
Unsaturated resin acids
(90%abietic acid). drug
composition varies
according to the source and
storage conditions, etc.
contains esters of oleic acid
and resin acids, 0.5 %
volatile oil; 5 to 6 %
resenes.
saponic acid and pimaric
acid. Unsaponifiable matter
of colophony, constitutes51 0 %, contains
hydrocarbons and high
molecular weight alcohols.
Storage
stored in the ungrounded
condition in well tilled,
well closed
containers away from light
and in cool places.
In the powder form, it gets
oxidized quickly and
looses its solubility in light
petroleum and gets
increased in the weight and
hence, it
should be stored properly.
Adulterants
black resin or apic resin.
However, both of them can
Confirmed by solubility.
Identification
(1) 1 gm of Colophony
and dissolve in 10 ml of
acetic anhydride by gentle
heat and a drop of
sulphuric acid, bright red
colour changing to violet is
produced.
(2) Alcoholic solution of
colophony is acidic to
litmus.
(3) Dissolve colophony in
light petroleum ether and
double the volume with
dilute solution of copper
acetate, petroleum layer
takes emerald green colour
(due to the coPr
abietic acid).
Uses
stimulant and diuretic.
ingredient of certain
plaster masses and
collodions.
preparation of ointments.
Rapin-esters are used as
protecuve
coatings like polymers.
Industrially, it is used in
the preparation of
varnishes, insulating
compounds, soaps, prinung
inks, paper sizing in the
preparation of floorings,
soldering compounds,
mastics and pressure
sensitive's adhesives.
Storage
stored in the ungrounded
condition in well filled,
well closed containers
away from light and in cool
places. In the powder form,
it gets oxidized quickly
and loses its solubility in
light petroleum and gets
increased in the weight and
hence,
Adulterants
black resin or apic resin.
However, both of them can
be
confirmed by solubility.
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