20 SPECMA SEALS HANDBOOK S T U F F I N G B OX PA C K I N G S Grafoil® rings – die-moulded expanded graphite Material description: Properties: Grafoil® is made of 100% natural graphite, which is treated with acids and high temperature according to a specially developed process. The result is expanded graphite, which after calendering, becomes a soft and flexible foil that is used for manufacturing gaskets. Grafoil® contains no binders or other additives, but is a pure carbon product in the form of graphite. Permanent elasticity, does not harden at high temperature, does not dry, does not shrink. Applications: Broad medium resistance range. Thanks to its unique properties, Grafoil® is ideal as a packing material for valves, pumps and agitators. Can be used for more or less all media such as water, steam, acids, alkalis, petroleum products, solvents and gases, but not for strongly oxidising acids such as sulphuric acid and nitric acid in combination with high temperature plus chromium solutions and hot permanganate. We do not recommend graphite in combination with sea water and stainless steel. Abrasive media and equipment with large shaft runout should be avoided. Standard types Stable volume, practically no compression set in heat. Fireproof, meets requirements as per API 607. Self-lubricating, low friction. Extremely good thermal conductivity. Very good sealing capability, hence low emissions. BAM-approved for oxygen and liquid oxygen*. Good resistance to radioactive media. Unlimited service life results in unsurpassed economy. Extremely low chloride content minimises the risk of corrosion of stainless steel. No corrosion inhibitor is needed. Technical data: Temperature limit: -200°C to +550°C in air max. +2500°C in nonoxidising atmosphere max. +200°C in oxygen pH range: 0-14 Graphite content: min. 98.0% industrial quality min. 99.5% nuclear power quality Max. content of leachable chlorides: Max. sulphur content: Max. surface speed: Square or rectangular cross-section Cover plate seal with 45° internal chamfer Cover plate seal with 45° external chamfer Special types of cover plate seals with stainless steel caps Cover plate seal with internal radius 50 ppm 550 ppm 25 m/s Max. pressure: 60 bar in pumps 700 bar in valves Purity: The Swedish nuclear power industry, which has the most stringent requirements, normally accepts max. 50 ppm leachable chlorides. We can supply Grafoil® with a certified max. 50 ppm, but the content in Grafoil® is normally approx. 10 ppm. Documented max. chloride content, as well as other quality documents can be supplied if requested. *) If BAM certification is required for this product, this must be specified at the time of ordering. Type SF Type SR Type ST The stated limit values apply under favourable conditions. Do not utilise more than one maximum value at a time. If in doubt please contact us, we will be happy to offer advice. SPECMA SEALS HANDBOOK S T U F F I N G B OX PA C K I N G S Manufacturing: Recommended densities for die-moulded Grafoil rings: Rings are manufactured with a square or rectangular cross-section, or with a chamfer (for valve covers) or other special cross-section. The rings can be pressed to different densities to specification from 1.3 to 1.8 g/cm3. All rings can be supplied endless or split, with straight or diagonal cut. Cut rings can be threaded onto a shaft even if the shaft end is not accessible. For normal use in valves: Die-moulded graphite ring with stainless steel antiextrusion caps. 1.8 g/cm3 For valve cover seals: 1.8 g/cm3 For rotating shafts: 1.4 g/cm3 If you wish to manufacture Grafoil® sealing rings yourself, we can offer the Grafoil® Ribbon Pack, expanded graphite in the form of corrugated ribbon supplied in the following standard dimensions: Dimensions: Standard tolerances for Grafoil rings: Inner diameter Ø < 50 mm Ø 50-150 mm Ø 150-300 mm Ø > 300 mm +0.3/-0+0.5/-0+0.7/-0+1.0/-0 Outer diameter Ø < 50 mm Ø 50-150 mm Ø 150-300 mm Ø > 300 mm +0/-0.3+0/-0.5+0/-0.7+0/-1.0 Ring height Dimensions Metres mm per box Part number 12.5 x 0.5 19 x 0.5 25 x 0.5 30 30 30 362212 362219 362225 38 x 0.5 50 x 0.5 30 30 362238 362251 We stock the most common dimensions for valves, pumps and sootblowers. Alternative versions of packing sets: We can offer complete sets in versions suitable for special requirements. A few examples are shown below: Std version with scraper end rings and extra diffusion barrier of soft gaskets. Die-moulded Grafoil rings ±5% Specmaseal Type S std version with scraper end rings made of die moulded carbon fibre braided packing, see page 24. For valves with large clearances: Grafoil® Ribbon Pack – ribbon material: For static applications with large clearance and/or high pressure, e.g. for valve covers and heat exchangers, die-moulded rings fitted with a stainless steel cap can be supplied to prevent the risk of extrusion. These rings normally have a rectangular cross section or a 45° chamfer. Std version with filler bushing. 1.4-1.5 g/cm3 Specmaseal Type F with bevelled rings and scraper end rings for improved transverse expansion, see page 24. Grafoil® is a registered trademark of GrafTech International Holdings Inc. 21 22 SPECMA SEALS HANDBOOK S T U F F I N G B OX PA C K I N G S Grafoil® rings – Ribbon Pack installation instructions For valves: 1. Clean the stem and stuffing box thoroughly. Replace damaged mechanical parts. Lubricate the stem with Grafex® GTL graphite paste and carefully rub in the graphite. Wipe off excess grease. 2. Select a suitable ribbon width. 3. Wind Ribbon Pack around the stem until the box is full. 4. Push the packing material down into the stuffing box. 5. Use a split mounting sleeve and push the first ring down to the bottom of the box. 6. The clearance between the mounting sleeve and the stem or box wall must not exceed 0.25-0.30 mm. 11.Do not mix Grafoil® Ribbon Pack with stuffing box packing braids of materials other than carbon fibre and expanded graphite. 12.For final adjustment of the gland: loosen it and check that the stem can be rotated. Then tighten the gland gradually until the valve does not leak under pressure. The gland does not normally need readjustment. Selection of Ribbon Pack width If packing space width is: Use Ribbon Pack width: Up to 6 mm 12.5 mm 6 mm - 10 mm 19.0 mm 10 mm - 13 mm 25.0 mm 13 mm and above 38.0 mm Note: In certain cases, the access between the upper edge of the stuffing box and the lower part of the gland can be limited, for which reason a narrower ribbon than recommended must be used. When ordering ready made die-moulded rings, state the required density or area of use. 7. Using the gland and the mounting sleeve to compress the first ring; at least 50 MPa pressure is recommended, which gives approx. 50% compression and a density of approx. 1.6 g/cm3. 8. Loosen the gland, remove the mounting sleeve and check that the stem can be rotated. 9. The following rings are installed and compressed one at a time, as described in sections 3-6. 10.We do not recommend installing more than 4 to 6 rings. If the stuffing box is very deep, a filler bushing of carbon or suitable metal should be fitted in the bottom. For pumps: 1. Follow the installation instructions for valves in sections 1-11, but the rings must be compressed to max. 25 MPa (250 bar) pressure, giving a density of approx. 1.4 g/cm3. 2. Once all the rings have been installed, start the pump. Leave the gland tightened only finger-tight to avoid overheating the shaft during the running-in period. 3. If the media so allows, a certain amount of leakage simplifies running in. Adjust the gland nuts one flat at a time, until the leakage is reduced to 20-60 drops/ minute, depending on the application. 4. The stuffing box does not need to be totally emptied for packing replacement with clean media. If necessary fill up with a Ribbon Pack ring. Fig. 1. Ribbon Pack is wound around the stem. Fig. 2. Use a split mounting sleeve for compression. Note: If the diametrical clearance between the stem and box bottom exceeds 0.5 mm or if the media contains abrasive particles, a ring of braided carbon fibre packing material (e.g. Garlock 98®) should be placed in the bottom. Installation instructions for readycut die-moulded rings: 1. If the stuffing box is unnecessarily deep (more than 5-6 rings) or if the clearance between the stem and the box bottom is too large (more than 0.5 mm diametrically), start by installing a suitable filler bushing of carbon or suitable metal, or shims. 2. Install the first Grafoil® ring separately and push down to the box bottom using a mounting sleeve (possibly split). This sleeve shall have max. 0.6 mm diametrical clearance toward the stem and box walls. If a free shaft or stem end is not available, you may cut the The stated limit values apply under favourable conditions. Do not utilise more than one maximum value at a time. If in doubt please contact us, we will be happy to offer advice. Fig. 3. Each ring is compressed individually. die-moulded ring, either straight or at an angle. Open the ring carefully axially and fit it over the shaft or stem. Make sure that the rings are installed with the cuts displaced by 120° to each other. 3. Compress the ring with the mounting sleeve, gland nuts and gland. Use normal ring spanners and tighten as hard as you can. 4. Repeat the process for the following rings, one or max. two at a time. 5. Then follow the instructions according to sections 10-12 for valves and 2-4 for pumps. Note: Only by compressing the rings one at a time with the mounting sleeve can you be sure that the first ring (bottom ring) seals. Note: The stuffing must be tightened as hard as possible and then loosened and thereafter be adjusted.