International Conference on Recent Advances in Mechanical Engineering and Interdisciplinary Developments [ICRAMID - 2014] DESIGN AND FABRICATION OF METAL MATRIX COMPOSITES AL6061/GRAPHENE AND ANALYZE THE MECHANICAL PROPERTIES Barnabas Swithan. J#1, Saravanapandi Solairajan. A*2 # Department of Mechanical Engineering, Infant Jesus College of Engineering and Technology, Tirunelveli, Tamil Nadu, India. * Assistant Professor, Department of Mechanical Engineering, Infant Jesus College of Engineering and Technology, Tirunelveli, Tamil Nadu, India. 1 j.barnabasswithan@gmail.com 2 solairajan2k@gmail.com By the study of the aluminium 6061 based metal matrix composites; a new emerging material graphene has been founded in 2004. Here aluminium 6061 used as a matrix and graphene used as a reinforcement material. Nowadays, research has been done on graphene reinforced metal matrix composites because of low friction, low wear rate. The mechanical, electrical and thermal properties of graphene are very high compared with traditional metals, making them a potentially promising reinforcement material in a metal matrix composite [1]. Generally the stir casting process for MMC’s involves preparing a melt in the furnace of the selected matrix material. Then the reinforcing material is poured into the melt matrix material to get dispersion by stirring. The stir casting process is widely used to fabricate metal matrix composites [2,3]. Abstract— Our motivation was to analysis the mechanical properties of metal matrix composite of AL6061/Graphene. Composite materials are stronger than conventional building materials, Graphene is a latest two-dimensional (2D) honeycomb lattice, and numerous engineering, including commercial applications in the transportation and construction widely uses aluminium 6061. Graphene has demonstrated exceptional electrical, mechanical and thermal properties. The reinforcing graphene particulates in the MMC are examined for aluminium 6061 and vary from 1% to 4% by weight. The ‘Stir casting process’ was employed to make the composites, in that the reinforcements is poured into the stir casting and created by stirring the molten metal by, with a mechanical agitator. Keywords— Aluminium 6061, Graphene, Stir II. MATRIALS AND METHODS casting method, Scanning electron microscope, mechanical properties. Al6061 is used for the study of metal matrix composite. It is studied for large production of weightless metal castings. Al6061 alloy is widely used because of its formability, connectivity, corrosion resistance and low price. Table-1 shows the chemical combination of Al6061 alloy. Graphene nanopowders particles are very thin in thickness measuring 5 to 10 nanometers with little large in diameters. They are applicable in van der waals attractive forces and have a tendency to reaggregate in dry state because of their flat shape of these particles. Alumina coated stainless steel stirrer was used in the molten metal pool through stir casting process and reinforcing materials were introduced. I. INTRODUCTION By the change in science and technology, there are competitive both in liberalization and global market [1]. Materials with high strength and low density have been used in industries. Aluminium alloy used as a matrix other material used as a fibre which has been reinforced widely use in technical applications because of their roughness and usability when compared with conventional aluminium alloys [2]. Many tests have been carried out on composite materials based on aluminium 6061. ISBN 978-1-4799-3158-3 275 International Conference on Recent Advances in Mechanical Engineering and Interdisciplinary Developments [ICRAMID - 2014] The migration of ferrous ions from the stair into the molten metal was prevented by a coating of alumina to the blades. The stirrer is coated at 550rpm and the immersion of the stirrer was done about two – thirds of the depth of the molten metal. The reinforcing materials were added into the stir casting process for about 3 – 4 minutes. The mixture was poured into the preheated permanent metal molds. every interval and the readings of the length are noted until breaking takes place. Using the readings compressive stress-strain curve is plotted. The nature of the test specimen can be seen under compression from this curve. Compressive properties and strength of the specimen are being calculated. Table-I. Chemical composition of element with Al6061 alloy by weight percentage. Element Weight% Mg (Magnesium) 1.08 Fe (Ferrous) 0.17 Si (Silicon) 0.63 Cu (copper) 0.32 Mn (Manganese) 0.52 V (Vanadium) 0.01 Ti (Titanium) 0.02 Al (Aluminium) Fig. 1 Tensile test specimen. Balance A. PREPARING AND TESTING A SPECIMEN The specimens were prepared in the form of a cylindrical bar castings. Each measure about 8mm in diameter X 60 mm length measuring 20 X 20 mm diameter is used for compression testing. Microscopic examination was done with keller’s reagents as agent. The specimens were cleaned with distilled water, acetone and dried thoroughly. B.TENSILE TEST Each specimen measuring 8 mm in diameter and 60 mm gauge length as per ASTM E8 – 82 standards as shown in the Fig. 1. The cross sectional area is measured for conducting a standard tensile test. Gauge length is placed in the machine and extensometer is attached. Readings of load and elongation are taken at uniform intervals of load and the Fig. 2 shows the specimen after tensile testing. Fig. 2 Composite specimen after tensile test. D. HARDNESS TEST Hardness test is carried out in a cast and metal matrix composites to know the participation of reinforcement graphene in matrix material aluminium 6061. A Vickers micro hardness machine is used to check the polished specimen. A load of 1N is given at every interval of 10 seconds. The hardness was seen by taking the diagonal length of the indentation. The test is carried at three different levels and the average value was taken as the hardness of the cast and composite specimen. C. COMPRESSION TEST Compression test is being done same as the tensile test. Specimen measures about 20 mm diameter and 20 mm length. Testing is done on the universal testing machine. A load of 2 tons is given at ISBN 978-1-4799-3158-3 276 International Conference on Recent Advances in Mechanical Engineering and Interdisciplinary Developments [ICRAMID - 2014] variation strength in the aluminium 6061 metal matrix composite material is shown in Fig. 6. Graphene reinforcement particulates increase the tensile strength of the metal matrix composite materials. Yielding point of metal matrix composite samples increases rapidly with increase in reinforcements. Al6061 alloy matrix increases the strength because of the increase of weight percentage of graphene. III. RESULTS AND DISCUSSIONS A. ANALYSISING MICROSTRUCTURE We can see a sample of microstructure of aluminium 6061 as a cast in Fig. 3. Precipitations are seen in both the grains. Fig. 5 Ultimate tensile strength and effect of graphene wt % of MMC’s. Fig. 3 Microstructure for aluminium 6061 as cast. Fig. 6 Graphene and yield variation strength in Al6061 matrix. C. COMPRESSIVE STRENGTH Fig. 4 Microstructure of 4 wt% Graphene Al6061 composite specimen. Fig. 4 shows the microstructure of aluminium 6061 along with graphene at 4 % weight. The grain size is little larger than the composites. Minimum micro porosities are seen in the micrograph. In the matrix there is no clustering of reinforcement and dispersion of graphene particle is uniform. There is no gap is found between the aluminium 6061 matrix and the reinforcing material graphene are seen well bonded. Fig. 7 Compression strength as a function of graphene content in wt %. B. TENSILE STRENGTH Ultimate tensile strength and effect of graphene is shown in Fig. 5. Increase of graphene and yield The uniaxial compression as a function of graphene content is shown in Fig. 7. An increase in ISBN 978-1-4799-3158-3 277 International Conference on Recent Advances in Mechanical Engineering and Interdisciplinary Developments [ICRAMID - 2014] the compressive strength is due to the increase of graphene content. Addition of graphene reinforcement to a soft matrix increases its density and compressive strength [11]. The results were studied on the compressive strength of metal matrix composite materials [12-16]. Saravanapandi Solairajan. A M. Tech Assistant Professor. Words are not enough to express my special thanks for his enhancing and encouraging ideas that sound in each and every process. REFERENCES [1] Alakesh Manna, B. Bhattacharayya. 2005. 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MICRO HARDNESS RESULTS Fig. 8 Hardness number Al6061 alloy and different wt % of graphene [5] The results of aluminium 6061 and metal matrix composite of different weight percentage of graphene are predicted using the Vickers micro hardness test as shown in Fig. 8. Hardness of the composite material is higher when compared with that of the parent metal. The weight percentage of graphene content increases the hardness of MMC’s and splitting of graphene particles also increases the hardness. DiWei, Hongwei Li, Dongxue Han, Qixian Zhang, Li Niu, Huafeng Yang, Chris Bower, Piers Andrew and Tapani Ryh¨anen. (2011) ‘Properties of graphene inks stabilized by different functional groups’ IOP PUBLISHING Nanotechnology 22 (2011) 245702 (7pp) [6] Fernanido Audebert, Fredic Prima, Mario Galano, (2002). ‘Structural charecterisation and Mechanical Properties of. Nanocomposite Al-based Alloy’. Materials Transaction, vol.43, No.8 (2002) pp. 2017 to 2025. [7] A.K. Geim and K.S. 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Rafiee, Javad Rafiee, Iti Srivastava, Zhou Wang, Huaihe Song, Zhong-Zhen Yu, and Nikhil Koratkar (2010) The following conclusions are made by analyzing the mechanical properties of metal matrix composite Al6061/ Graphene. a) Graphene was reinforced in the Al6061 alloy to fabricate metal matrix composite using stir casting method. b) The MMC’s which are fabricated have uniformly distributed of reinforcements and matrix in the microstructure analysis. c) The ultimate tensile strength of metal matrix composite Al6061 / graphene is significantly increased. d) Increase in weight percentage of graphene content increases the hardness of MMC’s. This because of graphene particles which strengthen the Al6061 alloy. ACKNOWLEDGEMENT I greatly acknowledge my project guide, who shared his valuable ideas in making my project Mr. ISBN 978-1-4799-3158-3 278 International Conference on Recent Advances in Mechanical Engineering and Interdisciplinary Developments [ICRAMID - 2014] ‘Fracture and Fatigue in Graphene Nanocomposites’. small 2010, 6, No. 2, 179–183 [14] D. OSSO, G. LE CAER, S. BEGIN-COLIN, A. MOCELLIN and P. MAmAZZI (1993) ‘Synthesis of alumina-metal nanocomposites by mechanical alloying’ JOURNAL DE PHYSIQUE IV Colloque C7, supplkment au Journal de Physique 111, Volume 3, pp. 1407 to 1412 [15] A. Ramesh, J. N. Prakash, A. S. 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