Deutsche Akkreditierungsstelle GmbH
Annex to the Accreditation Certificate D-PL-14234-01-00
according to DIN EN ISO/IEC 17025:2005
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
Holder of certificate:
GALAB Laboratories GmbH
Am Schleusengraben 7, 21029 Hamburg
Tests in the fields:
physical, physico-chemical and chemical investigations of water, soils, sediments, foods, animal
feedstuffs, commodities, tobacco and tobacco products, biota and air;
sampling of foods, water and sediments;
microbiological investigations of foods, commodities and water;
molecular-biological investigations of foods, animal feedstuffs, tobacco and tobacco products;
sensory analyses of foods, and commodities;
selected immunological investigations of foods;
microbiological investigations in accordance with the Drinking Water Ordinance, sampling of
drinking water for microbiological investigations
Abbreviations used: see last page
Within the given testing field marked with */**, the testing laboratory is permitted, without being
required to inform and obtain prior approval from DAkkS, the following:
*) the free choice of standard or equivalent testing methods.
**) the modification, development and refinement of testing methods.
The listed testing methods are exemplary.
The testing laboratory is permitted, without being required to inform and obtain prior approval
from DAkkS, to use standards or equivalent testing methods listed here with different issue dates.
The testing laboratory maintains a current list of all testing methods within the flexible scope of
accreditation.
This document is a translation. The definitive version is the original German annex to the accreditation certificate.
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1
Investigation of foods and animal feedstuffs
1.1
Physical, physico-chemical and chemical investigations
1.1.1
Determination of residues and contaminants by LC-MS-MS in foods
and animal feedstuffs **
DIN EN 15662
2009-02
Foods of plant origin - Determination of pesticide residues using
GC-MS and/or LC-MS/MS following acetonitrile extraction/partitioning
and clean-up by dispersive SPE - QuEChERS-method
(Modification: Here only with LC-MS-MS)
SOP no. 91
2014-07
Determination of coccidiostatics in foods by LC-MS-MS
SOP no. 129
2014-07
Determination of sulphonamides in foods LC-MS-MS
SOP no. 138
2012-05
Determination of mycotoxins in grain products, pastries and baby food
by LC-MS-MS
SOP no. 148
2012-05
Determination of mycotoxins in dried fruits by LC-MS-MS
SOP no. 151
2009-08
Determination of mycotoxins in spices, dried herbs , tea, tea products,
coffee and coffee products by LC-MS-MS
SOP no. 152
2012-05
Determination of mycotoxins in high-fat foods by LC-MS-MS
SOP no. 232
2011-06
Determination of glyphosate, AMPA and glufosinate in foods and
animal feedstuffs by LC-MS-MS
SOP no. 333
2013-08
Determination of quaternary ammonium compounds (QAC) in foods
and animal feedstuffs by LC-MS-MS
1.1.2
Determination of arsenic species by IC-ICP-MS in foods and animal feedstuffs **
DIN EN 16802
2014-11
Foodstuffs - Determination of elements and their chemical species Determination of inorganic arsenic in foodstuffs of marine and plant
origin by anion-exchange HPLC-ICP-MS following waterbath extraction
(Modification: Inclusion of animal feedstuffs)
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
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SOP no. 356
2013-08
1.1.3
Determination of arsenic compounds in foods by IC-ICP-MS coupling
Determination of residues and contaminants by gas chromatography (GC-MSD, GC-FID)
in foods and animal feedstuffs **
DIN EN 15662
2009-02
Foods of plant origin - Determination of pesticide residues using GCMS and/or LC-MS/MS following acetonitrile extraction/partitioning
and clean-up by dispersive SPE - QuEChERS-method
(Modification: Here only with GC-MS)
ASU L 00.00-36/2
2004-07
Investigations of foods - Determination of bromide residues in low-fat
foods - Part 2: Determination of inorganic bromide
SOP no. 86
2010-05
Determination of PCB in foods and animal feedstuffs by GC-MSD
SOP no. 119
2014-06
Determination of dithiocarbamates as CS2 in foods and animal
feedstuffs by GC-MSD
SOP no. 132
2007-05
Determination of phthalic acid esters and tenderizers in foods by
GC-MSD
SOP no. 139
2010-03
Determination of patulin in fruits and vegetables and their products
by GC-MSD
SO nor. 261
2011-05
Determination of MOSH and MOAH in foods and commodities
by GC-FID
(Modification: Here only for foods)
SOP no. 303
2014-01
Determination of phenoxy carbonic acids in foods by GC-MSD
SOP no. 335
2013-08
Determination of EC and EPA PAH in foods and animal feedstuffs
by GC-MSD
SOP no. 338
2013-08
Determination of MOSH and MOAH in foods by GC-FID
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
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1.1.4
Determination of contaminants by HRGC-HRMS in foods and animal feedstuffs
EPA 1613
1994-10
Tetra- through octa-chlorinated dioxins and furans by Isotope Dilution
HRGC-HRMS
SOP no. 399
2013-11
Determination of mass concentration of PCDD/PCDF and dioxin-like
PCB by HRGC-HRMS in fruit-based baby food by HRGC-HRMS
1.1.5
Determination of ingredients and additives in foods by HPAEC
SOP no. 248
2011-07
1.1.6
Determination of galacto-oligosaccharides (GOS) in baby food by
HPAEC-PAD
Determination of elements by ICP-MS in foods and animal feedstuffs **
DIN EN ISO 17294-2
2005-02
Water quality - Application of inductively coupled plasma mass
spectrometry (ICP-MS) - Part 2: Determination of 62 elements
(Modification: Inclusion of further elements; inclusion of digestion
solutions for foods and animal feedstuffs, including pressure digestion
according to ASU L 00.00-19/1)
ASU L 00.00-93
2008-12
Investigations of foods - Determination of iodine in foods
- ICP-MS method
SOP no. 66
2011-05
Determination of freely ionisable copper in Cu-chlorophyll
SOP no.81
2011-08
Determination of methylmercury in foods, animal feedstuffs and oils
by distillation/ICP-MS
1.1.7
Titrimetric determinations of ingredients in foods *
ASU L 00.00-46/1
1999-11
Investigation of foods - Determination of sulphite in foods Part 1: Optimised Monier-Williams method
ASU L 06.00-7
2014-08
Investigation of foods - Determination of raw protein content in meat
and meat products - Titrimetric method after Kjeldahl – Reference
method
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
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ASU L 13.00-5
2012-01
Investigation of foods - Determination of acid value and acidity of
animal and vegetable fats and oils
ASU L 13.00-37
2012-01
Investigation of foods - Determination of the peroxide value of animal
and vegetable fats and oils - Iodometric (visual) endpoint
determination
IFU 3
Rev. 2005
Titratable acidity
IFU 30
Rev. 2005
Determination of formol number
SOP no. 361
2013-08
Determination of nitrogen content in milk
1.1.8
Enzymatic determinations of ingredients and additives in foods *
ASU L 02.00-12
2009-06
Determination of foods - Determination of sucrose and glucose content
in milk products and ice cream - Enzymatic method
ASU L 48.02.07-2
1985-05
Determination of maltose in Brussels biscuit for children and Brussels
biscuit flour
IFU 21
Rev.2005
Determination of L-malic acid (enzymatic)
IFU 22
Rev.2005
Determination of citric acid (enzymatic)
IFU 52
Rev.2005
Determination of alcohol (enzymatic)
IFU 53
Rev.2005
Determination of lactic acid (enzymatic)
IFU 54
Rev.2005
Determination of D-isocitric acid (enzymatic)
IFU 55
Rev.2005
Determination of glucose und fructose (enzymatic)
IFU 56
Rev.2005
Determination of sucrose (enzymatic)
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
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IFU 62
Rev.2005
1.1.9
D-sorbitol (enzymatic)
Photometric determinations of ingredients and additives in foods *
ASU L 08.00-14
2008-06
Investigation of foods - Determination of nitrate and nitrite content in
sausage products following enzymatic reduction of nitrate to nitrite Spectrophotometric method
IFU 49
Rev.2005
Determination of proline
1.1.10 Gravimetric determinations of ingredients and additives in foods and animal feedstuffs *
ISO 665
2000-09
Oilseeds - Determination of moisture and volatile matter content
ASU L 00.00-18
1997-01
Corrigendum
2002-12
Investigation of foods - Determination of dietary fibres in foods
ASU L 01.00-9
2012-01
Investigation of foods - Determination of fat content in milk Gravimetric method (reference method)
ASU L 01.00-20
1988-05
Investigation of foods - Determination of fat content in milk and milk
products - Weibull method
(norm withdrawn)
ASU L 01.00-27
1988-12
Investigation of foods - Determination of dry matter content in milk
and cream - Reference method
ASU L 01.00-77
2002-05
Investigation of foods - Determination of total ash in milk and milk
products
ASU L 06.00-3
2014-08
Investigation of foods - Determination of water content in meat and
meat products - Gravimetric method - Reference method
ASU L 06.00-04
2007-04
Investigation of foods - Determination of ash in meat and meat
products
ASU L 06.00-6
1980-06
Determination of total fat content in meat and meat products
(norm withdrawn)
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
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DGF B-II 3
1987
Water and volatile matter in animal feedstuffs
IFU 36
2005
Determination of sulphate
UNECE DDP-11
1992
UNECE Standard DDP-11 concerning the marketing and commercial
quality control of dried grapes - Annex I: Determination of the
moisture content of dried fruit
VDLUFA III 3.1
1976
Determination of moisture in animal feedstuffs and grains
1.1.11 Refractometric investigations of foods
IFU 8
Rev. 2005
Determination of soluble solids (indirect method by refractometry)
1.1.12 Electrochemical investigations of foods
ASU L 31.00-2
1997-01
Investigation of foods - Determination of pH in
fruit and vegetable juices
1.1.13 Densitometric investigation of foods
IFU 1A
Rev. 2005
1.2
Relative density (method using density meter)
Immunological determinations of ingredients and additives and allergens
by ELISA in foods *
Veratox for Gliadin R5
(quantitative),
Produkt 8510
V-GliadinR5_0114_ENSP
Immunological determination of gliadin in foods by the
ELISA method (test kit)
(Modification: Wavelength 450 nm, colourless sulphuric acid)
Neomycin
Article 52400
Status: September
’05-9[07.2005-10]
Immunological determination of neomycin in foods by the
ELISA method(test kit)
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
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Gentamicin
Article 52300
Status: 28 February 2012
[12]02.12
Immunological determination of gentamicin in foods by the
ELISA method (test kit)
Streptomycin
Article 52500
5111STREP[16]02.12
Status: 13 August 2014
Immunological determination of streptomycin in foods by the
ELISA method (test kit)
1.3
Microbiological investigations
1.3.1
Determination and detection of bacteria in foods
by the bacteriological culture method *
ASU L 00.00-20
2008-12
Investigation of foods - Horizontal method for the detection of
Salmonella spp. in foods
ASU L 00.00-32
2006-09
Investigation of foods - Horizontal method for the detection and
counting of Listeria monocytogenes Part 1: Method of detection
ASU L 00.00-88
2004-07
Investigation of foods - Horizontal method for the counting of
microorganisms - Colony counting method at 30 °C
(norm withdrawn)
ASU L 00.00-132/2
2010-09
Investigation of foods - Horizontal method for the counting of
β-glucuronidase-positive Escherichia coli in foods - Part 2: Colony
counting method with 5-bromo-4-chloro-3-indolyl-β-D-glucuronide
ASU L 00.00-133/2
2010-09
Investigation of foods - Horizontal method for the detection and
counting of enterobacteriaceae in foods - Part 2: Colony counting
method
ASU L 01.00-3
1987-03
Investigation of foods - Determination of coliform bacteria in milk, milk
products, butter, cheese and ice cream - Solid substrate method
SOP no. 413
2015-02
TEMPO EC method: Automatic quantitative determination of
Escherichia coli in foods by determination of the most probable
number (MPN)
SOP no. 414
2015-02
TEMPO EB method: Automatic quantitative determination of
enterobacteriaceae in foods by determination of the most probable
number (MPN)
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
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SOP no. 415
2015-02
TEMPO TC method: Automatic quantitative determination of total
coliform bacteria in foods by determination of the most probable
number (MPN)
SOP no. 416
2015-02
TEMPO EB method: Automatic quantitative determination of aerobic
mesophilic bacterial count in foods by determination of the most
probable number (MPN)
1.3.2
Determination of yeasts and moulds in foods by the cultural mycological method
ASU L 01.00-37
1991-12
1.3.3
Investigation of foods - Determination of yeasts and moulds in milk and
milk products - Reference method
Hygrometric determinations
ISO 21807
2004-09
Microbiology of food and animal feeding stuffs - Determination of
water activity
1.4
Molecular-biological investigations
1.4.1
Detection of specific DNA sequences and determination of animal species
by real-time PCR in foods and animal feedstuffs *
ASU L 00.00-122
2008-06
Investigation of foods - Detection of a certain DNA sequence frequently
employed in genetically modified organisms (GMO) from the
cauliflower mosaic virus (CaMV 35S-Promotor, P35S) and
Agrobacterium tumefaciens (T-nos) in foods - Screening method
ASU L 10.00-12
2012-07
Investigation of foods - determination of fish species in raw fish and
fish products by sequential analysis of cytochrome-b sequences
ASU L 23.04/03-1
2010-09
Investigation of foods - Construct-specific real-time PCR method for the
detection of genetic modifications in linseed and linseed products
SOP no. 193
2010-10
GMO-screening for the detection of the construct P35:BAR by real-time
PCR in genetically modified rice
SOP no. 213
2010-10
GMO-screening for the detection of the CTP2-CP4-EPSPS sequence by
real-time PCR
SOP no. 216
2009-08
GMO-screening for the detection of pat and bar genetic sequence
by real-time PCR
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
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Annex to the accreditation certificate D-PL-14234-01-00
SOP no. 316
2014-02
Qualitative determination of animal species in foods
SOP no. 400
2014-01
Detection of a specific cashew DNA sequence in foods by real-time PCR
SOP no. 402
2014-01
Detection of a specific almond DNA sequence in foods by real-time PCR
SOP no. 403
2014-01
Detection of a specific sesame DNA sequence in foods by real-time PCR
SOP no. 406
2014-03
Animal species quantification
1.4.2
Determination of specific bacilli in foods by real-time PCR **
ASU L 00.00-98
2007-04
Investigation of foods - Qualitative determination of salmonella in
foods - Real-time PCR method
ASU L 00.00-147/2 (V)
2014-02
Investigation of foods - Horizontal method for the determination of
hepatitis A virus and norovirus in foods - Part 2: Method for qualitative
determination - Real-time RT-PCR
(Modification: Here only detection of norovirus)
ASU L 06.32-1
2013-08
Investigation of foods - Detection of Campylobacter spp. in
mincemeat - Real-time PCR method
(Modification: DNA extraction performed with extraction kit,
differentiation of C.jejuni, C.lari and C.Coli in duplex charges)
SOP no. 396
2013-10
Investigation of foods - Qualitative determination of Listeria
monocytogenes by real-time PCR
SOP no. 444
2014-12
Investigation of foods - Qualitative determination of shigatoxin-forming
Escherichia coli (STEC) and enterohaemorrhagic Escherichia coli (EHEC)
by real-time PCR
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
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1.5
Sensory analyses of foods
1.5.1
Simply characterised testing of sensory parameters for foods *
ASU L 00.90-6
1997-09
Investigation of foods - Sensory test methods - Simply characterised
testing
(norm withdrawn)
ASU L 00.90-7
2007-12
Investigation of foods - Sensory test methods - Triangular testing
ASU L 00.90-8
2007-12
Investigation of foods - Sensory test methods - Pair-wise comparative
testing
ASU L 00.90-14
2004-12
Investigation of foods - Sensory test methods - Descriptive testing
followed by quality evaluation
1.5.2
Special sensory testing of olive oil
VO (EC) no. 640/2008
2008-07
1.6
Characteristics of olive oils and olive residue oils and method for their
determination: Organoleptic testing of native olive oils
Sampling of foods
VO (EC) no. 401/2006
2006-02
Ordinance of the Commission for the specification of sampling
methods and analytical methods for the official control of mytotoxin
content in foods
SOP no. 307
2013-08
Sampling for the microbiological analysis of foods
2
Investigation of tobacco and tobacco products
2.1
Determination of GMOs by real-time PCR in tobacco
SOP no. 162
2010-10
GMO screening for the detection of DNA promotor from the cauliflower
mosaic virus and Agrobacterium tumefaciens terminator
by real-time PCR
(after DIN EN ISO 21570:2005 and Article 64 of the LFGB L 00.00-116)
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
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3
Investigation of commodities and textiles
3.1
Physical, physico-chemical and chemical investigations
3.1.1
Determination of residues and contaminants in commodities and textiles by liquid
chromatography (LC-MS-MS) **
SOP no. 201
2011-04
Method for the chemical analysis of paper-based materials on the
presence and the concentration of diisocyanates
(2,4-TDI: CAS no. 584-84-9; 2,6-TDI: CAS no. 91-08-7) by LC-MS-MS
SOP no. 214
2009-05
Determination of nicotine in textiles by LC-MS-MS
SOP no. 340
2013-08
Determination of quaternary ammonium compounds (QAC) in
commodities by LC-MS-MS
3.1.2
Determination of chromium (VI) in commodities and textiles by IC-ICP-MS **
DIN EN ISO 17075
2008-02
Leather - Chemical tests - Determination of chromium(VI) content
(Modification: Inclusion of paper-based materials; quantification
by IC-ICP-MS)
DIN EN 71-3
2014-12
Safety of toys - Part 3: Migration of certain elements
(Modification: Inclusion of pigments)
SOP no. 304
2012-11
Determination of heavy metals - Testing for chromium(VI)
in commodities and textiles by IC-ICP-MS following saline extraction
(after OEKO-TEX® test method no. 3.3; 2015/01)
3.1.3
Determination of residues and contaminants in commodities by gas chromatography
with standard detectors (GC- AED, GC-FID, GC-MSD) **
CPSC-CH-C1001-09.3
2010-04
Standard Operating Procedure for the Determination of Phthalates
SOP no. 20
2014-07
Determination of organic tin compounds in commodities by GC-AED
SOP no. 31
2007-01
Determination of phthalic acids in commodities and hygienic products
by GC-MSD
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
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SOP no. 55
2004-07
Determination of alkaline phenols, alkaline phenol ethoxylates and
bisphenol A in commodities by GC-MSD
SOP no. 261
2011-05
Determination of MOSH and MOAH in foods and commodities
by GC-FID
(Modification: Here only for commodities)
SOP no. 293
2012-04
Determination of phenol and chlorophenols in commodities
by GC-MSD
SOP no. 341
2013-08
Determination of EC and EPA PAH in environmental samples and
commodities by GC-MSD
(Modification: Here only for commodities)
SOP no. 342
2013-08
Determination of pesticides in commodities and
environmental samples by GC-MSD (QuEChERS)
(Modification: Here only for commodities)
SOP no. 405
2014-03
Determination of organic tin compounds in toys
after DIN EN 71-3
3.1.4
Determination of elements in commodities and textiles by ICP-MS **
ISO 7086-1
2000-03
Glass hollowware in contact with food - Release of lead and cadmium Part 1: Test method
(Modification: Inclusion of plastic containers)
DIN EN ISO 17294-2
2005-02
Water quality - Application of inductively coupled plasma mass
spectrometry (ICP-MS) - Part 2: Determination of 62 elements
(Modification: Inclusion of further elements; inclusion of digestion
solutions for commodities, including pressure digestion; also for heavy
metals in textiles
DIN EN 71-3
2014-12
Safety of toys - Part 3: Migration of certain elements
(Modification: Inclusion of pigments)
CPSC-CH-E1002-08
2009-02
Standard operating procedure for determining total lead (Pb)
in non-metal children’s products
CPSC-CH-E1003-09
2009-04
Standard operating procedure for determining lead (Pb) in paint and
other similar coatings
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
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Resolution AP (89) 1
1989-09
Resolution AP (89) 1 on the use of colourants in plastic materials
coming into contact with food
(Modification: Inclusion of quantification by ICP-MS after DIN EN ISO
17294-2)
CPSC-CH-E1002-08
2009-02
Standard operating procedure for determining total lead (Pb)
in non-metal children’s products
CPSC-CH-E1003-09
2009-04
Standard operating procedure for determining lead (Pb) in paint and
other similar coatings
SOP no. 272
2013-05
Determination of elements in commodities following saline extraction
by ICP-MS after DIN EN ISO 17294-2
3.1.5
Photometric determinations of contents and contaminants
in commodities and textiles *
ASU B 82.02-1
1985-06
Investigations of commodities - Determination of formaldehyde
emissions from textile commodities
(Here: by UV/VIS)
ASU B 82.10-1
2011-12
Investigation of commodities - Testing of brightly coloured toys for
saliva and perspiration fastness
SOP no. 13 ECB
2011-11
Determination of free and hydrolysed formaldehyde in
solid paper-based material by spectrophotometry
3.1.6
Gravimetric investigations of commodities
ASU B 80.30-1(EC)
1998-01
Investigation of commodities - Basic rules for the determination of
migration - Annex
ASU B 80.30-4
2008-10
Investigation of commodities - Plastics - Part 1: Guidelines for the
selection of test conditions and test methods for overall migration
ASU B 80.30-6
2008-10
Investigation of commodities Plastics - Part 3: Test methods for overall
migration in aqueous food test samples by total immersion
ASU B 80.30-8
2008-10
Investigation of commodities - Plastics - Part 5: Test methods for
overall migration in aqueous food test samples by cells
ASU B 80.30-10
2008-10
Investigation of commodities - Plastics - Part 7: Test methods for
overall migration in aqueous food test samples with a pouch
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
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ASU B 80.30-12
2008-10
Investigation of commodities - Plastics - Part 9: Test methods for
overall migration in aqueous food test samples filling of the object
ASU B 80.30-17
2008-10
Investigation of commodities - Plastics - Part 14: Test methods for
"alternative tests" for overall migration from plastics coming into
contact with high-fat foods, using the test media isooctane and 95%
ethanol
ASU B 80.30-18
2008-10
Investigation of commodities - Plastics - Part 15: Alternative test
methods for the determination of migration in high-fat food test
samples by fast extraction in isooctane
and/or 95% ethanol
ASU B 80.30-19
2008-10
Investigation of commodities - Substances in plastics subject to
restrictions - Part 1: Guidelines for the test methods for the
specific migration of substances from plastics into foods and food test
samples - Determination of substances in plastics and selection of
contact conditions with food test samples
Other relevant documentation
ASU B 80.30-3(EC)
2008-04
Investigation of commodities - Further regulations for testing
compliance with limit values for migration, Annex 1 of Directive
2002/72/EC of the Commission 6 August 2002 for plastic materials and
objects coming into contact with foods
ASU B 80.30-4
2008-10
Investigation of commodities - Plastics - Part 1: Guidelines for the
selection of test conditions and test methods for overall migration
3.2
Determination and detection of bacteria in furnishings and objects for the food area
by the bacterial culture method *
ASU B 80.56-5
2008-10
Investigation of commodities - Paper and cardboard coming into
contact with food - Determination of anti-microbial fraction transfer
ASU B 80.00-1 to 3
1998-01
Investigation of commodities - Determination of surface bacterial
content of furnishings and commodities in the food area
- Part 1: Quantitative swab technique
- Part 2: Semi-quantitative swab technique
- Part 3: Semi-quantitative method with substrate-coated extraction
devices - Impression method
Ph. Eur. 2.6.1
8th edition
Sterility testing
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
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Ph. Eur. 2.6.12
8th edition
Microbiological testing of non-sterile products: Counting of replicationcompetent microorganisms
Ph. Eur. 2.6.13
8th edition
Microbiological testing of non-sterile products: Detection of specific
microorganisms
Ph. Eur. 5.1.3
8th edition
Testing for sufficient anti-microbial conservation
3.3
Special sensory testing for the odour and taste of paper, cardboard and commodities *
DIN EN 1230-1
2010-02
Paper and board intended to come into contact with foodstuffs Sensory analysis - Part 1: Odour
DIN EN 1230-2
2010-02
Paper and board intended to come into contact with foodstuffs Sensory analysis - Part 2: Off-flavour (taint)
(Here: Triangular test)
ASU B 80.00-4
2008-10
Investigation of commodities - Sensory testing of packaging materials
and packaging for foods
(Here: Triangular test)
4
Investigation of cosmetic products
SOP no. 452
2015-03
5
Determination of polysilicon-15 in cosmetics by HPLC
Investigation of chemical products
SOP no. 249
2010-11
Determination of mass polymer stabilisers by HPLC DAD
SOP no. 315
2013-01
Determination of acrylic acids and residual monomers from
superabsorbent polymers after EDANA by HPLC-UV-VIS
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
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6
Investigation of water
6.1
Sampling
DIN EN ISO 5667-1 (A 4)
2007-04
Water quality - Sampling - Part 1: Guidance on the design of sampling
programmes and sampling techniques
DIN 38402-A 11
2009-02
Sampling of waste water
DIN 38402-A 12
1985-06
sampling from barrages and lakes
DIN ISO 5667-5 (A 14)
2011-02
Water quality - Sampling - Part 5: Guidance on sampling of drinking
water from treatment works and piped distribution systems
DIN 38402-A 15
2010-04
Sampling from running waters
DIN EN ISO 5667-3 (A 21)
2013-03
Water quality - Sampling - Part 3: Preservation and handling of water
samples
DIN EN ISO 19458 (K 19)
2006-12
Water quality - Sampling for microbiological analysis
DIN EN 1420-1
1999-11
Influence of organic materials on water intended for human
consumption - Determination of odour and flavour assessment of
water in piping systems - Part 1: Test method
LAWA AQS
Memorandum P-8/1
2009-09
Sampling of waste water
LAWA AQS
Memorandum P-8/3
2012-02
Sampling from running waters
LAWA AQS
Memorandum P-8/4
2002-05
Sampling of suspended matter and sediments
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
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6.2
Physical, physico-chemical and chemical investigations
6.2.1
Physical and physico-chemical parameters
DIN EN ISO 7887 (C 1)
2012-04
Water quality - Examination and determination of colour
DIN EN ISO 7027 (C 2)
2000-04
Water quality - Determination of turbidity
DIN 38404-C 4
1976-12
Determination of Temperature
DIN EN ISO 10523 (C 5)
2012-04
Water quality - Determination of pH
DIN 38404-C 6
1984-05
determination of the oxidation reduction (redox) potential
DIN EN 27888 (C 8)
1993-11
Water quality; determination of electrical conductivity
DIN EN ISO 5814 (G 22)
2013-02
Water quality - Determination of dissolved oxygen - Electrochemical
probe method
6.2.2
Determination of organic and metal-organic compounds by gas chromatography
(GC-MSD, GC-AED) **
DIN EN ISO 17353 (F 13)
2005-11
Water quality - Determination of selected organotin compounds - Gas
chromatographic method
SOP no. 85
2005-04
Determination of chlorobenzenes in water by GC-MSD
SOP no. 154
2008-05
Determination of phthalates in water by GC-MSD
SOP no. 156
2008-05
Determination of alkaline phenols, alkaline phenol ethoxylates and
bisphenols A in water by GC-MSD
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
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6.2.3
Determination of elements by ICP-MS
DIN EN ISO 17294-2 (E 29)
2005-02
6.2.4
Water quality - Application of inductively coupled plasma mass
spectrometry (ICP-MS) - Part 2: Determination of 62 elements
(Modification: Inclusion of the elements Fe, Hg, Si, Ta und Ti)
Further chromatographic investigations
DIN EN ISO 10304-1 (D 20)
2009-07
Water quality - Determination of dissolved anions by liquid
chromatography of ions - Part 1: Determination of bromide, chloride,
fluoride, nitrate, nitrite, phosphate and sulfate
SOP no. 234
2009-11
Determination of glyphosate, AMPA und glufosinate in water
by LC-MS-MS
6.3
Determination and detection of bacteria with the bacterial culture method
in water samples
DIN EN ISO 6222 (K 5)
1999-07
Water quality - Enumeration of culturable micro-organisms - Colony
count by inoculation in a nutrient agar culture medium
DIN EN ISO 16266 (K 11)
2008-05
Water quality - Detection and enumeration of Pseudomonas
aeruginosa - Method by membrane filtration
DIN EN ISO 9308-1 (K 12)
2001-07
Water quality - Detection and enumeration of Escherichia coli coliform
bacteria - Part 1: Membrane filtration method
(standard withdrawn)
DIN EN ISO 9308-1 (K 12)
2014-12
Water quality - Enumeration of Escherichia coli and coliform bacteria Part 1: Membrane filtration method for waters with low bacterial
background flora
DIN EN ISO 7899-2 (K 15)
2000-11
Water quality - Detection and enumeration of intestinal enterococci Part 2: Membrane filtration method
DIN EN ISO 11731-2 (K 22)
2008-06
Water quality - Detection and enumeration of Legionella - Part 2: Direct
membrane filtration method for waters with low bacterial counts
ISO 11731
1998-05
Water quality - Detection and enumeration of Legionella
ISO 14189
2013-11
Water quality - Enumeration of Clostridium perfringens - Method using
membrane filtration
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
19/25
Annex to the accreditation certificate D-PL-14234-01-00
TrinkwV 2001
Annex 5 I e)
2001-05
Detection of Clostridium perfringens
7
Investigation of sediments, soils and sludges
7.1
Sampling of sediments
DIN 38414-S 11
1987-08
7.2
sampling of sediments
Sample preparation
DIN EN 16174
2012-11
Sludge, treated biowaste and soil - Digestion of aqua regia soluble
fractions of elements
7.3
Physical, physico-chemical and chemical investigations
7.3.1
Determination of organic compounds by liquid chromatography (LC-MS-MS) **
SOP no. 112
2006-03
Determination of barbituates in soils and sediments
by LC-MS-MS
SOP no. 233
2009-11
Determination of glyphosate, AMPA und glufosinate in water
by LC-MS-MS
7.3.2
Determination of organic and metal-organic compounds
by gas chromatography (GC-MSD) **
ISO 23161
2009-09
Soil quality - Determination of selected organotin compounds -- Gaschromatographic method
DIN 38414-S 21
1996-02
Determination of 6 polynuclear aromatic hydrocarbons (PAH) by high
performance liquid chromatography (HPLC) with fluorescence
detection
SOP no. 341
2013-08
Determination of EC and EPA PAH in environmental samples and
commodities by GC-MSD
(Modification: Here only for sediments and soils)
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
20/25
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SOP no. 342
2013-08
7.3.3
Determination of metal-organic compounds by gas chromatography (GC-AED) **
SOP no. 1
2010-06
7.3.4
Water quality - Application of inductively coupled plasma mass
spectrometry (ICP-MS) - Part 2: Determination of 62 elements
(Modification: Here only determination in aqua regia digestion
solutions)
Gravimetric determinations
DIN 38414-S 2
1985-11
8
Tetra- through octa-chlorinated dioxins and furans by isotope dilution
HRGC/HRMS
Determination of elements by ICP-MS
DIN EN ISO 17294-2
2005-02
7.3.6
Determination of organic tin compounds in sediments
by GC-AED
Determination of PCDD/PCDF and dioxin-like PCB by HRGC-HRMS
EPA 1613
1994-10
7.3.5
Determination of pesticides in commodities and
environmental samples by GC-MSD (QuEChERS)
(Modification: Here only for sediments and soils)
determination of water content, of dry residue and of solids content
(standard withdrawn)
Investigation of biota
ASU L 00.00-19/1
2015-06
Foodstuffs - Determination of trace elements - Pressure digestion
(takeover of the standard DIN EN 13805 with the same name, version
of December 2014)
(Modification: Here for biota)
DIN EN ISO 17294-2 (E 29)
2005-02
Water quality - Application of inductively coupled plasma mass
spectrometry (ICP-MS) - Part 2: Determination of 62 elements
(Modification: Here for biota)
SOP no. 32
2001-10
Determination of musk compounds in biota by GC-MSD
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
21/25
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SOP no. 39
2012-10
9
Determination of arsenic compounds in biota by IC-ICP-MS
Investigations of air
VDI 2267 sheet 9
2002-07
10
Determination of suspended particulates matter in ambient air Measurement of the mass concentration of mercury - Sampling by
sorption as amalgam and determination by atomic fluorescence
spectrometry (AFS) with cold vapour technique
(Modification: No sampling)
Investigations in accordance with the Drinking Water Ordinance - TrinkwV 2001 -
Sampling
Method
DIN EN ISO 5667-01 (A 4)
2007-04
DIN ISO 5667-5 (A 14)
2011-02
DIN EN ISO 5667-3 (A 21)
2013-03
DIN EN ISO 19458 (K 19)
2006-12
Title
Water quality - Sampling - Part 1: Guidance on the design
of sampling programmes and sampling techniques
Water quality - Sampling - Part 5: Guidance on sampling of
drinking water from treatment works and piped
distribution systems
Water quality - Sampling - Part 3: Preservation and
handling of water samples
Water quality - Sampling for microbiological analysis
ANNEX 1: MICROBIOLOGICAL PARAMETERS
PART I:
No.
1
2
PART II:
No.
1
2
3
General requirements for drinking water
Parameter
Escherichia coli (E. coli)
Enterococci
Method
DIN EN ISO 9308-1 2014-12
DIN EN ISO 7899-2 (K 15) 2000-11
Requirements for drinking water dispensed from closed containers
Parameter
Escherichia coli (E. coli)
Enterococci
Pseudomonas aeruginosa
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
Method
DIN EN ISO 9308-1 2014-12
DIN EN ISO 7899-2 (K 15) 2000-11
DIN EN ISO 16266 (K 11) 2008-05
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Annex to the accreditation certificate D-PL-14234-01-00
ANNEX 2: CHEMICAL PARAMETERS
PART I: Chemical parameters for which the concentrations in the distribution network,
including the drinking water installation, as a rule no longer increase
not tested
PART II: Chemical parameters for which the concentrations in the distribution network,
including the drinking water installation, can increase
not tested
ANNEX 3: INDICATOR PARAMETERS
Part I: General indicator parameters
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
Parameter
Aluminium
Ammonium
Chloride
Clostridium perfringens
(including spores)
Coliform bacteria
Iron
Colouring (spectral absorption
coefficient Hg 436 nm)
Odour
Taste
Colony count at 22 °C
Colony count at 36 °C
Electrical conductivity
Manganese
Sodium
Total organic carbon (TOC)
Oxidisability
Sulphate
Turbidity
Hydrogen ion concentration
Calcite solubility
Tritium
Total indicative dose
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
Method
not tested
not tested
not tested
TrinkwV 2001 Annex 5 I e)
DIN EN ISO 9308-1 2014-12
not tested
not tested
not tested
not tested
DIN EN ISO 6222 (K 5) 1999-07
DIN EN ISO 6222 (K 5) 1999-07
not tested
not tested
not tested
not tested
not tested
not tested
not tested
not tested
not tested
not tested
not tested
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Annex to the accreditation certificate D-PL-14234-01-00
Part II: Special requirements for drinking water in drinking water installation facilities
Parameter
Method
ISO 11731 1998-05
DIN EN ISO 11731-2 (K 22) 2008-06
Legionella spec.
The accreditation does not replace the validation or certification process requirement of the
relevant authority in accordance with Article 15, Paragraph 4 of the Drinking Water Ordinance.
Abbreviations used:
AMPA
AP
ASU
CPSC-CH
CRL
DGF
DIN
DIS
ECB
EC-PAH
EDANA
ELISA
EN
EPA
EPA-PAH
GC-AED
GC-MSD
GC-FID
α-amino-3-hydroxy-5-methyl-4-isoxazole-propionic acid
Analytical procedure, Council of Europe Committee of Ministers
Amtliche Sammlung von Untersuchungen nach § 64 LFGB
(official collection of investigations acc. to Article 64 of the LFGB)
Consumer Product Safety Commission-Division of Chemistry
European Commission, Community Reference Laboratory
Deutsche Gesellschaft für Fettwissenschaft e. V.
(German Society of Fats Science)
Deutsches Institut für Normung e. V.
(German Institute for Standardization)
Draft International Standard
European Central Bank
European Community listed polycyclical aromatic hydrocarbons
European Disposables and Nonwovens Association
Enzyme-Linked Immunosorbent Assay
Europäische Norm (European standard)
Environmental Protection Agency
Environmental Protection Agency listed polycyclical aromatic
hydrocarbons
Gas chromatography with atomic emission detector
Gas chromatography with mass-selective detector
Gas chromatography with flame ionisation detector
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
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GMO
HPAEC
HPAEC-PAD
HPLC
HPLC-DAD
HRGC-HRMS
IC-ICP-MS
ICP-MS
IFU
IEC
ISO
LC-MS-MS
LFGB
MOAH
MOSH
OEKO-TEX
PCB
PCDD
PCDF
PCR
Ph. Eur.
QEChERS
RFPCR
SOP
TDI
TrinkwV
UNECE
UV/VIS
VDI
VDLUFA
VO (EC)
Genetically modified organism
High-performance anion exchange chromatography
High-performance anion exchange chromatography with pulsed
amperometric detection
High-performance liquid chromatography
High-performance liquid chromatography with diode array detector
High-resolution gas chromatography - high-resolution mass
spectroscopy
Ion chromatography with inductively coupled
plasma mass spectrometry
Inductively coupled plasma mass spectrometry
International Federation of Fruit Juice Producers
International Electrotechnical Commission
International Standards Organization
Liquid chromatography - Mass spectrometry - Mass spectrometry
Lebensmittel- und Futtermittelgesetzbuch
(Foodstuff and Animal Feedstuff Code)
Mineral oil aromatic hydrocarbons
Mineral oil saturated hydrocarbons
International association for research and testing in the area of textile
ecology
Polychlorinated biphenyls
Polychlorinated dibenzodioxins
Polychlorinated dibenzofurans
Polymerase chain reaction
Pharmacopoea Europaea
Quick Easy Cheap Effective Rugged Safe
Reverse transcription polymerase chain reaction
Standard in-house operating procedure of the institute
Toluene diisocyanate
Trinkwasserverordnung (German drinking water regulations)
United Nations Economic Commission for Europe
Ultraviolet-visible spectroscopy
Verein Deutscher Ingenieure (Association of German Engineers)
Verband deutscher landwirtschaftlicher Untersuchungs- und
Forschungsanstalten
(Association of German Agricultural Analytic and Research Institutes)
Verordnung der Kommission (Ordinance of the Commission)
Period of validity: 05.10.2015 to 04.10.2020
Date of issue: 05.10.2015
- Translation -
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