Deutsche Akkreditierungsstelle GmbH
Annex to the Accreditation Certificate D-PL-14170-01-00
according to DIN EN ISO/IEC 17025:2005
Period of validity: 19 December 2012 to 18 December 2017 (Date of issue: 13 February 2013)
Holder of certificate:
GBA Gesellschaft für Bioanalytik mbH
at these sites
Goldtschmidtstraße 5, 21073 Hamburg
Wiedehopfstraße 30, 45892 Gelsenkirchen
Flensburger Straße 15, 25421 Pinneberg
Brekelbaumstraße 1, 31789 Hameln
Daimlerring 37, 31135 Hildesheim
Meißner Ring 3, 09599 Freiberg
Im Emscherbruch 11, 45699 Herten
Berliner Ring 2, 38440 Wolfsburg
Tests in the areas of:
physical, physico-chemical and chemical analyses of water, sewage, groundwater, surface water,
leachate, bottled water, mineral water, bathing water, sewage sludge, sludges, waste, soils,
contaminated soils, compost, sediments, foods and commodities, wood, building materials and
mixtures, fuels, insulating and waste oil, soil gas, dust, raw materials for pharmaceutical purposes
and other pharmaceutical matrices, and chemical products;
microbiological analyses of foods and raw materials for pharmaceutical purposes;
selected molecular biological analyses of foods;
analyses in accordance with the Drinking Water Ordinance, with the exception of the
radiological parameters, sampling of untreated water and drinking water;
sampling of water, sewage, surface water, water from aquifers, water from stagnant bodies of
water, water from mineral and medicinal springs, flowing waters, sludges, sewage sludge, soils and
contaminated soils, sediments and waste;
Subject module Water, soil and contaminated sites, and waste
Abbreviations used: see last page
This document is a translation. The definitive version is the original German annex to the accreditation certificate.
Appendix to the accreditation certificate D-PL-14170-01-00
Table of contents:
1
4)
2
3
4
5
6
7
8
9
page 81)
Environmental analysis (water, waste, soil/contaminated sites, drinking water) (from page
Sector for insulating oil analysis (from page 32)
Sector for fuel analyses (secondary fuels, fuels, alternative fuels, biofuels) (from page 33)
Sector for food and commodity analysis (from page 35)
Sector for pharmaceuticals (from page 45)
Testing methods for the water subject module (from page 48)
Testing methods for the soil and contaminated sites subject module (from page 56)
Testing methods for the waste subject module (from page 69)
Testing methods in accordance with the Drinking Water Ordinance – TrinkwV 2001 – (from
The testing methods are marked with the following symbols for the sites at which they are performed:
HH = Hamburg
GE = Gelsenkirchen
PI = Pinneberg
HM = Hameln
HI = Hildesheim
FG = Freiberg
HE = Herten
WOB = Wolfsburg
The testing methods listed and marked with (A) comply with § 2 of the agreement of 22 May 2000
between the Oberfinanzdirektion Hannover and the DAP, DACH and DASMIN accreditation bodies
for the accreditation of testing laboratories and engineering firms in the context of investigating
contaminated areas/areas suspected of being contaminated on federal property.
For the sector for the sampling of water at the PI, GE and HI sites, competence for the full range of
the required parameters is confirmed.
For the sectors for the analysis of water, soil and soil gas at the PI and GE sites, competence for a
part of the required parameters is confirmed.
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
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Appendix to the accreditation certificate D-PL-14170-01-00
Flexibility:
The laboratories are authorised to apply the standardised testing methods listed under sections
1 to 5 (see table of contents), excluding the sampling methods, without the requirement for
prior information and consent from the DAkkS, with different versions of the standards.
Within the testing areas in the following table, the laboratories at the sites are authorised to
freely select the standardised testing methods or their equivalents, without the requirement
for prior information and consent from the DAkkS:
Site
Matrix
Testing type
Pinneberg Water, waste,
Atomic spectrometry, gas chromatography,
soil/contaminated
electrochemistry, gravimetry, measurement analysis,
sites (outside of the
photometry, physical, physicochemical characteristics, sum
subject module)
parameters, ion chromatography
Hamburg Raw materials and
Atomic spectrometry, electrochemistry, gravimetry,
solids for the
measurement analysis, sum parameters, non-specific and
pharmaceutical
specific cultivation techniques
industry
Hamburg Foods
Atomic spectrometry, gravimetry, photometry,
measurement analysis and non-specific and specific
microbiological cultivation techniques
The testing methods listed are examples. The laboratory has an up-to-date
list of all testing methods in the flexible scope of accreditation.
Within the testing areas in the following table, the laboratories at the sites are authorised to
modify and to further develop and redevelop the testing methods, without the requirement for
prior information and consent from the DAkkS:
Site
Matrix
Testing type
Hamburg Raw materials and
Gas chromatography
solids for the
pharmaceutical
industry
Hamburg Raw materials and
HPLC, LC-MS/MS
solids for the
pharmaceutical
industry
Hamburg Foods
Gas chromatography, HPLC, LC-MS/MS
Hamelin
Foods
LC-MS/MS, HPLC-MS/MS concerning analytes and matrices
Hamelin
Water, waste,
LC-MS/MS, HPLC-MS/MS concerning analytes and matrices
soil/contaminated
sites (outside of the
subject module)
The testing methods listed are examples. The laboratory has an up-to-date
list of all testing methods in the flexible scope of accreditation.
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
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Appendix to the accreditation certificate D-PL-14170-01-00
1
Environmental analysis (water, waste, soil/contaminated sites, drinking water)
Testing type: Atomic spectrometry (ICP-MS, ICP-OES, AAS)
Standard/issue date
Analyte – Title of the standard
In-house method/version Information on sample pre-treatment/testing
technology
DIN EN 1483 (E12)
Determination of mercury – Method using atomic
2007-07
absorption spectrometry
Replaces 1997-08 (A)
DIN EN ISO 17852
2008-04
AbfKlärV 1992
Appendix 1.3.1
LAGA guideline SM 1/78
1978
LAGA guideline
SM 2/79 1983-12
DIN EN ISO 11885 (E22)
1998-04 (A)
and 2009-09
DIN ISO 22036
2009-06
Determination of mercury using AFS
Dev.: microwave digestion with aqua regia or nitric
acid
Replaces DIN EN 13506 (E35) 2002-04
Heavy metals: Cd, Cr, Cu, Hg, Ni, Pb, Zn
Dev.: measurement using ICP-MS
Heavy metals dev.: determination using ICP-OES
(withdrawn directive)
Heavy metals using ICP-OES Cd, Cr, Cu, Hg, Ni, Pb,
Zn (withdrawn directive)
Water quality – Determination of selected elements
by inductively coupled plasma optical emission
spectrometry (ICP-OES): Al, Ba, Be, B, Ca, Cd, Co, Cr,
Cu, Fe, K, Mg, Mn, Na, Ni, Pb, Se, Sn, Te, Ti, V, Zn
Dev. for solids: determination from aqua regia or
microwave digestion: As, B, Ca, Cd, Co, Cr, Cu, Fe, K,
Mg, Mn, Mo, Na, Ni, P, Pb, Sb, Sn, Te, Ti, V and Zn;
additionally Te and Tl
Soil quality – Determination of trace elements in
extracts of soil by inductively coupled plasma –
atomic emission spectrometry (ICP-AES)
DIN EN ISO 17294-2 (E29) Water quality – Application of inductively coupled
2005-02
plasma mass spectrometry (ICP-MS) – Part 2:
Determination of 62 elements:
Dev.: here only for Al, As, B, Be, Ca, Cd, Co, Cr, Cu,
Fe, K, Hg, Mg, Mn, Mo, Na, Ni, Pb, Sb, Se, Sn, Sr, Tl,
Zn,
U only for drinking water
E DIN EN 16171
Sludge, treated biowaste and soil – Determination
2010-11
of trace elements using inductively coupled plasma
mass spectrometry (ICP-MS)
VGB-M 701
Serial no. 02 and 8
2008 -12
Sodium, potassium and magnesium as minor
constituents of gypsum after aqueous extraction
and measurement using ICP-OES and conversion to
the corresponding oxides
Test object
Site
WA, SE, SW, GW, PI
EL
WA, SS, DW, SO,
WO
PI
SS, SL
PI
WA, EL
PI
WS, SL
PI
WA, SE, SW, GW, PI
EL, AC, DW
SO, SL, SED, BW
PI
WA, SE, SW, GW, PI
DW, EL, AC
SO, SL, SED, SM,
SS
PI
GY
PI
Testing type: Gas chromatography (GC-FID, GC-ECD, GC-NPD, GC-MSD, GC-AED, GC-TCD, GC-MS/MS)
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
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Standard/issue date
Analyte – Title of the standard
In-house method/version Information on sample pre-treatment/testing
technology
In-house method
n-alkanes C1-C4 and n-alkenes C1-C4
SOP no. 0656
(Methane, ethane, ethylene, propane, propene,
2004-11
carbon dioxide, carbon monoxide) using GC-FID and
TCD
In-house method
Alkanes, volatile C1 to C5 using GC-FID
HI- MA-M 3-19
2008-11
In-house method
Alkanes, volatile C1 to C5 using GC-FID
HI- MA-M 3-20
2010-02
DIN EN ISO 22032
Water quality – Determination of selected
2009-07
polybrominated diphenyl ethers in sediment and
sewage sludge – Method using extraction and gas
chromatography/mass spectrometry:
Polybrominated diphenyl ether (PBDE),
polybrominated biphenyls (PBB),
tetrabromobisphenol-A (TBBP-A),
hexabromocyclododecane (HBCD), tribromoanisole
(TBA)
Dev.: liquid/liquid extraction with water samples,
additional matrices (biota, polymers and materials):
ultrasonic extraction, other internal standards
DIN 38407-F9-1
Determination of benzene and some of its
1991-05
derivatives using gas chromatography using
(A)
headspace analysis (HS-GC)
BTEX: benzene and some of its derivatives,
naphthalene, monochlorobenzene and
dichlorobenzene
by GBA-PI:
in addition, SPIMFAB and Aliphatics C5-C10
Dev.: analysis also using GC-MSD. for soil and waste:
elutriation with water
DIN ISO 22155
Soil quality – Gas chromatographic quantitative
2006-07
determination of volatile aromatic and halogenated
and 2009-08 (draft)
hydrocarbons and selected ethers – Static
headspace method (BTEX/VHH)
Replaces: HLUG, Contaminated sites handbook Vol.
7, Part 4 2000
HLUG, Contaminated
BTEX/ VHH: benzene and some of its derivatives
sites handbook Vol. 7,
using GC-MS after overcoating with methanol
Part 4 2000
VDI 3865 sheet 3
Measurement of organic soil pollutants – Gas
1998-06
chromatographic determination of volatile organic
compounds in addition to other solvents in soil gas
after adsorption at activated carbon and desorption
with organic solvents
Test object
Site
GA
GE
WA
HI
GA
HI
WA, SO, SL, SED,
PO, BIO, MAT
PI
WA, SE, SW, GW, PI, HI
DW, SO, WS, GA
SO, SL, SED
PI
SO
GE
GA
PI, GE
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
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Standard/issue date
Analyte – Title of the standard
In-house method/version Information on sample pre-treatment/testing
technology
VDI 2100 sheet 2
Determination of gaseous compounds in ambient
2010-11
air – Determination of indoor air pollutants – Gas
chromatographic determination of organic
compounds – Active sampling by accumulation on
activated charcoal – Solvent extraction
Dev.: determination of BTEX/VHH (benzene and
some of its derivatives, as well as volatile
halogenated hydrocarbons and C3 aromatics) using
GC-MSD after method adjustment (tube type,
internal standards, GC column)
In-house method
BTEX, VHH and C3 aromatics in air samples;
HI-MA-M U 3-25
determination from HS vials
2009-11
E DIN 38407-F37
Determination of organochlorine pesticides,
2011-11
polychlorobiphenyls and chlorobenzene in water –
Method using gas chromatography and mass
spectrometric detection (GC-MS) after liquid-liquid
extraction
Dev. measurement also using GC-MS/MS
DIN ISO 10382
Determination of organochlorine pesticides and
2003-5
polychlorinated biphenyls – Gas chromatographic
(A)
method with electron capture detection
(chlorobenzenes, organochlorine pesticides and
PCBs)
Dev.: analysis using GC-MSD
Dev: processing of sludge or sediment from freezedried samples
ISO 12010
Water quality – determination of short-chain
2012-03
chlorinated paraffins (SCCP) in water – method
using gas chromatography-mass spectrometry (GCMS) and negative chemical ionisation (NCI)
Dev.: additional determination of MCCPs, modular
clean-up, modified quantification, GC-MSD
detector, additional matrices (soil, sediment,
material)
DIN EN 12673-F15
Water quality – Gas chromatographic
1999-05
determination of some selected chlorophenols in
water using GC-MSD
Dev: in addition, phenol, cresols and xylenols are
also determined, as well as triclosan and bisphenol
A in PI
Replaces E-DIN EN 12673 1997-02
DIN ISO 14154
Soil quality – Determination of selected
2005-12
chlorophenols –
(A)
Gas-chromatographic method with electroncapture detection
Dev. PI: determination using GC-MS
Test object
Site
GA
PI
GA, SO
HI
WA, SE, SW, GW, PI
DW, EL
SO, SL, SED
PI, HI
WA, SW, GW,
DW, SO, SED,
MAT
PI
WA, SW, GW,
DW
PI, HI
SO
PI, HI
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
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Standard/issue date
Analyte – Title of the standard
In-house method/version Information on sample pre-treatment/testing
technology
AltholzV App. 1.4.4 in
Determination of selected chlorophenols
conjunction with
(chlorophenols, PCP, phenols, cresols, xylenols)
DIN EN 12673-F15
Dev: in addition, triclosan and bisphenol A are
1999-05
determined, additional determination in COM and
MAT
CEN TR 038101
Chlorophenols and alkylphenols using GC-MSD
(BAM method)
2002-02
In-house method
Glycols (ethylene-, diethylene-, triethylene- and
PI- MA-M 3-77
propylene glycol) in water and soil using GC-MSD
2012-05
In-house method
Determination of selected heterocyclic compounds
PI-MA-M 3-98
according to the Kora list, in water and eluates using
2012-03
GC-MSD
DECHEMA e.V.
2008-11
DIN EN ISO 9377-2-H53
Water quality – Determination of hydrocarbon
2001-07
index – Part 2: Method using solvent extraction and
(A)
gas chromatography
GBA-PI: additional analysis after petrol pack
DIN ISO 16703
Soil quality – Gas chromatographic determination of
2011-09
content of hydrocarbon in the range of C10 to C40
(A)
GBA-PI: additional analysis after petrol pack
DIN EN 14039
Characterisation of waste – Determination of
2005-01
hydrocarbon content in the range of C10 to C40 by
gas chromatography (GC-FID)
LAGA guideline KW/04
2004-11
DIN EN ISO 16588 (P 10)
2004-02
DIN EN ISO 10301-F4
1997-08 (A)
incl. DIN 38407-F5
1991-11
DIN EN ISO 15680-F19
2004-04
Test object
Site
SO, WO, SED,
COM, MAT
PI
WO
HI
SO, WA
PI
WA EL
PI
WA, SE, SW, GW
PI, HI, GE
SO, SL, SED
PI, HI, GE
WS, SO
PI, HI, GE
Hydrocarbons in waste using GC-FID
WS
PI, HI, GE
Water quality – Determination of six complexing
agents, EDTA, NTA and others – Gaschromatographic method (GC-MSD)
Dev.: additional matrices (soil and cleaning agents)
after aqueous eluate creation
Water quality – determination of volatile
halogenated hydrocarbons – gas chromatographic
method or GC-MSD
Dev.: additional matrices (solids and air)
Gas chromatographic determination of a number of
monocyclic aromatic hydrocarbons, naphthalene
and several chlorinated compounds using purgeand-trap and thermal desorption
WA, SO, CA
PI
WA, SE, SW, GW, PI, HI, GE
DW, SO, SL, SED,
WS, GA
WA
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
GE
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Standard/issue date
Analyte – Title of the standard
In-house method/version Information on sample pre-treatment/testing
technology
In-house method
Musk compounds in water and solids using GC-MSD
PI-MA-M 3-81
2012-06
DIN ISO 15009
Gas chromatographic determination of the content
2004-08
of volatile aromatic hydrocarbons, naphthalene and
volatile halogenated hydrocarbons – Thermal
desorption after blowing out and collecting on an
adsorbent
DIN 38407-F 17
Determination of selected nitroaromatic
1999-02
compounds by gas chromatography (GC-MSD)
Contaminated sites
Nitroaromatics by GC-MSD
handbook
Vol. 7, part 5 2004
DIN EN ISO 18857 -1
Water quality – Determination of selected
2007-02
alkylphenols – Part 1: Method for non-filtered
samples using liquid-liquid extraction and gas
chromatography with mass selective detection
Dev.: in addition, octylphenols and ethoxylate are
determined
Dev.: extraction with hexane and other clean-up
DIN EN ISO 18857-2
Water quality – Determination of selected
2012-01
alkylphenols – Part 2: Gas chromatographic mass
spectrometric determination of alkyl phenols, their
ethoxylates and bisphenol A for non-filtered
samples using solid-phase extraction and
derivatisation;
Deviation: here only for alkylphenols and their
ethoxylates; only used for measurement, other
internal standards, additional analytes: OP3EO and
NP3EO
Nonylphenol standard –
Soils sludges and treated bio-waste – Organic
horizontal – 13.1
constituents- Nonylphenols (NP) and nonylphenol2006
mono- and diethoxylates by gas chromatography
with mass selective detection (GC-MS)
Dev.: only used for extraction
In-house method
Determination of organic acids (C1-C5) in water
HI-MA-M U-03-22
after derivatisation using GC
2010-06
DIN EN ISO 10695 F6
2000-11
(A)
In-house method
PI-MA-M 3-79
2012-06
Water quality – Determination of selected organic
nitrogen and phosphorous compounds – Gas
chromatographic method (GC-MSD) pesticides SWEEPA, neutral reprocessing (GC method 2)
Dev.: for SO: extraction in an ultrasonic bath and
enrichment through concentration
Organophosphorous flame retardants: TCPP, TCEP,
TDCP after solvent extraction and measurement by
GC-MS
Test object
Site
WA, SO, BIO,
SED, CA
PI
SO
GE
WA
PI
SO
PI
WA, SW, SE, DW, PI
GW, FW
SO, SL, SED
PI
SO, SL, SED
PI
WA, SL
HI
WA, SW, GW,
DW, SO
PI
WA, SW, GW,
BUI
PI
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
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Standard/issue date
Analyte – Title of the standard
In-house method/version Information on sample pre-treatment/testing
technology
DIN 38407-39
Jointly determinable substance groups (group F) –
2011-09
Part 39: Determination of selected polycyclic
aromatic hydrocarbons (PAH) – Method using gas
chromatography with mass spectrometric detection
(GC-MS) (F 39)
LUA NRW leaflet 1
PAH: 16 polycyclic aromatic hydrocarbons according
(A) 1994
to EPA/TVO incl. methylnaphthalene and
benzo[e]pyrene using GC-MSD
Dev: processing of sludge or sediment from freezedried samples
DIN ISO 18287
Soil quality – Determination of polycyclic aromatic
2006-05
hydrocarbons (PAH) – Gas chromatographic method
with mass spectrometric detection (GC-MS)
Dev: different solvent mixture
DIN EN 15527
Characterisation of waste – Determination of
2008-09
polycyclic aromatic hydrocarbons (PAH) in waste
using gas chromatography mass spectrometry (GCMSD)
Dev.: different solvent mixture
E DIN EN 16181
Sludge, treated biowaste and soil – Determination
2010-11
of polycyclic aromatic hydrocarbons (PAH) by gas
chromatography (GC))
ZEK 01.4-08
Harmonised method for the determination of
2011-11
polycyclic aromatic hydrocarbons (PAH) in polymers
DIN EN ISO 6468-F1
1997-02
(A)
DIN 38407-F3
1998-07
EPA 524.2
1995
EPA 8260 B
1996-12
DIN ISO 10382
2003-05
(A)
Test object
Site
WA, DW, SE, EL
PI, GE
SO, SL, SED
PI, GE
SO, SL, SED
PI, GE, HI
WS, SO, SL, FU
PI
WS, BW, SO, SL,
FU, SED
PI
PO
PI
Water quality – Determination of certain
organochlorine insecticides, polychlorinated
biphenyls and chlorobenzenes – Gaschromatographic method after liquid-liquid
extraction
(PCB: 6 polychlorinated biphenyls according to
Balschmitter using GC-MSD: PCB 28, PCB 52, PCB
101, PCB 138, PCB 153, PCB 180)
Dev.: additionally PCB 118, measurement with GCMSD or GC-MS/MS
Gas chromatographic determination of
polychlorinated biphenyls (using GC-MSD or ECD)
WA, SE, SW, GW, PI, HI
DW, EL
WA, DW
PI, HI, GE
Purge + Trap “measurement of purgeable organic
compounds in water by capillary column gas
chromat./mass spectr.”
“Volatile organic compounds by gas chromat./mass
spectr.”
Soil quality – Determination of organochlorine
pesticides and polychlorinated biphenyls using GC
(PCB: polychlorinated biphenyls according to
Balschmitter: PCB 28, PCB 52, PCB 101, PCB 138,
PCB 153, PCB 180, as well as: PCB 118 )
WA
GE
SM
GE
SO, BUI, JS, SL,
SED
PI
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
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Standard/issue date
Analyte – Title of the standard
In-house method/version Information on sample pre-treatment/testing
technology
Dev: processing of sludge or sediment from freezedried samples after Soxhlet extraction and clean-up
with silica gel (in accordance with DIN 38407-F3)
Measurement using GC-MS or MS/MS, additional
matrices
E DIN EN 16167
Sludge, treated biowaste and soil – Determination
2011-01
of polychlorinated biphenyls (PCB) by gas
chromatography-mass spectrometry (GC-MS)
ASU L 00.00-34
Analysis of foods – Modular multi-method for the
2010-09
determination of pesticide residues in foods
(PAH and PCB: 16 polycyclic aromatic hydrocarbons,
according to EPA; 6 polychlorinated biphenyls
according to Balschmitter, in addition: PCB 118;
tetra- to hexachlorobenzenes and organochlorine
pesticides after processing and measurement using
GC-MSD)
Dev.: clean-up in accordance with 64 LFGB L 00.0038/1-4
DIN 38414-S20
Determination of 6 polychlorinated biphenyls (PCB)
1996-01
Dev. PI: sediments are freeze-dried and
(A)
extracted for 8h using Soxhlet, measurement by GCMS
Dev. GE: drying at 105 °C, 3h Soxhlet extraction,
implementation in conjunction with LUA leaflet 6
(1996)
LUA NRW
PCB: 6 polychlorinated biphenyls using GC-MSD or
Leaflet 6
ECD PCB 28, PCB 52, PCB 101, PCB 138, PCB 153,
1996
PCB 180
AltholzV 2002 Appendix
PCB: 6 polychlorinated biphenyls using GC-MSD or
IV no. 1.4.5 in conjunction ECD PCB 28, PCB 52, PCB 101, PCB 138, PCB 153,
with
PCB 180
DIN 38414-S20
1996-01
NIOSH 5503
PAH and PCB: polycyclic aromatic hydrocarbons,
1994-08
according to EPA and 6 polychlorinated biphenyls
NIOSH 5515
according to Balschmitter, after adsorption on PU
foam XAD-2 or Florisil and measurement using GC1994-08
OSHA PV2088
MSD
1988-12
VDI 2464 sheet 1
2009-09
ISO 17858
Water quality – Determination of dioxin-like
2007-02
polychlorinated biphenyls – Method using gas
chromatography/mass spectrometry
in line with DEV-F33
(Determination of WHO-PCB: PCB 77, PCB 81, PCB 105,
(Blueprint) 52nd delivery PCB 114, PCB 118, PCB 123, PCB 126, PCB 156, PCB
157, PCB 167, PCB 169, PCB 189) using GC-MSD
2002
Dev.: additional matrices (solids) after Soxhlet
Test object
Site
WS, BW, SO, SL,
FU, SED
PI
BIO
PI
SO, SS, SED
PI, HI, GE
SO
GE
WO, SO, SL, WS
PI, HI, GE
GA
PI
WA, SW, SE, DW, PI
GW, FW,
SO, SL, SED
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
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Standard/issue date
Analyte – Title of the standard
In-house method/version Information on sample pre-treatment/testing
technology
in line with AbfKlärV 1992 extraction in accordance with DIN 38414-24 (200010)
in line with VDI 3499
sheet 1
2003-07
DIN EN 12766-1
Determination of PCBs and related products – Part
2000-11
1: Separation and determination of selected PCB
congeners by gas chromatography (GC) using an
electron capture detector (ECD)
Dev.: measurement using GC-MS
DIN EN 12766-2
Determination of PCBs and related products – Part
2001-12
2: Calculation of polychlorinated biphenyl (PCB)
content; dev.: measurement using GC-MS
DIN EN 15308
Characterisation of waste – Determination of
2008-05
selected polychlorinated biphenyls (PCB) in solid
waste by using capillary gas chromatography with
electron capture or mass spectrometric detection
VDI 2464 sheet 1
Measurement of emissions – Indoor air
2009-09
measurement – Measurement of polychlorinated
biphynyls (PCBs) – GC/MS method for PCB 28, 52,
101,138, 153, 180; adsorption PU foam
Determination of polychlorinated dibenzodioxins
DEV-F33 (Blueprint)
(PCDD) and polychlorinated dibenzofuranes (PCDF)
52nd delivery 2002
PCDD/F: 17 polychlorinated dibenzodioxins and
dibenzofurans using GC-MSD
DIN 38414-S24
Determination of polychlorinated dibenzodioxins
2000-10
(PCDD) and polychlorinated dibenzofurans (PCDF)
(S 24)
VDI 3499 sheet 1
Emission measurement – Determination of
2003-07
polychlorinated dibenzo-p-dioxins (PCDDs) and
dibenzofurans (PCDFs)
Dev.: determination in other matrices (filter dust,
boiler ash, slag) using GC-MS
DIN EN 12766-3
Petroleum products and used oils – Determination
2005-02
of PCBs and related products – Part 3:
Determination and quantification of the content of
polychlorinated terphenyls (PCT) and
polychlorinated benzyl toluenes (PCBT) by gas
chromatography (GC) using an electron capture
detector (ECD)
Dev.: measurement using GC-MS, liquid/liquid
extraction with water samples, additional matrices
(solids): ultrasonic extraction
ISO 8165-2
Determination of selected phenols – Part 2: Method
1999-07
by derivatisation and gas chromatography
Dev.: analysis using GC-MSD
DIN 38407-F14
Determination of phenoxyalkyl carbonic acids by
1994-10
gas chromatography and mass-spectrometric
(A)
detection after solid-liquid-extraction and
Test object
Site
OIL
PI
OIL
PI
WS
PI, GE
GA
GE
WA
PI
SL, SED
PI
DU, SM
PI
SO, WO, WA, OIL PI
WA, SW, SE, DW, PI
GW, FW
WA, SW, SE, DW, PI
GW, FW
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
11/89
Appendix to the accreditation certificate D-PL-14170-01-00
Standard/issue date
Analyte – Title of the standard
In-house method/version Information on sample pre-treatment/testing
technology
derivatisation
Test object
Site
DIN EN ISO 15913 (F20)
2003-05
WA, SO, DW
PI
WA
PI
SO, SL, SED, WS,
COM
PI
GA
GE
SO, SED, SL
PI
WA, DW
PI, HI, GE
WA, SO
PI
WA, DW, SO, GA
HI
DIN EN ISO 18856 (F 26)
2005-11
E DIN 19742
2012-04
In-house method
GE-MA-M U 3-4
2009-08
In-house method
PI-MA-M 3-6
2010-09
DIN 38407-F2
1993-02
(A)
Supplementary
instruction f. calibr. and
quantity. in analysis of
hydrocarbons in SPIMFAB
samples
DIN 38413-P2
1988-05
DIN EN ISO 17353 (F 13)
2005-11
Water quality – Determination of selected
phenoxyalkanoic herbicides, including bentazones
and hydroxybenzonitriles as well as clopyralid and
Quinmerac by gas chromatography and mass
spectrometric detection after solid-liquid extraction
and derivatisation
GBA: pesticides in accordance with Swedish EPA,
method 1, acidic work-up
Dev. for soil: extraction in an ultrasonic bath and
enrichment through concentration
Replaces DIN 38407-20, 2000-09
Water quality – Determination of selected
phthalates using gas chromatography / mass
spectrometry
Dev.: liquid-liquid extraction
Soil quality – Determination of selected phthalates
in sludge, sediment, solid waste and soil after
extraction and determination using gas
chromatography mass spectrometry (GC-MS)
Dev.: additional analytes:
Dimethyl, diethyl-, dipropyl-, diisobutyl-, dipentyl-,
butyl benzyl, dicyclohexyl-, dioctyl-, diisononyl-,
diisodecyl phthalate
Dev.: additional matrix: Commodity
Oxygen, nitrogen, carbon monoxide, carbon dioxide
and methane in soil gas, landfill gas and gases using
GC-FID and TCD
Screening (GC-MS), qualitative and semiquantitative orientation analysis after extraction of
solids with n-hexane, acetone or n-hexane/acetone
(50:50, v:v)
Gas chromatographic determination of low volatile
halogenated hydrocarbons
GBA HI: only chlorobenzenes: tri- to
hexachlorobenzene
GBA GE: in combination with DIN 51527 T1 (PCB
only)
SPIMFAB after liquid extraction using GC-MSD
Determination of vinyl chloride (chloroethene) by
headspace gas chromatography
Water quality – Determination of selected
organotin compounds – Gas chromatographic
WA, SW, SE, DW, PI
GW, FW
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
12/89
Appendix to the accreditation certificate D-PL-14170-01-00
Standard/issue date
Analyte – Title of the standard
In-house method/version Information on sample pre-treatment/testing
technology
method
Test object
Site
DIN EN ISO 23161
2011-10
Soil quality – Determination of selected organotin
compounds – Gas-chromatographic method (GCFPD)
SO, SL, SED
PI
in conjunction with E DIN
19744
2003-08
§ 35 LMBG
§ 64 LFGB
L 10.00-9
2002-12
Identification and quantification of organotin
compounds in solids (soils, sediments, waste):
withdrawn 2007-12
Analysis of foods – Gas chromatographic
determination of organotin compounds in fish and
mussels
(Determination of mono-, di-, tri- and tetrabutyltin,
mono- and diooctyltin, tricyclohexyltin, mono-, diand triphenyltin using GC-FPD in biota)
Organotin compounds using GC-FPD in passive
collectors and adsorber materials
BIO
PI
In-house method
PI-MA-M 3-93
2012-06
In-house method
HI-MA-M U-03-24
2012-01
PASSIVE ADSORB PI
Determination of furan, thiophene, 3WA EL
methylthiophene and 2,5-dimethylthiophene
(heterocyclic compounds) in water using headspace
gas chromatography
HI
Testing type: HPLC (HPLC-DAD, HPLC-UV, HPLC-FLD, LC-MS/MS)
Standard/issue date
Analyte – Title of the standard
In-house method/version Information on sample pre-treatment/testing
technology
In-house method
Acrylamide using LC-MS/MS
HM-MA-M U 02-01
2012-01
In-house method
Determination of aldehydes in water and eluates
HI-MA-M U-02-42
2011-01
In-house method
Determination of aldehydes in solids (incl.
HI-MA-M U-02-43
formaldehyde)
2011-01
In-house method
Pharmaceutical substances using LC-MS/MS
HM-MA-M U2-25
2011-01
In-house method
HM-MA-M U-02-30
2011-06
In-house method
HM-MA-M U-02-27
2011-06
In-house method
HM-MA-M U-02-28 2011-
Test object
DW
HM
WA, EL
HI
SO
HI
GW, SW, DW,
SO, SED
HM
Determination of selected LAS in detergents (solid
and liquid)
DE, CA
Determination of selected LAS in water
WA, SW, DW,
GW
Determination of selected LAS in solids
Site
HM
SO, SS, SL
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
HM
HM
13/89
Appendix to the accreditation certificate D-PL-14170-01-00
Standard/issue date
Analyte – Title of the standard
In-house method/version Information on sample pre-treatment/testing
technology
06
DIN EN ISO 22478-F21
Determination of certain explosives and related
2006-07
compounds using HPLC-DAD
DIN ISO 11916-1
Soil quality – Determination of selected explosives–
2011-03
Part 1: Method using high-performance liquid
chromatography (HPLC) with UV detection
Dev. Measurement using LC-MS/MS
ISO 21458
Glyphosate, glufosinate, AMPA and amitrole after
2008-12
derivatisation with FMOC and measurement
In-house method
Dev. using LC-MS/MS
HM-MA-M 2-5
2009-08
In-house methods
Determination of selected heterocyclic compounds
HM-MA-M-U-02-26
in water using LC-MS/MS
2012
In-house method
Oestrogens using LC-MS/MS
HM-MA-M 2-2
2011-01
LUA NRW leaflet 1 1994
Determination of polynuclear aromatic
DIN ISO 13877
hydrocarbons using HPLC-UV/DAD/FLD
2000-01
DIN EN ISO 17993
2004-03
DIN EN ISO 11369 (F 12)
1997-11
In-house method
HM-MA-M U-02-35
2011-12
DIN 38407-35 (F 35)
2010-10
DIN 38407-F 42
2011-03
DIN 38414-S 14
2011-08
Determination of 15 polycyclic aromatic
hydrocarbons (PAH) in water by HPLC with
fluorescence detection after liquid-liquid extraction
(replaces: DIN 38407-F18 1999-05)
Determination of selected plant treatment agents –
Method using high performance liquid
chromatography with UV detection after solid-liquid
extraction
Dev. HM: LC-MS/MS in conjunction with HM-MA-M
U 2-4
Determination of PSM in solids using LC-MS/MS
Determination of selected phenoxyalkyl carbonic
acids and further acid plant treatment agents –
Method using high performance liquid
chromatography and mass spectrometric detection
(HPLC-MS/MS)
Determination of selected polyfluorinated
compounds (PFC) in water – Method using high
performance liquid chromatography and mass
spectrometric detection (HPLC-MS/MS) after solidliquid extraction
Determination of selected polyfluorinated
compounds (PFC) in sludge, compost and soil –
Method using high performance liquid
Test object
Site
WA, EL, SO
HM
SO
HM
WA, SW, DW,
GW
HM
WA
HM
GW, SW, DW
HM
SO, WS, AS, MIR
HI
WA, SE, SW, GW, HI
DW
WA, SW, GW, SO HM
SO, SED
HM
WA, SW, DW,
GW
HM
WA, SW, DW,
GW
HM
SL, SED
SS, SO
HM
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Standard/issue date
Analyte – Title of the standard
In-house method/version Information on sample pre-treatment/testing
technology
chromatography and mass spectrometric detection
(HPLC-MS/MS)
Test object
Site
In-house method
HM-MA-M 2-3
2009-11
WA, GW, SW,
DW
HM
Test object
Site
WA, SE, GW,
DW, AC
SE, EL, AC
PI, HE, FG
X-ray contrast medium using LC-MS/MS
Individual testing methods of electrochemistry
Standard/issue date
Analyte – Title of the standard
In-house method/version Information on sample pre-treatment/testing
technology
DIN 38405- D4-1
Determination of fluoride
1985-07 (A)
GBA: also in acids
DIN 38405- D4-2
Determination of total inorganic bound fluoride
1985-07 (A)
after digestion and distillation; GBA: also in eluates
VGB-M 701 serial no. 02
Fluoride from soda extract using ion-selective
and 8.8.1
electrode
2008-12
DIN EN 25814-G22
Determination of dissolved oxygen; electrochemical
1992-11 (A)
method (also on-site)
DIN 38408-G 23
Oxygen saturation index
1987-11
(withdrawn standard)
DIN EN 60814
Determination of water by automatic Karl Fischer
1999-03
titration (IEC 60814:1997);
FG
GY, CC, DU
PI
WA, SW, GW,
PI, GE,
DW
HM, FG
WA, SW, SE, DW, PI, FG
GW, FW
SM, IO, OIL
HE
Testing type: Gravimetry
Standard/issue date
Analyte – Title of the standard
In-house method/version Information on sample pre-treatment/testing
technology
DIN 52183
Moisture content and dry residue (withdrawn
1977-11
standard)
VGB-M 701 serial no. 1
Moisture content at 40 °C.
2008-12
DIN 38414-S 22
Determination of dry residue by freezing and
2000-09
preparation of the freeze dried mass of sludge
Dev.: also from biota samples
DIN EN ISO 16720
Soil quality – Pre-treatment of samples by freeze2007-06
drying for subsequent analysis
DIN EN 15169
2007-05
DIN 19684-3
2000-08
Test object
Site
WO
GY
PI, HI, GE,
HM, FG
PI
SL, SED, BIO
PI
SO
PI
Characterisation of waste – Determination of loss
WS, SL, SED
on ignition in waste, sludge and sediments
Methods of soil investigations for agricultural water SO
engineering – Chemical laboratory tests – Part 3:
Determination of the loss on ignition and the
residue of soil after ignition
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
PI, GE
PI, GE, FG
15/89
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Standard/issue date
Analyte – Title of the standard
In-house method/version Information on sample pre-treatment/testing
technology
DIN 18128
Soil – Investigation of soil samples – Determination
2002-12
of ignition loss
DIN EN 12879 (S 3a)
Characterisation of sludges – Determination of the
2001-02
loss on ignition of dry mass
PI-MA-M 4-41
Silicon dioxide, aqua regia insoluble
2011-05
VGB M701 serial no. 7
Sieve residue at 32 µm
2008-12
DIN 38409-H1
Determination of total dry residue, filtrate dry
1987-01
residue and residue on ignition
(A)
DIN ISO 11465
Soil quality – Determination of dry matter and
1996-12
water content on a mass basis – Gravimetric
(A)
method
DIN EN 14346
Characterisation of waste – Calculation of dry
2007-09
matter by determination of dry residue or water
content
DIN 38414-S2 and S3
Dry residue and loss on ignition
1985-11
(withdrawn standard)
DIN EN 12880-S2a
Characterisation of sludges – Determination of dry
2001-02
residue and water content
DIN ISO 11272
Soil quality – Determination of dry bulk density
2001-01
DIN 18125-2
Soil – Investigation of soil samples – Determination
2011-03
of density of soil – Part 2: Field tests
(withdrawn standard)
DIN 38414-S4
Determination of leachability by water (steam
1984-10
method)
DIN 38409-H1
Determination of total dry residue, filtrate dry
1987-01
residue and residue on ignition (H 1)
Bundesgütegemeinschaft Plant compatibility in the seed planting experiment
Kompost e.V.
with spring barley
Methodenbuch zur
Analyse (Federal Compost
Association methods
book for the analysis of
compost), Chapter IV A3
2006-09
Test object
Site
SO
PI
SS, SL
PI, HI, GE
DU, CC, GY
GY
PI
PI
WA, SW, SE, DW, PI, HI, GE,
GW, FW
FG
SO, BW, WS
PI, HI, GE,
FG
WS
PI, GE
SO, SL
SO
PI, HI, GE,
FG
PI, HI, GE,
FG
PI, GE
SO
GE
SO
SO, WS
PI, HI, GE,
FG
PI, HI, GE
SO
GE
SO, SL, SS
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
16/89
Appendix to the accreditation certificate D-PL-14170-01-00
Testing type: Measurement analysis
Standard/issue date
Analyte – Title of the standard
In-house method/version Information on sample pre-treatment/testing
technology
DIN 38406-E 5-2
Determination of ammonia-nitrogen (E 5)
1983-10
in
Dev.: also from soil
conjunction with AbfKlärV
1992 BGBl. S. 912, App. 1
AbfKlärV 1992 BGBl. I S.
Basic active substances
912, App. 1 in conjunction
with Federal Compost
Association methods
book for the analysis of
compost, Chapter III, B
2.1
2006/09
DIN 4030-2
Assessment of water, soils and gases for their
2008-6
aggressiveness to concrete – Part 2: Sampling and
analysis of water and soil samples: Smell, pH,
potassium-permanganate consumption,
Hardness (dev. using ICP-OES),
Magnesium (dev. using ICP-OES),
Ammonium (dev. using CFA),
Sulphate and chloride (dev. using IC), lime solubility
as Heyer marble test, sulphide
DIN 4030-2
Assessment of water, soils and gases for their
2008-6
aggressiveness to concrete – Part 2: Sampling and
analysis of water and soil samples: Acidity according
to Baumann-Gully, sulphate and chloride
(Dev. after aqueous elution using IC), sulphide
DIN EN 206-1
Concrete – part 1: Specification, performance,
2001-07
production and conformity
2004-10 (A1)
2005-09 (A2)
2012-03 (draft)
VGB-M 701 serial no. 2.4 Calcium as calcium oxide, complexometric
2008-12
Federal Compost
Carbonate according to Scheibler
Association methods
book for the analysis of
compost, Chapter III, B
2.2 2006-09
VDLUFA book of methods Carbonate according to Scheibler
on soil analysis Vol. I, A
5.3.1 1991
DIN 19684-5
Carbonate content
1977-02
(withdrawn standard)
Test object
Site
WA, SW, SE, GW, PI
FW, SO
SO, SED, SS, BW
PI
WA, SW, SE, GW, PI
FW
SO
PI
WA, SO
PI
GY
PI
SO, SED
PI, GE
SO, SED
PI, GE
SO
PI
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Standard/issue date
Analyte – Title of the standard
In-house method/version Information on sample pre-treatment/testing
technology
LAGA CN/ 2 79
Determination of total cyanide
1983-12
(withdrawn directive)
in conjunction with ISO
11262
2003-09 and 2012-04
TL Streu 2003 edition
Ferrocyanide (anti-caking agent)
DIN 38409-H 6
1986-01
DIN 38405-D 8
1971-1975
DIN EN ISO 8467 (H5)
1995-05
DIN 38409-H7
2005-12
DIN CEN/TS 15364
2006-07
PI-MA-M 8-38
2011-04
DEV H 12
DIN ISO 11261
1997-05
VDLUFA book of methods
on soil analysis Vol. 1
1991
DIN 38409-H28
1992-04
Swedish standard SS 02
81 01
Test object
Site
SO, WS
PI
DS
HI
Water hardness (H 6)
Dev.: measurement of Ca and Mg using ICP
Carbon dioxide chemistry: Calculation of dissolved
carbon dioxide (free carbon dioxide), carbonate and
bicarbonate ion
(withdrawn standard)
Water quality – Determination of permanganate
index
Determination of acid and base-neutralizing
capacities (H 7)
WA, DW
PI
WA
PI, GE
WA, DW
PI
WA, SW, GW
PI, HI, GE,
FG
Leaching behaviour test – Acid and base
neutralisation capacity test
Acidity (HCl) by titration using sodium hydroxide
WS
FG
AC
PI
Nitrogen (total), calculation
Soil quality – Determination of total nitrogen –
Modified Kjeldahl method
Dev.: also from biota samples
WA, DW
GE
SO, BW, SED, BIO PI
Nitrogen (bound); Method after reduction with
Devarda's alloy and catalytic digestion
Dev.: also from soil, sediment
(withdrawn standard)
WA, SE, SO, SED
DIN EN 25663 (H11)
1993-11
Water quality – determination of Kjeldahl nitrogen;
method after mineralisation with selenium
WA, SW, SE, DW, PI
GW, FW
VGB-M 701 serial no. 8.9
2008-12
DIN EN 13342
2001-01
TL Streu 2003 edition
Sulphur dioxide (SO2) as calcium sulphite
hemihydrate, titrimetically with iodine
Characterisation of sludges – Determination of
Kjeldahl nitrogen
Thawing substance
GY
DEV-D15
Thiosulphate
(withdrawn DEV-regulation)
Estimation of the permanganate consumption
(SOD) in soil according to ASTM D 7262-10
ASTM D 7262-10
2010-07
SL SS
DS
PI
PI
PI
HI
WA, SW, SE, DW, PI
GW, FW
SO
HI
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Appendix to the accreditation certificate D-PL-14170-01-00
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
19/89
Appendix to the accreditation certificate D-PL-14170-01-00
Testing type: Photometry
Standard/issue date
Analyte – Title of the standard
In-house method/version Information on sample pre-treatment/testing
technology
DIN 38404-C3
Determination of absorption in the range of the UV
2005-07
radiation, Spectral absorptions coefficient
DIN 38406-E5
Determination of ammonia-nitrogen
1983-10
(A)
DIN EN ISO 11732 (E 23)
Water quality – Determination of ammonium
2005-05
nitrogen – Method by flow analysis (CFA) and
(A)
spectrometric detection
DIN EN ISO 7393-2 (G4)
Water quality – Determination of free chlorine and
2000-04
total chlorine – Part 2: Colorimetric method using
N,N-diethyl-1,4-phenylenediamine, for routine
control purposes
Deviation: also in acids
DIN 38405-D 24
Photometric determination of chromium(VI) using
1987-05 (A)
1,5-diphenylcarbonohydrazide (D 24)
DIN EN ISO 18412 (D 40) Water quality – Determination of chromium(VI) –
2007-02
Photometric method for weakly contaminated
water
DIN EN 15192
Characterisation of waste and soil – Determination
2007-02
of Chromium(VI) in solid material by alkaline
digestion and ion chromatography with
spectrophotometric detection
DIN ISO 17380
Soil quality – Determination of total cyanide and
2006-05
easily liberatable cyanide – Continuous-flow
E DIN EN ISO 17380
analysis method
2011-10
DIN EN ISO 14403 (D6)
Cyanide (total and easily liberatable) using
2009-11
continuous flow analysis (CFA)
DIN EN ISO 14403-2
Replaces DIN EN ISO 14403, 2002-07
2012-10
DIN 38405-D 13
Determination of cyanides
1981-02 (A)
Replaces DIN 38405-D13: 1981-02
2011-04
Replaces DIN 38405-D14: 1988-12
DIN 38405-D 14
Determination of cyanides in drinking water, weakly
1988-12
contaminated groundwater and surface water:
Cyanide (total and easily liberatable) after
separation process
(withdrawn standard)
LAGA guideline. CN 1/75 Cyanide, total and easily liberatable
1975
(withdrawn directive)
DIN 38406-E1
Determination of iron
1983-05
DIN EN ISO 7887 (C 1)
Water quality – Examination and determination of
1994-12 (A)
colour
Test object
Site
WA, SW, SE, DW, PI
GW, FW
WA, SW, SE, DW, PI
GW, FW
WA, SW, GW, EL, PI, GE
DW
WA, AC
PI
WA, DW
PI, GE
DW GW SW
PI
SO
PI
SO
PI
WA, SW, GW, EL
PI
WA, SW, GW, SE, PI
DW
WA, DW, GW,
SW
PI
WS
PI
WA, DW
PI
WA, SW, GW
PI, HI, GE
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Standard/issue date
Analyte – Title of the standard
In-house method/version Information on sample pre-treatment/testing
technology
DIN 38413-P 1
Determination of hydrazine
1982-03
In-house method
Iodine, iodide
PI-MA-M 6-70
2012-06
DIN 38405-D 9-2
Photometric determination of nitrate
1979-05 (A)
And 2011-09
DIN EN ISO 13395 (D 28) Water quality – Determination of nitrite nitrogen
1996-12
and nitrate nitrogen and the sum of both by flow
(A)
analysis (CFA and FIA) and spectrometric detection
DIN EN 26777 (D 10)
Water quality – Determination of nitrite;
1993-04 (A)
spectrometric method
EN ISO 14402 (H 37)
Water quality – Determination of phenol index by
1999-12 (A)
flow analysis (FIA and CFA)
DIN 38409-H 16-2
Determination of phenol index after distillation and
1984-06
colouring extraction using 4-Aminoantipyrine
Dev.: soil/waste samples after suspension in
phenol-free water quantification by CFA
DIN EN ISO 6878 (D 11)
Water quality – Determination of phosphorus –
2004-09
Ammonium molybdate spectrometric method
DIN EN ISO 15681-2 (D46) Water quality – Determination of orthophosphate
2005-05
and total phosphorus contents by flow analysis (FIA
and CFA) – Part 2: Method by continuous flow
analysis (CFA)
DIN EN ISO 11905-1 (H36) Water quality – Determination of nitrogen – Part 1:
1998-08
Determination of nitrogen using oxidative digestion
with peroxodisulfate
DIN 38405-D 26
Photometric determination of dissolved sulphide
1989-04 (A)
DIN 38405-D 27
Determination of easily liberated sulphide
1992-07
VGB M701 serial no. 5
Degree of whiteness
2008-12
Federal Compost
Association methods
book for the analysis of
compost, Chapter IV A5
2006-09
Stability of the nitrogen cycle of organic materials
Dev: measurement of ammonium with CFA and
measurement of nitrate with IC
Test object
Site
WA, SW, SE, DW, PI
GW, FW
AC
PI
WA, DW
PI
WA, SW, GW, SE, PI
EL, DW
WA, SW, GW, SE, PI
DW
WA, SE, SW, GW, PI
EL
WA, SO, DU
PI
WA, SE, SW, GW, PI
SS
WA, SW, SE, DW, PI
GW, FW
WA, SE, SW
PI
WA, SW, SE, DW, PI, GE
GW, FW
WA, SE, SW
PI, GE
GY
PI
SO
GE
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Testing type: Physical and physicochemical characteristics
Standard/issue date
In-house
method/version
DIN EN ISO 9963-1 C23
1996-02
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Water quality – Determination of alkalinity – Part 1:
Determination of total and composite alkalinity
Test object
DIN 38404-C 10
1995-04
Calculation of the calcite saturation of water
WA, SW, SE, DW, PI, GE,
GW, FW
HM
DEV C 9
Determination of density
Deviation: also from dust, mixed salts, waste
Soil – Investigation of soil samples – Uniaxial
compression test
(withdrawn standard)
WA, DU, CC, WS
PI
SO, WS
GE
Water quality – Examination and determination of
colour
(withdrawn standard from 1994)
Vane testing – Dimensions of apparatus, mode of
operation, evaluation
(withdrawn standard)
Soil quality – Determination of the specific electrical
conductivity
WA, DW
PI, GE
SO, WS
GE
SO
PI, HI, GE,
FG
Water quality – Determination of electrical
conductivity
(also on site)
Soil quality – Determination of pH-value (C 5) (also on
site)
(withdrawn standard)
Soil quality – Determination of pH-value (H2O, CaCl2,
KCl)
(withdrawn standard)
WA, SW, GW, EL, PI, HI, GE,
DW
HM, FG
SO, BW, WS
PI, HI, GE,
FG
DIN EN 12176 (S 5)
1998-06
in conjunction with
AbfKlärV 1992 Appendix
1.3.1
VGB-M 701 serial no. 4
2008-12
DIN 38404-C6
1984-05
Characterisation of sludge – Determination of pHvalue (H2O)
Replaces DIN 38414- S5 1981-09
SS, SL
PI, HI, GE,
FG
pH-value
GY
PI
Determination of redox potential
WA, GW
PI, HI, GE,
HM, FG
BioAbfV 1998 Appendix
3
Salt content, calculation as potassium chloride after
measurement of conductivity
BW
PI, HI, GE
DIN 38404-C 4
1976-12
Determination of temperature (C 4)
(also on site)
WA, SW, GW,
DW
PI, HI, GE,
HM, FG
DIN 18136
1996-08
DIN EN ISO 7887-C1
1994-12 (A)
2012-04
DIN 4096
1980-05
DIN ISO 11265
1997-06 (A)
DIN EN 27888-C 8
1993-11 (A)
DIN 38404-C 5
2009-07
DIN ISO 10390
1997-05 (A)
Site
WA, SW, SE, DW, PI
GW, FW
WA, SW, GW, EL, PI, HI, GE,
DW
HM, FG
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
22/89
Appendix to the accreditation certificate D-PL-14170-01-00
Standard/issue date
In-house
method/version
DIN EN ISO 7027 (C 2)
2000-04 (A)
In-house method
GE-MA-M 11-6
2008-01
with DIN 53019 Part
1(2008-09) + Part 2
(2001-02)
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Water quality – Determination of turbidity (also on
site)
Determination of dynamic viscosity using rotation
viscometer
Test object
Site
WA, DW
PI, HI
OIL solutions,
viscous liquids
HE
Test object
Site
WA, SE, SW
PI, HI, GE,
FG
PI, HI, GE
Testing type: Sum parameters
Standard/issue date
In-house
method/version
DIN 38409-H2-2/3
1987-03
DIN EN 15216
2008-01
DIN EN 872 (H 33)
1996-03
DIN 38409-H9-2
1980-07
DIN 38414-S18
1989-11
DIN EN 1485 (H 14)
1996-11
DIN EN ISO 9562 (H 14)
2005-02
DIN 38409-22 (H 22)
2001-02
DIN EN 1899 (H 51)
1998-05
DIN 38409-H 41
1980-12 (A)
DIN ISO 15705 (H 45)
2003-01
DIN 38409-H8
1984-09
DIN 38414-S 17
1989-11 (A)
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Determination of filterable matter and the residue on
ignition (H 2)
Determination of total dissolved solids (TDS) in water
and eluates
Determination of suspended solids – Method by
filtration through glass fibre filters (withdrawn
standard)
Determination of the settleable matter by volume in
water and waste water (H 9); Volume GE, HM, FG
with a sample volume of 2 l
Determination of adsorbed organically bound
halogens (AOX)
AOX: adsorbable organically bound halogens,
method: batch test and column method (withdrawn
standard)
Water quality – Determination of adsorbable
organically bound halogens (AOX)
Replaces method H14: 1996-11 and 2003-07
Determination of dissolved adsorbable organically
bound halogens in salt-loaded water after solid-phase
extraction (SPE-AOX) (H 22)
Determination of biochemical oxygen demand after n
days (BSBn) – Part 1: Dilution and seeding method
with allylthiourea acid addition
Determination of the chemical oxygen demand
(COD), in the range above 15 mg/l
Water quality – Determination of the COD: chemical
oxygen demand index (ST-COD), cuvette test
Determination of extractable organically bound
halogens; PI: also from acids
Dev.: combustion in oxygen flow
(withdrawn standard)
Determination of strippable and extractable
organically bound halogens (S 17)
WA, EL
WA, SW, SE, DW, PI, HI
GW, FW
WA, SW, SE, DW, PI, HI, GE,
GW, FW
HM, FG
SS, SL
GE
WA, SE, SW, GW, GE
EL
WA, SE, SW, GW, PI, GE
EL
WA, SE, SW, GW
GE
WA, SE
PI, GE
WA, SE
PI
WA, SE, SW
PI, HI, GE
WA, AC
PI, GE
SO, SL
PI, GE
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
23/89
Appendix to the accreditation certificate D-PL-14170-01-00
Standard/issue date
In-house
method/version
2012-02 (draft)
DEV H 22
DIN 19684-2
1977-02
DIN EN 14582
2007-06
DIN 38409-H 56
2009-06
LAGA KW/04 Point 6.8
2004-11
AbfAblVO Appendix 4
no. 2.3
DIN 38409-H 16-3
1984-06
DIN EN 38409 (H 23)
1980-05
VGB-B 401, sheet
4.4.2.1
DIN EN 12260 (H 34)
2003-12
In-house method
PI-MA-M 7-31
2012-05
DIN EN 872 (H 33) 200504
DIN EN 1484 (H 3)
1997-08 (A)
DIN EN 13137
2001-12
DIN ISO 10694
1996-08
Federal Compost
Association methods
book for the analysis of
compost, Chapter IV B1
2006-09
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Deviation for GE: only extractable organically bound
halogens
Decaying ability
(withdrawn standard)
Humus content
(withdrawn standard)
Characterisation of waste – Halogen and sulphur
content – Oxygen combustion in closed systems and
determination methods
Gravimetric determination of low volatile lipophilic
substances after solvent extraction (H 56)
Dev. for soil, waste: solid-liquid extraction, in PI also
with various solvents
Lipophilic substances, total extractable
Test object
Site
WA
PI, GE
SO
GE
WS
HE
WA, SE, SO, WS
PI, HI, GE
WS, SO, CS
PI, HI, GE
Lipophilic substances, total extractable
WS
PI, HI, GE
Determination of phenol index
WA, SW, SE, DW, PI
GW, FW
WA
GE
Determination of methylene blue and bismut active
substances (H 23)
(withdrawn standard)
Residual carbon content
SO, WS
GE
Water quality – Determination of nitrogen –
Determination of bound nitrogen (TNb) following
oxidation to nitrogen oxides
Oxygen consumption in sediments according to
requirements of the BfG
WA, SE, SW
GE
SED
PI
Water quality – Determination of suspended solids–
Method by filtration through glass fibre filters
Water analysis – Guidelines for the determination of
total organic carbon (TOC) and dissolved organic
carbon (DOC)
Characterisation of waste – Determination of total
organic carbon (TOC) in waste, sludges and sediments
Soil quality – Determination of organic and total
carbon after dry combustion (elementary analysis)
Content of germinable seeds and plant parts capable
of budding
WA, SW, SE, DW, PI, HI
GW, FW
WA, SE, SW, GW, PI, GE
EL, DW
WS, SL, SED
PI, GE
SO
PI, GE
BW
GE
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
24/89
Appendix to the accreditation certificate D-PL-14170-01-00
Individual testing methods of aquatic toxicity tests
Standard/issue date
In-house
method/version
Dep V 2009 Appendix 4
no. 3.3.1
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Breathability over 4 days (AT 4)
DIN EN ISO 9888 (L 25)
1999-11
Water quality – Determination of aerobic
WA, SE
biodegradability of organic substances in aqueous
medium – Static test (Zahn-Wellens method)
Determination of the tolerance of Daphnia to the
WA, SE
toxicity of waste water by way of a dilution series (L
30)
Gas formation rates in fermentation test over 21 days WS
(GB 21)
DIN 38412-L 30
1989-03
Dep V 2001 Appendix 4
no. 3.3.2 in conjunction
with
DIN 38414-S 8
1985-06
DIN EN ISO 11348-2
2009-05
Test object
Site
WS
GE
Water quality – Determination of the inhibitory effect WA
of water samples on the light emission of Vibrio
fischeri, Part 2: Method using liquid-dried bacteria
GE
GE
GE
GE
Individual testing methods of non-specific cultivation techniques
Standard/issue date
In-house
method/version
DIN EN ISO 6222 (K5)
1999-07
TrinkwV 2001, Annex 5
Part 1 d) bb)
2011-11
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Quantitative determination of culturable microorganisms – Determination of colony count by
inoculation in a nutrient agar culture medium
Quantitative determination of culturable microorganisms – Determination of colony count by
inoculation in a nutrient agar culture medium
(Colony count at 22 °C and 36°C)
Test object
Site
DW, SW, GW
HH, HM
DW, SPW
HH, WOB
Testing type: Specific cultivation method
Standard/issue date
In-house
method/version
TrinkwV 2001, Annex 5
Part 1 e)
2011-11
Colilert® -18 / Quanti®
Tray
UBA (German Federal
Environment Agency)
communication,
Bundesgesundheitsblatt
49, 2006, p. 1071 ff
Analyte – Title of the standard
Test object
Information on sample pre-treatment/testing
technology
Detection of Clostridium perfringens using membrane DW
filtration (mCP-agar at 44 +/-1°C over 21 +/-3 hours)
Site
Detection of Escherichia coli and coliform bacteria
using finished reagents
HH, HM
DW, SPW
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
HH, WOB
25/89
Appendix to the accreditation certificate D-PL-14170-01-00
Standard/issue date
In-house
method/version
DIN EN ISO 9308-1
(K 12)
2001-07
DIN EN ISO 7899-2
(K 15)
2000-11
DIN EN ISO 11731-2
(K 22)
2008-06
UBA recommendation
23.08.2012
DIN EN ISO 11731-2
2008-06
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Water quality – Detection and enumeration of
Escherichia coli and coliform bacteria;
Part 1: Membrane filtration method
Water quality – Detection and enumeration of
intestinal enterococci;
Part 2: Membrane filtration method
Detection of Legionella in drinking water and bathing
water
Water quality – Detection and enumeration of
Legionella –
Part 2: Direct membrane filtration method with low
bacterial count
DIN EN ISO 16266 (K 11) Water quality – Detection and enumeration of
2008-05
Pseudomonas aeruginosa – Method by membrane
filtration
Test object
Site
DW, SPW, GW
HH, WOB
DW, SW, GW
HH, WOB
DW, SPW
HH, WOB
DW, SPW
HH, WOB
DW, SPW
HH, WOB
Testing type: Sampling of water and other applicable documentation for sampling
Standard/issue date
In-house
method/version
DIN 38402-A11
2009-02
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Sampling of waste water
Replaces DIN 38402-A11 1995-12
DIN 38402-A13
1985-12 (A)
Sampling from aquifers
Test object
Site
SE, LE
PI, GE, HI,
HM
GW
PI, GE,
HM, HI,
FG
PI, HI, GE,
HM, FG,
WOB
PI, GE,
HM, FG,
HI
PI, HI, GE,
HM, FG
PI, HI, GE,
HM, FG
DIN EN ISO 19458 (K 19) Sampling for microbiological analysis
2006-12
WA
DIN 38402-A12
1985-06 (A)
Sampling from stagnant bodies of water
SW, DW
DIN 38402-A14
1986-03
DIN ISO 5667-5
2011-02
Sampling of drinking water and untreated water
WA, DW
(withdrawn standard)
Water quality – sampling – part 5: Guidance on
WA, DW
sampling of drinking water from treatment works and
piped distribution systems
Sampling from flowing waters
FW, DW
DIN 38402-A15
1986-07 (A)
DIN EN ISO 5667-13
(S 1)
2011-08
Water quality – Sampling – Part 13: Guidance on
sampling of sludges
(withdrawn standard)
Replaces DIN 38414-S1 1986-11
SL, SS
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
PI, GE,
HM, FG,
HI
PI, GE, HI
26/89
Appendix to the accreditation certificate D-PL-14170-01-00
Standard/issue date
In-house
method/version
DIN 38414-S 11
1987-08
DIN 38402-A 18
1991-05
DIN ISO 10381-2
2003-08
DIN EN ISO 22475-1
DIN 4021
1990-10
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Sampling of sediments using soil core sampler, box
gripper, Van-Veen soil sampler, downpipe
Sampling of water from mineral springs and spas
Test object
Site
SED
PI, GE,
HM, HI
PI, GE,
HM, HI
PI
WA, DW
Soil quality – Sampling – Part 2: Guidance on sampling SO
techniques
Geotechnical investigation and testing – Sampling
SO
methods and groundwater measurements – Part 1:
Technical principles for execution
Replaces DIN 4021: 1990-10
Soil – Exploration by excavation and borings, as well
SO
as sampling:
Sampling in the investigation of areas with suspected
contamination and contaminated sites (ramming core
sampling)
(withdrawn standard)
PI
PI
Other applicable documentation
Standard/issue date
In-house
method/version
Federal Compost
Association methods
book for the analysis of
compost, Chapter IV A4
2006-09
DIN 38402-A 30
1998-07
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Gaseous phytotoxins in the seed planting experiment
with cress
Test object
Pre-treatment, aliquotation and homogenisation of
non-homogeneous water samples
WA, SW, SE, DW, PI, GE,
GW, FW
HM, FG,
HI
WA, DW
PI, GE, FG
DIN EN ISO 5667-1 (A 4) Water quality – Sampling – Part 1: Guidance on the
2007-04
design of sampling programmes and sampling
techniques
Replaces DIN EN 25667-1: 1993-11
Replaces DIN EN 25667-2: 1993-07
DIN EN ISO 5667-3 (A21) Guidance on the preservation and handling of water
2004-05 incl. Corr. 1,
samples
2006-08 (A, B)
2011-01 (draft)
ISO 5667–11
Guidance on sampling of groundwater
1993-03
(withdrawn standard)
2009-04
FHH-UB Leaflet 4,
Sampling of ground water
quality assurance 199910
LAWA AQS leaflet
Waste water digestion
P 3/2
2001-01
Site
GE
WA, SW, SE, DW, PI, GE,
GW, FW
HM, FG,
HI
WA, DW
GW, DW
PI, GE,
HM, FG,
HI
PI, HI
SE
HI
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
27/89
Appendix to the accreditation certificate D-PL-14170-01-00
Standard/issue date
In-house
method/version
LAWA AQS leaflet
P 8/1
1993-01
2009-09
LAWA AQS leaflet
P 8/2
1995-05
LAWA AQS leaflet
P-8/3
2012-02 (A)
LAWA gauge regulations
Appendix D 1998
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Sampling of waste water and leachate
Test object
Site
SE, LE
PI, GE,
HM
Sampling of ground water
GW, DW
Sampling from flowing waters
WA, FW
PI, GE,
HM, FG,
HI
PI, GE,
HM, FG
Guidelines for measuring and detecting drains and
flows
WA
PI
DVGW leaflet W 112
Principles of ground water sampling from
groundwater measuring points
WA, GW
PI, FG, GE
Collection and scope of analysis of groundwater
WA, DW
samples
(withdrawn rule)
Vertical sampling from groundwater measuring points WA, GW
PI, GE, FG
Guidance on performing sampling from a drinking
water installation for testing for Legionella
Holes for the exploration, observation and extraction
of groundwater
Construction and expansion of groundwater
measurement points
Guidelines for waste water sampling in NRW
DW
PI
GW
PI
GW
PI
WA
GE
WA, GW
PI, GE, FG
WS
PI, GE, FG
WS, SO
PI, GE, FG,
HI
PI, GE, FG,
HI
2011-10
Containing the same
content as
DWA-A 909
2011-12
DVWK rule 128
1992
DVWK leaflet 245, 1997
DVGW leaflet 74
2012-01
DVGW leaflet W 115
2008-07
DVGW leaflet W 121
2003-07
LUA leaflet no. 31
2001-04
LAGA guideline PN
1/75,
1975
LAGA guideline
PN 2/78K
1983-12
LAGA guideline PN 98,
2002
LAGA guideline EW 98
2002
VDI 3865 sheet 1
2005-06
VDI 3865 sheet 2
1998-01
Guidance on the method for physical and chemical
analyses in connection with the removal of waste;
Water sampling (withdrawn directive)
Guidance on the method for physical and chemical
analyses in connection with the removal of waste;
Principles for the sampling of waste and deposited
substances (withdrawn directive)
Method for physical, chemical and biological analyses
in connection with the processing / removal of waste
Method for physical and chemical analyses of waste,
contaminated soils and materials from the
contaminated sites sector
Planning of measurements for the determination of
volatile organic compounds in soil gas
Techniques for the active sampling of soil gas
WS, SO
PI, GE, FG
GA
PI
GA
PI
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
28/89
Appendix to the accreditation certificate D-PL-14170-01-00
Standard/issue date
In-house
method/version
DIN EN 932-1
1996-11
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Test for general properties of aggregates – Methods
for sampling
Test object
Site
SO
PI
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
29/89
Appendix to the accreditation certificate D-PL-14170-01-00
Other applicable documentation for sample pre-treatment
Standard/issue date
In-house
method/version
VDLUFA method
handbook I
A 6.2.1.1
1991
VDLUFA book of
methods I
A 6.2.4.1
1991
VDLUFA book of
methods I
1991
DIN ISO 11464
2006-07 (A)
DIN 19747
2009-07
(A)
DIN ISO 14507
2004-07
DIN ISO 22155
2006-07
2009-08 (draft)
DIN ISO 11277
2002-08
DIN 18123
1996-11 (A)
2011-04
DIN 38414-S 4
1984-10 (A)
LAGA guideline EW 98S
DIN EN 12457-1
2003-01
DIN EN 12457-2
2003-01
In conjunction with
AbfAblV 2001 Appendix
4 no. 2.4
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Extraction with calcium acetate lactate (CAL) for the
determination of phosphorous and potassium
Test object
Site
SO
PI, HI
Extraction with calcium chloride (CaCl2) for the
determination of plant-available magnesium
SO
PI, HI
DL extract
SO
PI
Soil quality – Pre-treatment of samples for physicochemical analyses
(withdrawn standard)
Investigation of solids – Pre-treatment, preparation
and processing of samples for chemical, biological
and physical investigations
Replaces DIN ISO 11464 2006-07(A)
SO
PI, HI, GE,
FG
SO, SM, SL, SED
PI, HI, GE,
FG
Soil quality – Pre-treatment of samples for
determination of organic contaminants in soils
Soil quality – Sample pre-treatment for the gas
chromatographic quantitative determination of
volatile aromatic and halogenated hydrocarbons and
selected ethers – Static headspace method
Soil quality – Determination of particle size
distribution in mineral soil material – Method by
sieving and sedimentation
Soil, investigation and testing –
Determination of grain-size distribution
SO
SO
PI, HI, GE,
FG
PI
SO
PI
SO
PI, GE
Determination of leachability by water
SO, SL, SED
PI, HI, GE,
FG
Characterisation of waste – Leaching of granular
WS, SED, SL
waste and sludges – Part 1: One-stage batch test at a
liquid to solid ratio of 2 l/kg with particle size below 4
mm (without or with size reduction);
Characterisation of waste – Leaching of granular
WS, SED, SL
waste and sludges – Part 2: One-stage batch test at a
liquid to solid ratio of 10 l/kg with particle size below
4 mm
(without or with size reduction)
PI, HI, GE,
FG
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
PI, HI, GE,
FG
30/89
Appendix to the accreditation certificate D-PL-14170-01-00
Standard/issue date
In-house
method/version
DIN EN 12457-3
2003-01
Analyte – Title of the standard
Test object
Information on sample pre-treatment/testing
technology
Characterisation of waste – Leaching of granular
WS, SED, SL
waste and sludges – Part 3: Two-stage batch test at a
liquid to solid ratio of 2 l/kg and 8 l/kg for materials
with high solid content with particle size below 4 mm
(without or with size reduction)
Leaching of granular waste and sludges – Part 4: One- WS, SED, SL
stage batch test at a liquid to solid ratio of 10 l/kg for
materials with particle size below 10 mm
(without or with size reduction)
DIN EN 12457-4
2003-01
in conjunction with
AbfAblV
2001 Appendix 4 no. 2.4
BBodSchV Appendix 1,
Elution method – Soil saturation extract
3.1.2
1999-07
DIN EN 1744-3
Tests for chemical properties of aggregates –
2002-11
Part 3: Preparation of eluates by leaching of
aggregates
DIN 19527
Elution of solid materials – Batch test for the
2010-05
examination of the elution behaviour of
organic substances at a liquid to solid ratio of 2 L/kg
(withdrawn standard)
DIN 19528
Elution of solid materials – Percolation method for
2009-01
the joint examination of the elution behaviour of
inorganic and organic substances
Site
PI, HI, GE,
FG
PI, HI, GE,
FG
SO
PI, HI, GE
WS
HI, PI
SO
HI, GE
SO, SED, WS
HI
DIN 19529
2009-01
Elution of solid materials – Batch test for the joint
examination of the elution behaviour of inorganic
substances at a liquid to solid ratio of 2 l/kg
SO, SED, WS
PI, HI, GE
LUA leaflet no. 20
(March 2000)
in conjunction with
BBodSchV 1999-07,
DIN V 19736
1998-10
DIN 19738
2004-07
(A)
FGSV no. 28/1
LAGA guideline EW 98T
Column experiment (column eluate) for the
determination of organic contaminants in soils
SO
HI
Absorption availability of organic and inorganic
pollutants from contaminated soil material
SO
HI
Leachability (trough eluate)
WS
PI, HI, GE
DIN CEN/TS 14405
Leachability – Up-flow percolation test
Prestandard 2004-09
(under specified conditions)
LAGA guideline EW 98 p Determination of leachability by water at a constant
pH-value (pH-stat method)
WS
HI
SO
FG
DIN 19730
2009-07
SO
PI, HI
SO, WS
PI, HI
DIN ISO 11466
1997-06
Soil quality – Extraction of trace elements using
ammonium nitrate solution
(withdrawn standard)
Soil quality – Extraction of trace elements soluble in
aqua regia
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
31/89
Appendix to the accreditation certificate D-PL-14170-01-00
Standard/issue date
In-house
method/version
(A)
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Test object
Site
DIN EN 13346-S7a
2001-04
Characterisation of sludges – Extraction of trace
elements and phosphorus with aqua regia method A
(backflow) and method C: (microwave)
Guidance on the method for physical and chemical
analyses in connection with the removal of waste;
Determination of leachability of solid and sludgy
waste by water
Water quality – Digestion for the determination of
selected elements in water,
Part 2: Nitric acid digestion
SL, SED, SO, WS,
BW, WO, SS
PI, HI
WS
PI, GE, FG
WA, SE, LE
PI
Sample preparation and partial sampling, sieving < 10
mm, crushing < 0.25 mm
Sample preparation: homogenisation, centrifugation,
freeze drying
Sample preparation: reduction, crushing and grinding
of solid samples to laboratory sample
Sample preparation: Reduction, rolling of pasty and
muddy samples to laboratory samples
Administrative arrangement
BW
PI, GE
SS, SL
PI
WS
PI, GE, FG
WS
GE
SO
PI, GE
Digestion for subsequent determination of aquaregia-soluble portion of elements in waste
Sampling and sample preparation; Sample
preparation
WS, SS, SO, WO,
BW
WO
PI, HI
Sample preparation: Homogenisation, drying and
crushing < 2 mm
Stones and impurities (glass, plastics, metals)
WO
HI, GE
BW
PI, GE
BW
PI, GE
GY
PI
LAGA guideline EW 77
1977
DIN EN ISO 15587-2
(A32)
2002-07
in conjunction with
AbfAblV 2001 Appendix
4 no. 2.4
BioAbfV 1998
Appendix 3 no. 1.2
AbfKlärV 1992
Appendix 1 no. 1.2
DepV 2002
Appendix 4 no. 3.1.1
DepV 2002
Appendix 4 no. 3.1.1
OFD-H-BAM
2008-10
DIN EN 13657
2003-01
AltholzV Appendix IV
no. 1.2 2002 in
conjunction with DIN
51701 Part 3
2006-09
AltholzV 2002
Appendix IV no. 1.3
BioAbfV 1998
Appendix 3 no. 1.3.3
Federal Compost
Stones and impurities (glass, plastics, metals)
Association methods
book for the analysis of
compost, Chapter II C 13, 2006-09
VGB M701
Analysis of FGD gypsum, preparatory measures
2008-12
(digestion, eluate, etc.)
HI
Individual testing methods of ion chromatography
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
32/89
Appendix to the accreditation certificate D-PL-14170-01-00
Standard/issue date
In-house
method/version
DIN EN ISO 10304-1
(D19)
1995-04 (A)
and 2009-07
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Determination of dissolved anions bromide, fluoride,
chloride, nitrate, orthophosphate and sulphate, and
additionally nitrite, using ion chromatography
Part 1: Method for weakly contaminated water
Dev.: additional matrix waste in soda digestion
Dev. PI: no determination of nitrite and phosphate
replaces DIN EN ISO 10304-2: 1996-11
DIN EN ISO 10304-2Water quality – Determination of dissolved anions by
D20 1996-11 (A)
ion chromatography –
Part 2: Determination of bromide, chloride, nitrate,
nitrite, orthophosphate and sulphate in waste water
Dev. PI: no determination of nitrite and phosphate
(withdrawn – replaced by DIN EN ISO 10304-1: 200907)
DIN EN ISO 10304-3Water quality – Determination of dissolved anions by
D22 1997-11 (A)
ion chromatography –
Part 3: Determination of chromate, iodide, sulphite,
thiocyanate and thiosulphate HE: only iodide,
thiosulphate PI: only sulphite
DIN EN ISO 15061 (D 34) Water quality – Determination of dissolved bromate –
2001-12
Method by ion chromatography
VGB-M 701 serial no. 02 Bromide, chloride and sulphate from soda extract
and 8.8.1
using ion chromatography
2008-12
VGB-M 701 serial no. 02 Chloride from aqueous extract by ion
and 8.8.2
chromatography
2008-12
Test object
Site
WA, SW, GW, EL, PI, HE
DW, WS
WA, SW, GW, SE, PI, HE
EL, DW
WA, SE, EL
PI, HE
DW
PI
GY, CC, DU
PI
GY
PI
Individual testing methods of XRF
Standard/issue date
In-house
method/version
In-house method
HE-MA MU 18-1/2/3
2010-05
In-house method
GE-MA-M 11-1
2008-01
AltölV 1987 Appendix 2
Point. 3.3.1
DIN EN 15309
2007-08
Analyte – Title of the standard
Test object
Information on sample pre-treatment/testing
technology
Semi-quantitative analysis of solids using XRF (X-ray
SM
fluorescence), energy-dispersive method with the
range of elements from sodium to uranium in pellets,
loose bulk, solids with smooth surfaces, as well as
liquids
Testing of silicon-iron alloys – Determination of
Si-Fe metals
silicon and iron content
Total halogen, semi-quantitatively using energyOIL
dispersive XRF
Characterisation of waste and soil – Determination of WS, SO
elemental composition by X-ray fluorescence;
Dev: only loose bulk and pellet
Site
HE
HE
HE
HE
Individual testing methods of calorimetry
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Standard/issue date
In-house
method/version
Federal Compost
Association methods
book for the analysis of
compost, Chapter IV A1
2006-09
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Degree of rotting
Test object
Site
SO
GE
Test object
Site
WA, DW
PI, HI, GE,
HM
Individual testing methods of qualitative sample description
Standard/issue date
In-house
method/version
DEV-B1/2
6. edition 1971
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Smell, qualitative (also on site)
DIN EN 1622 (B 3)
2006-10
Water quality – Determination of the threshold odour WA, SW, SE, DW, PI
GW, FW
number (TON) and threshold flavour number (TFN)
Replaces DIN EN 1622-B3 1997-10
DEV-B1/2
6. edition 1971
Taste (also on site)
2
DW
PI, HI, GE,
HM
Test object
Site
IO
HE
Measurement of relative permittivity, dielectric
dissipation factor (tan δ) and d.c. resistivity
IO
HE
Colour (VDEW colour table) and purity (appearance)
IO
HE
Determination of neutralisation number; colourindicator titration, insulating oils
Oil-filled electrical equipment – Sampling of gases
and oil for the analysis of free and dissolved gases.
Dev. Only sampling
(withdrawn standard)
Saponification number; Colour-indicator titration,
insulating oils
(withdrawn standard)
IO
HE
IO
HE
IO
HE
Sector for insulating oil analysis
Individual testing methods of insulating oil analysis
Standard/issue date
In-house
method/version
DIN EN 60156; VDE
0370-5
1996-03
DIN EN 60247 VDE
0380-2
2005-1
In-house method
HM-MA-M U 10-4
2009-09
DIN 51558-2
1990-03
DIN EN 60567; VDE
0370-9
2006-5
DIN 51559-2
1990-03
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Determination of the breakdown voltage at power
frequency – Test method
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Testing type: Electrochemistry
Standard/issue date
In-house
method/version
DIN EN ISO 12937
2002-03
DIN 60814
1999-03
3
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Determination of water content – Karl Fischer
method; Coulometric titration
Determination of water by automatic Karl Fischer
titration
Test object
Site
IO
HE
IO
HE
Sector for fuel analyses (secondary fuels, fuels, alternative fuels, biofuels)
Individual testing methods of fuel analysis
Standard/issue date
In-house
method/version
DIN 51719
1997-07
DIN EN 14775
2010-04
DIN CEN/TS 15440
App. B/E
2007-02, Prestandard
DIN 51729-10
1996-05
DIN EN 14961-1
2010-04
DIN 51900-1
2000-04
DIN EN 15170
2009-05
DIN 51727
2001-06
DIN 51408
1983-06
In-house method
GE-MA M 7-1
2008-01 in conjunction
with
DIN ISO 13878
1998-11
DIN ISO 15178
2001-02
DIN ISO 10694
1996-08
DIN 51720
2001-03
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Determination of ash content
Test object
Site
FU
GE
Determination of ash content
FU
GE
Biomass
FU
GE
Determination of chemical composition of fuel ash
FU
HE
Fuel specifications and classes Part 1 General
requirements
Determination of gross calorific value by the bomb
calorimeter and calculation of net calorific value –
Part 1: Principles, apparatus, methods
Determination of calorific value,
Dev.: only determination of gross calorific value
Determination of chlorine content
FU
GE
FU
HE
FU
HE
FU
GE
Determination of chlorine content; Wickbold
combustion method
Elementary analysis: nitrogen, carbon, hydrogen,
sulphur, oxygen total by dry combustion
FU
GE
SO, solid and
liquid sample
matrix
GE
Determination of volatile matter content
FU
GE
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Standard/issue date
In-house
method/version
DIN 51755
1974-03
DIN 51723
2002-06
DIN EN 14918
2010-04
DIN EN 15104
2011-04
DIN EN 15149 Part 1
2010-04
DIN EN 15149 Part 2
2010-04
DIN EN 12766 Part 1,
2000-11
DIN EN 12766 Part 2,
2001-12
DIN EN 15103 2010-04
DIN EN 15408
2011-05
DIN EN 15289
2011-04
DIN CEN/ TS 15290,
2006-06
DIN EN 24260
1994-05
DIN 51718
1995-09
DIN 51777 Part 1
1983-03
DIN 51777 Part 2
1974-09
GE-MA-M 11-6
2008-01
with DIN 53019-1
2008-09
and DIN 53019-2
2001-02
DIN EN 14774-1
2010-04
DIN EN 14774-2
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Determination of flash point by the closed tester
according to Abel-Pensky
Determination of fluoride content
Test object
Site
FU
HE
FU
HE
Determination of calorific value
FU
HE
Determination of total content of carbon, hydrogen
and nitrogen
Determination of particle size distribution – Part 1:
Oscillating screen method using sieve apertures of 1
mm and above
Determination of particle size distribution – Part 2:
Oscillating screen method using sieve apertures of
3.15 mm and below
Determination of PCBs and related products – Part 1:
Separation and determination of selected PCB
congeners by gas chromatography (GC) using an
electron capture detector (ECD)
Dev.: measurement using GC-MS
Determination of PCBs and related products – Part 2:
Calculation of polychlorinated biphenyl (PCB) content
Dev.: measurement using GC-MS
Determination of bulk density
FU
GE
FU
GE
FU
GE
FU
GE
FU
GE
FU
GE
Solid recovered fuels – Methods for the
determination of sulphur (S), chlorine (Cl), fluorine (F)
and bromine (Br) content
Solid biofuels – Determination of total content of
sulphur and chlorine
Determination of major elements – Al, Ca, Fe, Mg, P,
K, Si, Na and Ti
Determination of sulphur content; Wickbold
combustion method
Determination of the water content and the moisture
of analysis sample
Water content according to Karl Fischer (direct
method)
Determination of water content according to Karl
Fischer; Indirect Method
Determination of dynamic viscosity using rotation
viscometer
FU
HE
FU
HE
FU
HE
FU
GE
FU
GE
FU
HE
FU
HE
FU
HE
FU
GE
FU
GE
Determination of moisture content – Oven dry
method – Reference method
Determination of moisture content – Oven dry
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Standard/issue date
In-house
method/version
2010-04
4
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
method – Simplified method
Test object
Site
Test object
Site
CO
PI
Sector for food and commodity analysis
Testing type: Atomic spectrometry (ICP-MS, ICP-OES, AAS)
Standard/issue date
In-house
method/version
In-house method K&W
KWHH-MA-ML 1-4
2008-02
ASU L 00.00-19/1 200312
DIN EN 13805
2002-06
DIN EN 15763
2010-04
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Arsenic, arsine (ICP/OES after adsorption)
Determination of trace elements – Pressure digestion FO in general
Dev.: microwave digestion
HH
Foodstuffs – Determination of trace elements –
FO in general
Determination of arsenic, cadmium, mercury and lead
in foodstuffs by inductively coupled plasma mass
spectrometry (ICP-MS) after pressure digestion
PI
Testing type: Gas chromatography (GC-FID, GC-ECD, GC-NPD, GC-MSD, GC-MS/MS)
Standard/issue date
In-house
method/version
ASU L 00.00-24 2002-12
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Determination of benzene, toluene and xylene
isomers in foods
BTEX benzene, toluene, xylenes, ethylbenzene
(Adsorption on Carbotrap, thermodesorption GC/MS)
Carbonyl sulphide (GC-MS)
ISBT Procedure 12.0;
2000-10
In-house method
GE-MA-M 3-8#2
2009-09
ASU L 05.00-16; 2011-01 Determination of cholesterol content in eggs and egg
products – gas chromatographic method
ASU L 22.02/04-1,
Determination of cholesterol content in egg pasta –
2006-12
GC method after acid and alkaline digestion
In-house method
Dimethyl ether (adsorption on TDS pipe, GC/MS)
GE-MA-M 3-8#4
2009-09
ASU L 00.00-49-2 2002- Determination of dithiocarbamate- and thiuram
12
disulfide residues – Part 2: Gas chromatographic
DIN EN 12396-2
method
1998-12
ASU L 53.00-1 1999-11
Gas chromatographic determination of ethylene
oxide and 2-Chloroethanol in spices
ASU L 00.00-47, 1999-11 Determination of ethephon by headspace gas
chromatography in plant-based foods
Test object
Site
Low-fat FO
HH
CO
GE
CO
GE
Eggs, egg
products
Pasta
HH
CO
GE
Low-fat FO
HH
Spices
HH
Plant-based FO
HH
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
HH
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Standard/issue date
In-house
method/version
DGF C-VI 11d
1998
ASU L 13.04-1 2006-12
ISBT Procedure 5.0,
2000-10
ISBT Procedure 10.0,
2000-10
In-house method GEMA-M 3-2
2008-01
GE-MA ML 3-8#1
2009-09
In-house method
GE-MA-ML 3-8#3
2009-09
ASU L 00.00-36/2
2004-07
ASU L 17.00-12 1999-11
ISBT Procedure 8.0
2000-10
EPA 625
DFG S 19.
11/1999
DIN EN 15662
2007-06 (draft)
ASU L 00.00-115, 200902
ASU L 00.00-34
2010-09
ISBT Procedure 4.0
2000-10
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Fatty acids using GC-FID
Test object
Site
FO in general
HH
OIL
HH
CO
GE
Hydrocarbons, volatile methane, ethane, propane,
CO
butane total (calculated as methane) using GC-FID
VCH: Dichloromethane, 1,2-dichloromethane,
CO
trichloromethane, 1,1,1-trichloroethane,
tetrachloromethane, trichloroethylene,
tetrachloroethylene
(Adsorption on Carbotrap, thermodesorption GC/MS;
Freons: F11, F12, F 21, F 113, F 114, R22
(Adsorption on Carbotrap, thermodesorption GC/MS)
Methanol, ethanol
CO
(Absorption in silica gel, desorption)
GE
Bromide using GC-ECD
Plant-based FO
HH
Determination of butyric acid as methyl ester in fat
from bread including small baked products from
dough
Oil and fat (extraction of snow sample residue,
analysis.: DIN EN ISO 9377-2 (H53) GC/FID)
PAH (polycyclic aromatic hydrocarbons) (GC/MSD
after adsorption)
Pesticides using GC-MS and GC-MS/MS
Bread, small
baked products
HH
CO
GE
CO
GE
FO
HH
Plant-based FO
HH
FO in general
HH
Direct. ind.
GE
Test object
Site
CO
HI
Determination of low-boiling halogenated
hydrocarbons in edible oils
Carbon monoxide (GC-FID)
Multi-method for the determination of pesticide
residues in plant-based foods using GC-MS(/MS) or
LC-MS/MS following acetonitrile
extraction/partitioning and clean-up by dispersive
SPE (QuEChERS1)
Pesticide residues: Modular multi-method, extended
new version of the DFG method S 19
Dev.: variation of the terms for the GPC and SC
Oxygen (sensor)
GE
GE
Testing type: HPLC, LC (HPLC-DAD, HPLC-UV, HPLC-FLD, LC-MS/MS)
Standard/issue date
In-house
method/version
ISBT Procedure 11.0
2000-10
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Acetaldehyde (DNPH derivatisation, HPLC-DAD)
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Standard/issue date
In-house
method/version
In-house method
HH-MA M 02-084
2010-12
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Acrylamide using LC-MS/MS
Test object
Site
Plant-based FO
HH
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Standard/issue date
In-house
method/version
ASU L 23.05-2 2012-01
DIN EN 14123
2008-03
ASU L 15.00-2 2001-07
in conjunction with
ASU L 23.05-2 2012-01
§ 64 L 10.00-5
1999-11
ASTA 21.3
2004-10
In-house method
HM-MA ML 2-12
2009-08
ASU L 00.00-76 2008-12
In-house method
HH-MA-M 2-4
2010-06
In-house method
HM-MA ML 2-8
2009-08
In-house method
HH-MA-M 02-107
2012-02
In-house method
HH-MA-M 02-108
2012-02
ASU L 15.05-2 2004-07
DIN EN 13585
2002-03
ASU L 43.08-1 1996-02
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Determination of aflatoxin B1 and the sum of
aflatoxin B1, B2, G1 and G2 in peanuts, pistachios, figs
and paprika powder – HPLC method with
immunoaffinity column clean-up and post-column
derivatisation
Determination of aflatoxin B1 and the sum of
aflatoxin B1, B2, G1 and G2 in cereals, nuts and
related products
Dev.: modified post-column derivatisation
Determination of the content of biogenic amines in
fish and fish products – high-performance liquidchromatographic determination;
Capsaicin
Site
Nuts, figs,
paprika powder
HH
Cereals, nuts,
related products
HM
Fish, fish
products
HH
Chillies, peppers
HH
Chloramphenicol after liquid extraction using LCMS/MS
Animal-based FO HM
Determination of chlormequat and mepiquat in lowfat foods – LC-MS/MS method
Coumarin using HPLC-DAD
Plant-based FO
HM
Cinnamoncontaining FO,
cinnamon,
spices, tea
Cereals, cereal
products
HH
Dithianon with LC-MS/MS
Plant-based FO
HH
Dodine with LC-MS/MS
Plant-based FO
HH
Determination of fumonisins B1 and B2 in maize –
HPLC method with solid phase extraction clean up
Plant-based FO
HH
Liquorice,
liquorice
products
Crustaceans,
crustacean
products
FO in general
HH
Deoxynivalenol using LC-MS/MS
Determination of glycyrrhizin in liquorice and
liquorice-containing confectionery using reversedphase high-performance liquid chromatography
ASU L 12.01-2 2001-07 Determination of indole content in crustaceans and
crustacean products – high-performance liquidchromatographic determination
ASU L 00.00-9 1984-11
Determination of preservatives in low-fat foods
In-house method
HM-MA ML 2-14
2009-08
Standard/issue date
Test object
HM
HH
HH
Malachite green and its leuco base, as well as brilliant Animal-based FO HM
green and crystal Violet after liquid extraction using
LC-MS/MS
Analyte – Title of the standard
Test object
Site
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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In-house
method/version
ASU L 00.00-29
2006-12
ASU L 26.00-01
2001-07
In-house method
HM-MA ML 2-10
2009-08
ASU L 15.03-1
2010-01
DIN EN 14132
2009-09
ASU L 31.00-20
2004-12
DIN EN 15662
2009-02
ASU L 00.00-115
2007-12
ASU L 00.00-113
2007-12
In-house method
HM-MA ML 2-16
2009-08
In-house method
HM-MA ML 2-21
2009-08
In-house method
HH-MA-M 02-109
2012-04
In-house method
HH-MA-M 02-110
2012-04
ASU L 00.00-28
2001-07
In-house method
HM-MA ML 2-17
2009-08
ASU L 18.00-16 1999-11
ASU L 46.00-3 2000-07
ASU L 47.00-6 1996-02
Standard/issue date
In-house
Information on sample pre-treatment/testing
technology
Determination of sodium cyclamate in foods – HPLC
method
Determination of nitrate content in vegetables
products – HPLC/IC method
Nitrofurans and their metabolites using LC-MS/MS
Animal-based FO HM
Determination of ochratoxin A in barley – HPLC
method with immunoaffinity column clean-up
Barley, roasted
coffee
Determination of patulin in clear and cloudy apple
juice and apple purée – HPLC method with clean-up
by liquid/liquid distribution
Multi-method for the determination of pesticide
residues in plant-based foods using GC-MS(/MS) or
LC-MS/MS following acetonitrile
extraction/partitioning and clean-up by dispersive
SPE (QuEChERS1)
Multi-method for the determination of pesticide
residues in foods using LC-MS/MS after methanol
extraction and clean-up using diatomaceous earth
(alder)
Streptomycin using LC-MS/MS
Apple juice,
HH
apple juice purée
FO in general
HH
Vegetables
HH
HH, HM
FO in general
HH
FO in general
HH
Honey
HM
Sulphonamides using LC-MS/MS
Honey
HM
Phenoxyalkane carbonic acid with LC-MS/MS
Plant-based FO
HH
Phenyl ureas with LC-MS/MS
Plant-based FO
HH
Determination of acesulfame K, aspartame and
sodium saccharin in foods – HPLC method
Tetracyclines using LC-MS/MS
FO in general
HH
Honey, fish,
meat
HM
Coffee, coffee
products, tea,
pastry products,
soft drinks,
plant-based FO
HH
HM
Test object
Site
Determination of theobromine and caffeine in
pastries
Analysis of coffee and coffee products; Determination
of caffeine content – Part 2: Rapid HPLC method
Analysis of tea – Determination of caffeine content;
HPLC method
Dev. HM vanillin and ethylvanillin using HPLC-DAD
Analyte – Title of the standard
Information on sample pre-treatment/testing
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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method/version
technology
ASU L 00.00-63/1
2001-07
DIN EN 12823-1
2000-07
ASU L 00.00-83 2004-07
DIN EN 14122
2003-09
ASU L 00.00-84 2006-12
DIN EN 14152
2006-03
Determination of vitamin A in foods by HPLC – Part 1: FO in general
Determination of all-trans-retinol and 13-cis-retinol
HH
Determination of vitamin B1 by HPLC
FO in general
HH
Determination of vitamin B2 by HPLC
FO in general
HH
ASU L 00.00-97 2006-12
DIN EN 14663
2006-03
ASU L 00.00-85 2011-01
DIN EN 14130
2003-09
ASU L 00.00-61 2010-01
DIN EN 12821
2009-08
ASU L 00.00-62 2001-07
DIN EN 12822
2000-07
ASU L 00.00-86 2004-07
Determination of vitamin B6 (including its
glycosylated forms) in foods – HPLC method
FO in general
HH
Determination of vitamin C (ascorbic acid) using
HPLC-DAD
FO in general
HH
Determination of vitamin D3 (cholecalciferol) using
HPLC-UV
FO in general
HH
Determination of vitamin E (α-, β-, γ- and δTocopherol) in foods by HPLC-FLD
FO in general
HH
Determination of vitamin K1 using HPLC-FLD
FO in general
HH
In-house method
HM-MA ML 2-7
2009-08
Zearalenone using LC-MS/MS
Cereals, cereal
products
HM
Individual testing methods of electrochemistry
Standard/issue date
In-house
method/version
ASU L 06.00-2
1980-09
ASU L 07.00-5
2010-01
Analyte – Title of the standard
Test object
Information on sample pre-treatment/testing
technology
Measurement of pH-value in meat and meat products Meat, meat
products
Determination of the cooking salt content (sodium
Meat, meat
chloride) in meat products
products
Site
HH
HH
Testing type: Gravimetry
Standard/issue date
In-house
method/version
ASU L 53.00-5
2010-09
ASU L 06.00-4
2007-04
ASU L 53.00-4
1996-02
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Determination of essential oil content – Distillation
process
Determination of ash in meat and meat products
Determination of total ash and acid-insoluble ash
Test object
Site
Spices
HH
Meat, meat
products
Spices
HH
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
HH
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Standard/issue date
In-house
method/version
ASU L 17.00-3
2002-12
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Determination of ash in bread including small baked
products from dough
ASU L 16.01-2
2008-12
ASU L 00.00-18
2002-12
ASU L 31.00-1
1997-01
ASU L 01.00-20
1988-05
ASU L 17.00-1
1982-05
ASU L 16.01-1
2008-12
ASU L 06.00-6
1980-09
ASU L 53.00-4
1996-02
ISBT Procedure 8.0
2000-10
ASU L 06.00-3
2004-07
ASU L 44.00-3
1985-12
ASU L 39.00-2
1981-04
ASU L 53.00-8
2004-07
ASU L 80.30-01
1998-01
ASU L 80.30-02
2008-04
ASU L 80.30-03
2008-10
ASU L 80.30-04
2008-10
ASU L 80.30-06
2008-10
ASU L 80.30-08
2008-10
ASU L 80.30-10
2008-10
ASU L 80.30-12
2008-10
ASU L 80.30-17
2008-10
Determination of ash in cereal flour
Determination of dietary fibre in foods
Test object
Site
Bread, small
baked products,
pastries
Cereal flour,
coarse meal
FO in general
HH
HH
HH
Determination of the relative density of fruit and
vegetable juices (according to DIN EN 1131)
Determination of the fat content of milk and dairy
products (Weibull Stoldt)
Determination of the loss on drying in bread including
small baked products from dough
Determination of the moisture content in cereal flour
Juices
HH
Dairy products,
cheeses
Bread, small
baked products
Flour
HH
Determination of total fat content in meat and meat
products
Determination of total ash and acid-insoluble ash
Meat, meat
products
Spices
HH
Particles
CO
GE
Determination of dry matter in meat and meat
products
Determination of dry matter content in solid
chocolate
Dry matter (vacuum method)
Meat, meat
products
Chocolate
HH
HH
Sugar
HH
Determination of spices and seasoning ingredients –
Determination of water content (distillation method)
Basic rules for testing migration
Spices
HH
Commodities
HH
List of simulants
Commodities
HH
Additional regulations for testing compliance with the
migration limits
Guidelines for selecting test conditions and testing
methods for overall migration
Testing methods for overall migration into aqueous
test foods by total immersion
Testing methods for overall migration into aqueous
test foods through cells
Testing methods for overall migration into aqueous
test foods with a bag
Testing methods for overall migration into aqueous
test foods by filling of the matter
Testing method for “substitute test” for the overall
migration from plastics intended for contact with
Commodities
HH
Commodities
HH
Commodities
HH
Commodities
HH
Commodities
HH
Commodities
HH
Commodities
HH
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
HH
HH
HH
43/89
Appendix to the accreditation certificate D-PL-14170-01-00
Standard/issue date
In-house
method/version
ASU L 80.30-18
2008-10
ASU L 80.30-27
2009-11
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
fatty foods, using the test media iso-octane and 95%
ethanol
Alternative test for the determination of migration in
fatty test foods by rapid extraction in iso-octane
and/or 95% ethanol
Testing method for overall migration from plastics at
high temperatures
Test object
Site
Commodities
HH
Commodities
HH
Individual testing methods of sensor technology (sensory evaluation)
Standard/issue date
In-house
method/version
ISBT Procedure 15.016.0
2000-10
In-house method
HM-MA ML 10-11
2012-08
In-house method
HH-MA M 10-16
2002-05
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Taste and smell in water (sensor technology)
Test object
Site
CO
GE
Sensor technology
FO in general
HM
Sensory evaluation
FO in general
HH
Test object
Site
CO
GE
Bread, bread
dough, small
baked products
FO in general.
HH
HH
Test object
Site
Fruit and
vegetable
products
HH
Test object
Site
Individual testing methods of polarimetry and other methods
Standard/issue date
In-house
method/version
ISBT Procedure 13.014.0
2000-10
ASU L 17.00-5
2003-12
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Sulphur, total (sum of COS, H2S and SO2) (calculated)
ASU L 00.00-14
1986-11
Analysis of foods; Measurement of the radioactivity
of foods
Determination of the starch content in bread
including small baked products from dough
Individual testing methods of refractometry
Standard/issue date
In-house
method/version
ASU L 30.00-2
1993-08
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Refractometer method for the determination of the
soluble dry-matter content in processed fruit and
vegetable products
Individual testing method of PCR
Standard/issue date
In-house
Analyte – Title of the standard
Information on sample pre-treatment/testing
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Appendix to the accreditation certificate D-PL-14170-01-00
method/version
Analog ASU
L 00.00-52
2000-07
technology
Method for the detection of salmonella in foods by
polymerase chain reaction (in accordance with DIN
10135)
FO in general
HH
Test object
Site
FO in general
HH
Testing type: Photometry
Standard/issue date
In-house
method/version
SLMB 62/10.2.1
2000-03
ASU L 26.11.03-5
1983-05
ASU L 31.00-12
1997-01
ASU L 00.00-87
2004-07
ASU L 06.00-9
2008-06
ASU L 06.00-8
2010-01
ASU L 01.00-17
2010-09
ASU L 01.00-26
2011-01
SLMB 62/12.2.1
2000-03
ASU L 08.00-14
2008-06
SLMB 62/13.2.1
2000-03
ASTA 12.1
1997-01
ASU L 31.00-13
1997-09
SLMB 62/9.2.1
2000-03
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Biotin using microbiological test
Determination of citric acid in tomato purée
Tomato purée
(enzymatic method)
Enzymatic determination of D-glucose and D-fructose Juice
contents in fruit and vegetable juices – NADPH
spectrophotometric method
Microbiological determination of folate
FO in general
Determination of total phosphorus content in meat
and meat products – Photometric method
Determination of hydroxyproline content in meat and
meat products – Photometric method after acid
digestion
Determination of the lactose and galactose content of
milk and dairy products – Enzymatic method
Determination of L and D lactic acid (L- and D lactate)
content in milk and dairy products – Enzymatic
method
Niacin using microbiological test
HH
HH
HH
Meat, meat
products
Meat, meat
products
HH
Milk, milk
products
Milk, milk
products
HH
FO in general
HH
Determination of nitrate and nitrite content in
Sausage
sausage products after enzymatic reduction of nitrate products
to nitrite – Spectral photometric method
Pantothenic acid using microbiological test
FO in general
HH
Piperine
Spices
HH
Enzymatic determination of sucrose content in fruit
and vegetable juices – NADP spectrophotometric
method
Vitamin B 12 using microbiological test
Juice
HH
FO in general
HH
Test object
Site
HH
HH
HH
Individual testing methods of qualitative evidence using DC
Standard/issue date
In-house
method/version
ASU L 26.11.03-14
1983-11
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Detection of water-soluble dyes in tomato purée,
tomato ketchup and comparable products
Tomato purée,
HH
tomato products
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
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Standard/issue date
In-house
method/version
ASU L 06.00-15
2002-12
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Detection of condensed phosphates in meat and
meat products
Test object
Site
Meat, meat
products
HH
Test object
Site
Bread, small
baked products,
pastries
Fats, oils
HH
HH
Fats, oils
HH
Meat, meat
products
Fats, oils
HH
Testing type: Measurement analysis
Standard/issue date
In-house
method/version
ASU L 17.00-15
1988-12
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Determination of the crude protein content in bread
including small baked products from dough (Kjeldahl)
DGF C III 4, Corr.
Ölsäure 2006
ASU L 13.00-6 1991-06
Fatty acids, free
ASU L 06.00-7
2007-04
ASU L 13.00-5
2012-01
ASU L 26.04-4
1987-06
Joint FHO/WHO Expert
Committee on Food
Additives
ASU L 00.00-46/1-2
1999-11
DIN EN 1988-1
1998-05
ASU L 10.00-3
1988-12
Determination of the peroxide number in fats and
oils; method according to Wheeler; method according
to Sully
Determination of crude protein content in meat and
meat products
Determination of acid value and acidity (in
accordance with DIN EN ISO 660)
Determination of titratable acids (total acidity) in the
cover brine and the press liquor of sauerkraut
Acid (JECFA test)
Press liquor of
sauerkraut
CO
Determination of sulphite in foods – Part 1:
FO in general
Optimised Monier-Williams method
Determination of sulphite in foods – Part 2: Enzymatic
method (adoption of the standard of the same name,
DIN EN 1988 Part 2, May 1998 Edition)
Determination of volatile nitrogenous base content
Meat, meat
(TVB-N) in fish and fish products; Reference method
products
HH
HH
GE
HH
HH
Individual testing method of adsorption methods
Standard/issue date
In-house
method/version
ISBT Procedure 2.0
2000-10
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Purity (with KOH absorbable components)
Test object
Site
CO
GE
Individual testing methods of direct-reading indicator tubes
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Appendix to the accreditation certificate D-PL-14170-01-00
Standard/issue date
In-house
method/version
ISBT Procedure 6.0
2000-10
ISBT SM-1.0
2000-10
ISBT Procedure 9.0
2000-10
Dräger tubes handbook
1994,
9. edition
ISBT Procedure 14.0
2000-10
Dräger tubes handbook
1994
9. edition
ISBT Procedure 7.0-7.1
2000-10
Dräger tubes handbook
1994
9. edition
ISBT Procedure 3.0
2000-10
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Ammonia
Test object
Site
CO
GE
Hydrogen cyanide (sampling tube)
CO
GE
Phosphine (no turbidity in ammonia AgNO3 solution)
CO
GE
Sulphur dioxide (sampling tube)
CO
GE
Hydrogen sulphide (sampling tube)
CO
GE
Nitrogen oxides (NO/NO2) (sampling tube)
CO
GE
Sensor (Mitchel instruments)
CO
GE
Individual testing methods of non-specific cultivation techniques
Standard/issue date
In-house
method/version
ASU L 01.00-37
1991-12
ASU L 00.00-88
2004-07
Analyte – Title of the standard
Test object
Information on sample pre-treatment/testing
technology
Determination of the number of yeasts and moulds in FO in general
milk and dairy products (reference method)
Horizontal method for the enumeration of
FO in general
microorganisms, colony-count technique at 30 °C (in
accordance with DIN EN ISO 4833)
Site
HH
HH
Testing type: Specific cultivation method
Standard/issue date
In-house
method/version
ASU L 00.00-33
2006-09
ISO 4831
2006-12
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Horizontal method for the enumeration of
presumptive Bacillus cereus – Colony-count
technique at 30 °C (in accordance with DIN EN ISO
7932, 2005-03)
Horizontal method for the detection and
enumeration of coliforms – MPN technique
Test object
Site
FO in general
HH
FO in general
HH
ISO 4832
2006-02
Horizontal method for the enumeration of coliforms – FO in general
Colony-count technique
HH
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Standard/issue date
In-house
method/version
ASU L 00.00-133/2
2010-09
ASU L 00.00-132/2
2010-09
ISO 7251
2005-02
ASU L 00.00-22
2006-09
ASU L 00.00-32
2006-09
ASU L 00.00-20
2008-12
ASU L 00.00-55
2004-12
5
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Horizontal method for the detection and
enumeration of Enterobacteriaceae in foods – Part 2:
Colony-count technique (in accordance with DIN ISO
21528-2, 2009-12)
Analysis of foods – Horizontal method for the
enumeration of β-glucuronidase-positive Escherichia
coli in foods – Part 2: Colony-count technique with 5bromo-4-chloro-3-indolyl-β-D-glucuronide (in
accordance with DIN ISO 16649-2, 2009-12)
Microbiology of food and animal feeding stuffs –
Horizontal method for the enumeration of
presumptive Escherichia coli – MPN technique
Horizontal method for the detection and
enumeration of Listeria monocytogenes in foods; Part
2: Enumeration method
(in accordance with DIN EN ISO 11290 part 2)
Horizontal method for the detection and
enumeration of Listeria monocytogenes in foods; Part
1: Detection method
(in accordance with DIN EN ISO 11290 part 1)
Horizontal method for the detection of salmonella
spp. in foods
(in accordance with DIN EN ISO 6579)
Method for the enumeration of coagulase-positive
staphylococci (Staphylococcus aureus and other
species) in foods;
Part 1: Technique using Baird-Parker agar medium
(in accordance with DIN EN ISO 6888-1)
Test object
Site
FO in general
HH
FO in general
HH
FO in general
HH
FO in general
HH
FO in general
HH
FO in general
HH
FO in general
HH
Test object
Site
Raw materials
for the
pharmaceutical
industry
HH, PI
Test object
Site
Sector for pharmaceuticals
Individual testing methods of atomic spectrometry (ICP-OES)
Standard/issue date
In-house
method/version
In-house method
PI-MA-M 1-3 2011-01
HH-MA-M-01-003
2012-04
in conjunction with
Ph.Eur. Paragraph
2.2.22
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
45 elements by atomic emission spectrometry with
inductively coupled plasma (HH digestion only)
Individual testing methods of gas chromatography (GC-MSD, GC-MS/MS)
Standard/issue date
In-house
Analyte – Title of the standard
Information on sample pre-treatment/testing
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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method/version
In-house method
HH-MA M 3-23
2010-05 in conjunction
with Ph. Eur. 2.8.13
In-house method
HH-MA MP 9-3
2012-04
technology
Limit testing of dithiocarbamates by headspace GC
In-house method
HH-MA MP 3-24
2009-11
Limit testing of limit Testing of pesticides using GCMS/MS
In-house method
GE-MA M-P 3-1
2011-05
Impurities using GC-MS
Pesticides – sample preparation for chromatographic
determination
Raw materials
HH
for the
pharmaceutical
industry
Raw materials
HH
for the
pharmaceutical
industry
Raw materials
HH
for the
pharmaceutical
industry
PEEK material for GE
vertebral body
implants
Testing type: HPLC (HPLC-DAD, HPLC-FLD, LC-MSMS)
Standard/issue date
In-house
method/version
In-house method
HH-MA MP 2-80
2009-11
In-house method
HH-MA-MP 2-56
2009-11
In-house method K&W
SOP no. 1263
2007-03
In-house method K&W
SOP Nr. 1265
2007-03
In-house method K&W
KWHH-MA-MP 2-12
2008-03
In-house method
HH-MA-MP 2-55
2009-11
In-house method
HH-MA-MP 2-94
2007-07
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Limit testing of pesticides using LC-MS/MS
Test object
Raw materials
for the
pharmaceutical
industry
Purity and content tests of Xipamide content using
Solids for the
HPLC-DAD
pharmaceutical
industry
Purity and content tests of Xipamide content using
Solids for the
HPLC-DAD (in Aquaphoril)
pharmaceutical
industry
Purity and content tests of prothipendyl HCL hydrate Solids for the
using HPLC-DAD
pharmaceutical
industry
Purity and content tests of Buserelin using HPLC-DAD Solutions for the
pharmaceutical
industry
Purity and content tests of Methformin using HPLCSolids for the
DAD
pharmaceutical
industry
Purity and content tests of gluconic acid and 2Solutions for the
aminoethyl dihydrogen phosphate using HPLC-DAD/ - pharmaceutical
FLD
industry
Site
HH
HH
HH
HH
HH
HH
HH
Individual testing methods of electrochemistry
Standard/issue date
In-house
method/version
USP 6.4.5.
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Determination of electrical conductivity in ultra-pure
water
Test object
Site
Ultra-pure water HH
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Individual testing methods of gravimetry
Standard/issue date
In-house
method/version
Ph.Eur. Paragraph
2.4.14
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Determination of sulphated ash
Ph.Eur. Paragraph
2.2.32
Determination of loss on drying
Test object
Site
Solids for the
pharmaceutical
industry
Solids for the
pharmaceutical
industry
HH
Test object
Site
HH
Individual testing methods of measurement analysis
Standard/issue date
In-house
method/version
Ph.Eur. Paragraph
2.5.11 USP <541>
Ph.Eur. Monograph
CaCl2
Ph.Eur. Monograph
Ca(OH)2
FCC IV Monograph CaO
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Calcium carbonate: Content determination using
complexometric titration
CaCO3 (gypsum,
cigarette paper,
CP)
Calcium chloride: Content determination using
CaCl2 (gypsum,
complexometric titration
cigarette paper,
CP)
Calcium hydroxide: Content determination using acid- Ca(OH)2
base titration
(gypsum,
cigarette paper,
CP)
Calcium oxide: Content determination using
CaO (gypsum,
complexometric titration
cigarette paper,
CP)
HH
HH
HH
HH
Individual testing method of sum parameters
Standard/issue date
In-house
method/version
Ph.Eur. USP<643>,
Paragraph. 2.2.44
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
TOC and DOC determination
Test object
Site
Ultra-pure water HH
Individual testing methods of non-specific cultivation techniques
Standard/issue date
In-house
method/version
Ph.Eur. Paragraph
2.6.14
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
Bacteria endotoxins
Test object
Site
Solids for the
pharmaceutical
industry
HH
Test object
Site
Individual testing methods of specific cultivation techniques
Standard/issue date
In-house
Analyte – Title of the standard
Information on sample pre-treatment/testing
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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method/version
technology
Ph.Eur. Paragraph
2.6.13
Microbiological testing of non-sterile products:
Detection of specified microorganisms
Ph.Eur. Paragraph
2.6.12
Microbiological testing of non-sterile products:
Enumeration of replicable microorganisms
Ph.Eur. Paragraph
2.6.31
Microbiological testing of oral herbal medicines
Solids for the
pharmaceutical
industry
Solids for the
pharmaceutical
industry
Plant-based raw
materials
HH
Test object
Site
Solids for the
pharmaceutical
industry
GE
HH
HH
Individual testing method of IR spectroscopy
Standard/issue date
In-house
method/version
In-house method
GE-MA M-P 16-1
2011-05
Analyte – Title of the standard
Information on sample pre-treatment/testing
technology
IR spectrum: Recording and comparison with
reference spectra (FT-IR)
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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6
Testing methods for the water subject module
Notes:
Sew:
relevant to sewage (incl. landfill leachate)
Sur:
relevant to surface water
Grw:
relevant to untreated water and groundwater
Minimum size of the investigation parameters
Parameter is accredited
Sub-section 1: Sampling and general parameters
Parameters
Method
Sewage sampling
DIN 38402 - A 11 : 1995-12
PI, HI, GE, HM
Sampling from flowing waters
DIN 38402 - A 15 : 1986-07
PI, GE, HI, HM,
FG
Sampling from aquifers
DIN 38402 - A 13 : 1985-12
PI, HI, GE, HM,
FG
Sampling from stagnant bodies of water
DIN 38402 - A 12 : 1985-06
PI, HI, GE, HM,
FG
Homogenisation of samples
DIN 38402 - A 30 : 1998-07
PI, HI, GE, HM,
FG
Temperature
DIN 38404 - C 4: 1976-12
PI, HI, GE, HM,
FG
pH-value
DIN 38404 - C 5 : 1984-01
PI, HI, GE, HM,
FG
Conductivity (25 C)
DIN EN 27888: 1993-11 (C8)
PI, HI, GE, HM,
FG
Smell
DEV B 1/2: 1971-6 Delivery
PI, HI, GE, HM,
FG
Colouring
DIN EN ISO 7887: 1994-12 (C1)
section 2
PI, HI, GE, FG
Turbidity
DIN EN ISO 7027: 2000-04 (C2)
PI, HI
Redox potential
DIN 38404-C 6 : 1984-05
o
Sew
Sur
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
Grw Site
PI, HI, GE, HM,
FG
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Sub-section 2: Photometry, ion chromatography, measurement analysis
Parameters
Method
Sew
Sur
UV absorption at 254 nm (SAK 254)
DIN 38 404 – C3 : 1976-12
PI
UV absorption at 436 nm (SAK 436)
DIN EN ISO 7887: 1994-12 (C1)
PI
DIN EN ISO 11732: 1997-09 (E23)
Ammonium nitrogen
DIN 38406-E 5 - 1983-10
Grw Site
PI, GE
PI
DIN EN ISO 14911: 1999-12 (E34)
DIN 38406-E 23: 1993-12
Nitrite nitrogen
Nitrate nitrogen
Total phosphorus
Orthophosphate
DIN EN 26777: 1993-04 (D10)
PI
DIN EN ISO 10304-1:1995-04 (D19)
HE
DIN EN ISO 10304-2:1996-11 (D20)
HE
DIN EN ISO 13395: 1996-12 (D28)
PI
DIN EN ISO 10304-1:1995-04 (D19)
PI, HE
DIN EN ISO 10304-2:1996-11 (D20)
PI, HE
DIN EN ISO 13395: 1996-12 (D28).
PI
DIN 38405-D 9-2 / 9-3:1979-05
PI
DIN 38405-D 29: 1994-11
PI
DIN EN ISO 11885: 1998-04 (E22)
PI
DIN EN 1189: 1996-12 (D11)
PI
DIN EN ISO 10304-1: 1995-04 (D19)
PI, HE
DIN EN ISO 10304-2: 1996-11 (D20)
PI, HE
DIN EN 1189: 1996-12 (D11)
Fluoride (dissolved and total)
DIN 38405-D 4: 1985-07
DIN EN ISO 10304-1: 1995-04 (D19)
DIN 38405-D 1: 1985-12
Chloride
PI
PI, HE, FG
PI, HE
PI
DIN EN ISO 10304-1:1995-04 (D19)
PI, HE
DIN EN ISO 10304-2: 1996-11 (D20)
PI, HE
DIN EN ISO 10304-4: 1997-08 (D25)
DIN EN ISO 15682: 2002-01 (D31)
Sulphate
DIN EN ISO 10304-1: 1995-04 (D19)
PI, HE
DIN EN ISO 10304-2: 1996-11 (D20)
PI, HE
DIN 38405-D 5: 1985-01
Sulphite
DIN EN ISO 10304-3: 1997-11 (D22),
Section 5
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Parameters
Method
Sulphide (easily liberated)
DIN 38405-D 27: 1992-07
Cyanide (easily liberated)
Sew
Sur
Grw Site
PI, GE
DIN 38405-D 13-2: 1981-02
PI
DIN 38405-D 14-2: 1988-12
PI
DIN EN ISO 14403: 2002-07 (D6)
PI
DIN 38405-D7: 2002-04 (D7)
Cyanide (total)
DIN 38405-D 13-1: 1981-02
PI
DIN 38405-D 14-1: 1988-12
PI
DIN EN ISO 14403: 2002-07 (D6)
PI
DIN 38405-D7: 2002-04 (D7)
DIN 38405-D 24: 1987-05
Chromium VI
DIN EN ISO 10304-3: 1997-11 (D22)
section 5 (dissolved chromate)
Oxygen
DIN EN 25814 : 1992-11 (G22)
PI, GE
PI, GE, HM,
FG
Sub-section 3: Elemental analysis
Parameters
Method
Sew
Sur
DIN EN ISO 11885: 1998-04 (E22)
Aluminium
Grw Site
PI
DIN EN ISO 12020: 2000-05 (E25)
DIN 38406-E 29: 1999-05
PI
DIN EN ISO 15586: 2004-02 (E4)
DIN EN ISO 11969: 1996-11 (D18)
Arsenic
DIN EN ISO 11885: 1998-04 (E22)
PI
DIN 38406-E 29: 1999-05
PI
DIN EN ISO 15586: 2004-02 (E4)
DIN 38406-E 6: 1998-07
DIN EN ISO 11885: 1998-04 (E22)
Lead
PI
DIN 38406-E 16: 1990-03
DIN 38406-E 29: 1999-05
PI
DIN EN ISO 15586: 2004-02 (E4)
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
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Parameters
Method
Sew
Sur
Grw Site
DIN EN ISO 5961: 1995-05 (E19)
DIN EN ISO 11885: 1998-04 (E22)
Cadmium
PI
DIN 38406-E 16: 1990-03
DIN 38406-E 29: 1999-05
PI
DIN EN ISO 15586: 2004-02 (E4)
DIN EN ISO 11885: 1998-04 (E22)
PI
DIN 38406-E 3: 2002-03
Calcium
DIN EN ISO 7980:2000-07 (E3a)
DIN 38406-E 29: 1999-05
PI
DIN EN ISO 14911: 1999-12 (E34)
DIN EN ISO 11885: 1998-04 (E22)
PI
DIN EN 1233: 1996-08 (E10)
Chromium
DIN 38406-E 29: 1999-05
PI
DIN 38406-E 22: 1988-03
DIN EN ISO 15586: 2004-02 (E4)
DIN EN ISO 11885: 1998-04 (E22)
Iron
PI
DIN 38406-E 1: 1983-05
DIN 38406-E32: 2000-05
DIN EN ISO 15586: 2004-02 (E4)
DIN 38406-E 13: 1992-07
Potassium
DIN EN ISO 11885: 1998-04 (E22)
PI
DIN 38406-E 29: 1999-05
PI
DIN EN ISO 14911: 1999-12 (E34)
DIN EN ISO 11885: 1998-04 (E22)
PI
DIN 38406-E 7: 1991-09
Copper
DIN 38406- E 16: 1990-03
DIN 38406-E 29: 1999-05
PI
DIN EN ISO 15586: 2004-02 (E4)
Manganese
DIN EN ISO 11885: 1998-04 (E22)
PI
DIN 38406-E 29: 1999-05
PI
DIN 38406-E 33: 2000-06
DIN EN ISO 15586: 2004-02 (E4)
DIN EN ISO 14911: 1999-12 (E34)
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Appendix to the accreditation certificate D-PL-14170-01-00
DIN 38406-E 14: 1992-07
Sodium
DIN EN ISO 11885: 1998-04 (E22)
PI
DIN 38406-E 29: 1999-05
PI
DIN EN ISO 14911: 1999-12 (E34)
DIN EN ISO 11885: 1998-04 (E22)
PI
DIN 38406-E 11: 1991-09
Nickel
DIN 38406-E 29: 1999-05
PI
DIN 38406-E 16: 1990-03
DIN EN ISO 15586: 2004-02 (E4)
DIN EN 1483: 1997-08 (E12)
Mercury
PI
DIN EN 12338: 1998-10 (E31)
DIN EN 13506: 2002-04 (E35)
PI
DIN 38406-E 29: 1999-05
PI
DIN EN ISO 11885: 1998-04 (E22)
PI
DIN 38406-E 8-1: 1980-10
Zinc
DIN 38406-E 16: 1990-03
DIN 38406-E 29: 1999-05
PI
DIN EN ISO 15586: 2004-02 (E4)
DIN EN ISO 11885: 1998-04 (E22)
PI
According to DIN EN ISO 5961: 199505 (Section 3) (E19)
Tin
Boron
According to DIN EN ISO 11969: 199611 (D18)
(Digestion in accordance with
paragraph 8.3.1)
DIN 38406-E 29: 1999-05
PI
DIN EN ISO 11885: 1998-04 (E22)
PI
DIN 38405-D 17: 1981-03
DIN 38406-E 29: 1999-05
PI
DIN EN ISO 11885: 1998-04 (E22)
PI
DIN 38406-E 3: 2002-03
Magnesium
DIN EN ISO 7980:2000-07 (E3a)
DIN 38406-E 29: 1999-05
PI
DIN EN ISO 14911: 1999-12 (E34)
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
56/89
Appendix to the accreditation certificate D-PL-14170-01-00
Sub-section 4: Group and sum parameters (Part 1)
Parameters
Method
BOD5
DIN EN 1899-1 : 1998-05 (H51)
Sew
Sur
Grw Site
PI, GE
DIN 38409-H 41: 1980-12
COD
PI
DIN 38409-H44: 1992-05
DIN ISO 15705: 2003-01 (H45)
PI, HI, GE,
FG
Low volatile lipophilic substances
DEV H56 (46nd delivery 2000)
PI, HI, GE
Phenol index
DIN 38409-H 16: 1984-06
(with and without distillation)
DIN EN ISO 14402: 1999-12 (H37)
Filtrable substances
PI
PI, GE
PI, HI, GE,
FG
DIN 38409-H 2 : 1987-03
DIN EN 872 : 1996-03 (H33)
Acid and base capacity
PI, HI
PI, HI, GE,
FG
DIN 38409-H 7 : 2004-03
Sub-section 5: Group and sum parameters (Part 2)
Parameters
Method
Sew
Sur
Grw Site
TOC
DIN EN 1484 : 1997-08 (H3)
PI, GE
DOC
DIN EN 1484 : 1997-08 (H3)
PI, GE
DIN ENV 12260: 1996-06 (H 34)
Total bound nitrogen (TNB)
Hydrocarbons
AOX
DIN EN 12260: 2003-12 (H 34)
GE
DIN 38409-H 27: 1992-07
DIN EN ISO 11905-1: 1998-08 (H36)
PI
DIN EN ISO 9377-2: 2001-07 (H53)
PI, HI, GE
DIN EN 1485: 1996-11 (H14)
PI, GE
DIN 38409-H22: 2001-02
GE
Sub-section 6: Gas chromatographic method
Method
Volatile halogenated hydrocarbons
DIN EN ISO 10301 : 1997-08 (F4)*
PI, HI
Benzene and derivatives
DIN 38407-F 9 : 1991-05*
PI, HI
DIN EN ISO 6468 : 1997-02 (F1)*
PI, HI
Organochlorine insecticides
Sew
Sur
Grw Site
Parameters
DIN 38407-F2: 1993-02*
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Appendix to the accreditation certificate D-PL-14170-01-00
Parameters
Method
Sew
Sur
PI, HI
DIN EN ISO 6468: 1997-02 (F1)*
Polychlorinated biphenyls
DIN 38407-F2: 1993-02*
DIN 38407-F3: 1998-07
Mono-, dichlorbenzenes
Grw Site
PI, HI, GE
DIN EN ISO 10301: 1997-08 (F4)*
PI, HI
DIN EN ISO 6468 : 1997-02 (F1)*
PI, HI
DIN 38407-F 2 : 1993-02*
PI, HI
Chlorophenols
DIN EN ISO 12673 : 1999-05 (F15)
PI, HI
Organophosphorous and organic
nitrogen compounds
DIN EN ISO 10695: 2000-11 (F6)*
PI
Tri- to hexachlorobenzene
* Mass spectrometric detection permissible
Sub-section 7: HPLC method
Parameters
Polycyclic aromatic hydrocarbons
Plant treatment agents
Method
Sew
Sur
Grw Site
DIN 38407-F 18 : 1999-05
HI
DIN EN ISO 17993: 2004-03
HI
DIN EN ISO 11369 : 1997-11 (F12)*
HM
* Mass spectrometric detection permissible
Sub-section 8: Microbiological method
Parameters
Method
Colony count
DIN EN ISO 6222 : 1999-07 (K5)
Total coliform count
Faecal coliform count
Intestinal enterococci
**
Sew
Sur
Grw Site
HH, HM
DIN 38411- K 6 : 1991-06 **
DIN EN ISO 9308-1: 2001-07 (K12)
HH, WOB
DIN EN ISO 9308-1: 2001-07 (K12)
HH, WOB
DIN EN ISO 9308-3: 1999-07 (K13)
DIN EN ISO 7899-2: 2000-11 (K15)
HH, WOB
DIN EN ISO 7899-1: 1999-07 (K14)
Only in conjunction with DIN EN ISO 9308-1 : 2001-07
Sub-section 9: Biological method, Biotests
Parameters
Method
Saprobic index
DIN 38410-M 2 : 1990-10
Chlorophyll a
DIN 38412-L 16 : 1985-12
Phaeophytin
DIN 38416-L 16 : 1985-12
Fish toxicity (egg)
DIN 38415-T6: 2003-08
Sew
Sur
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
Grw Site
58/89
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Parameters
Method
Sew
Sur
Grw Site
DIN 38412 L34: 1997-07 in conjunction
with DIN 38412-L34-1: 1993-10
Luminescent bacteria inhibition test
DIN EN ISO 11348-1: 1999-04 (L34-1)
DIN EN ISO 11348-2: 1999-04 (L34-2)
GE
DIN EN ISO 11348-3: 1999-04 (L34-3)
Daphnia test
DIN 38412-L 30 : 1989-03
Algae test
DIN 38412-L 33 : 1991-03
Umu test
DIN 38415-T3: 1996-12
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
GE
59/89
Appendix to the accreditation certificate D-PL-14170-01-00
7
Testing methods for the soil and contaminated sites subject module
Minimum size of the investigation parameters
Parameter is accredited
Testing area 1: Solids, inorganic parameters
Investigation parameters
Procedure
Method
Acc. Site
Sampling
Manual drilling
Sampling in the investigation
of areas with suspected
contamination and
contaminated sites
DIN 19761 sheet 1; 1964
ISO 10381-2, 2002-11 *
Ramming core sampling
DIN 4021, 10.90
Samples in undisturbed
bedding
ISO 10381-2, 2002-11
DIN 19672, Part 1; 1968
ISO 10381-2,
Edition: 2002-11 *
Sampling in the investigation
of natural, semi-natural and
cultural locations
Pedological mapping guide
4th Edition, 1994,
Reprinted 1996,
VDLUFA book of methods
Volume 1
DIN ISO 10381-3, 2002-08 *
Occupational safety during
sampling
ZH 1/183: 1997
On-site
Pedological mapping guide
Grain-size distribution
Finger test in
the field *
4th edition, 1994,
reprinted 1996
DIN 19682-2: 04.97
Laboratory
Sample pre-treatment,
sample preparation
DIN ISO 11464; 12.96
PI, HI, GE,
FG
Dry matter
Soil samples fresh from the
DIN ISO 11465; 12.96
field or air-dried
PI, HI, GE,
FG
Organic and total carbon
after dry combustion
Air-dried soil samples
pH-value (CaCl2)
Soil samples fresh from the
field or air-dried, c(CaCl2): DIN ISO 10390; 05.97
0.01 mol/l
DIN ISO 10694; 08.96
PI, GE
PI, HI, GE,
FG
* Cannot be used on contaminated sites out of consideration for occupational safety.
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
60/89
Appendix to the accreditation certificate D-PL-14170-01-00
Investigation parameters
Procedure
1) Screening, dispersion,
pipette-analysis
Grain-size distribution
2) Screening, dispersion,
areometer method
Method
DIN ISO 11277, 2002-08 *
DIN 18123; 11.96
DIN ISO 11277, 2002-08 *
Drying of a soil sample
DIN ISO 11272, 2001-01 *
taken in the proper volume
o
at 105 C, back weighing
DIN 19683-12; 04.73
Aqua-regia extract
from ground samples
(particle size < 150 µm)
Arsenic (As)
Extraction with aqua regia
Cadmium (Cd)
Extraction with aqua regia
Chromium (total)
Chromium (VI)
Extraction with aqua regia
PI
DIN 19683-2; 04.97
Bulk density
Ammonium nitrate extract
Acc. Site
PI, GE
PI
PI, GE
DIN ISO 11466; 06.97
PI, HI
DIN 19730: 06.97
ICP – AES
DIN EN ISO 11885; 04.98
ICP – MS
DIN 38406-29 ; 05.99
ET – AAS
in analogy to
E DIN ISO 11047; 06.95
Hydride AAS
DIN EN ISO 11969; 11.96
AAS
ISO 11047,1998-05 *
ICP – AES
DIN EN ISO 11885; 04.98
ICP – MS
DIN 38406-29 ; 05.99
AAS
ISO 11047,1998-05 *
ICP – AES
DIN EN ISO 11885; 04.98
ICP – MS
DIN 38406-29 ; 05.99
PI, HI
Extraction with phosphateSpectrophotometry
buffered aluminium
DIN 19737; 01.99
sulphate solution
PI
PI
PI
PI
PI
PI
PI
* Cannot be used on contaminated sites out of consideration for occupational safety.
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
61/89
Appendix to the accreditation certificate D-PL-14170-01-00
Copper (Cu)
Nickel (Ni)
Lead (Pb)
Extraction with aqua regia
Extraction with aqua regia
Extraction with aqua regia
AAS
ISO 11047,1998-05 *
ICP – AES
DIN EN ISO 11885; 04.98
ICP – MS
DIN 38406-29; 05.99
AAS
ISO 11047,1998-05 *
ICP – AES
DIN EN ISO 11885; 04.98
ICP – MS
DIN 38406-29; 05.99
AAS
E DIN ISO 11047; 06.95
ICP-AES
DIN EN ISO 11885; 04.98
ICP-MS
DIN 38406-29; 05.99
Zinc (Zn)
Cyanide
PI
PI
PI
PI
PI
AAS
E DIN ISO 11047: 06.95
ICP-AES (ICP-MS possible)
DIN EN ISO 11885: 04.98
PI
AAS – Cold vapour
technique extraction with
aqua regia Drying
temperature must not
o
exceed 40 C
DIN EN 1483; 08.97
Reduction with Sn(II) chloride
or NaBH4
PI
Thallium (Tl)
Mercury (Hg)
PI
Extraction with aqua regia
AAS
ISO 11047,1998-05 *
ICP-AES
DIN EN ISO 11885; 04.98
ICP-MS
DIN 38406-29; 05.99
(Draft standard) ISO/DIS
11262, 1999-02 *
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
PI
PI
PI
62/89
Appendix to the accreditation certificate D-PL-14170-01-00
Testing area 2: Solids, organic parameters
Investigation parameters
Procedure
Method
Acc. Site
Sampling
Manual drilling
Sampling in the investigation
of areas with suspected
contamination and
contaminated sites
DIN 19761 sheet 1; 1964
ISO 10381-2, 2002-11 *
Ramming core sampling
DIN 4021, 10.90
Samples in undisturbed bedding
ISO 10381-2, 2002-11 *
DIN 19672, Part 1; 1968
ISO 10381-2, 2002-11 *
Pedological mapping
guide
4th edition, 1994,
reprinted 1996,
VDLUFA book of methods
Volume 1
Sampling in the investigation
of natural, semi-natural and
cultural locations
DIN ISO 10381-3
Occupational safety during
sampling
ZH 1/183: 1997
On-site
Grain-size distribution
Finger test in the field *
Pedological mapping
guide
4th edition, 1994,
reprinted 1996,
E DIN 19582-2; 05.95
Laboratory
Sample handling,
Sample preparation
E DIN ISO 14507; 02.96
Dry matter
Soil samples fresh from the field
or air-dried (parallel)
DIN ISO 11465; 12.96
Organic and total carbon
after dry combustion
Air-dried soil samples
DIN ISO 10694; 08.96
pH-value (CaCl2)
Grain-size distribution
Soil samples fresh from the field
DIN ISO 10390; 05.97
or air-dried, c(CaCl2): 0.01 mol/l
1) Screening, dispersion, pipette- DIN ISO 11277, 2002-08 *
analysis
DIN 19683-2; 04.97
DIN
18123; 11.96
2) Screening, dispersion,
areometer method
PI, HI, GE,
FG
PI, HI, GE,
FG
PI, GE
PI, HI, GE,
FG
PI, GE
E DIN ISO 11277; 06.94
* Cannot be used on contaminated sites out of consideration for occupational safety.
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
63/89
Appendix to the accreditation certificate D-PL-14170-01-00
Bulk density
Polycyclic aromatic
hydrocarbons (PAH)
16 PAH (EPA)
Benzo[a]pyrene
Note:
Acenaphthylene cannot be
determined using a
fluorescence detector
Hexachlorobenzene
Pentachlorophenol
Aldrin, DDT, HCH-mix
Drying of a soil sample taken in
o
the proper volume at 105 C,
back weighing
1) Soxhlet extraction with
acetone/toluene or
acetone/cyclohexane,
chromatographic clean-up
2) Extraction with
tetrahydrofuran or acetonitrile
DIN ISO 11272, 2001-01 *
PI, GE
DIN 19683; 04.73
GC-MS
Leaflet no 1. of LUA NRW,
1994
HPLC-UV/DAD/F*
Leaflet no 1. of LUA NRW, 1994*
3) Extraction with acetone,
addition of petroleum ether,
HPLC-UV/F
removal of acetone,
DIN ISO 13877, 2000-01 *
chromatographic clean-up of the
petroleum ether extract, take-up GC-MS, HPLC-UV/DAD/F
in acetonitrile
VDLUFA book of
4) extraction with a
methods, Vol. VII, 3.3.3.1
water/acetone/petroleum etherManual Contaminated
mix in the presence of NaCl
Sites, Vol. 7, LfU Hesse
Extraction with acetone/
cyclohexane-mix or
acetone/petroleum ether, if
GC-ECD, GC-MS
applicable chromatographic
E DIN ISO 10382; 02.98
clean-up after removal of the
acetone
Soxhlet-extraction with heptane
or acetone/heptane (50:50);
GC-ECD, GC-MS
Derivatisation with acetic
E DIN ISO 14154; 10.97
anhydride
1) Extraction with petroleum
GC-ECD, GC-MS
ether or acetone/petroleum
ISO 10382, 2002-10 *
ether-mix, chromatographic
clean-up
GC-ECD, GC-MS
2) Extraction with
water/acetone/petroleum ether- VDLUFA book of methods
Vol. VII, 3.3.2
mix
PI, HI, GE
HI
HI
PI, HI
PI, HI
PI, HI
* Cannot be used on contaminated sites out of consideration for occupational safety.
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Appendix to the accreditation certificate D-PL-14170-01-00
PCB
Extraction with heptane or
acetone/petroleum ether,
chromatographic clean-up
Soxhlet-extraction with heptane,
hexane or pentane,
chromatographic clean-up on
AgNO3/silicic acid Extraction
with a water/acetone/petroleum
ether-mix in the presence of
NaCl
ISO 10382, 2002-10 *
PI, HI
DIN 38414-20: 01.96
PI, GE
VDLUFA book of methods
Vol. VII, 3.3.2
Testing area 3: Solids, dioxins and furans
Investigation parameters
Procedure
Method
Acc. Site
Sampling
Manual drilling
Sampling in the investigation
of areas with suspected
contamination and
contaminated sites
DIN 19761 sheet 1; 1964
ISO 10381-2, 2002-11 *
Ramming core sampling
DIN 4021, 10.90
Samples in undisturbed
bedding
ISO 10381-2, 2002-11 *
DIN 19672, Part 1; 1968
ISO 10381-2, 2002-11 *
Pedological mapping guide
4th edition, 1994, reprinted
1996,
Sampling in the investigation
of natural, semi-natural and
cultural locations
VDLUFA book of methods
Volume 1
DIN ISO 10381-3
Occupational safety during
sampling
ZH 1/183: 1997
On-site
Pedological mapping guide
Grain-size distribution
Finger test in the field *
4th edition, 1994, reprinted
1996,
E DIN 19582-2; 05.95
Laboratory
Sample treatment, sample
preparation
Dry matter
Soil samples fresh from the
field or air-dried (parallel)
E DIN ISO 14507; 02.96
PI, HI, GE
DIN ISO 11465; 12.96
PI, HI, GE,
FG
* Cannot be used on contaminated sites out of consideration for occupational safety.
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
65/89
Appendix to the accreditation certificate D-PL-14170-01-00
Investigation parameters
Procedure
Method
Organic and total carbon
after dry combustion
Air-dried soil samples
pH-value (CaCl2)
Soil samples fresh from the
(Draft standard) DIN ISO
field or air-dried, c(CaCl2): 0.01
10390, 2002-11 *
mol/l
Grain-size distribution
1) Screening, dispersion,
pipette-analysis
2) Screening, dispersion,
areometer method
Bulk density
Polychlorinated
dibenzodioxins and
dibenzofurans
DIN ISO 10694; 08.96
Acc. Site
PI, GE
PI, HI, GE
DIN ISO 11277, 2002-08 *
DIN 19683-2; 04.97
DIN 18123; 11.96
PI, GE
DIN ISO 11277, 2002-08 *
Drying of a soil sample taken in DIN ISO 11272, 2001-01 *
o
the proper volume at 105 C,
DIN 19683; 04.73
back weighing
GC-MS in accordance with
the Sewage Sludge
Freeze-dried samples, Soxhlet- Ordinance in consideration
of
extraction of samples fresh
DIN 38414-24, 2000-10 *
from the field with toluene,
internal standard,
VDI guideline 3499, sheet
chromatographic clean-up
1: 03.90
GC-MS with internal
standard
PI, GE
PI
PI
PI
Testing area 4: Groundwater, leachate, surface water
Investigation parameters
Method
Acc. Site
Sampling
Sampling of ground water
DIN EN ISO 25667, Part 2; 1993-07
PI, GE,
HM, FG
DIN 38402-13; 1985-12
PI, GE,
HM, HI,
FG
German working group on water (LAWA): Groundwater
directive, Part 3; 03.93
AQS leaflet P 8/2; 01.96
PI, GE,
HM, HI,
FG
German association for water management and land
improvement (DVWK): DVWK rules 128/92
DVWK leaflet 245/1997
Sampling of leachate
Currently no standardised method available
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
PI, GE,
HM, HI
66/89
Appendix to the accreditation certificate D-PL-14170-01-00
Investigation parameters
Method
DIN 38402-15; 07.86
Sampling of surface waters
(flowing waters)
AQS leaflet P 8/3; 05.98
Sampling of surface water
(stagnant bodies of water)
DIN 38402-12; 06.85
Acc. Site
PI, GE,
HM, HI,
FG
PI, GE,
HM, HI,
FG
PI, GE,
HM, HI,
FG
On-site
Temperature
DIN 38404-4; 12.76
pH-value
DIN 38404-5; 01.84
Oxygen content
DIN EN 25814; 11.92
Electrical conductivity
DIN EN 27888; 11.93
PI, GE,
HM, HI,
FG
PI, GE,
HM, HI,
FG
PI, GE,
HM, HI,
FG
PI, GE, HI,
FG
Laboratory
Elution method 1 (soil
saturation extract)
Elution method 2 (modified
S4 method)
Elution method 3 (column
or lysimeter test)
Antimony (Sb)
According to the specifications of the BBodSchV (annex 1,
3.1.2)
DIN 38414-4; 10.84 taking account of the procedural
directions of the BBodSchV (annex 1, 3.1.2)
Currently no standardised method available; possibilities for
carrying out column or lysimeter tests must be verified in
accordance with up-to-date analytics
PI, HI GE
PI, HI GE
HI
ICP-AES in accordance with DIN EN ISO 11885; 04.98
PI
ICP-MS DIN 38406-29; 05.99
PI
Hydride-AAS E DIN 38405-32; 11.96
Arsenic (As)
ICP-AES in accordance with DIN EN ISO 11885; 04.98
PI
ICP-MS DIN 38406-29; 05.99
PI
Hydride-AAS DIN EN ISO 11969; 11.96
Lead (Pb)
ICP-AES in accordance with DIN EN ISO 11885; 04.98
PI
ICP-MS DIN 38406-29; 05.99
PI
AAS E DIN 38406-6; 06.97
Cadmium (Cd)
ICP-AES in accordance with DIN EN ISO 11885; 04.98
PI
ICP-MS DIN 38406-29; 05.99
PI
AAS DIN EN ISO 5961; 05.95
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
67/89
Appendix to the accreditation certificate D-PL-14170-01-00
Chromium (Cr), total
ICP-AES in accordance with DIN EN ISO 11885; 04.98
PI
ICP-MS DIN 38406-29; 05.99
PI
AAS DIN EN 1233; 08.96
Chromium (Cr VI)
Spectrophotometry DIN 38405-24; 05.87
Ion chromatography DIN EN ISO 10304-3; 11.97
PI
ICP-AES in accordance with DIN EN ISO 11885; 04.98
PI
Cobalt (Co)
AAS DIN 38406-24; 03.93
Copper (Cu)
ICP-AES in accordance with DIN EN ISO 11885; 04.98
PI
ICP-MS DIN 38406-29; 05.99
PI
AAS DIN 38406-7; 09.91
ICP-AES in accordance with DIN EN ISO 11885; 04.98
PI
ICP-MS DIN 38406-29; 05.99
PI
ICP-AES in accordance with DIN EN ISO 11885; 04.98
PI
ICP-MS DIN 38406-29; 05.99
PI
Molybdenum (Mo)
Nickel (Ni)
AAS DIN 38406-11; 09.91
Mercury (Hg)
Selenium (Se)
AAS – cold vapour technique DIN EN 1483; 08.97
PI
ICP-AES in accordance with DIN EN ISO 11885; 04.98
PI
ICP-MS DIN 38406-29; 05.99
PI
AAS DIN 38405-23; 10.94
Zinc (Zn)
ICP-AES in accordance with DIN EN ISO 11885; 04.98
PI
ICP-MS DIN 38406-29; 05.99
PI
AAS DIN 38406-8; 10.80
ICP-AES in accordance with DIN EN ISO 11885; 04.98
PI
ICP-MS DIN 38406-29; 05.99
PI
Spectrophotometry DIN 38405-13; 02.81
PI
Tin (Sn)
Cyanide, total
DIN EN ISO 14403, 2002-07 *
PI, GE
-
Cyanide (CN ), easily
liberated
Spectrophotometry DIN 38405-13; 02.81
PI
Fluoride selective electrode DIN 38405-4; 07.85
PI, HE, FG
Ion chromatography DIN EN ISO 10304-1; 04.95
PI, HE
BTEX
GC-FID DIN 38407-9; 05.91 (observe matrix loading)
PI, HI
Volatile halogenated
hydrocarbons (VHH)
GC-ECD DIN EN ISO 10301; 08.97
PI, HI
Aldrin
GC-ECD, GC-MS possible DIN 38407-2; 02.93
PI, HI
DDT
GC-ECD, GC-MS possible DIN 38407-2; 02.93
PI, HI
Phenols
ISO 8165-2, 1999-07 *
-
Fluoride (F )
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
PI
68/89
Appendix to the accreditation certificate D-PL-14170-01-00
Chlorophenols
GC-ECD, GC-MS E DIN EN 12673; 02.97
PI, HI
Chlorobenzenes
GC-ECD, GC-MS possible DIN 38407-2; 02.93
PI, HI
Polychlorinated biphenyls
(PCB): 6 PCB-congeners
(No. 28, 52, 101, 138, 163,
180 in accordance with
Ballschmiter)
GC-ECD, GC-MS DIN 38407-2; 02.93
E DIN 38407-3; 10.95
HI
16 PAH (EPA)
HPLC-F DIN 38407-18; 05.99
HI
Naphthalene
GC-FID, GC-MS DIN 38407-9; 05.91
Mineral oil hydrocarbons
Extraction with petroleum ether; gas chromatographic
determination in accordance with ISO/TR 11064; 06.94
PI, HI, GE
PI, HI
PI
Testing area 5: Soil gas, landfill gas
Method
Investigation parameters
Acc. Site
Sampling
Association of German engineers (VDI)
PI, GE
Sampling of soil gas
VDI guideline 3865, sheet 2, section 4.4.3
VDI guideline 3865, sheet 2, section 4.4.4
VDI guideline 3865, sheet 2, section 4.4.5
PI, GE
On-site
Carbon dioxide (CO2)
direct-reading measurement device
GE
Methane (CH4)
direct-reading measurement device
GE
Hydrogen sulphide (H2S)
direct-reading measurement device
GE
Oxygen (O2)
direct-reading measurement device
GE
Sum parameters trace gases
direct-reading measurement device
GE
Laboratory
BTEX
VDI guideline 3865, sheet 3, section 3.2
PI
Volatile halogenated
hydrocarbons (VHH)
VDI guideline 3865, sheet 3, section 3.2
PI
Testing area 6: Dry and wet deposition
Investigation parameters
Procedure
Method
Acc. Site
Sampling
Particulate precipitation
Sampling of rainwater
Bergerhoff device
(Standard method)
Collection device ARS 721
VDI 2119, sheet 2; 09.96
VDI 3870, sheet 10; 12.96
Laboratory
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Appendix to the accreditation certificate D-PL-14170-01-00
Investigation parameters
Procedure
Method
Acc. Site
Dust precipitation
Be, Cd, Co, Cr, Cu, Fe, Mn,
VDI 2267, sheet 5; 12.96
Ni, Pb, Sb, V, Zn
Thallium
VDI 2267, sheet 7; 11.88
PI
Lead and cadmium
VDI 2267, sheet 4; 03.87
Rainwater
VDI 3870, sheet 10; 12.96
pH-value
For low-iron water
DIN 38404-C5; 01.84
PI, GE
VDI 3870, sheet 11; 12.96
Chloride, nitrate, sulphate
DIN EN ISO 10304-1; 04.95
PI, HE
Chloride
Titrimetric
DIN 38405-D1; 12.85
PI
Nitrate
Photometric
DIN 38405-D9; 05.79
PI
Free acidity
Gran method
VDI 3870, sheet 11; 12.96
Alkalinity
Titrimetrically or
potentiometrically in
accordance with the Gran
method or using two-point
titration (pH 4.5 / pH 8.3)
DIN EN ISO 9963-1; 02.96
PI
PI, GE,
HM, FG,
HI
electrical conductivity
DIN EN 27888; 11.93
TOC
DIN 38409-H3-1; 06.83
Ntotal
DIN EN 12260, 2002-05 *
GE
Photometric molybdenum
blue method
DIN EN 1189; 12.96
PI
Ion chromatography
DIN EN ISO 10304-1; 04.95
HE
DIN 38406-E5-1; 10.83
PI
DIN 38406-E23-1; 12.93
PI, GE
PO4- P
NH4
PI, GE
DIN 38406-E13 1992-07
Na, K
DIN 38406-E14 1992-07
Ca, Mg
DIN 38406-E3-1; 09.82
Hg
DIN EN 12338 (E31), 07.98
* Cannot be used on contaminated sites out of consideration for occupational safety.
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
70/89
Appendix to the accreditation certificate D-PL-14170-01-00
Investigation parameters
Procedure
Al, Na, K, Ca, Mg, Mn, Fe, Cu,
Zn, Pb, Co, Cd, Mo, S, Cr, Ni,
Ptotal
Method
Acc. Site
DIN EN 1483, 08.97
PI
DIN 38406-E22; 03.88
PI
DIN EN ISO 11885 (E22),
1998-04
PI
Testing area 7: Forest soil investigations
Investigation parameters
Procedure
Method
Acc. Site
Sampling
BMELF (ed.): Nationwide
forest soil condition survey
(BZE) – instructions; 2nd
edition, Bonn 1994
Section C, pages 13-68
Section D, pages 69-87
BMELF (ed.): Permanent
observation plots for
environmental monitoring in
the forest, Level II – method
guidelines; 1st edition, Bonn
1997
Sampling of soil, humus,
peat
Laboratory
Corg.
DIN ISO 10694: 08.96
PI, GE
E DIN ISO 13878, 1998-11 *
N
Kjeldahl elemental analyser
DIN ISO 11261, 1997-05
PI
VDLUFA book of methods
Vol. II,
A 2.2.1; 1991
PI
BZE 2.1.5, p. 97 ff
VDLUFA book of methods
Vol. II,
A 13.2.1; 1991
Dry space density
(H2O)
BZE 2.2.1, p. 101 or
(KCl)
DIN ISO 10390: 05.97
pH-value
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
PI, HI, GE,
FG
71/89
Appendix to the accreditation certificate D-PL-14170-01-00
Investigation parameters
Effective cation-exchange
capacity (CECe)
Procedure
NH4Cl
Potential cation-exchange
capacity (CECpot)
Aqua regia digestion
Total digestion for humus
HNO3/HF pressure digestion
and mineral soil
Al, Ca, Fe, Mg, Mn, P, S, Zn
Pb, Cd, Cr, Co, Cu, Mn, Ni, Zn
As
Na
Method
Acc. Site
BZE 2.2.2, p. 101 ff
Note: the BaCl2 method
described in DIN ISO 11260
leads to completely different
results and is not
recommended for the
forestry sector in Germany
DIN ISO 13536, 1997-04
DIN ISO 11466, 1997-06 or
PI, HI
VDLUFA book of methods
Vol. VII,
2.1.2; 1996
PI, HI
BZE 1.2.5, p. 92 ff
DIN 38406-E22; 03.88
PI
DIN 38406-E22; 03.88 or
PI
DIN ISO 11047; 05.98
DIN EN ISO 11969, 11.96
DIN 38406-E22; 03.88 or
PI
DIN ISO 9964-3, 1996-08
Testing area 8:
Investigations for the assessment of terrestrial eco-toxicity of pollutants: not used
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
72/89
Appendix to the accreditation certificate D-PL-14170-01-00
8
Testing methods for the waste subject module
Notes:
Parameter is accredited
Minimum size of the investigation parameters
Testing area 1: Sewage sludge
Sub-sections/
Basis/
Parameters
Method
1.1
Sampling
Appendix 1
1.2
Heavy metals
§ 3 Paragraph 5 AbfKlärV
Aqua regia digestion
DIN 38414 Part 7 (01.83)
DIN EN 13346 (04.01)
Lead (from aqua regia digestion)
Accr. Site
PI, GE, HI
PI
PI, HI
DIN 38406, Part 6 (05.81)
DIN 38406 Part 22 (03.88)
PI
DIN EN ISO 11885 (04.98)
PI
DIN 38406 Part 6 (07.98)
Cadmium (from aqua regia digestion)
DIN 38406 Part 19 (07.80)
DIN 38406, Part 22 (03.88)
PI
DIN EN ISO 11885 (04.98)
PI
DIN EN ISO 5961 (05.95)
Chromium (from aqua regia digestion)
DIN 38406 Part 10 (06.85)
DIN 38406, Part 22 (03.88)
PI
DIN EN ISO 11885 (04.98)
PI
DIN EN 1233 (08.96)
Copper (from aqua regia digestion)
DIN 38406 Part 22 (03.88)
PI
DIN 38406 Part 7 (09.91)
Nickel (from aqua regia digestion)
DIN EN ISO 11885 (04.98)
PI
DIN 38406 Part 22 (03.88)
PI
DIN 38406 Part 11 (09.91)
Mercury (from aqua regia digestion)
DIN EN ISO 11885 (04.98)
PI
DIN 38406 Part 12 (07.88)
PI
DIN EN 1483 (08.97)
PI
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
73/89
Appendix to the accreditation certificate D-PL-14170-01-00
Zinc (from aqua regia digestion)
1.3
1.4
DIN 38406 Part 8 (10.80)
DIN 38406 Part 22 (03.88)
PI
DIN EN ISO 11885 (04.98)
PI
Adsorbed organically bound halogens
§ 3 Paragraph 5 AbfKlärV
AOX (from dry residue)
DIN 38414 Part 18 (11.89)
Physical parameters, nutrients
§ 3 Paragraph 5 AbfKlärV
Dry residue
DIN 38414 Part 2 (11.85)
GE
PI, GE, FG,
HI
DIN EN 12880 (02.01)
PI, GE
Organic matter
as loss on ignition (from dry residue)
DIN 38414 Part 3 (11.85)
PI, GE
DIN EN 12879 (02.01)
PI, HI, GE
pH-value
DIN 38414 Part 5 (09.81)
PI, HI, GE
DIN EN 12176 (06.98)
PI, HI, GE
Aqua regia digestion
DIN 38414 Part 7 (01.83)
DIN EN 13346 (04.01)
Basic active substances as CaO
Ammonium nitrogen (NH4-N)
Total nitrogen (Ntotal)
P2O5 (from aqua regia digestion)
K2O (from aqua regia digestion)
Appendix 1 AbfKlärV
Calculation according to:
% CaO = (50-x-2y)* 1.402
DIN 38406 Part 5 (10.83)
DIN 19684 Part 4 (02.77)
Distillation method
DIN ISO 11261b (05.97)
PI
PI, HI
PI
PI
PI
DIN 38 414 Part 12 (11.86)
DIN 38 406 Part 22 (03.88)
PI
DIN EN ISO 11885 (04.98)
PI
DEV E13 (5th del. 68)
DIN 38406 Part 22 (03.88)
PI
DIN EN ISO 11885 (04.98)
PI
DIN 38406 Part 13 (07.92)
Magnesium (from aqua regia digestion)
DIN 38 406 Part 3 (09.82)
DIN 38 406 Part 22 (03.88)
PI
DIN EN ISO 11885 (04.98)
PI
DIN EN ISO 7980 (07.00)
1.5
Persistent organic pollutants:
§ 3 Paragraph 6 AbfKlärV
PCB
Appendix 1, no. 1.3.3.1
AbfKlärV
DIN 38 414 T20 (01.96)
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
PI
HI, GE
74/89
Appendix to the accreditation certificate D-PL-14170-01-00
1.6
PCDD/PCDF
PI
Appendix 1, no. 1.3.3.2
AbfKlärV
Testing area 2: Soil
2.1
Basis/
Parameters
Method
Sampling and sample preparation
§ 3 Paragraph 2 AbfKlärV
and
§9 BioAbfV
Appendix 1, no. 2.1
AbfKlärV
Appendix 1, no. 2.1
AbfKlärV
§ 3 Paragraph 2 AbfKlärV
§ 9 Paragraph 2 BioAbfV
DIN 38414 Part 7 (01.83)
PI, HI
DIN ISO 11466 (06.97)
PI, HI
Sampling
Sample preparation
2.2
Accr. Site
Sub-sections/
Heavy metals
Aqua regia digestion
Lead (from aqua regia digestion)
???
DIN 38406 Part 22 (03.88)
PI
DIN EN ISO 11885 (04.98)
PI
DIN 38406 Part 6 (07.98)
DIN ISO 11047 (05.03)
Cadmium (from aqua regia digestion)
DIN 38406, Part 22 (03.88)
PI
DIN EN ISO 11885 (04.98)
PI
DIN EN ISO 5961 (05.95)
DIN ISO 11047 (05.03)
Chromium (from aqua regia digestion)
DIN 38406, Part 22 (03.88)
PI
DIN EN ISO 11885 (04.98)
PI
DIN EN 1233 (08.96)
DIN ISO 11047 (05.03)
Copper (from aqua regia digestion)
DIN 38406 Part 22 (03.88)
PI
DIN EN ISO 11885 (04.98)
PI
DIN 38406 Part 7 (09.91)
DIN ISO 11047 (05.03)
Nickel (from aqua regia digestion)
DIN 38406 Part 22 (03.88)
PI
DIN EN ISO 11885 (04.98)
PI
DIN 38406 Part 11 (09.91)
DIN ISO 11047 (05.03)
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
75/89
Appendix to the accreditation certificate D-PL-14170-01-00
Accr. Site
Sub-sections/
Basis/
Parameters
Method
Mercury (from aqua regia digestion)
DIN 38406 Part 12 (07.88)
PI
DIN EN 1483 (08.97)
PI
DIN 38406 Part 22 (03.88)
PI
DIN EN ISO 11885 (04.98)
PI
Zinc (from aqua regia digestion)
DIN 38406 Part 8 (10.80)
DIN ISO 11047 (05.03)
Soil type
pH-value
2.3
DIN 18123 (1983)
PI, GE
DIN 18123 (1996)
PI, GE
VDLUFA book of methods I,
D2.1
DIN 19684 Part 1 (02.77)
DIN ISO 10390 (05.97)
PI
PI, HI, GE
PI, HI, GE,
FG
pH-value
VDLUFA book of methods I,
A 5.1.1
§ 3 Paragraph 4 AbfKlärV
§ 9 Paragraph 2 BioAbfV
DIN 19 684 T1 (02.77)
Clay content/soil type
DIN 18123 (1983)
PI, GE
DIN 18123 (1996)
PI, GE
Physical parameters, nutrients
PI, HI, GE
VDLUFA book of methods I,
PI
D2.1
)1
P2O5 CA/DL *
VDLUFA book of methods A
PI
2.1.1 or A 6.2.1.1
)1
K2O CA/DL *
VDLUFA book of methods A
PI
6.2.1.1 or A 6.2.1.1
)1
MgCaCl2 *2 *
VDLUFA book of methods
PI
6.2.4.1
)1
* Parameters are only part of the minimum scope of investigation in the event of notifications under AbfKlärV
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
76/89
Appendix to the accreditation certificate D-PL-14170-01-00
Testing area 3: Biowaste
Sub-sections/
Basis/
Parameters
Method
3.1
Sampling
3.2
Heavy metals
§ 4 Paragraph 5 BioAbfV
Appendix 3 BioAbfV
§ 4 Paragraph 5 BioAbfV
Aqua regia digestion
DIN 38414 Part 7 (01.83)
DIN EN 13657 (01.03)
Lead (from aqua regia digestion)
Accr. Site
PI
PI, HI
DIN 38406, Part 6 (05.81)
DIN 38406, Part 22 (03.88)
PI
DIN ISO 11047 (06.95)
DIN 38406 Part 6 (07.98)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 (04.98)
Cadmium (from aqua regia digestion)
PI
DIN EN ISO 5961 (05.95)
DIN 38406, Part 22 (03.88)
PI
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 (04.98)
Chromium (from aqua regia digestion)
PI
DIN EN 1233 (08.96)
DIN 38406, Part 22 (03.88)
PI
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 (04.98)
Copper (from aqua regia digestion)
PI
DIN 38406, Part 7 (09.91)
DIN 38406, Part 22 (03.88)
PI
DIN ISO 11407 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 (04.98)
Nickel (from aqua regia digestion)
PI
DIN 38406, Part 11 (09.91)
DIN 38406, Part 22 (03.88)
PI
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 (04.98)
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
PI
77/89
Appendix to the accreditation certificate D-PL-14170-01-00
Accr. Site
Sub-sections/
Basis/
Parameters
Method
Mercury (from aqua regia digestion)
DIN 38406, Part 12 (07.80)
PI
DIN EN 1483 (08.97)
PI
Zinc (from aqua regia digestion)
DIN 38406, Part 8 (10.80)
DIN 38406, Part 22 (03.88)
PI
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 (04.98)
3.3
Physical parameters, impurities
§ 4 Paragraph 5 BioAbfV
Dry residue
DIN ISO 11 465(12.96)
pH-value
VDLUFA book of methods
Vol. I, A 5.1.1
Salt content
organic matter as loss on ignition
(from dry residue)
Impurities (stones, glass, plastic, metal)
3.5
PI, HI, GE,
FG
PI
DIN ISO 10390 (05.97)
PI, HI, GE,
FG
Appendix 3 BioAbfV
PI, HI, GE
VDLUFA book of methods
PI, GE
DIN 19 684 Part 3 (02.77)
PI, GE
DIN 19 684 Part 3 (08.00)
PI, HI, GE
Appendix 3 BioAbfV, no.
1.3.3
PI
Federal Compost
Association methods book
for the analysis of compost
3.4
PI
PI, GE
Epidemics hygiene
§ 3 Paragraph 4 BioAbfV
Salmonella (product testing)
Appendix 2 BioAbfV
HH
Salmonella senftenberg W 775 (H2S-neg.) (process
testing)
Appendix 2 BioAbfV
HH
Phytohygiene
§ 3 Paragraph 4 BioAbfV
Germinable seeds and plant parts capable of budding
(product testing)
Appendix 2 BioAbfV
Plasmodiophora brassicae (clubroot) (product testing)
Appendix 2 BioAbfV
Tomato seeds (process testing)
Appendix 2 BioAbfV
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
PI, GE
78/89
Appendix to the accreditation certificate D-PL-14170-01-00
Testing area 4: Waste oil, insulating liquid
Sub-sections/
4.1
Basis/
Parameters
Method
Sampling
§ 5 Paragraph 2 AltölV /
Accr. Site
DIN 51750 Part 1 (08.83)
DIN 51750 Part 2 (03.84)
4.2
PCB, halogen (only in accordance with AltölV)
§ 5 Paragraph 2 AltölV /
Appendix 4 no. 3 DepV
PCB
DIN EN 12 766 Part 1
(11.00)
in conjunction with:
DIN EN 12 766 Part 2
(12.01)
Only for investigations in accordance with DepV:
IEC 61619 (04.97)
Total halogen (only for AltölV)
GE
EN 12766-1
GE
Annex 2, no. 3 AltölV
GE
Testing area 5: Waste to be deposited
Sub-sections/
Parameters
Basis/
Method
5.1
Sampling, sample preparation
Appendix 4 no. 2 DepV /
LAGA PN 98 (12.01) and
Appendix 4, no. 3.1.1 DepV
5.2
Sample preparation, general parameters
Appendix 4 no. 3 DepV
Digestion method (aqua regia)
E DIN EN 13657 (10.99)
Acc.
Site
GE, FG,
HI, PI
DIN EN 13657 (01.03)
DIN EN 13346 (04.01)
PI, HI
Production of eluates
DIN EN 12457-4 (01.03)
in conjunction with:
Appendix 4 no. 2.4 AbfAblV
PI, HI, GE,
FG
pH-value (soil quality)
DIN ISO 10390 (05.97)
PI, HI, GE,
FG
pH-value of eluate
DIN 38404-Part 5 (01.84)
PI, HI, GE,
FG
Conductivity of eluate
DIN EN 27888 (11.93)
PI, HI, GE,
FG
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
79/89
Appendix to the accreditation certificate D-PL-14170-01-00
Sub-sections/
Parameters
Basis/
Method
Dry residue (soil quality)
DIN ISO 11465 (12.96)
PI, HI, GE,
FG
E DIN EN 14346 (02.02)
GE
(Waste)
Acc.
Site
DIN EN 12880 (02.01)
PI, HI, GE,
FG
Water-soluble component of dry residue of original
substance determined from dry filtrate residue of
eluate
DIN 38409 Part 1-2 (01.87)
PI, HI, GE,
FG
Loss on ignition of dry residue of original substance
DIN 38414 Part 3 (11.85)
PI, GE, FG
DIN EN 12879 (02.01)
PI, HI, GE,
FG
Cyanide, total
Cyanide, easily liberatable (from eluate)
E DIN ISO 11262 (06.94)
PI
ISO 11262 (09.03)
PI
DIN 38405 Part 14-2 (12.88)
For sulphide-containing
waste:
PI
DIN 38405 Part 13-2 (02.81)
Fluoride (from eluate)
Ammonium nitrogen (from eluate)
5.3
DIN EN ISO 14403 (07.02)
PI
DIN 38405 Part 4-1 (07.85)
PI, HE, FG
DIN EN ISO 10304 (04.95)
PI, HE
DIN 38406 Part 5-1 (10.83)
PI
DIN EN ISO 11732 (09.97)
PI, GE
DIN EN ISO 11732 (05.05)
PI, GE
Arsenic and other heavy metals
Appendix 4 no. 3 DepV
Arsenic (from aqua regia digestion)
DIN EN ISO 11969 (11.96)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 (04.98)
Arsenic (from eluate)
PI
DIN EN ISO 11969 (11.96)
DIN EN ISO 11885 (04.98)
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
PI
80/89
Appendix to the accreditation certificate D-PL-14170-01-00
Sub-sections/
Parameters
Basis/
Method
Lead (from aqua regia digestion)
DIN ISO 11047 (06.95)
Acc.
Site
DIN ISO 11047 (05.03)
DIN 38406 Part 6 (07.98)
DIN EN ISO11885 (04.98)
Lead (from eluate)
PI
DIN 38406 Part 2 (07.98)
DIN EN ISO 11885 (04.98)
PI
DIN 38406 Part 6 (07.98)
Cadmium (from aqua regia digestion)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 5961 (05.98)
DIN EN ISO11885 (04.98)
Cadmium (from eluate)
DIN EN ISO 5961 (05.98)
DIN EN ISO 11885 (04.98)
Chromium (from aqua regia digestion)
PI
PI
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 (04.98)
PI
Chromium-VI (from eluate)
DIN 38405 Part 24 (05.87)
PI, GE
Copper (from aqua regia digestion)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 (04.98)
Copper (from eluate)
DIN 38406 Part 7 (09.91)
DIN EN ISO 11885 (04.98)
Nickel (from aqua regia digestion)
PI
PI
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 (04.98)
Nickel (from eluate)
Mercury (from aqua regia digestion)
PI
DIN 38406 Part 11 (09.91)
DIN 38406 Part 22 (03.88)
PI
DIN EN ISO 11885 (04.98)
PI
DIN EN 1483 (08.97)
PI
DIN EN ISO 12338 (10.98)
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Appendix to the accreditation certificate D-PL-14170-01-00
Sub-sections/
Parameters
Basis/
Method
Acc.
Site
Mercury (from eluate)
DIN EN 1483 (08.97)
PI
DIN 38406 Part 12 (07.80)
PI
DIN EN ISO 12338 (10.98)
Zinc (from aqua regia digestion)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 (04.98)
Zinc (from eluate)
DIN 38406 Part 8-1 (10.80)
DIN EN ISO 11885 (04.98)
5.4
PI
PI
Group and sum parameters
Appendix 4 no. 3 DepV
Extractable organically bound halogens
(EOX)
Adsorbable organically bound halogens
(AOX) (from eluate)
Total organic carbon (TOC) of dry residue
of original substance
DIN 38414 Part 17 (11.89)
PI, GE
DIN EN 1485 (11.96)
PI, GE
Appendix 4 no. 2.2.2
AbfAblV
Analog:
DIN 38409 Part 3 (06.83)
DIN EN 1484 (08.97)
PI, GE
DIN EN 13137 (12.01)
PI, GE
Total organic carbon (TOC) (from eluate)
DIN EN 1484 (08.97)
PI, GE
Extractable lipophile substances
Appendix 4 no. 2.3 AbfAblV
PI, HI, GE
Phenols (from eluate)
DIN 38409 Part 16-3 (06.84)
PI
DIN EN ISO14402 (12.99)
PI
E DIN EN 14039 (12.00)
in conjunction with LAGA
KW/04 (11.04)
DIN EN 14039 (01.05)
PI, HI, GE
Hydrocarbons
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
PI, GE
PI, HI, GE
82/89
Appendix to the accreditation certificate D-PL-14170-01-00
5.5
Sub-sections/
Parameters
Basis/
Method
Single organic substances
Appendix 4 no. 3 DepV
Polycyclic aromatic hydrocarbons
(PAH)
Contaminated sites
handbook, Vol. 7: Methods
of analysis; Hess. State
Office for the Environment
and Geology, Wiesbaden
(1998)
LUA leaflet no. 1 NRW
Federal Environment
Agency,
Essen (1994)
DIN 38414-21 (02.96)
For solids from the contaminated sites sector or
determination of PAH in soils:
Acc.
Site
PI
PI, HI, GE
PI
DIN 38414-23 (02.02)
5.6
5.7
Volatile halogenated hydrocarbons
DIN EN ISO 10301 (08.97)
PI, HI
Benzene and derivatives (BTEX)
DIN 38407 Part 9 (05.91)
PI, HI
Polychlorinated biphenyls
DIN 38414 Part 20 (01.96)
PI, HI, GE
Strength
Appendix 4 no. 3 DepV
Vane shear strength
DIN 4096 (05.80)
GE
Axial deformation
DIN 18136 (08.96)
GE
Unconfined compressive strength
DIN 18136 (08.96)
GE
Biological degradability
§ 6 Paragraph 4 DepV
Breathability (AT4)
Appendix 4 no. 2.5 AbfAblV
GE
Gas formation rates in fermentation test (GB21)
Appendix 4 no. 2.6 AbfAblV
GE
Testing area 6: Wood waste
6.1
Sub-sections/
Parameters
Sampling, sample preparation
Sample preparation
Basis/
Method
Appendix IV no. 1.1
1.3,1.4.1 AltholzV
Appendix IV no. 1.1,
AltholzV
Appendix IV no. 1.2,
AltholzV, in conjunction
with:
DIN 51701 Part 3 (08.85)
Appendix IV no. 1.3
Moisture content
DIN 52183 (11.77)
Metals
Appendix IV no. 1.1.4.3
AltholzV
E DIN EN 13657 (10.99)
Sampling
Production of the laboratory sample
6.2
Aqua regia digestion
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
Acc.
Site
HI, GE
HI, GE
PI, HI, GE,
FG
HI
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Appendix to the accreditation certificate D-PL-14170-01-00
Sub-sections/
Parameters
Basis/
Method
DIN EN 13657 (01.03)
Arsenic (from aqua regia digestion)
DIN EN ISO 11969 (11.96)
Lead (from aqua regia digestion)
DIN EN ISO 11885 (04.98)
Acc.
Site
HI
PI
DIN 38406, Part 6 (07.98)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
Cadmium (from aqua regia digestion)
DIN EN ISO 11885 (04.98)
PI
DIN EN ISO 5961 (05.95)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
Chromium (from aqua regia digestion)
DIN EN ISO 11885 (04.98)
PI
DIN EN 1233 (08.96)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
Copper (from aqua regia digestion)
DIN EN ISO 11885 (04.98)
PI
DIN 38406, Part 7 (09.91)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
Mercury (from aqua regia digestion)
DIN EN ISO 12338 (10.98)
DIN EN 1483 (08.97)
6.3
Halogen
Fluorine
Chlorine
6.4
Appendix IV no. 1.4.2
AltholzV
DIN 51727 (06.01)
In conjunction with:
DIN EN ISO 10304-1 (04.95)
DIN 51727 (06.01)
in conjunction with:
DIN EN ISO 10304-1 (04.95)
PI
HE
HE
Organic parameters
Appendix IV no. 1.4.4 and
1.4.5 AltholzV
Pentachlorophenol (PCP)
Appendix IV AltholzV no.
1.4.4
PI, HI, GE
Polychlorinated biphenyls (PCB)
Appendix IV AltholzV no.
1.4.5
in conjunction with:
DIN 38414, Part 20 (01.96)
PI, HI, GE
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Appendix to the accreditation certificate D-PL-14170-01-00
9
Testing methods in accordance with the Drinking Water Ordinance – TrinkwV 2001 –
Sampling
Parameters
DIN EN 5667-5
2011-02
DIN EN ISO 5667-3
2004-05
DIN EN ISO 19458 (K 19)
Method
Acc.
Guidance on sampling of drinking water
from treatment works and piped
distribution systems
PI, HI, GE, HM, FG
Guidance on preservation and handling of
water samples
PI, HI, GE, HM, FG
Sampling for microbiological parameters
2006-12
DIN 38402-A 12
Sampling from stagnant bodies of water
1985-06
DIN 38402-A13
Sampling from aquifers
1985-12
DIN 38402-A 15
Sampling from flowing waters
2010-04
DIN 38402-A 18
PI, HI, GE, HM, FG,
WOB
PI, HI, GE, HM, FG
PI, HI, GE, HM, FG
PI, HI, GE, HM, FG
Sampling of water from mineral springs
and spas
PI, HI, GE, HM, FG
DVWK 128 1992
Collection and scope of analysis of
groundwater samples
PI, HI, GE, HM, FG
LAWA AQS leaflet P 8/2 1995-05
Sampling from ground water
PI, HI, GE, HM, FG
1991-05
ANNEX 1: MICROBIOLOGICAL PARAMETERS
PART I: General requirements for drinking water
Parameters
Serial no.
1
Escherichia coli (E. coli)
2
Enterococci
Method
DIN EN ISO 9308-1 (K12) 2001-07
®
®
with Colilert -18/ Quanti-Tray
DIN EN ISO 7899-2 (K 15) 2000-11
with Chromocult enterococci agar
Acc.
HH, WOB
HH, HM
HH, WOB
PART II: Requirements for drinking water intended for distribution in sealed containers
Serial no.
Parameters
1
Escherichia coli (E. coli)
2
Enterococci
3
Pseudomonas aeruginosa
Method
Acc.
DIN EN ISO 9308-1 (K12) 2001-07
®
®
with Colilert -18/ Quanti-Tray
DIN EN ISO 7899-2 (K 15) 2000-11
with Chromocult enterococci agar
HH, WOB
HH, HM
HH, WOB
DIN EN ISO 16266 (K 11) 2008-05
HH, WOB
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
85/89
Appendix to the accreditation certificate D-PL-14170-01-00
ANNEX 2: CHEMICAL PARAMETERS
PART I: Chemical parameters whose concentration does not usually increase in the distribution
network including the domestic distribution network
Serial no.
Parameters
Method
Acc.
1
Acrylamide
2
Benzene
DIN 38407-F 9-1
PI, HI
3
Boron
DIN EN ISO 11885-E 22;
DIN EN ISO 17294-2 (E29)
PI
4
Bromate
DIN EN ISO 15061
PI
5
Chromium
DIN EN ISO 11885-E 22;
DIN EN ISO 17294-2 (E29)
PI
6
Cyanide
DIN 38405-D 13/14
PI
7
1,2-dichloroethane
8
Fluoride
9
Nitrate
10
Pesticides
and biocidal products
11
Total pesticides and
biocidal products
12
Mercury
13
Selenium
14
Tetrachloroethylene and
trichloroethylene
DIN 38407-F 5
DIN 38407-F 4
DIN 38405-D 4
DIN EN ISO 10304-1-D 19/
DIN EN ISO 10304-2-D 20
DIN EN ISO 10304-1-D 19/
DIN EN ISO 10304-2-D 20
DIN EN ISO 13395-D28
DIN EN ISO 6468-F1
DIN 38407-F2
DIN 38407-35 (F35)
EN IDIN SO 10695-F6
DIN EN ISO 11369-F12
DIN EN ISO 15391-F20
DIN EN ISO 6468-F1
DIN 38407-F2
DIN 38407-35 (F35)
DIN EN ISO 10695-F6
DIN EN ISO 11369-F12
DIN EN 1483-E 12
DIN EN ISO 17294-2 (E29)
DIN EN ISO 11885-E 22;
DIN EN ISO 17294-2 (E29)
DIN 38407-F 5
DIN 38407-F 4
15
Uranium
DIN EN ISO 17294-2 (E 29)
PI, HI
PI
PI, HE
PI,
HE
PI
PI
HM
PI
HM
HI
PI
PI
HM
PI
HM
PI
PI
PI, HI
PI
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
86/89
Appendix to the accreditation certificate D-PL-14170-01-00
PART II: Chemical parameters whose concentrations in the distribution network including the
domestic distribution network can increase
Serial no.
Parameters
Method
Acc.
1
Antimony
DIN EN ISO 11885-E 22
DIN EN ISO 17294-2 (E29)
PI
2
Arsenic
DIN EN ISO 17294-2 (E29)
PI
3
Benzo[a]pyrene
in line with DIN 38407-F 8
PI, HI
4
Lead
5
Cadmium
6
Epichlorohydrin
7
Copper
8
Nickel
9
Nitrite
10
Polycyclic aromatic hydrocarbons
11
Trihalomethanes
12
Vinyl chloride
DIN EN ISO 11885-E 22
DIN EN ISO 17294-2 (E29)
DIN EN ISO 11885-E 22;
DIN EN ISO 17294-2 (E29)
DIN EN ISO 11885-E 22;
DIN EN ISO 17294-2 (E29)
DIN EN ISO 11885-E 22;
DIN EN ISO 17294-2 (E29)
PI
PI
PI
PI
DIN EN ISO 13395 (D28)
PI
in line with DIN 38407-F 8
DIN 38407-39 (draft standard)
2008-08
DIN 38407-F 5
DIN 38407-F 4
DIN 38413-P2
DIN EN ISO 15680 (F19)
PI, HI
GE
PI, HI
HI
GE
ANNEX 3: INDICATOR PARAMETERS
Part I: General indicator parameters
Serial no.
Parameters
Method
DIN EN ISO 11885-E 22
Acc.
1
Aluminium
2
Ammonium
3
Chloride
4
Clostridium perfringens (including
spores)
DIN 38406-E5
DIN EN ISO 11732
PI, GE
DIN EN ISO 10304-1-D 19 /
PI, HE
DIN EN ISO 10304-2-D 20
DIN 38405-D 1
in accordance with Annex 5 TrinkwV
HH, WOB
2001
5
Coliform bacteria
DIN EN ISO 9308-1 (K12) 2001-07
6
Iron
7
Colour (spectral absorption
coefficient Hg 436 nm)
8
Smell
9
Taste
DIN EN ISO 11885-E 22;
DIN EN ISO 17294-2 (E29)
DIN 38404-C 3
DIN EN ISO 7887 (C1)
DIN EN 1622–B 3
DEV-B1/2
DEV-B1/2
PI
HH, WOB
PI
PI, HI
PI
PI, HI, HM
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
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Appendix to the accreditation certificate D-PL-14170-01-00
Serial no.
10
11
12
Parameters
Method
TrinkwV 2001, Annex 5 Part 1 d) bb)
Colony count at 22 °C
EN ISO 6222
Electrical conductivity
HH, WOB
HH, HM
TrinkwV 2001, Annex 5 Part 1 d) bb)
Colony count at 36 °C
Acc.
HH, WOB
EN ISO 6222
HH, HM
DIN EN 27888-C 8
PI, HI, GE, HM, FG
DIN EN ISO 11885-E 22;
DIN EN ISO 17294-2 (E29)
DIN EN ISO 11885-E 22;
DIN EN ISO 17294-2 (E29)
13
Manganese
14
Sodium
15
Total organic carbon (TOC)
DIN EN 1484 (H3)
PI, GE
16
Oxidisability
DIN EN ISO 8467 (H5)
PI
17
Sulphate
DIN EN ISO 10304-1-D 19 /
DIN EN ISO 10304-2-D 20
PI, GE
18
Turbidity
DIN EN ISO 7027-C 2
PI, HI
19
Hydrogen ion concentration
DIN 38404-C 5
PI, HI, GE, FG
20
Calcite solubility
DIN 38404-C 10 1995-04
PI, GE, HM
21
Tritium
Not used
22
Total indicative dose
Not used
PI
PI
Part II Special requirements for drinking water in drinking installation equipment
Parameters
Method
ISO 11731, DIN EN ISO 11731-2
(K22) 2008-06;
UBA (Federal Environmental
Agency) recommendation
23.08.2012
Legionella spe.
Acc.
HH, WOB
Parameters that are not included in annexes 1 to 3 of the Drinking Water Ordinance 2011
Additional periodic investigations
Parameters
Calcium
Potassium
Magnesium
Acid capacity
Method
DIN EN ISO 11885-E 22;
DIN EN ISO 17294-2 (E29)
DIN EN ISO 11885-E 22;
DIN EN ISO 17294-2 (E29)
DIN EN ISO 11885-E 22;
DIN EN ISO 17294-2 (E29)
DIN 38409-H 7
Acc.
PI
PI
PI
PI, HI, GE, FG
The accreditation does not replace the recognition or approval method of the competent authority according
to § 15 Paragraph. 4 TrinkwV.
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
88/89
Appendix to the accreditation certificate D-PL-14170-01-00
Abbreviations used:
Terms:
AbfKlärV
AbfAblV
AltölV
BioAbfV
BZE
Waste and sewage sludge ordinance
Waste depositing ordinance
Waste oil ordinance
Biowaste ordinance
Soil condition survey
EN
FHH
HBU
HFA
ISBT
European standard
The Free and Hanseatic city of Hamburg
Ground survey handbook
Forestry analysis handbook
International Society of Beverage Technologists
DAB
DIN
DepV
Ph.Eur.
German Pharmacopoeia
German Institute for Standardisation
Landfill ordinance
European Pharmacopoeia
LAGA
LAWA
MTVO
Trinkw
V
Working group on waste
Working group on water
Mineral and table water ordinance
Drinking water ordinance
Matrix:
WS
CS
Waste
Contaminated sites
SE
AS
BW
BUI
COM
BIO
FU
SO
CC
CO
EL
SM
JS
FW
GY
GW
IO
Sewage
Asphalt
Biowaste (compost)
Building materials
Commodity
Biota
Fuels
Soil
Mixed salts
Carbonic acid
Eluate
Solid and powdered materials
Joint sealant
Flowing water
Gypsum
Groundwater
Insulating oil
WO
SS
FO
Wood (waste)
Sewage sludge
Foods
GA
MAT
Soil / gas
Material as a generic term for raw materials,
auxiliary materials and operating materials
MIR
Mineral products in road construction
MiW Mineral water
SW
Surface water
OIL
Oil (waste)
Passive Passive collectors
PEEK Polyetheretherketone
PO
Polymers
CA
Cleaning agents
AC
Acid (product/raw)
SED
Sediment
SPW
Swimming pool water
SL
Sludge
DU
Dust (filter/boiler)
LE
Leachate
BoW Bottled water
DS
De-icing salt
DW
Drinking water as a generic term for bottled
water, spring water, mineral water and tap water
WA
Water as a generic term
DE
Detergent
CP
Cigarette paper
Period of validity: 19 December 2012 to 18 December 2017, Date of issue: 13 February 2013
Translation
89/89