Exploring thermal decomposition Some compounds can break down into smaller compounds or elements, usually when they are heated. This is called ‘decomposition’. Make sure you wear eye protection and tie back hair during this practical. Limewater is an irritant, so avoid contact with skin. Boiling tubes can smash if the clamp is closed too tight Be careful when handling glass apparatus. Inform your teacher immediately if there is any broken glass. Set up clamp Using a spatula, add some calcium carbonate to your boiling tube Place the bung and delivery tube into the boiling tube Position the boiling tube in the clamp as shown in the diagram (Make sure the apparatus is clamped high enough to allow you to remove the test tube of limewater easily) Pour around 1cm3 limewater into the test tube Place the test tube into the test tube rack Fit the delivery tube into the test tube containing limewater Place a Bunsen burner onto a heat proof mat underneath the boiling tube as shown in diagram Check the Bunsen burner tube and set the Bunsen to safety flame