See discussions, stats, and author profiles for this publication at: https://www.researchgate.net/publication/224141077 Highly sensitive picoampere meter Conference Paper · July 1996 DOI: 10.1109/CPEM.1996.547100 · Source: IEEE Xplore CITATIONS READS 16 261 2 authors, including: G. Rietveld VSL - Dutch Metrology Institute 142 PUBLICATIONS 981 CITATIONS SEE PROFILE Some of the authors of this publication are also working on these related projects: Trazability in High Voltage and High Current View project SASensor development View project All content following this page was uploaded by G. Rietveld on 24 November 2015. The user has requested enhancement of the downloaded file. WEl A-2. HIGHLY SENSITWE PICOAMPERE METER Gert Rietveld and Hans Heimeriks NMi Van Swinden Laboratorium P.O. Box 654, 2600 AR Delft, The Netherlands Abstract We have developed a sensitive picoampere meter for accurate room temperature measurement of currents below 10 PA. The main characteristics of the instrument are an extremely low input current, far below 1 fA, and fully automated operation. Preliminary calibration of the instrument with a separately developed facility has been done at the accuracy level of a few parts in io4. The ability to control the motion of single electrons through a nanostmctured device [ 11 has started worldwide activities on the development of a current standard based on this effect. One of the main problems encountered in the realisation of such a standard is the fact that the current generated by the devices is limited to a few picoampere. An accurate measurement of such a low current requires an extremely low leakage current of the input stage of the measurement setup. This can only be realised using cryogenic equipment [2]. reed capacitor. The slope in Vout is measured by a digital voltmeter DVM1, triggered by an accurate timebase, and is related to the input current by where E represents the integrator error, e.g., caused by leakage. Note that this method of single slope integration is very similar to that used for decades in accurate teraohmmeters [4]. There the current is generated by applying a voltage across a highohmic resistor. Circuit considerations In order to limit leakage currents and noise we have paid extensive attention to correct shielding and guarding, especially of the input terminal. The cable between the current source and the picoampere meter was kept as short as possible. As a first step towards such a cryogenic current measurement, we have built a room temperature picoampere meter. Essential part of the instrument is the input head that was taken from an old vibrating reed electrometer. Since the input stage of such an electrometer only contains two capacitors, leakage currents of less than 100 electrons per second can be realised. A completely new electronic measurement system has been built around the input head in order to achieve a higher accuracy than the few parts in lo3 of the old electrometer [ 3 ] . Picoamperemeter LIA LPF Vout VibratinP Reed Picoamperemeter The block dlagrm of the new instrument is shown schematically in the top part of Fig. 1. The DC input current I,nput charges the vibrating reed capacitor q,, which consequently transforms the DC charge into an AC voltage. This voltage is amplified and then rectified by a lock-in amplifier (LIA), that is using the function generator driving C, (not shown in the fibwe) as reference. The output voltage of the LIA is integrated and the resulting voltage V,, is fed back to the feedback capacitor C, via a low pass filter (LPF). If Iinput is constant, Vout will increase linearly in time, thus continuously nulling the charge on the vibrating Figure 1 Schematic diagram of the picoampere meter with calibration facility. Essential elements of the meter are the vibrating reed capacitor C, and the feedback capacitor C,. Cr, transforms the DC input current into an AC voltage, and a linearly increasing voltage Vout is applied across C;, such that the effect of the incoming charge on C, is compensated. Further explanation is given in the text. 332 each applied current the value of AVOUt/At is determined by a linear fit through the measured values of VOUt. With respect to the original electrometer the sensitivity was considerably increased by changing the driving frequency to the resonance frequency of the vibrating reed capacitor, by improving the preamplifier, and by using a modem LIA. The use of a sinusoidal driving signal instead of the original square wave helped reducing the noise. The measured leakage current of the picoampere meter when no input is applied amounts to (15 f 10) aA. If the calibration setup is connected to the meter, without an intermelate cable, the leakage increases significantly to approximately 0,3 fA. The reproducability of current measurements with the calibration setup is 0,11 fA. Essential part of the new meter is the integrator in the feedback loop, which makes the vibrating reed capacitor a null-indicating amplifier and makes continuous measurements of current possible. Another important aspect is the automation of instrument (including sources) so that many measurement cycles can be repeated automatically. Using the calibrator, the value of the integrator error E was found to be (Sk 2).10-4.Contributions to h s non-zero value include a possible AC/DC error in the value of C,, a non-optimised measurement procedure, and leakage in the capacitors C,, C,, and Cst Calibration of the instrument The basic requirements for accurate measurements with the picoampere meter are directly clear fi-omEq. 1. The two limiting factors for obtaining a high accuracy are determination of the value of C, and the influence of integration errors E . We have developed a room temperature picoampere meter, based on a vibrating reed capacitor, for measurement of currents below 10 PA. Features of the instrument are: a low leakage current, automated control, and an accuracy in the range of a few parts in lo4. Calibration can be carried out with a separately developed setup for generating currents in the pArange. The feedback capacitor is an air capacitor, where the distance between the plates determined by a sapphire spacer. The construction is such that edge effects are important, so that an in situ calibration is necessary. The value of C,, as measured with an AC capacitance bridge operating at 1000 Hz, is (20,6023 f 0,001) pF. Note that the instrument probably can not be used for measurement of the current generated by single electron devices since part of the AC signal generated by the vibrating reed capacitor returns into the current source (even though this effect is limited by an input resistor of 200 MQ, see Fig. 1). Since it is difficult to accurately estimate the effect of integrator errors, we have built a separate facility for generating currents in the range of a few PA. The idea is to reverse the principle of the picoampere meter, namely to apply a linearly ramping voltage across a capacitor. The setup is schematically shown in the bottom part of Fig. 1. The ramp voltage is generated by integrating the DC input voltage Vin . The output of the integrator is applied to a standard capacitor C,, (General Radio, type 1404-C; value 10 pF) and simultaneously measured with a digital voltmeter, DVM2. References -111 L.J. Geerligs, V.F. Anderegg. P.A.M. Holweg, J.E. Mooij, H. Potlhier, D. Esteve, C. Urbina, and M. H. Devoret, “Frequency-Locked Turnstile Device for Single Electrons”, Phys. Rev. Lett., Vol. 64, pp. 269 1-2694, 1990. 121 S.M. Verbrugh, “Development of a Single Electron Turnstile as a Current Standard’, Thesis, Delft University of Technology, Ch. 6, pp. 109122, 1995. [3] “Model 40 1 vibrating reed electrometer”, Cary Instruments, instrument manual. [4] G.C.C. Chen, W.Y.C. Lin, J.C.M. Hsu, S.H. Tsao, “Accurate Stelf-Checking Digital Teraohmmeter”, IEEE Trans. Instrum. and Meas., Vol. IM-44, No. 2, pp. 192-195, April 1995. Measurement results The procedure for measurement of a certain current I is an at least 10 times repetition of the cycle of values +I, 0, -I, 0. The measurements with zero applied current give the possibility to correct for the effect of the leakage current. The voltage ramp during the current measurement always is within symmetrical limits, that vary from f 2 V to f 10 V, depending on the value of the current. The measurement time ranges tiom 40 to 200 seconds. The driving frequency of the vibrating reed capacitor is 575 Hz, and the time constant of the feedback loop is a few seconds. For 333 View publication stats