PURE CHEMISTRY Name: _________________________ Date: ________ CHAPTER 11: SALTS (SALT PREPRATION) PRACTICAL WORKSHEET (PREPARING SODIUM SULFATE SALT) In this worksheet, we will attempt to prepare sodium sulfate salt using each of the three salt preparation methods: 1. Precipitation method 2. “Excess” method 3. Titration method 1. Using the precipitation method i.e. solution + solution a) Let’s try sodium chloride and magnesium sulfate… Word equation: sodium chloride + magnesium sulfate sodium sulfate + magnesium chloride Chemical equation (including state symbols): ________________________________________________________ Pros Cons We will not be able to ___________ off the sodium sulfate salt Conclusion: 1 PURE CHEMISTRY 2. Using the “excess” method i.e. insoluble + acid a) Let’s try sodium metal and sulfuric acid… Word equation: sodium + sulfuric acid sodium sulfate + water Chemical equation (including state symbols): ________________________________________________________ Pros Cons Allows us to obtain sodium Sodium catches fires in water - sulfate too _______________! Sodium sulfate can be easily separated from water by crystallisation Conclusion: b) Let’s try sodium hydroxide and sulfuric acid… Word equation: sodium hydroxide + sulfuric acid sodium sulfate + water Chemical equation: ________________________________________________________ Pros Cons Sodium hydroxide is _____________ in water so we will never be able to _____________ off the excess sodium hydroxide We cannot actually obtain the sodium sulfate salt Conclusion: 2 PURE CHEMISTRY 3. Using the titration method i.e. acid + alkali a) Let’s try sodium hydroxide and sulfuric acid… Word equation: sodium hydroxide + sulfuric acid sodium sulfate + water Chemical equation (including state symbols): 2NaOH (s) + H2SO4 (aq) Na2SO4 (aq) + H2O (l) Pros Cons The use of _____________ allows us to know how much reagents to add Sodium sulfate can be easily separated from water by crystallisation Conclusion: b) Let’s try sodium carbonate and sulfuric acid… Word equation: sodium carbonate + sulfuric acid sodium sulfate + carbon dioxide + water Chemical equation: Na2CO3 (s) + H2SO4 (aq) Na2SO4 (aq) + CO2 (g) + H2O (l) Pros Allows us to obtain sodium sulfate Cons _____________ will affect the observation of the colour change at end point Sodium sulfate is easily obtainable using crystallisation Conclusion: 3