Deutsche Akkreditierungsstelle GmbH
Annex to the Accreditation Certificate D-PL-14162-01-00
Accreditation based on DIN EN ISO/IEC 17025:2005
Period of validity: 01.10.2012 bis 13.09.2016
Holder of certificate:
WESSLING GmbH
For their sites
Oststraße 6-7, 48341 Altenberge
Haynauer Straße 60, 12249 Berlin
Am Umweltpark 1, 44793 Bochum
Kohlenstraße 51-55, 44795 Bochum
Ludwig-Erhard-Straße 22, 28179 Bremen
Moritzburger Weg 67, 01109 Dresden
Humboldtstraße 51-55, 22083 Hamburg
Feodor-Lynen-Straße 23, 30625 Hannover
Daniel-Seizinger-Weg 8, 68307 Mannheim
Johann-Krane-Weg 42, 48149 Münster
Forstenrieder Straße 8-14, 82061 Neuried
Hübelkamp 1, 45739 Oer-Erkenschwick
Hallesches Dreieck 4/5, 06188 Landsberg OT Oppin
An der Heide 1, 03130 Spremberg
Impexstraße 5, 69190 Walldorf
Rudolf-Diesel-Straße 23, 64331 Weiterstadt
Tests in the fields:
sampling as well as physical, physicochemical, chemical and microbiological analyses of waters,
waste water, groundwater and flowing water, raw water, bathing and swimming pool water,
eluates, soil, contaminated soil, sludge, sediments, material samples, organic fertilizers, soil
conditioners and substrates, fermentation residues, compost, biowaste, and sewage sludge,
sampling and analyses of drinking water according to the Drinking-water Ordinance: 2001, excluding
radiological parameters; selected physicochemical analyses during water sampling; sampling as well
as physical, physicochemical and chemical analyses of soil and sewage sludge according to the
Sewage Sludge Ordinance, waste for disposal and recycling, mineral oils, petrochemical products,
fuels, waste wood, secondary fuels, dust, slags, ashes, soil air, and gases; organoleptic, chemical,
This document is a translation. The definitive version is the original German annex to the accreditation certificate.
Annex to the Accreditation Certificate D-PL-14162-01-00
biological and microbiological analyses of foodstuffs, feeding stuffs, commodities, cosmetics and
specific pharmaceutical products; sampling and molecular-biological analyses of foodstuffs and
feeding stuffs; ecotoxicological and biological analyses of waters, waste water, groundwater and
flowing water, eluates of soil and contaminated soil; determination (sampling and analytics) of
polyhalogenated dibenzo-p-dioxins and dibenzofurans in waters, waste water, soil, contaminated
soil, sediments, sewage sludges, organic fertilizers, soil conditioners and substrates, compost and
biowaste, dust, slags, ashes, building waste, foodstuffs, feeding stuffs, periphyton materials, in
emissions, immissions, work place measurements and in interior rooms as well as from wiping
samples; determination (sampling and analytics) of inorganic and organic gas and particleous air
constituents in emissions, immissions, work place measurements and in interior rooms;
determination (sampling and analytics) of fibrous particles in emissions, immissions, work place
measurements and in interior rooms as well as in solid matters, dust and soil; modules water, soil
and contaminated sites as well as waste; module immission control
Abbreviations used: see page 140
The test methods listed, which are marked by (A) correspond to § 2 of the Agreement between the
Revenue Department of Hanover and the accreditation bodies DAP, DACH and DASMIN on the
accreditation of testing laboratories and engineering offices under the exploration of contaminated
sites or sites suspected of contamination on federal real estate of 22 May 2000.
Within the given test areas (or: with * marked test areas) the laboratory is permitted, without being
required to inform and obtain prior approval from the DAkkS,
*
the use of standard methods or equivalent/similar methods
**
the modification, development and introduction of test methods. The listed test methods are
given only as examples. The laboratoy has an actual list with all test methods of the flexible
accreditation area
Altenberge: For the areas of sampling and chemical analyses of water, soil and soil air the competence
is confirmed for the full scope of all required parameters
Hannover: For the areas of sampling of water, soil and soil air the competence is confirmed for the full
scope of all required parameters. For the areas of chemical analyses of water and soil the competence
for inorganic parameters is confirmed completely and the competence for organic parameters is
confirmed restricted.
München: For the areas of sampling of water, soil and soil air the competence is confirmed for the full
scope of required parameters. For the areas sampling of water, soil and soil air the competence is
confirmed fort he full scope of parameters. For the areas of chemical analytics of water, soil and soil
air the competence is confirmed completely (Variation: TOC in soil).
Oppin: For the areas of sampling of water and soil the competence is confirmed fort he full scope of
required parameters. For the areas of chemical analytics of water, soil and soil air the competence is
confirmed completely. (Variation: PBSM in water)
Walldorf: For the areas of sampling of water, soil and soil air the competence is confirmed fort the full
scope of parameters.
Period of validity: 01.10.2012 to 13.09.2016
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Annex to the Accreditation Certificate D-PL-14162-01-00
The offices, where the test methods are executed, are labelled as follows:
AL
BE
BO
BOi
BR
DR
HA
MA
MS
MÜ
OE
OP
RM
WA
= Altenberge
= Berlin
= Bochum (Am Umweltpark)
= Bochum (Kohlenstraße)
= Bremen
= Dresden
= Hannover
= Mannheim
= Münster
= München (Neuried)
= Oer-Erkenschwick
= Oppin
= Rhein-Main (Weiterstadt)
= Walldorf
Part 6 and 7:
(SA) = Sampling
(AN) = Analytic
According to the requirements of the legislator, this accreditation does not replace any recognition or
approval procedure of the responsible authority.
Period of validity: 01.10.2012 to 13.09.2016
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Content
1
Investigations in the areas water, waste water, ground water, raw water, drinking water according
to drinking-water ordinance: 2001, eluates and digestion solutions as well as extracts and migration
solutions of foodstuffs, feeding stuffs, cosmetics and commodities ..................................................... 6
1.1
Sampling......................................................................................................................................... 6
1.2
Physicochemical parameters ............................................................................................................ 8
1.3
Anions .......................................................................................................................................... 10
1.4
Cations ......................................................................................................................................... 11
1.5
Determination of Elements in all environmental matrices* ............................................................... 12
1.6
Jointly determinable substances and further organic compounds ..................................................... 13
1.7
Quick test procedure with ready-made reagents ............................................................................. 15
1.8
Investigation of water, waste water, ground water, raw water, eluates and drinking water according
to drinking water ordiance: 2001 by gas chromatography ** ............................................................ 15
1.9
Investigation in the aereas water, waste water, ground water, raw water, eluates, extracts and
drinking water (according to drinking-water ordinance 2001) by liquid cromatography (detektion by
DAD, FCD and MS/MS) ** .............................................................................................................. 18
2
Analyses of soil, contaminated soil, sludges, sewage sludge, sediments, waste, materials for
recycling, waste wood, wood, fuels, secondary fuels, organic fertlizers, soil conditioners, substrates,
compost and other biowaste, fermentation residues, digestion solutions of feeding stuffs material
samples although from fire galvanizing plants , oils, dust as well as road constructon materials .......... 20
2.1
Sampling....................................................................................................................................... 20
2.2
Sample pretreatment and sample preparation ................................................................................ 24
2.3
Physical and physicochemical paramenters ..................................................................................... 27
2.4
Anions .......................................................................................................................................... 29
2.5
Elements ...................................................................................................................................... 30
2.6
Determination of Elements using atomic absorption/atomic emission spectroscopy, ICP-OES and ICPMS in all environmental solid matters in digestion solutions, extracts and migration solutions of
foodstuffs, feeding stuffs, cosmetics and commodities * .................................................................. 32
2.7
Jointly determinable substances and further compunds ................................................................... 32
2.8
Analyses of soil, contaminated soil, sludges, sediments, waste, waste wood, wood, plastic, packaging
materials and migrates by gas chromatography** ........................................................................... 36
2.9
Analyses of soil, contaminated soil, sewage sludge, sludge, sediments and migrates by liquid
chromatography (LC by DAD-, FLD- and MS/MS -detection)** .......................................................... 40
2.10
Analysis of fuels, recovered fuels and substitute fuels- Determination of calorimetric parameters,
determination of humidity and water contents, determination of elementary materials,
stoichiometric calculation of materials ............................................................................................ 41
3
List of test methods according to Drinking Water Ordinance (TrinkwV 2001) ..................................... 44
4
List of test methods fort he Technical Module WATER ..................................................................... 50
5
List of test methods for Technical Module SOIL AND CONTAMINATES SITES As of: 20.10.2000 ........... 60
6
List of test methods fort he Technical Module WASTE ...................................................................... 74
7
Sampling and analysis of pollutants in the air .................................................................................. 87
7.1
Determination of indoor air pollutants ............................................................................................ 87
7.2
Analysis of building materials and other material samples, test chamber analyses ............................. 91
Period of validity: 01.10.2012 to 13.09.2016
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7.3
Sampling of soil gas and determination of hazardous substances in soil air and landfill gases .............. 92
7.4
Fields of testing subject to administrative regulation on pollution protection, here: technical fields
(„fields“) ....................................................................................................................................... 94
7.5
Methods for the determination and assessment of concentrations of dangerous air constituents at
working places ............................................................................................................................ 105
8
Sampling and tests of inorganic fibrous particles using scanning electron microscopy * .................... 108
9
Determination of polyhaloginated dioxines and furanes by HRGC/HRMS * ...................................... 109
10
Biological tests in surface, ground, leachate and waste water, waste, organic fertilizers, soil
improvers, substrates, compost and eluates as well as determination of the biodegradation of
chemical substances .................................................................................................................... 110
11
Test of foodstuffs, animal feeding stuffs, drinking water, mineral and table water, commodity goods,
cosmetics, air, organic fertilizers, soil improvement materials, substrates and compost .................... 113
11.1
Sampling..................................................................................................................................... 113
11.2
Microbiological methods **; Culture tests (aerobic and anaerobic) ................................................. 113
11.2.1
Cast iron plate, surface spatulate, titre, MPN, concentration method by membrane filtration and
sedimentation techniques ............................................................................................................ 113
11.2.2
Agardiffusions-method ................................................................................................................ 120
11.2.3
Microbiological technique for detection of vitamins ....................................................................... 120
11.3
Determination of constituents and contaminants using high-pressure liquid chromatography (HPLC)
using the UV/VIS-, DAD-, RI-, LF fluorescence and MS/MS detector ** ............................................. 120
11.4
Determination of constituents and contaminants using gas chromatography (GC)** ........................ 124
11.5
Atomic absorption spectrometric determination of heavy metal residues and metals using graphite
furnace and FIAS measurements as well as CV technology * ........................................................... 126
11.6
Determination of constituents using enzymatic methods (photometric, enzyme-test-kit) *............... 126
11.7
Photometric determination of constituents ** .............................................................................. 127
11.8
Thin-layer chromatographic detections of constituents * ............................................................... 128
11.9
Titrimetric determination of the content of constituents * ............................................................. 128
11.10
Gravimetric determination of constituents * ................................................................................. 129
11.11
Determination of chemical-physical parameters * ......................................................................... 130
11.12
Sensory analysis .......................................................................................................................... 131
11.13
Determination by ELISA of constituents and contaminants * .......................................................... 131
11.14
Microscopic examination of foodsuffs and feeding stuffs* .............................................................. 133
11.15
Tests of commodity goods ........................................................................................................... 133
11.16
Molecular-biological tests - detection of specific DNA segments using PCR in foodstuffs and animal
feeding stuffs **.......................................................................................................................... 134
11.17
Molecular biological analysis fort he detection of pathogens and non- pathogenic microorganisms
using PCR (thermal cycler with integrated detection) in foodstuffs, feeding stuffs and cosmetics** ... 136
11.18
Microbiological analysis in accordance with international pharmacopoeias in the respectively valid
version of proprietary medicinal products, raw materials, excipients and active substances, food
supplements, foodstuffs and feeding stuffs* ................................................................................. 136
11.19
Chemical-physical analysis in accordance with international pharmacopoeias in the respectively valid
version of proprietary medicinal products, raw materials, excipients and active substances, food
supplements, foodstuffs and feeding stuffs* ................................................................................. 137
Period of validity: 01.10.2012 to 13.09.2016
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1
1.1
Investigations in the areas water, waste water, ground water, raw water, drinking water
according to drinking-water ordinance: 2001, eluates and digestion solutions as well as extracts
and migration solutions of foodstuffs, feeding stuffs, cosmetics and commodities
Sampling
ISO 5667-4
1987-04
(A)
Water quality; Sampling; Part 4 : Guidance on sampling
from lakes, natural and man-made
ISO 5667-5
2011-02
Water quality - Sampling - Part 5: Guidance on sampling AL, BE, BO,
of drinking water from treatment works and piped
BOi, DR, HA,
distribution systems
MA, MÜ, OP,
RM, WA
ISO 5667-6
2005-07
(A)
Water quality - Sampling - Part 6: Guidance on sampling AL, BE, BO, DR,
of rivers and streams
HA, MÜ, OP,
RM, WA
ISO 5667-11
2009-04
(A)
Water quality - Sampling - Part 11: Guidance on sampling AL, BE, BO, DR,
of groundwaters
HA, MÜ, OP,
RM, WA
DIN EN ISO 5667-1 (A 4)
2007-04
(A)
Water quality - Sampling - Part 1: Guidance on the
design of sampling programmes and sampling
techniques
AL, BE, BO, DR,
HA, MA, MÜ,
OP, RM, WA
DIN EN ISO 5667-3 (A 21)
2004-05
(A)
Water quality - Sampling - Part 3: Instructions for
conservation and handling of water samples
AL, BE, BO, DR,
HA, MA, MÜ,
OP, RM, WA
DIN EN ISO 19458 (K 19)
2006-12
Water quality - Sampling for microbiological analyses
AL, BE, BO, DR,
HA, MA, MÜ,
OP, RM, WA
DIN 19559-1
1983-07
Measurement of flow of waste water in open channels
and gravity conduits; general information
AL, BE, BO, HA,
OP
DIN 19559-2
1983-07
Measurement of flow of waste water in open channels
and gravity conduits; venturi flumes
AL, BE, BO, HA,
OP
DIN 38402-11
(A 11)
2009-02
German standard methods for the examination of water, AL, BE, BO, DR,
waste water and sludge - General information (group A) HA, MÜ, OP,
- Part 11: Sampling of waste water (A 11)
RM, WA
Period of validity: 01.10.2012 to 13.09.2016
Translation
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HA, MÜ, OP,
RM, WA
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DIN 38402-12 (A 12)
1985-06
(A)
German standard methods for the examination of water, AL, BE, BO, DR,
waste water and sludge; general information (group A); HA, MÜ, OP,
sampling from barrages and lakes (A 12)
RM, WA
DIN 38402-13 (A 13)
1985-12
(A)
German standard methods for the examination of water, AL, BE, BO, DR,
waste water and sludge; general information (group A); HA, MÜ, OP,
sampling from aquifers (A 13)
RM WA
DIN 38402-14 (A 14)
1986-03
German standard methods for the examination of water, AL, BE, BO, DR,
waste water and sludge; general information (group A); HA, MA, MÜ,
sampling of untreated water and drinking water (A 14) OP, RM, WA
(withdrawn standard)
DIN 38402-15 (A 15)
2010-04
(A)
German standard methods for the examination of water, AL, BE, BO, DR,
waste water and sludge - General information (group A) HA, MÜ, OP,
- Part 15: Sampling from running waters
RM, WA
(A 15)
DIN 19643-1
2011-05
Treatment of water of swimming pools and baths - Part
1: General requirements
AL, BE, BO, DR,
HA, MÜ, OP,
RM, WA
LAWA AQS
Bulletin P-8/1
2009-09
Sampling of waste water
AL, BE, BO, DR,
HA, MÜ, OP,
RM, WA
LAWA AQS
Bulletin P-8/2
1995-05
Sampling of groundwater
AL, BE, BO, DR,
HA, MÜ, OP,
RM, WA
LAWA AQS
Bulletin P-8/3
1998-05
Sampling from flowing waters
AL, BE, BO,
BOi, DR, HA,
MÜ, OP, RM,
WA
LAWA AQS
Bulletin P-8/4
2002-05
Sampling of sediment and suspended matter
AL, BE, BO,
BOi, DR, HA,
MÜ, OP, RM,
WA
LAGA PN 1/75
1976
Taking of water samples
(withdrawn standard)
AL, BOi, OP
Period of validity: 01.10.2012 to 13.09.2016
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Further applicable documents:
DVGW W 112
2010-05
(A)
Water sampling for preparation, extraction and
monitoring of groundwater
DVGW W 115
2008-07
(A)
Bore holes for exploration, extraction and monitoring of AL, BE, BO,
groundwater
BOi, DR, HA,
MÜ, OP, RM,
WA
DVGW W 121
2003-07
(A)
Construction of groundwater measurement points
AL, BE, BO,
BOi, DR, HA,
MÜ, OP, WA
DVWK Regulations 128
1992
(A)
Taking of groundwater samples and extent of analyses
AL, BE, BO,
BOi, DR, HA,
MÜ, OP
DVWK Regulations 136
1999
German association for Water Management and cultural AL, BOi, OP
builidings e.V.: Pedological analyses in the fields for the
determination of characteristic values for site
characterisation,
Part II: Discharges to the water and air economy of soils
DVWK Regulations 245
1997
(A)
German association for Water Management and cultural AL, BE, HA,
builidings e.V.: Depth-oriented sampling from
MÜ, OP
groundwater measuring points
1.2
AL, BE, BO,
BOi, DR, HA,
MÜ, OP, RM,
WA
Physicochemical parameters
DIN 38402-30 (A 30)
1998-07
Pretreatment, homogenization and aliquotation of non- AL, BE, BO, HA,
homogeneous water samples
MÜ, OP, RM,
WA
DIN EN ISO 15587-2 (A32)
2002-07
Water quality - Digestion for the determination of
elements in water - Part 2: Nitric acid digestion
AL, HA, MÜ,
OP
DEV B 1/2
1971
Testing with regard to odour and taste
(withdrawn standard)
AL, BE, BO, HA,
MÜ, OP, RM,
WA
DIN EN 1622 (B 3)
2006-10
Determination of the threshold odour number (TON)
and threshold flavour number (TFN)
AL, HA, MÜ,
RM, WA
Period of validity: 01.10.2012 to 13.09.2016
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DIN EN ISO 7887 (C 1)
1994-12
(A)
Water quality - Examination and determination of colour AL, HA, MÜ,
OP, RM, WA
DIN EN ISO 7027 (C 2)
2000-04
(A)
Water quality - Determination of turbidity
DIN EN ISO 7393-2 (G 4-2)
2000-04
Water quality - Determination of free chlorine and total AL, BE; BO,
chlorine - Part 2: Colorimetric method using N,N-diethyl- HA, MÜ, OP,
1,4-phenylenediamine, for routine control purposes
RM, WA
DIN EN 25814 (G 22)
1992-11
(A)
Determination of dissolved oxygen by the
electrochemical probe method
AL, BE, BO,
BOi, DR, HA,
MÜ, OP, RM,
WA
DIN EN 27888 (C 8)
1993-11
(A)
Water quality - determination of electrical conductivity
AL, BE, BO,
BOi, DR, HA,
MÜ, OP, RM,
WA
DIN 38404-3 (C 3)
2005-07
Physical and physico-chemical parameters (group C) Part 3: Determination of absorption in the range of the
ultraviolet radiation, Spectral absorptions coefficient
(C 3)
AL, HA, MÜ,
OP, RM
DIN 38404-4 (C 4)
1976-12
(A)
Physical and physico-chemical Parameters (Group C);
Determination of Temperature (C4)
AL, BE, BO,
BOi, DR, HA,
MÜ, OP, RM,
WA
DIN 38404-5 (C 5)
2009-07
(A)
Physical and physico-chemical characteristics (group C) - AL, BE, BO, DR,
Part 5: Determination of pH value (C 5)
HA, MÜ, OP,
RM, WA
DIN EN ISO 10523
2012-04
Water quality - determination of pH
AL, BE, BO,
DR, HA, OP,
RM, MÜ, WA
DIN 38404-6 (C 6)
1984-05
(A)
Physical and physico-chemical parameters (group C);
determination of the oxidation reduction (redox)
potential (C 6)
AL, BE, BO, DR,
HA, MÜ, OP,
RM, WA
DIN 38404-10 (C 10)
1995-04
Physical and physico-chemical parameters (group C) Part 10: Calcit saturation of water (C 10)
AL, HA, MÜ,
OP, RM, WA
Period of validity: 01.10.2012 to 13.09.2016
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OP, RM, WA
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EPA method 180.1
1993-08
1.3
Determination of turbidity by nephelometry
RM
Anions
DIN EN ISO 6878 (D11)
2004-09
(A)
Water quality - Determination of phosphorus Ammonium molybdate spectrometric method
AL, HA, MÜ,
OP, WA
DIN EN ISO 10304-1 (D 20)
2009-07
(A)
Water quality - Determination of dissolved anions by
liquid chromatography of ions - Part 1: Determination
of bromide, chloride, fluoride, nitrate, nitrite,
phosphate and sulfate
(BO without nitrite)
(OP: without fluoride, nitrite, orthophosphate)
(MÜ: additionally: acetate and formate
AL, BO, HA,
MÜ, OP, RM,
WA
DIN EN ISO 10304-1 (D 19)
1995-04
Water quality - Determination of dissolved anions by
liquid chromatography of ions - Part 1: Determination
of bromide, chloride, fluoride, nitrate, nitrite,
phosphate and sulfate
(withdrawn standard)
AL, BO, HA,
MÜ, OP, RM,
WA
DIN EN ISO 10304-2 (D 20)
1996-11
Water quality - Determination of dissolved anions by
liquid chromatography of ions - Part 2: Determination
of bromide, chloride, nitrate, nitrite, orthophosphate
and sulfate in waste water
(withdrawn standard)
AL, BO, HA,
MÜ, OP, RM,
WA
DIN EN ISO 10304-3 (D 22)
1997-11
(A)
Water quality - Determination of dissolved anions by
liquid chromatography of ions - Part 3: Determination
of chromate, iodide, sulfite, thiocyanate and
thiosulfate
AL, HA
DIN EN ISO 14403 (D 6)
2002-07
(A)
Water quality - Determination of total cyanide and free
cyanide by continuous flow analysis
AL, MÜ, OP,
WA
E DIN EN ISO 14403-2 (D 3) Water quality - Determination of total cyanide and free
2009-11
cyanide using flow analysis (FIA and CFA) - Part 2:
Method with continuous flow analysis
AL, MÜ, OP,
WA
DIN EN ISO 15061 (D 34)
2001-12
AL, RM
Water quality - Determination of dissolved bromate Method by liquid chromatography of ions
Period of validity: 01.10.2012 to 13.09.2016
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DIN EN ISO 18412 (D 40)
2007-02
Water quality - Determination of chromium(VI) Photometric method for weakly contaminated water
AL, HA, MÜ,
OP RM, WA,
DIN EN 1189 (D 11)
1996-12
Water quality - Determination of phosphorus Ammonium molybdat spectrometric method
(withdrawn standard)
AL, HA OP, WA
DIN EN 26777 (D 10)
1993-04
(A)
Water quality; determination of nitrite; molecular
absorption spectrometric method
AL, HA, MÜ,
OP, RM, WA
DIN 38405-4 (D 4)
1985-07
(A)
Determination of fluoride
AL, HA, MÜ,
OP, WA
DIN 38405-8-(D 8)
1971
Calculation of dissolved carbon dioxide, of carbonateund hydrogen carbonate
AL, HA, MÜ,
OP, RM, WA
DIN 38405-13 (D 13)
1981-02
(A)
Determination of cyanides
AL, HA, MÜ,
WA
DIN 38405-14 (D 14)
1988-12
(A)
Determination of cyanides in drinking water, and in
groundwater and surface water with low pollution
levels
AL, HA, MÜ,
WA
DIN 38405-21 (D 21)
1990-10
Determination of dissolved silicate by spectrometry
AL, OP
DIN 38405-24 (D 24)
1987-05
(A)
Photometric determination of chromium(VI) using 1,5diphenylcarbonohydrazide
AL, HA, MÜ,
OP, RM, WA
DIN 38405-26 (D 26)
1989-04
(A)
Determination of dissolved sulfide by spectrometry
AL, HA, MÜ,
OP
DIN 38405-27 (D 27)
1992-07
Determination of readily liberatet sulfide
1.4
AL, HA, MÜ,
OP, WA
Cations
DIN EN ISO 11732 (E 23)
2005-05 (A)
Water quality - Determination of ammonium nitrogen Method by flow analysis (CFA and FIA) and
spectrometric detection
Period of validity: 01.10.2012 to 13.09.2016
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DIN EN ISO 11885 (E 22)
2009-09
(A)
Water quality - Determination of selected elements by
inductively coupled plasma optical emission spectrometry (ICP-OES)
AL, HA, MÜ,
OP
DIN EN ISO 17294-2 (E 29) Water quality - Application of inductively coupled
2005-02 (A)
plasma mass spectrometry (ICP-MS) - Part 2:
Determination of 62 elements
(HA, RM, WA : additionally determination of mercury)
AL, HA, RM,
WA
DIN EN 1483 (E 12)
2007-07
(A)
Water quality - Determination of mercury - Method
using atomic absorption spectrometry
AL, HA, MÜ,
OP
DIN EN 26595 (D12)
1993-01
Water quality; determination of total arsenic; silver
diethyldithiocarbamate spectrophotometric method
HA
DIN 38406-1 (E 1)
1983-05
Determination of iron
AL, HA, MÜ,
OP, WA
DIN 38406-2 (E 2)
1983-05
Determination of manganese
HA
DIN 38406-5 (E 5)
1983-10
(A)
Determination of ammonia-nitrogen
AL, BO, HA,
MÜ, OP, RM,
WA
DIN 38406-29 (E 29)
1999-05
Determination of 61 elements by mass spectrometry
with inductively coupled plasma atomic emission
spectroscopy (ICP-MS)
(AL, HA, RM, WA: additionally determination of
phosphorous and iron)
(RM, WA: additionally determination of mercury)
(withdrawn standard)
1.5
AL, HA, RM,
WA
Determination of Elements in all environmental matrices*
DIN EN ISO 11885 (E 22)
2009-09
(A)
Water quality - Determination of selected elements by
inductively coupled plasma optical emission
spectrometry
HA
DIN EN ISO 17294-2 (E 29)
2005-02
Water quality - Application of inductively coupled
plasma mass spectrometry (ICP-MS) - Part 2:
Determination of 62 elements
HA
Period of validity: 01.10.2012 to 13.09.2016
Translation
12/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN EN 1483 (E 12)
2007-07
(A)
Water quality - Determination of mercury - Method
using atomic absorption spectrometry
HA
WES 292
2008-05
Semi quantitative element screening by ICP-MS
HA
1.6
Jointly determinable substances and further organic compounds
ISO 8245
1999-03
(A)
Water quality - Guidelines for the determination of total AL, OP, RM
organic carbon (TOC) and dissolved organic carbon
(DOC)
DIN EN ISO 8467 (H 5)
1995-05
Water quality - Determination of permanganate index
DIN EN ISO 9377-2 (H 53)
2001-07
(A)
Water quality - Determination of hydrocarbon oil index - AL, HA, MÜ,
Part 2: Method using solvent extraction and
OP, RM, WA
gas chromatography
DIN EN ISO 9562 (H 14)
2005-02
(A)
Water quality - Determination of adsorbable organically AL, HA, MÜ,
bound halogens (AOX)
OP, RM
DIN EN ISO 11905-1 (H 36)
1998-08
Water quality - Determination of nitrogen - Part 1:
Method using oxidative digestion with peroxodisulfate
HA
DIN EN ISO 14402 (H 37)
1999-12
Water quality - Determination of phenol index by flow
analysis (FIA and CFA)
AL, MÜ, OP,
WA
DIN ISO 15705 (H 45)
2003-01
Water quality - Determination of the chemical oxygen
demand index (ST-COD) - Small-scale sealed tube
method
AL, MÜ, OP
DIN EN 872 (H 33)
2005-04
Water quality - Determination of suspended solids Method by filtration through glass fibre filters
AL, HA, OP,
WA
DIN EN 1484 (H 3)
1997-08
(A)
Water analysis - Guidelines for the determination of
AL, HA, MÜ,
total organic carbon (TOC) and dissolved organic carbon OP, RM
(DOC)
DIN EN 1485 (H 14)
1996-11
Water quality - Determination of adsorbable organically AL, HA, MÜ,
bound halogens (AOX)
OP, RM
(withdrawn standard)
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL, HA, MÜ,
OP, RM
13/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN EN 1899-1 (H 51)
1998-05
Water quality - Determination of biochemical oxygen
demand after n days (BODn - Part 1: Dilution and
seeding method with allylthiourea acid addition
(Variation MÜ: respirometric measurement)
AL, HA, MÜ,
OP
DIN EN 1899-2 (H 52)
1998-05
Water quality - Determination of biochemical oxygen
demand after n days (BODn) - Part 2: Method for
undiluted samples
(Variation MÜ: respirometric measurement)
AL, HA, MÜ,
OP
DIN EN 25663 (H 11)
1993-11
(A)
Water quality- Determination of Kjedahl nitrogen;
method after mineralization with selenium
(Variation AL: Digestion with Titandioxid-catalyst)
(Variation HA: Digestion with Missouri-catalyst)
AL, HA, OP
DIN 38409-1 (H 1)
1987-01
(A)
Determination of total dry residue, filtrate dry residue
and residue on ignition
AL, HA, MÜ,
OP, RM, WA
DIN 38409-2 (H 2)
1987-03
Determination of filterable matter and the residue on
ignition
AL, HA, MÜ,
OP, RM, WA
DIN 38409-6 (H 6)
1986-01
Water hardness
AL, HA, MÜ,
(Variation: Determination of the calcium and magnesium OP, RM, WA
content with the ICP-OES or ICP-MS)
DIN 38409-7 (H 7)
2005-12
Determination of acid and base-neutralizing capacities
AL, HA, MÜ,
OP, RM, WA
DIN 38409-8 (H 8)
1984-09
(A)
Determination of the extractable, organically bound
halogens (EOX)
(withdrawn standard)
AL, HA, MÜ,
OP, RM
DIN 38409-9 (H 9)
1980-07
Determination of the settleable matter by volume in
water and waste water
AL, HA, MÜ,
OP, RM, WA
DIN 38409-16 (H 16)
1984-06
(A)
Determination of the phenol index
AL, HA, MÜ,
OP, WA
DIN 38409-17 (H 17)
1981-05
Determination of not easily volatised, lipophile
substances (Boiling point > 250 °C)
(withdrawn standard)
OP
DIN 38409-22 (H 22)
2001-02
Determination of dissolved adsorbable and organically
bound halogens in salt loaded water (SPE-AOX)
AL, HA, MÜ,
OP
Period of validity: 01.10.2012 to 13.09.2016
Translation
14/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN 38409-23 (H 23)
1980-05
Determination of methylen blue active and bismut active OP
substances
V DEV H 25
1989
Determination of strippable organically bound halogens AL, HA, OP
(POX)
DIN 38409-27 (H 27)
1992-07
Determination of total bound nitrogen TNb
(withdrawn standard)
OP
DIN 38409-28 (H 28)
1992-04
Determination of bound nitrogen after reduction with
Devarda's alloy and catalytic digestion
(withdrawn standard)
HA, OP
DIN 38409-41 (H 41)
1980-12
(A)
Determination of the Chemical Oxygen Demand (COD) in AL, HA, OP
the Range over 15 mg/l (H41)
DIN 38409-44 (H 44)
1992-05
Determination of the chemical oxygen demand (COD),
ranging from 5 to 50 mg/l (H 44)
HA
DIN 38409-56 (H 56)
2009-06
Gravimetric determination of low volatile lipophilic
substances after solvent extraction
AL, HA, MÜ,
OP, WA
DIN 38413-1 (P 1)
1982-03
Determination of hydrazine
HA
1.7
Quick test procedure with ready-made reagents
Machery & Nagel
Visocolor 914015
1.8
Detergents, cationic 1-20 mg
OP
Investigation of water, waste water, ground water, raw water, eluates and drinking water
according to drinking water ordiance: 2001 by gas chromatography **
Flexible accreditation area: AL**, BE**, BO**, MÜ**, OP**; RM*
ISO 18857-2
2009-09
Water quality - Determination of selected alkylphenols - BO
Part 2: Gas chromatographic-mass spectrometric
determination of alkylphenols, their ethoxylates and
bisphenol A in non-filtered samples following solidphase extraction and derivatisation
Period of validity: 01.10.2012 to 13.09.2016
Translation
15/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN EN ISO 6468 (F 1)
1997-02
(A)
Water quality - Determination of parathion, parathionmethyl and some other organophosphorus compounds
in water by dichloromethane extraction and gas
chromatographic analysis
(Variation AL, BO, OP: MS-Detection, without
Chlorbenzenes)
AL, BO, OP
DIN EN ISO 10301 (F 4)
1997-08
(A)
Water quality - Determination of highly volatile halogenated hydrocarbons - Gas-chromatographic methods
(Additionally: Mono- and dichlorobenzene)
AL, HA, MÜ,
OP, RM
DIN EN ISO 10695 (F 6)
2000-11
(A)
Determination of selected organic nitrogen and
phosphorus compounds - Gas- chromatographic
methods
(Variation BE: MS-Detection and FPD)
AL, BO, BE
DIN EN ISO 16588 (P10)
2004-02
Water quality - Determination of six complexing agents - MÜ
Gas-chromatographic method
(Variation: Determination of five complexing agents)
DIN EN ISO 17353 (F 13)
2005-11
Water quality - Determination of selected organotin
compounds - Gas- chromatographic method
DIN EN ISO 17495 (F 23)
2003-09
Water quality - Determination of selected nitrophenols - MÜ
Method by solid phase extraction and gas
chromatography with mass spectrometric detection
(Variation: Liquid-liquid extraction)
DIN EN ISO 22032 (F 28)
2009-07
Water quality - Determination of selected
BO
polybrominated diphenyl ethers in sediment and sewage
sludge - Method using extraction and gas
chromatography/mass spectrometry
DIN EN 12673 (F 15)
1999-05
(A)
Water quality - gas chromatographic determination of
some selected chlorophenols in water
AL, MÜ, OP
DIN EN 12918 (F 24) mod.
1999-11
Water quality - Determination of parathion, parathionmethyl and some other organophosphorus compounds
in water by dichloromethane extraction and gas
chromatographic analysis
BO
DIN EN 14207 (P 9)
2003-09
Water quality - Determination of epichlorohydrin
BE
Period of validity: 01.10.2012 to 13.09.2016
Translation
OP
16/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN EN 61619, VDE 0371-8
1998-02
Insulating liquids - Contamination by polychlorinated
AL
biphenyls (PCBs) - Method of determination by capillary
column gas chromatography
DIN 38407-2 (F 2)
1993-02
(A)
Determination of low volatile halogenated hydrocarbons AL, HA, MÜ,
by gas chromatography
OP
(Variation: MS-detection)
DIN 38407-3 (F 3)
1998-07
(A)
Determination of polychlorinated biphenyls
DIN 38407-9 (F 9)
1991-05
(A)
Determination of benzene and some of ist derivatives by AL, HA, MÜ,
gas chromatography
OP, RM
(Additionally: Detemination of naphthalenes)
(MÜ: additionally: Determination of naphthalenes, nAlkane, test spirit)
(OP: additionally: Determination of naphthalenes, C5 to
C12 Alkane)
DIN 38407-16 (F16)
1999-06
Determination of aniline derivates by gas
chromatography
DIN 38407-17 (F 17)
1999-02
Determination of selected nitroaromatic compounds by MÜ, OP
gas-liquid chromatography
(Additionally: Chlornitroaromate)
E DIN 38407-27 (F27)
2008-11
Determination of selected phenols in groundwater and
leachate
E DIN 38407-39 (F39)
2008-08
Determination of selected polycyclic aromatic
WA
hydrocarbons (PAH) - Method using gas chromatography
with mass spectrometric detection (GC-MS)
DIN 38413-2 (P 2)
1988-05
(A)
Determination of vinyl chloride by headspace gas
chromatography
AL, BE, HA,
MÜ, OP, RM
EPA 8032A
1996-12
Determination of Acrylamide by gas Chromatography
BE
WES 103
1996
GC-MS-survey analysis in water, soil and ground air
(Extraction procedure with pentane and HeadspaceProcedure)
AL, OP, RM
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL, BO, HA,
MÜ, OP, RM,
WA
MÜ
MÜ
17/141
Annex to the Accreditation Certificate D-PL-14162-01-00
WES 105
2007
Simultaneous determination of highly volatile
hydrocarbon oil index and of BTEX-aromatics in Water
and Soil by headspace gas chromatography (GC-MS- in
house method)
AL
WES 199
2010-03
Determination of chlorinated paraffins C10-C13 (PCA
C10-C13) in water by GC/MS
BO
WES 418
2008-12
Determination of ethylene glycol / propylene glycol in
water by GC-MS after derivatisation
MÜ
WES 421
2009-01
Determination of alkyl-, chlorine und nitrophenols in
water by GC-MS after derivatisation
MÜ
WES 470
2009-07
Determination of herbicides in water by GC-MS after
solid phase extraction
MÜ
WES 494
2009-12
Determination of biphenyl in water/eluate by
GC/MS
BO
1.9
Investigation in the aereas water, waste water, ground water, raw water, eluates, extracts
and drinking water (according to drinking-water ordinance 2001) by liquid cromatography
(detektion by DAD, FCD and MS/MS) **
Flexible accreditation area: AL**
ISO 16000-3
2002-08
Determination of formaldehyde and other carbonyl
compounds - Active sampling method
(Variation: Messurement of water samples with and
without enrichment over SPE- collums)
HA
ISO 25101
2009-03
Water quality - Determination of
perfluorooctanesulfonate (PFOS) and
perfluorooctanoate (PFOA) - Method for unfiltered
samples using solid phase extraction and liquid
chromatography/mass spectrometry
AL
DIN EN ISO 11369 (F 12)
1997-11
(A)
Water quality - Determination of selected plant
treatment agents - Method using high performance
liquid chromato-graphy with UV detection after solidliquid extraction
(Variation: Acidification of the sample with
trifluoroacetic acid before concentration)
AL, HA, MÜ
Period of validity: 01.10.2012 to 13.09.2016
Translation
18/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN EN ISO 17993 (F 18)
2004-03
Water quality - Determination of 15 polycyclic aromatic AL, HA, MÜ,
hydrocarbons (PAH) in water by HPLC with fluorescence OP, RM
detection after liquid-liquid extraction
DIN EN ISO 22478 (F 21)
2006-07
Water quality - Determination of certain explosives and AL
related compounds - Method using high-performance
liquid chromatography (HPLC) with UV detection
DIN 38407-8 (F 8)
1995-10
(A)
Determination of 6 polynuclear aromatic hydrocarbons
(PAH) in water by high performance liquid chromatography (HPLC) with fluorescence detection
DIN 38407-22 (F 22)
2001-10
Determination of Glyphosate and Aminomethyl phosphic MÜ
acid (AMPA) by high performance liquid chromatography
(HPLC), post-column derivatization and fluorescence
detection
(Variation: precolumn derivatisation)
DIN 38407-42 (F 42)
2011-03
Determination of selected polyfluorinated compounds
(PFC) in water - Method using high performance liquid
chromatography and mass spectrometric detection
(HPLC/MS-MS) after solid-liquid extraction
AL
DIN 38414-14 (S 14)
2011-08
Determination of selected polyfluorinated compounds
(PFC) in sludge, compost and soil - Method using high
performance liquid chromatography and mass
spectrometric detection (HPLC-MS/MS) (S 14)
AL
WES 010
2001
Determination of polycyclic halogenated hydrocarbons
in foodstuffs according to ASU L 07.00-40 (12/89);
Determination by HPLC
(Variation: Sample preparation by product analytics)
AL
WES 050
2008-08
PFT: Perfluorinated carbonic- and sulfonic acids in water AL
WES 412
2008-08
Determination of pesticides by LC-MS/MS ESI and online AL
accumulation
WES 438
2009-02
Determination of X-ray contrast medium in water/eluate AL
by LC-MS/MS
WES 452
2010-04
Determination of pesticide metabolites in water, direct
injection and measurement by LC-MS/MS
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL, HA, MÜ,
OP, RM
AL
19/141
Annex to the Accreditation Certificate D-PL-14162-01-00
WES 524
2010-04
Determination of pesticide metabolites (UBA-list) by LC- AL
MS/MS
WES 532
2010-09
Determination of medicinal products in water LC-MS/MS AL
2
Analyses of soil, contaminated soil, sludges, sewage sludge, sediments, waste, materials for
recycling, waste wood, wood, fuels, secondary fuels, organic fertlizers, soil conditioners,
substrates, compost and other biowaste, fermentation residues, digestion solutions of
feeding stuffs material samples although from fire galvanizing plants , oils, dust as well as
road constructon materials
2.1
Sampling
DIN ISO 10381-1
2003-08
(A)
Soil quality - Sampling - Part 1: Guidance on the design
of sampling programmes
AL, BE, BOi,
DR, HA, MA,
MÜ, OP
DIN ISO 10381-2
2003-08
(A)
Soil quality - Sampling - Part 2: Guidance on sampling
techniques
AL, BE, BO,
BOi, DR, HA,
MA, MÜ, OP,
WA
DIN ISO 10381-3
2002-08
(A)
Soil quality - Sampling - Part 3: Guidance on safety
AL, BE, BOi,
DR, HA, MA,
MÜ, OP, WA
DIN ISO 10381-4
2004-04
(A)
Soil quality - Sampling - Part 4: Guidance on the
AL, BE, BOi,
procedure for investigation of natural, near-natural and DR, HA, MA,
cultivated sites
MÜ, OP, WA
DIN ISO 10381-5
2007-02
(A)
Soil quality - Sampling - Part 5: Guidance on the
procedure for the investigation of urban and industrial
sites with regard to soil contamination
ISO 10381-8
2006-04
(A)
Soil quality - Sampling - Part 8: Guidance on sampling of AL, BE, BO,
stockpiles
BOi, DR, HA,
MA, MÜ, OP,
RM, WA
DIN EN ISO 5667-13 (S 1)
1998-02
Water quality - Sampling - Part 13: Guidance on sampling AL, BE, BO,
of sludges
BOi, DR, HA,
MÜ, OP, RM,
WA
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL, BE, BOi,
Dr, HA, MA,
OP
20/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN EN ISO 14688-1
2003-01
(A)
Geotechnical investigation and testing - Identification
and classification of soil - Part 1: Identification and
description
AL, BE, BOi,
DR, HA, MA,
MÜ, OP
DIN EN ISO 14688-2
2004-11
Geotechnical investigation and testing - Identification
and classification of soil - Part 2: Principles for a
classification
AL, BE, BOi,
DR HA, MA,
OP
DIN EN ISO 14689-1
2004-04
(A)
Geotechnical investigation and testing - Identification
and classification of rock - Part 1: Identification and
description
AL, BE, BOi,
DR, HA, MA,
MÜ, OP
DIN EN ISO 22475-1
2007-01
(A)
Geotechnical investigation and testing - Sampling
methods and groundwater measurements - Part 1:
Technical principles for execution
AL, BE, BOi,
DR, HA, MA,
MÜ, OP
DIN EN 932-1
1996-11
(A)
Test for general properties of aggregates - Part 1:
Methods for sampling
AL, BE, BOi,
HA, MA, MÜ,
OP
DIN 4023
2006-02
Geotechnical investigation and testing - Graphical
presentation of logs of boreholes, trial pits, shafts and
adits
AL, BE, BOi,
DR, HA, MA,
OP
DIN 4030-2
2008-06
(A)
Assessment of water, soil and gases for their aggressive- AL, BE, BOi,
ness to concrete; collection and examination of water
DR, HA, MA,
and soil samples
MÜ, OP, RM
DIN 19671-1
1964-05
Soil drilling apparatus for drawing soil samples in
agricultural engineering; groove borers, tube borers
AL, BE, BOi,
HA, MA, MÜ,
OP, WA
DIN 19682-2
2007-11
(A)
Soil quality - Field tests - Part 2: Determination of soil
texture
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
DIN 19682-10
2007-11
Methods of soil investigations for agricultural water
engineering - Field tests - Part 2: Determination of soil
texture
AL, BE, BOi,
HA, MA, OP
DIN 38414-11 (S 11)
1987-08
Sampling of sediments
AL, BE, BO,
BOi, DR, HA,
MÜ, OP
Period of validity: 01.10.2012 to 13.09.2016
Translation
21/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN 51750-1
1990-12
Sampling of petroleum products; general information
AL, BO, DR,
HA, MÜ, OP
DIN 52101
2005-06
(A)
Aggregates test methods - Sampling
AL, BE, BO,
BOi, HA, MA,
MÜ, OP
LAGA PN 98
2001-12
(A)
Directive for the procedure in physical, chemical and
biological investigations in connection with the
utilisation / disposal of waste basic rules for taking
samples from solid and compact waste as well as stored
materials
AL, BE, BO,
BOi, DR, HA,
MA, MÜ, OP,
RM, WA
LAGA PN 2/78 K
1983-12
Basic rules for taking samples from waste and stored
materials
(withdrawn standard)
AL, BE, BO,
BOi, DR, HA,
MA, MÜ, OP,
RM, WA
LAGA PN 2/78
1983-12
Taking and preparation of samples from solid sludgy
and liquid waste
(withdrawn standard)
AL, BE, BO,
BOi, DR, HA,
MA, MÜ, OP,
RM, WA
AbfKlärV, Annex 1
1992-04
Sampling, sample preparation and analysis of sewage
sludge and soil
AL, BE, BO,
BOi, DR, HA,
MA, MÜ, OP,
WA
AltholzV, Annex IV No. 1.1
2002-08
Sampling of wood chips and splints
AL, BE, BO,
DR, HA, MÜ,
OP, RM, WA
AltölV, Annex 2
2002-04
Sampling and analysis of waste oils
AL, BE, BO;
HA, MÜ, OP,
WA
BioAbfV, Annex 3, No. 1.1
1998-09
Sampling of treated and untreated biowaste
AL, BE, BO,
BOi, HA, MÜ,
OP, WA
Federal Compost
Association: Book of
method chapter I A
2006-09
Sampling
AL, BO, DR,
HA, MÜ, OP,
WA
Period of validity: 01.10.2012 to 13.09.2016
Translation
22/141
Annex to the Accreditation Certificate D-PL-14162-01-00
WES 101
1999
Sampling of building substance; Material sampling of
building materials to test for chemical and biological
pollutants
BE, DR
Further applicable documents:
BBodSchG; BBodSchV
German Federal Soil Protection Act and Ordinance
BAM-OFD-H
(respectively valid version)
Demands on sampling, sample preparation and chemical AL, BE, BO,
analysis methods on federal real property
BOi, DR, HA,
MA, MÜ, OP,
RM, WA
DVWK Regulations 129
1995
Pedological analyses in the fields for the determination
of characteristic values for site characterisation,
Part I: Response of soils
AL, BOi, MA,
OP
NLfB/BGR
2010-03
Symbol key Geology, Hanover
AL, BE, BOi,
HA, MA, OP
ITVA
1995-09
(A)
Engineer-technical Association for Contaminated Sites:
Technical Aid F2-1, exploration procedures for solid
matter sampling to be used for suspicious areas and
contaminated sites
AL, BE, BOi,
HA, MA, OP
Working Group for
Pedology of the Geological
State Authorities and the
BGR
2005
Instructions for Pedological Mapping, 5th edition
AL, BE, BOi,
HA, MA, MÜ,
OP, WA
Working Group for Rural
Soils 1997
Recommendations of the Working Group for Rural Soils AL, BE, BOi,
of the German Pedological Association for Pedological
HA, MA, OP
Mapping of Urban, Commercial, Industrial and
Montanely Overshaped Areas (Urban Soils), Part1: Field
Guide
ad-hoc-Working Group
Soil of the FederationLänder-Committee Soil
Research
1996
Instructions for Taking Soil Samples
Geol. Yearbook, Series G, H. 1, Hanover
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL, BE, BO,
BOi, DR, HA,
MA, MÜ, OP,
RM, WA
AL, BE, BOi,
HA, MA, OP
23/141
Annex to the Accreditation Certificate D-PL-14162-01-00
BGR 128
Rules of the Professional Association for Safety and
Health during Work (BG-rules)
BGR 128 - Contaminated Areas
AL, BE, BO,
BOi, HA, MA,
MÜ, OP
BioAbfV Annex
Sampling - Determination of the soil type
BE
2.2
Sample pretreatment and sample preparation
DIN ISO 11466
1997-06
(A)
Soil quality - Extraction of trace elements soluble in aqua
regia
(Additionally: Digestion with DigiPREP)
AL, HA, MÜ,
OP, RM, WA
DIN ISO 14507
2004-07
(A)
Soil quality - Pretreatment of samples for determination of
organic contaminants
AL, HA, MÜ,
OP, RM, WA
DIN EN 420
2010-03
Protective gloves - General requirements and test methods
AL
DIN EN 12457-1
2003-01
Characterization of waste - Leaching; Compliance test for
AL, HA, MÜ,
leaching of granular and sludges - Part 1: One stage batch
OP
test at a liquid to solid ration of 2 l/kg with particle size below
4 mm (without or with size reduction)
DIN EN 12457-2
2003-01
Characterization of waste - Leaching; Compliance test for
AL, HA, MÜ,
leaching of granular and sludges - Part 2: One stage batch
OP
test at a liquid to solid ratio of 10 l/kg with particle size below
4 mm (without or with size reduction)
DIN EN 12457-4
2003-01
Characterization of waste - Leaching; Compliance test for
leaching of granular waste materials and sludges - Part 4:
One stage batch test at a liquid to solid ratio of 10 l/kg for
materials with particle size below 10 mm (without or with
limited size reduction)
DIN EN 13346 (S 7a)
2001-04
Characterization of sludges - Determination of trace elements AL, HA, MÜ,
and phosphorus - Aqua regia extraction methods
OP, RM, WA
(Additionally: Digestion with DigiPREP)
DIN EN 13656
2003-01
Characterization of waste - Microwave assisted digestion with AL, OP
hydrofluoric (HF), nitric (HNO3) and hydrochloric (HCl) acid
mixture for subsequent determination of elements in waste
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL, HA, MÜ,
OP, RM, WA
24/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN EN 13657
2003-01
Characterization of waste - Digestion for subsequent
determination of aqua regia soluble portion of elements in
waste
(Additionally: Use of a closed microwave)
Note: MÜ, HA, WA only thermic digestion
E DIN 19527
2010-05
Leaching of solid materials - Batch test for the examination of AL, HA, MÜ,
the leaching behaviour of organic substances at a liquid to
OP
solid ratio of 2 l/kg
DIN 19528
2009-1
Leaching of solid materials - Percolation method for the joint AL, MÜ, OP
examination of the leaching behaviour of inorganic and
organic substances
DIN 19529
2009-01
Leaching of solid materials - Batch test for the examination of AL, HA, MÜ,
the leaching behaviour of inorganic substances at a liquid to OP
solid ratio of 2 l/kg
DIN 19730
2009-07
(A)
Soil quality - Extraction of trace elements with ammonium
nitrate solution
AL, HA, MÜ,
RM
DIN 19731
1998-05
Soil quality - Utilization of soil material
AL, BOi, HA,
MA, OP
DIN 19747
2009-07
(A)
Investigation of solids - Pre-treatment, preparation and
processing of samples for chemical, biological and physical
investigations
AL, BO, HA,
MÜ, OP, RM,
WA
DIN 38414-4 (S 4)
1984-10
(A)
Determination of leachability by water
AL, HA, MÜ,
OP, RM, WA
DIN 38414-12 (S 12)
1986-11
Determination of phosphorus in sludges and sediments
AL
DIN 38414-22 (S 22)
2000-09
(A)
Determination of dry residue by freezing and preparation
of the freeze dried mass of sludge
AL, OP
AbfKlärV
Annex 1
1997-03
Sampling, sample preparation and analysis of sewage sludge AL, BO, HA,
and soil
MÜ, OP, WA
(BO: only sampling)
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL, HA, MÜ,
OP, WA
25/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Annex 1 No. 1.1
AbfKlärV
1997-03
Preparation of collected samples and partitioning of samples AL
Annex 1 No. 1.2
AbfKlärV
1997-03
Sample preparation, homogenization, centrifugation, freeze
drying
AL
Annex IV No. 1.2
Preparation of the laboratory sample, partitioning of samples AL, WA
AltholzV in conjunction
with DIN 51701-3
(08.85)
BbodSchV Annex 1
1999
Leaching method 1 - Soil saturation extract
AL, HA, MÜ
DIN 38414-4 (S4)
1984-10
Leaching method 2 (modified S4-method) regarding the
procedural notes of the BBodSchV (Annex 1, 3.1.2)
AL, HA, MÜ,
OP
column test - or
lysimeter-test
Possibilities for execution of state of the art column test - or
lysimeter-test;
e.g.. LUA-bulletin No. 20 - DIN V 19736
AL, MÜ
LUA-bulletin No. 20
2000-03
Recommendation for procedure and evaluation of column
experiments according to Federal Soil Protection and
Contaminated Sites Ordinance (BbodSchV)
MÜ
DepV, Annex 4, No.
3.1.1
2006-12
Sample preparation: Reduction, breaking and milling of solid AL, MÜ, OP
samples to laboratory samples
Method book BGK e. V. Sample pretreatment
chapter I B
2006-09
AL, OP
E DIN IEC 62554
2009-10
AL, BO
Measurement of mercury level in fluorescent lamps (IEC
34A/1344/CD:2009)
(only sample preparation)
in conjunction with:
Regulation (EG) No.
244/2009 of the
commission of 18
March 2009
Period of validity: 01.10.2012 to 13.09.2016
Implementation of Directive 2005/327EG of
the European Parliament and the Council
concerning establishment of requirements for
ecodesign of directional household lamps.
Translation
26/141
Annex to the Accreditation Certificate D-PL-14162-01-00
2.3
Physical and physicochemical paramenters
DIN ISO 10390
2005-12
(A)
Soil quality - Determination of pH-value
(Additionally: Soils of fields directly after ploughing)
AL, HA, MÜ,
OP, RM, WA
DIN ISO 11265
1997-06
(A)
Soil quality - Determination of the specific electrical
conductivity
AL, HA, MÜ,
OP, RM, WA
DIN ISO 11277
2002-08
Soil quality - Determination of particle size distribution in
mineral soil material - Method by sieving and sedimentation
B) Sedimentation by areometer method
AL
DIN ISO 11464
2006-12
(A)
Soil quality - Pretreatment of samples for physicochemical analyses
(withdrawn standard)
AL, HA, MÜ,
OP, RM, WA
DIN ISO 11465
1996-12
(A)
Soil quality - Determination of dry matter and water
content on a mass basis - Gravimetric method
AL, BO, HA,
MÜ, OP, RM,
WA
DIN EN ISO 2719
2003-09
Determination of flash point - Pensky-Martens closed cup BO
method
DIN EN ISO 3680
2004-07
Determination of flash/no flash - Rapid equilibrium closed BO
cup method
DIN EN ISO 6245
2003-01
Petroleum products - Determination of ash
BO
DIN EN 196-2
2005-05
Methods of testing cement - Part 2: Chemical analysis of
cement
(Variation: only determination of loss on ignition)
OP
DIN EN 322
1993-08
Wood-based panels; determination of moisture content
OP
DIN EN 12176 (S 5)
1998-06
Characterization of sludge - Determination of pH-value
AL, BO, HA,
MÜ, OP, RM,
WA
DIN EN 12880 (S 2a)
2001-02
(A)
Characterization of sludges - Determination of dry residue AL, BO, HA,
and water content
MÜ, OP, RM,
WA
Period of validity: 01.10.2012 to 13.09.2016
Translation
27/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN EN 12879 (S 3a)
2001-02
Characterization of sludges - Determination of the loss on AL, BO, HA,
ignition of dry mass
MÜ, OP, RM,
WA
DIN EN 14629
2007-06
Products and systems for the protection and repair of
concrete structures - Test methods - Determination of
chloride content in hardened concrete
OP
DIN EN 15216
2008-01
Characterization of waste - Determination of total
dissolved solids (TDS) in water and eluates
AL, HA, MÜ,
OP, RM, WA
E DIN EN 15935
2010-11
Sludge, treated biowaste, soil and waste - Determination
of loss on ignition
OP
DIN 18123
1996-11
Soil, investigation and testing - Determination of grain-size AL
distribution
DIN 19683-12
1973-04
(A)
Methods of soil investigations for agricultural water
engineering - Physical laboratory tests - Part 12:
Determination of dry bulk density
AL
DIN 19684-3
2000-08
(A)
Methods of soil investigations for agricultural water
engineering - Chemical laboratory tests - Part 3: Determination of the loss on ignition and the residue of soil
after ignition
AL, RM
DIN 52182
1976-09
Testing of wood; determination of density
WA
DIN 52183
1977-11
Testing of wood; Determination of humidity content
(withdrawn standard)
AL, BO, OP
CEN/TC 343/WG3 N47
Version 1.3
Determination of the biomass content by the selective
solution method
BO
LAGA EW 98
2002
Directive for the procedure in physical and chemical
BE, HA, MÜ,
investigations of waste, contaminated soils and materials OP
from the abandoned polluted areas
AbfKlärV
Annex 1
1997-03
Sampling, sample preparation and analysis of sewage
sludge and soil
AL, HA, MÜ,
OP, RM, WA
BioAbfV
1998-09
Determination of the salt content, the content of foreign
matter, dry raw unit weight
AL
Period of validity: 01.10.2012 to 13.09.2016
Translation
28/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Book of methods BGK e.
V., Chapter II A1
2006-09
Determination of the water content
AL, OP
Book of methods
BGK e. V.
Chapter III C 1
2006-09
Determination of the pH-value
AL, OP
Book of methods
BGK e. V.
Chapter III C 2
2006-09
Determination of the salt content
AL, OP
VDLUFA method D 2.1
1997
Determination of soil texture of fine soil by finger test
MÜ, OP
HLUG method
Handbook Contaminated
Sites, volume 7, part 3
Determination of selected explosives and their
degradation products in solids from the waste sector
OP
ISO 11262
2003-09
(A)
Soil quality - Determination of cyanide
(Variation MÜ: additionallyly photometric measurement
of absorption solutions by CFA)
AL, HA, MÜ,
OP
DIN ISO 17380
2006-05
(A)
Soil quality - Determination of total cyanide and easily
released cyanide - Continuous-flow analysis method
AL, MÜ, OP,
WA
DIN 4030-2
2008-06
Assessment of water, soil and gases for their aggressive- AL, HA, MÜ,
ness to concrete; collection and examination of water and OP, RM
soil samples
DIN 38405-4 (D 4)
1985-07
Determination of fluoride
AL, HA, MÜ,
OP
DIN 38405-27 (D 27)
1992-07
Determination of dissolved sulfide by spectrometry
(Variation for soils: Addition of soda lye)
AL, HA, OP
2.4
Anions
Period of validity: 01.10.2012 to 13.09.2016
Translation
29/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN 51084
2008-11
(A)
Testing of oxidic raw materials for ceramic, glass and
glazes; determination of fluoride content
(Variation for soils: Hydrolysis with soda lye; absorption
and shaking with water, determination with ion-selective
electrode)
AL, OP
DIN ISO 16772
2005-06
(A)
Soil quality - Determination of mercury in aqua regia soil
extracts with cold-vapour atomic spectrometry or coldvapour atomic fluorescence spectrometry
AL, HA, MÜ,
OP
DIN ISO 22036
2009-06
Soil quality - Determination of trace elements in extracts
of soil by inductively coupled plasma - atomic emission
spectrometry (ICP-AES)
AL, HA, MÜ,
OP
E DIN IEC 62554
2009-10
Measurement of mercury level in fluorescent lamps (IEC
34A/1344/CD:2009)
AL
2.5
Elements
in conjunction with:
Regulation (EG) No. 244/2009 Implementation of Directive
2005/327EG of the European
of the commission of 18
March 2009
Parliament and the Council
concerning establishment of
requirements for ecodesign of
directional household lamps.
DIN EN ISO 11885 (E 22)
2009-09
(A)
Water quality - Determination of selected elements by
AL, HA, MÜ,
inductively coupled plasma optical emission spectrometry OP
(ICP-OES)
(Variation for soils: Digestion with aqua regia, calibration
of the matrix)
(Additionally: Determination of nutrients pursuant to
AbfKlärV)
DIN EN ISO 17294-2 (E 29) Water quality - Application of inductively coupled plasma AL, HA, RM,
2005-02
mass spectrometry (ICP-MS) - Part 2: Determination of
WA
62 elements
(Additionally: Digestion with aqua regia)
DIN EN 1483 (E 12)
2007-07
Determination of mercury
(Additionally: Digestion with aqua regia)
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL, HA, MÜ,
OP
30/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN EN 10240
1998-02
Internal and/or external protective coatings for steel
tubes - Specification for hot dip galvanized coatings
applied in automatic plants
DIN EN 12441-1 bis 11
2004-10
Zinc and zinc alloys - Chemical analysis
OP
Digestion and determination of differnt metals
(Variation: Determination of Elements by ICP-OES (DIN EN
ISO 11885) in the extraction solution. Poor weighted
sample, bore chips)
DIN EN 15309
2007-08
Characterization of waste and soil - Determination of
elemental composition by X-ray fluorescence
BO
DIN 19734
1999-01
(A)
Soil quality - Determination of Cr(VI) in phosphatebuffered solution
(withdrawn standard)
AL, HA, MÜ
DIN 38406-5-2 (E 5-2)
1983-10
Determination of ammonia-nitrogen
AL, HA, OP,
RM, WA
DIN 38406-29 (E 29)
1999-05
Determination of 61 elements by mass spectrometry with AL, HA, RM,
inductively coupled plasma (ICP-MS)
WA
(Variation for soils: Determination in aqua regia-extraction
solution, compensation of matrix disturbances),
(withdrawn standard)
VDLUFA method / A
6.2.1.1
1991
Soil investigation;
Determination of phosphorus and potassium in calciumacetate-lactate-extract
AL, HA, MÜ,
OP
VDLUFA method / A
6.2.1.2
1991
Soil investigation;
Determination of phosphorus and potassium in double
lactate extract
AL, HA, OP
VDLUFA method / A
6.2.4.1
1991
Soil investigation;
Determination of the plant-available magnesium in the
calcium chloride-extract
AL, HA, MÜ,
OP
AbfKlärV
Annex 1
1997-03
Sampling, sample preparation and analysis of sewage
sludge and soil
AL, HA, MÜ,
OP, WA
Period of validity: 01.10.2012 to 13.09.2016
Translation
OP
31/141
Annex to the Accreditation Certificate D-PL-14162-01-00
2.6
Determination of Elements using atomic absorption/atomic emission spectroscopy, ICP-OES
and ICP-MS in all environmental solid matters in digestion solutions, extracts and migration
solutions of foodstuffs, feeding stuffs, cosmetics and commodities *
DIN ISO 16772
2005-06
Soil quality - Determination of mercury in aqua regia soil
extracts with cold-vapor atomic spectrometry or coldvapor atomic fluorescence spectrometry
HA
DIN ISO 22036
2009-06
Soil quality - Determination of trace elements in extracts
of soil by inductively coupled plasma - atomic emission
spectrometry (ICP-AES)
HA
DIN EN ISO 11885 (E 22)
2009-09
(A)
Determination of selected elements by inductively
coupled plasma optical emission spectrometry (ICP-OES)
HA
DIN EN ISO 17294-2 (E 29) Water quality - Application of inductively coupled
2005-02
plasma mass spectrometry (ICP-MS) - Part 2:
Determination of 62 elements
HA
DIN EN 1483 (E 12)
2007-07
(A)
Water quality - Determination of mercury - Method
using atomic absorption spectrometry
HA
DIN EN 14538
2006-09
Fat and oil derivatives - Fatty acid methyl ester (FAME) - HA
Determination of Ca, K, Mg and Na content by optical
emission spectral analysis with inductively coupled plasma
(ICP OES)
DIN 51396-1
2005-08
Testing of lubricants - Determination of wear elements Part 1: Direct determination by inductively coupled
plasma optical emission spectroscopy (ICP-OES)
HA
WES 292
2008-05
Semi quantitative element screening by ICP-MS
HA
2.7
Jointly determinable substances and further compunds
DIN ISO 10694
1996-08
(A)
Soil quality - Determination of organic and total carbon
after dry combustion (elementary analysis)
BO, HA, OP,
WA
DIN ISO 11261
1997-05
(A)
Soil quality - Determination of total nitrogen - Modified
Kjeldahl method (TiO2 as catalyst)
AL, HA
Period of validity: 01.10.2012 to 13.09.2016
Translation
32/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN EN ISO 14402 (H 37)
1999-12
Water quality - Determination of phenol index by flow
analysis (FIA and CFA)
(Variation for soils: slurry mixing of the samples with
destilled water and external destillation)
AL, MÜ, OP,
WA
DIN EN 120
1992-08
Wood-based panels; determination of formaldehyde
content; extraction method called perforator method
OP
DIN EN 12506
2003-09
Characterization of waste - Analysis of eluates AL, OP
Determination of pH, As, Ba, Cd, CI-, Co, Cr, Cr(VI), Cu, Mo,
Ni, NO2-, Pb, total S, SO42-, V and Zn
DIN EN 13137
2001-12
Characterization of waste - Determination of total organic BO, HA, OP,
carbon (TOC) in waste, sludges and sediments
WA
DIN EN 13639
2002-07
Determination of total organic carbon in limestone
OP
DIN EN 13370
2003-09
Characterization of waste - Analysis of eluates Determination of Ammonium, AOX, conductivity, Hg,
phenol index, TOC, CN- easily liberatable, F-
AL, OP
DIN EN 14345
2004-12
Characterization of waste - Determination of hydrocarbon AL
content by gravimetry
DIN EN 14582
2007-06
Characterization of waste - Halogen and sulfur content - BO, OP, WA
Oxygen combustion in closed systems and determination
methods
(Variation: only for the determination of sulfur, chlorine,
fluorine and bromine)
E DIN EN 15171
2005-04
Characterization of sludges - Determination of adsorbable OP
organically bound halogens
(withdrawn standard)
DIN EN 62321
2009-12
Electrotechnical products - Determination of levels of six
regulated substances (lead, mercury, cadmium,
hexavalent chromium, polybrominated biphenyls,
polybrominated diphenyl ethers)
BO
DIN 38409-16 -2 (H 16-2)
1984-06
(A)
Determination of the phenol index
(Variation for soils: slurrying the samples with distilled
water)
AL, HA, MÜ,
OP
Period of validity: 01.10.2012 to 13.09.2016
Translation
33/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN 38409-17 (H 17)
1981-05
Determination of not easily volatised, lipophile substances OP
(Boiling point > 250 °C)
(Variation for soils: Extraction with 1,1,2-trichlorotrifluoroethane and ultrasound)
(withdrawn standard)
DIN 38409-56 (H 56)
2009-06
Gravimetric determination of low volatile lipophilic
substances after solvent extraction
(Variation for soils: Soxhlet Extraction or ultrasound)
AL, HA, MÜ,
OP, WA
DIN 38414-17 (S 17)
1989-11
(A)
Determination of strippable and extractable organically
bound halogens
(Additionally: soils)
AL, HA, MÜ,
OP, RM
DIN 38414-18 (S 18)
1989-11
Determination of adsorbed organically bound halogens
(AOX)
(Additionally: soils)
AL, HA, MÜ,
OP
DIN 51084
2008-11
Testing of oxidic raw materials for ceramic, glass and
glazes; determination of fluoride content- method A:
Fused cast bead method; electrometric determination
(Variation: no distillation)
OP
DIN 51777-1
1983-03
Testing of mineraloil hydrocarbons and solvents;
BO
determination of water content according to Karl Fischer;
direct method
VDLUFA book of
methods,
Volume VII, 3.3.3.1
1996
Determination of herbicides in soils by means of high
power liquid-chromatography with UV-detection
WA
AbfKlärV, Annex 1
1997-03
Sampling, sample preparation and analysis of sewage
sludge and soil
AL, BO, HA,
MÜ, OP, WA
AbfKlärV, Annex 1
1997-03
Determination of low volatile, lipophile substances
AL
AbfKlärV, Annex 1
1997-03
(A)
Alkaline effective compounds
AL, HA, OP
AbfAblV
Annex 4 No. 3.3
2006-12
Extractable lipophile compounds
AL, HA, MÜ,
OP
Period of validity: 01.10.2012 to 13.09.2016
Translation
34/141
Annex to the Accreditation Certificate D-PL-14162-01-00
AltholzV
2002-08
Determination of fluorine and chlorine content
BO, WA
AltölV
2002-04
Determination of the total halogen content
BO, OP
Federal Technical
Association derived fuels
2008-10
Sampling - sample preparation - and analysis regulation
Determinination of humidity, net calorific value, chlorine
and ash content
BO, OP, WA
Book of methods
BGK e. V.
chapter III A 1
2006-09
Total content of plant nutrients
AL, OP
Book of methods
BGK e. V.
chapter III A2
2006-09
Soluble vegetable nutrients
AL, OP
Book of methods
BGK e. V.
chapter III B 1
2006-09
Organic compounds
AL, OP
Book of methods
BGK e. V.
chapter III B 2
2006-09
Anorganic compounds
AL, OP
Book of methods
BGK e. V.
chapter III C 4
2006-09
Potential hazardous substances
AL, OP
Book of methods
BGK e. V.
chapter III C 5
2006-09
Organic hazardous substances
(Variation: PCB and F2-parameter, measurement by
GC-MS)
AL
WES 560
2011
Determination of elemental carbon (EC) and degradable
carbon (AOC)
WA
Period of validity: 01.10.2012 to 13.09.2016
Translation
35/141
Annex to the Accreditation Certificate D-PL-14162-01-00
2.8
Analyses of soil, contaminated soil, sludges, sediments, waste, waste wood, wood, plastic,
packaging materials and migrates by gas chromatography**
Flexible accreditation area: AL**, BO**, MÜ**, OP**, RM*
DIN ISO 10382
2003-05
(A)
Soil quality- Determination of organochlorine pesticides and AL, BO, HA,
polychlorinated biphenyls- gas chromatographic method
MÜ, OP, WA
with electron capture detection
(Note: Organochlorine pesticides, low volatila
halogenhydrocarbons: Extraction with iso-hexan/acetone
(50:50), if required, chromatographic purification after
elimination of acetone; Chlorobenzene-extraction with
acetone/iso-hexane; GC-ECD or GC-MS)
(WA and HA: only analysis of polychlorinated biphenyls)
(BO: additionally PCB in platics, mod. analysis)
DIN ISO 14154
2005-12
(A)
Soil quality - Determination of some selected chlorophenols - Gas-chromatographic method with electroncapture detection
(Additionally: Phenol, PCP and alkyl phenols)
AL, MÜ
DIN ISO 16703
2005-12
(A)
Soil quality - Determination of content of hydrocarbon in
the range C10 to C40 by gas chromatography
AL, HA, MÜ,
OP, RM, WA
DIN ISO 18287
2006-05
Soil quality - Determination of polycyclic aromatic
hydrocarbons (PAH) - Gas chromatographic method with
mass spectrometric detection (GC-MS)
WA
ISO 18857-2
2009-09
Water quality - Determination of selected alkylphenols Part 2: Gas chromatographic-mass spectrometric
determination of alkylphenols, their ethoxylates and
bisphenol A in non-filtered samples following solid-phase
extraction and derivatisation
BO
DIN ISO 22155
2006-07
Soil quality- Gas chromatographic quantitative
determination of volatile aromatic and halogenated
hydrocarbons and selected ethers - Static headspace
method
(RM: additionally extraction with 2-Methoxyethanol),
(MU: additionally naphthalene, n-alkane, test spirit),
(OP: additionally naphthalene, C5- to C12 alkane)
(RM: additionally HLUG method Handbook Contaminated
Sites, volume 7, part 4)
AL, HA, MÜ,
OP, RM
Period of validity: 01.10.2012 to 13.09.2016
Translation
36/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN ISO 22892
2006-09
Soil quality - Guidelines for the identification of target
AL
compounds by gas chromatography and mass spectrometry
DIN EN ISO 22032 (F 28) Water quality - Determination of selected polybrominated
2009-07
diphenyl ethers in sediment and sewage sludge - Method
using extraction and gas chromatography/mass
spectrometry
BO
DIN EN 12766-1
2000-11
Petroleum products and used oils - Determination of PCBs AL, BO, HA
and related products - Part 1: Separation and determination
of selected PCB congeners by gas chromatography (GC)
using an electron capture detector (ECD)
DIN EN 12766-2
2001-12
Petroleum products and used oils - Determination of PCBs AL, BO, HA
and related products - Part 2: Calculation of polychlorinated
biphenyl (PCB) content
DIN EN 12766-3
2005-02
Petroleum products and used oils - Determination of PCBs
and related products - Part 3: Determination and
quantification of polychlorinated terphenyls (PCT) and
polychlorinated benzyl toluenes (PCBT) content by gas
chromatography (GC) using an electron capture detector
(ECD)
BO
DIN EN 14039
2005-01
Characterization of waste - Determination of hydrocarbon
content in the range of C10 to C40 by gas chromatography
AL, HA, MÜ,
OP, RM, WA
DIN EN 15308
2008-05
Characterization of waste - Determination of selected
polychlorinated biphenyls (PCB) in solid waste by using
capillary gas chromatography with electron capture or
mass spectrometric detection
AL, OP, RM,
WA
DIN EN 15527
2008-09
Characterization of waste - Determination of polycyclic
aromatic hydrocarbons (PAH) in waste using gas
chromatography mass spectrometry (GC/MS)
WA
E DIN 19744
2003-08
Identification and quantitative determination of organic
stannic compounds in solid materials (soils, sediments,
wastes)
(withdrawn standard)
OP
DIN 38407-2 (F 2)
1993-02
determination of low volatile halogenated hydrocarbons by AL, OP
gas chromatography
(Variation: Measurement with mass detector)
(Additionally: Chlorobenzenes)
Period of validity: 01.10.2012 to 13.09.2016
Translation
37/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN 38407-3 (F 3)
1998-07
Determination of polychlorinated biphenyls
AL, BO, OP,
WA
DIN 38407-9 (F 9)
1991-05
(A)
Determination of benzene and some of its derivatives by
headspace gas chromatography
(Variation for soils: Extraction with methanol or 2-methoxy
ethanol, conversion of an aliquot in water, GC-MS)
(MÜ: additionally naphthalene, n-alkane, test spirit)
AL, HA, MÜ,
OP, RM
DIN 38407-9-2 (F 9-2)
1991-05
(A)
Determination of benzene and some of its derivatives by
gas chromatography
(Variation for soil: Extraction with pentane or iso-hexane
and ultrasound, GC-MS)
(Additionally: Mono- and dichlorobenzene)
AL, RM
DIN 38413-2 (P 2)
1988-05
(A)
Determination of vinyl chloride by headspace gas
chromatography
(Variation for soils: Extraction with methanol or
2-methoxyethanol, conversion of an aliquot in water, GCMS)
AL, HA, MÜ,
OP, RM
DIN 38414-20 (S 20)
1996-01
(A)
Determination of 6 polychlorinated biphenyls (PCB)
(Additionally for soils: Ultrasound extraction of air-dried
samples; cleaning at acid and neutral silica gel/
benzenesulfonic acid)
AL, BO, HA,
MÜ, OP, RM,
WA
DIN 51527-1
1987-05
Testing of petroleum products; determination of polychlorinated biphenyls (PCB); preseparation by liquid
chromatography and determination of six selected PCB
compounds by gas chromatography using an electron
capture detector
(withdrawn standard)
AL, BO, HA,
MÜ, OP
ISO/TR 11046
1994-06
(A)
Soil quality;
Determination of the mineral oil content - procedure by
means of infrared-spectrometry and gas-chromatographic
procedure
(Additionally: extraction with iso-hexane and ultrasound)
AL, HA, OP
KW/04
2009-12
Determination of hydrocarbon content in waste
AL, HA, MÜ,
OP, WA
AltholzV
2002-08
Determination of pentachlorophenol (PCP)
AL
Period of validity: 01.10.2012 to 13.09.2016
Translation
38/141
Annex to the Accreditation Certificate D-PL-14162-01-00
AltholzV
2002-08
Determination of polychlorinated biphenyls (PCB)
VDLUFA book of
methods, Volume VII,
3.3.3.1
1996
Determination of PAH in soils, sewage sludge and composts WA
WES 041
2002-07
Determination of Trinidad Epuré in asphalt and mineral oil BE
bitumen on the basis of typical biomarkers by means of GCMS
WES 103
1996
GC-MS-survey analysis in water, soil and ground air
(Extraction procedure with pentane and HeadspaceProcedure)
AL, OP, RM
WES 199
2010-03
Determination of chlorinated paraffins C10-C13
(PCA C10-C13)in solids by GC/MS
BO
WES 212
2007-12
Determination of short chain aliphatic acids in fermentation AL
residues by GC-FID
WES 429
2009-10
Determination of alkyl-, chloro- and nitrophenols in soil by
GC-MS after extraction and following derivatisation
WES 449
2009-04
Determination of ethylene/propylene glycol in solids by GC- MÜ
MS after derivatisation
WES 466
2009-08
Determination of anilines in soils by GC-MS after direct
extraction
MÜ
WES 494
2009-12
Determination of biphenyl in solids by GC/MS
BO
WES 498
2010-02
Determination of organo-Phosphates in solids by GC/MS
BO
WES 499
2010-01
Determination of phosphates and phthalates in plastics by
GC/MS
BO
WES 512
2010-02
Determination of nonylphenol/octylphenol, their
ethoxylates and bisphenol A in plastics by GC/MS
BO
WES 517
2010-06
Determination of poly aromatic hydrocarbons (PAH’s)
BO
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL, BO, HA,
OP, WA
MÜ
39/141
Annex to the Accreditation Certificate D-PL-14162-01-00
WES 530
2010-08
2.9
Determination of anilines in soils by GC-MS after acid
elution
MÜ
Analyses of soil, contaminated soil, sewage sludge, sludge, sediments and migrates by liquid
chromatography (LC by DAD-, FLD- and MS/MS -detection)**
Flexible accreditation area: AL**
DIN ISO 11264
2005-11
(A)
Soil quality- Determination of herbicides- Method using HPLC
with UV-detection
(Variation: acidification of samples with trifluoroacetic acid
before extraction)
AL
DIN ISO 13877
2000-01
(A)
Soil quality - Determination of polynuclear aromatic
hydrocarbons - Method using high-performance liquid
chromatographic
AL, HA, MÜ,
OP, RM
ISO 16000-3
2002-08
Determination of formaldehyde and other carbonyl
HA
compounds
(Variation: Measurement of solids after extraction with DNPHsolution)
DIN EN ISO 22478
2006-07
Water quality- Determination of certain explosives and related AL
compounds- Method using high- performance liquid
chromatography (HPLC) with UV detection
(Varation for soils: Extraction by shaking with
methanol/acetonitril)
DIN 38414-23 (S 23)
2002-02
(A)
Determination of 15 polycyclic aromatic hydrocarbons (PAH)
by high performance liquid chromatography (HPLC) and
fluorescence detection
AL, HA, MÜ,
OP, RM
LUA-bulletin No. 1
1994-04
(A)
Determination of polycyclic aromatic hydrocarbons (PAHs) in
soil samples
AL, HA, MÜ,
OP, RM
VDLUFA books of
methods,
Chapter VII, 3.3.1
1996
Determination of herbicides in soils by means of high power
liquid-chromatography with UV-detection
AL
WES 077
2008-08
Perfluorinated carbonic- and sufonic acids in solid materials
AL
WES 401
2008-08
PFT: Perfluorooctanoic acid (PFOA) and
Perfluorooctanesulfonic acid (PFOS) in soil
AL
Period of validity: 01.10.2012 to 13.09.2016
Translation
40/141
Annex to the Accreditation Certificate D-PL-14162-01-00
WES 402
2008-08
PFT: Perfluorooctanoic acid (PFOA) and
Perfluorooctanesulfonic acid (PFOS) in sewage sludge
AL
DFG 405
1991
Determination of residue of pesticides- Glyphosat in water and MÜ
soil by high performance liquid chromatography (HPLC), postcolumn derivatization and fluorescence detection
(Variation: precolumn derivatisation with FMOC)
2.10 Analysis of fuels, recovered fuels and substitute fuels- Determination of calorimetric
parameters, determination of humidity and water contents, determination of elementary
materials, stoichiometric calculation of materials
DIN EN 451-1
2004-05
Method of testing fly ash - Part 1: Determination of free
calcium oxide content
OP
DIN EN 14346
2007-03
Characterization of waste - Calculation of dry matter by
determination of dry residue or water content
AL, BO, HA,
MÜ, OP, WA
DIN EN 14582
2007-06
Characterization of waste - Halogen and sulfur content Oxygen combustion in closed systems and determination
methods
(Variation: only for determination of sulfur, chlorine, fluorine
and bromine)
BO, OP, WA
DIN EN 14774-2
2010-04
Solid biofuels - Determination of moisture content - Oven dry
method - Part 2: Total moisture - Simplified method
WA
DIN EN 14775
2010-04
Solid biofuels - Determination of ash content
OP, WA
DIN EN 14918
2009-05
Solid biofuels - Determination of calorific value
OP, WA
DIN EN 15103
2010-04
Solid biofuels - Determination of bulk density
WA
DIN EN 15169
2007-05
Characterization of waste - Determination of loss on ignition in AL, BO, HA,
waste, sludge and sediments
MÜ, OP, RM,
WA
DIN EN 15170
2009-05
Characterization of sludges - Determination of calorific value
BO, OP, WA
DIN CEN/TS 15289
2006-07
Solid biofuels - Determination of total content of chlorine and
sulfur
OP, WA
Period of validity: 01.10.2012 to 13.09.2016
Translation
41/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN CEN/TS 15414-1
Prestandard, 200701
Solid recovered fuels - Determination of moisture content
using the oven dry method - Part 1: Determination of total
moisture by a reference method
OP
DIN CEN/TS 15414-2
Prestandard, 200701
Solid recovered fuels - Determination of moisture content
using the oven dry method - Part 2: Determination of total
moisture by a simplified method
OP, WA
DIN EN 15414-3
Draft standard,
2009-08
Solid recovered fuels - Determination of moisture content
using the oven dry method - Part 3: Moisture in general
analysis sample
OP
DIN EN 15440
2011-05
Solid recovered fuels - Methods for the determination of
biomass content
BO, OP
DIN CEN/TS 15440
Prestandard, 200702
Annex B, D, E
Solid recovered fuels - Method for the determination of
biomass content
BO, OP
Annex B:
Determination of biomass content by using the method of
selective dissolution
Annex D:
Determination of biomass content as percentage of energy
content (calorific value)
Annex E:
Determination of total carbon content of biomass and not
biomass fraction by selective dissolution
(Variation: the carbon content of the SRF-sample-ash is strictly
arithmetically included, even if the ash content is < 10% )
DIN 22022-1
2001-02
Solid fuels - Determination of contents of trace elements - Part OP
1: General rules, sampling and sample preparation;
Preparation of samples for the analyses (dissolution method)
(Additionally: digestion after addition of hydrochloric acid and
determination of main elements)
DIN 51701-2
2006-09
Testing of solid fuels - Sampling and sample prepara-tion Execution of sampling
DIN 51720
2001-03
Testing of solid fuels - Determination of volatile matter content OP
(Variation: no special crucible)
DIN 51718
2002-06
Testing of solid fuels - Determination of the water content and BO, OP, WA
the moisture of analysis sample
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL, BO, HA,
OP, RM
42/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN 51719
1997-07
Testing of solid fuels - Solid mineral fuels - Determination of
ash content
BO, OP, WA
DIN 51727
2001-06
Testing of solid fuels- Determination of chlorine content Prozess B (calometric bomb) - Determination with
potentiometric titration (Argentometry)
BO, OP, WA
DIN 51732
2007-08
Testing of solid mineral fuels - Determination of total carbon,
hydrogen and nitrogen - Instrumental methods
OP
DIN 51777-1
1983-03
Testing of mineraloil hydrocarbons and solvents;
determination of water content according to Karl Fischer;
direct method
BO, OP
DIN 51900-1
2000-04
Correction 1
2004-02
Testing of solid and liquid fuels - Determination of gross
calorific value by the bomb calorimeter and calculation of net
calorific value - Part 1: Principles, apparatus, methods
(Variation for BO: without element analysis)
BO, OP
DIN 51900-2
2003-05
Testing of solid and liquid fuels - Determination of the gross
BO
calorific value by the bomb calorimeter and calcu-lation of the
net calorific value - Part 2: Method using isoperibol ot static,
jacket calorimeter
DIN 51900-3
1977-08
Follow-up document
2005-01
Testing of solid and liquid fuels - Determination of gross
OP
calorific value by the bomb calorimeter and calculation of net
calorific value - Part 3: Method using adiabatic jacket
(Variation for OP: Determination of N optional by element
analysis (DIN 51732) or ion chromatography;
Determination of S optional by ion chromatography or ICP-OES)
Period of validity: 01.10.2012 to 13.09.2016
Translation
43/141
Annex to the Accreditation Certificate D-PL-14162-01-00
3
List of test methods according to Drinking Water Ordinance (TrinkwV 2001)
Sampling
by own staff
DIN EN ISO 5667-5
DIN EN ISO 5667-3 (A 21)
DIN EN ISO 19458 (K 19)
by external staff
Test method2
Water quality - Sampling - Part 5: Guidance
on sampling of drinking water from
treatment works and piped distribution
systems
Water quality - Sampling - Part 3: Guidance
on the preservation and handling of water
samples
Water quality - Sampling for microbiological
analysis
DIN 38402-12 (A 12)
DIN 38402-13 (A 13)
DIN 38402-15 (A 15)
DVWK Regulation 128
1992
LAWA AQS Bulletin P-8/2
2
Sites
AL, BE, BO,
HA, MÜ, OP,
RM, WA
AL, BE, BO,
HA, MÜ, OP,
RM, WA
AL, BE, BO,
HA, MÜ, OP,
RM, WA
AL, BE, BO,
HA, MÜ, OP,
RM, WA
German standard methods for the
examination of water, waste water and
sludge; general information (group A);
sampling from barrages and lakes
German standard methods for the
AL, BE, BO,
examination of water, waste water and
HA, MÜ, OP,
sludge; general information (group A);
RM, WA
sampling from aquifers
German standard methods for the
AL, BE, BO,
examination of water, waste water and
HA, MÜ, OP,
sludge - General information (group A) RM, WA
Part 15: Sampling from running waters
Taking of groundwater samples and extent AL, BE, BO,
of analyses
HA, MÜ, OP,
RM, WA
Sampling of groundwater
AL, BE, BO,
HA, MÜ, OP,
RM, WA
current valid version
Period of validity: 01.10.2012 to 13.09.2016
Translation
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Annex to the Accreditation Certificate D-PL-14162-01-00
ATTACHMENT 1: MICROBIOLOGICAL PARAMETERS
Part I: General requirements for water intended for human consumption
No.
Parameter
1
Escherichia coli (E. coli)
2
Enterococci
Test methods2
DIN EN ISO 9308-1
with Colilert®-18/Quanti-Tray®
DIN EN ISO 7899-2
with Chromocult® Enterococci agar
Sites
AL, OP, WA
OP, WA
AL, OP, WA
Part II: Requirements for water intended for human consumption for filling in bottles or other
containers for purpose of export
No.
Parameters
1
Escherichia coli (E. coli)
2
Enterococci
3
Pseudomonas aeruginosa
Test methods2
DIN EN ISO 9308-1
with Colilert®-18/Quanti-Tray®
DIN EN ISO 7899-2
with Chromocult® Enterococci agar
DIN EN ISO 16266
Sites
AL, OP, WA
OP, WA
AL, OP, WA
AL, OP, WA
ATTACHMENT 2: CHEMICAL PARAMETERS
Part I: Chemical parameters- constant concentration in distribution network including house
installation
No.
Parameters
1
Acrylamide
2
Benzene
Test methods2
calculated on the basis of product
specification
DIN 38407-9 (F 9)
DIN EN ISO 11885 (E22)
3
Boron
EN ISO 17294-2 (E 29)
4
Bromate
DIN EN ISO 15061 (D 34)
DIN EN ISO 11885 (E22)
5
Chromium
EN ISO 17294-2 (E 29)
3
Sites
3
AL, HA, MÜ,
OP, RM
AL, HA, MÜ,
OP
AL, HA, RM,
WA
AL, RM
AL, HA, MÜ,
OP
AL, HA, RM,
WA
The calculation can not be accredited.
Period of validity: 01.10.2012 to 13.09.2016
Translation
45/141
Annex to the Accreditation Certificate D-PL-14162-01-00
No.
6
Parameters
Cyanide
Test methods2
DIN 38405-13 (D13)
DIN 38405-14 (D14)
DIN EN ISO 14403 (D 6)
7
1,2-Dichlorethan
DIN EN ISO 10301 (F 4)
DIN EN ISO 10304-1 (D 20)
8
Fluoride
DIN 38405-4 (D 4)
9
Nitrate
10
Pesticides and biocidal products
11
Total pesticides and biocidal
products
12
Mercury
DIN EN ISO 10304-1 (D 20)
DIN EN ISO 11369 (F12)
DIN EN ISO 6468 (F 1)
DIN 38407-2 (F 2)
DIN 38407-35 (F35)
DIN EN ISO 10695 (F 6)
DIN EN 12918 (F 24)
DIN 38407-22 (F22)
DIN EN ISO 11369 (F12)
DIN EN ISO 6468 (F 1)
DIN 38407-2 (F 2)
DIN 38407-35 (F35)
DIN EN ISO 10695 (F 6)
DIN EN 12918 (F 24)
DIN 38407-22 (F22)
DIN EN 1483 (E 12)
EN ISO 17294-2 (E 29)
DIN EN ISO 11885 (E 22)
13
Selenium
EN ISO 17294-2 (E 29)
14
15
Tetrachlorethen and
trichlorethen
Uranium
Period of validity: 01.10.2012 to 13.09.2016
DIN EN ISO 10301 (F 4)
DIN EN ISO 17294-2 (E 29)
Translation
Sites
AL, HA, MÜ
AL, HA, MÜ
AL, MÜ, OP,
WA
AL, HA, MÜ,
OP, RM
AL, HA, MÜ,
RM, WA
AL, HA, MÜ,
OP
AL, HA, MÜ,
OP, RM, WA
AL, HA, MÜ
AL
AL
AL
BO
BO
MÜ
AL, HA, MÜ
AL
AL
AL
BO
BO
MÜ
AL, HA, MÜ,
OP
HA, RM, WA
AL, HA, MÜ,
OP
AL, HA, RM,
WA
AL, HA, MÜ,
OP, RM
AL, HA, RM
46/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Part II: chemical parameters- concentration in distribution network including house installation can
increase
No.
Parameters
Test methods2
DIN EN ISO 11885 (E 22)
1
Antimony
EN ISO 17294-2 (E 29)
DIN EN ISO 11885 (E 22)
2
Arsenic
EN ISO 17294-2 (E 29)
DIN EN ISO 17993 (F 18)
3
Benzo-(a)-pyrene
E DIN 38407-39 (F 39)
DIN 38407-8 (F 8)
DIN EN ISO 11885 (E 22)
4
Lead
EN ISO 17294-2 (E 29)
DIN EN ISO 11885 (E 22)
5
Cadmium
EN ISO 17294-2 (E 29)
6
Epichlorhydrine
calculated on the basis of product
specification
DIN EN ISO 11885 (E 22)
7
Copper
EN ISO 17294-2 (E 29)
DIN EN ISO 11885 (E 22)
8
Nickel
EN ISO 17294-2 (E 29)
9
Nitrite
DIN EN 26777 (D 10)
DIN EN ISO 17993 (F 18)
10
Polycyclic aromatic hydrocarbons
E DIN 38407-39 (F 39)
DIN 38407-8 (F 8)
2
3
Sites
AL, HA, MÜ,
OP
AL, HA, RM,
WA
AL, HA, MÜ,
OP
AL, HA, RM,
WA
AL, HA, RM,
MÜ
WA
OP
AL, HA, MÜ,
OP
AL, HA, RM,
WA
AL, HA, MÜ,
OP
AL, HA, RM,
WA
3
AL, HA, MÜ,
OP
AL, HA, RM,
WA
AL, HA, MÜ,
OP
AL, HA, RM,
WA
AL, HA, MÜ,
OP, RM, WA
AL, HA, MÜ,
RM
WA
OP
respectively valid version
The calculation can not be accredited.
Period of validity: 01.10.2012 to 13.09.2016
Translation
47/141
Annex to the Accreditation Certificate D-PL-14162-01-00
No.
Test methods2
Parameters
11
Trihalomethanes
DIN EN ISO 10301 (F 4)
12
Vinyl chloride
DIN 38413-2 (P 2)
DIN EN ISO 10301 (F 4)
Sites
AL, HA, MÜ,
RM
AL, HA, MÜ
AL, HA, MÜ
ATTACHMENT 3: INDICATOR PARAMETERS
Part I: General indicator parameters
No.
Test methods2
Parameters
DIN EN ISO 11885 (E 22)
1
Aluminium
EN ISO 17294-2 (E 29)
DIN 38406-5 (E 5)
2
Ammonium
DIN EN ISO 11732 (E 23)
Sites
AL, HA, MÜ,
OP
AL, HA, RM,
WA
AL, HA, MÜ,
RM, WA
MÜ, OP
3
Chloride
DIN EN ISO 10304-1 (D 20)
AL, HA, MÜ,
OP, RM, WA
4
Clostridium perfringens
(including spores)
according to attachment 5 TrinkwV 2001
AL, OP, WA
5
Coliform organisms
DIN EN ISO 9308-1
with Colilert®-18/Quanti-Tray
AL, OP, WA
OP, WA
AL, HA, MÜ,
OP
AL, HA,
RM,WA
AL, HA, MÜ
RM
AL, HA, MÜ,
RM, WA
AL, HA, MÜ,
RM, WA
DIN EN ISO 11885 (E 22)
6
Iron
EN ISO 17294-2 (E 29)
7
Coloring (spectral absorption
coefficient Hg 436 nm)
DIN EN ISO 7887 (C 1)
DIN 38404-3 (C3)
8
Threshold odour number
DIN EN 1622 (B 3)
9
Taste
DEV B 1/2,
10
Colony count at 22 °C
11
12
Colony count at 36 °C
Electrical conductivity
Period of validity: 01.10.2012 to 13.09.2016
according to attachment 1 No. 5 TrinkwV
1990
EN ISO 6222
according to attachment No. 5 TrinkwV
1990
EN ISO 6222
DIN EN 27888 (C 8)
Translation
AL, OP, WA
AL, OP, WA
AL, OP, WA
AL, OP, WA
AL, HA, MÜ,
OP, RM, WA
48/141
Annex to the Accreditation Certificate D-PL-14162-01-00
No.
Test methods2
Parameters
DIN EN ISO 11885 (E 22)
13
Manganese
EN ISO 17294-2 (E 29)
DIN EN ISO 11885 (E 22)
14
Sodium
EN ISO 17294-2 (E29)
15
Organic carbon (OC)
DIN EN 1484 (H 3)
ISO 8245
16
Oxidation stability
DIN EN ISO 8467 (H 5)
17
Sulphate
DIN EN ISO 10304-1 (D 20)
18
Turbidity
DIN EN ISO 7027 (C 2)
19
Hydrogen ions-concentration
DIN 38404-5 (C 5)
20
21
Tritium
Total concentration
22
Capacity of calcite solution
DIN 38404-10
Sites
AL, HA, MÜ,
OP
AL, HA ,RM,
WA
AL, HA, MÜ,
OP
AL, HA, RM,
WA
AL, HA,
MÜ, OP,
RM
AL
AL, HA,
MÜ, OP,
RM
AL, HA,
MÜ, OP,
RM, WA
AL, HA,
MÜ, OP,
RM, WA
AL, HA,
MÜ, OP,
RM, WA
AL, HA, MÜ,
OP, RM, WA
Part II: Special requirements on drinking water in plants of drinking water installations
Parameters
Legionella spec.
Period of validity: 01.10.2012 to 13.09.2016
Test methods2
DIN EN ISO 11731
DIN EN ISO 11731-2
UBA-recommendation (2012)
Translation
Sites
AL, OP, WA
AL, OP, WA
AL, OP, WA
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Annex to the Accreditation Certificate D-PL-14162-01-00
Parameters, which are not included in attachment 1 to 3 of the drinking water ordiance 2001
Other periodical analysis
Test methods2
Parameters
DIN EN ISO 11885 (E 22)
Calcium
EN ISO 17294-2 (E 29)
DIN EN ISO 11885 (E 22)
Potassium
EN ISO 17294-2 (E 29)
DIN EN ISO 11885 (E 22)
Magnesium
EN ISO 17294-2 (E 29)
Acid capacity
4
DIN 38409-7 (H 7)
Sites
AL, HA,
MÜ, OP
AL, HA, RM,
WA
AL, HA,
MÜ, OP
AL, HA, RM,
WA
AL, HA,
MÜ, OP
AL, HA, RM,
WA
AL, HA,
MÜ, OP,
RM, WA
List of test methods fort he Technical Module WATER
As of: 06.04.2005
Annotation:
Abw: appropriate for waste water (incl. Dumpsite leakage water)
Ofw: appropriate for surface water
Grw: appropriate for untreated water and drinking water
Part 1: Sampling and general parameters
Parameter
Test method
Abw Ofw Grw
Sampling of waste water
DIN 38402-A 11: 1995-12
Sampling from flowing waters DIN 38402-A 15: 1986-07
Sampling from aquifers
DIN 38402-A 13: 1985-12
Period of validity: 01.10.2012 to 13.09.2016
Translation
Sites
AL, BE, BO,
HA, MÜ, OP,
RM, WA
AL, BE, BO,
HA, MÜ, OP,
RM, WA
AL, BE, BO,
HA, MÜ, OP,
RM, WA
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Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
Test method
Abw Ofw Grw
Sampling from stagnant
waters
DIN 38402-A 12: 1985-06
Sample homogenization
DIN 38402-A 30: 1998-07
Temperature
DIN 38404-C 4: 1976-12
pH-Value
DIN 38404-C 5: 1984-01
Conductivity (25°C)
DIN EN 27888: 1993-11 (C 8)
Odour
DEV B 1/2: 1971 - 6. delivery
Dye
DIN EN ISO 7887: 1994-12 (C 1)
chapter. 2
Turbidity
DIN EN ISO 7027: 2000-04 (C 2)
Redox potential
DIN 38404-C 6: 1984-05
Oxygen
DIN EN 25814: 1992-11 (G 22)
Sites
AL, BE, BO,
HA, MÜ, OP,
RM WA
AL, BE, BO,
HA, MÜ, OP,
RM, WA
AL, BE, BO,
HA, MÜ, OP,
RM, WA
AL, BE, BO,
HA, MÜ, OP,
RM, WA
AL, BE, BO,
HA, MÜ, OP,
RM, WA
AL, BE, BO,
HA, MÜ, OP,
RM, WA
AL, BE, BO,
HA, MÜ, OP,
RM, WA
AL, BE, BO,
HA, MÜ, OP,
RM WA
AL, BE, BO,
HA, MÜ, OP,
RM, WA
AL, BE, BO,
HA, MÜ, OP,
RM, WA
Part 2: Photometry, ion chromatography, volumetry
Parameter
UV-absorption at 254 nm
(SAK 254)
UV-absorption at 436 nm
(SAK 436)
Test method
Abw Ofw Grw
DIN 38404-C 3: 1976-12
DIN EN ISO 7887: 1994-12 (C 1)
Period of validity: 01.10.2012 to 13.09.2016
Translation
Sites
AL, HA, MÜ,
OP, RM
AL, HA, MÜ,
OP, RM
51/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
Ammonium nitrogen
Test method
DIN EN ISO 11732: 1997-09 (E 23)
DIN 38406-E 5: 1983-10
Abw Ofw Grw
Sites
MÜ, OP
AL, HA, MÜ,
RM, WA
DIN EN ISO 14911: 1999-12 (E 34)
DIN 38406-E 23: 1993-12
DIN EN 26777: 1993-04 (D 10)
Nitrite nitrogen
DIN EN ISO 10304-1: 1995-04 (D 19)
DIN EN ISO 10304-2: 1996-11 (D 20)
DIN EN ISO 13395: 1996-12 (D 28)
DIN EN ISO 10304-1: 1995-04 (D 19)
Nitrate nitrogen
DIN EN ISO 10304-2: 1996-11 (D 20)
AL, HA, MÜ,
OP, RM WA
AL
AL
AL, HA, MÜ,
OP, RM, WA
AL, HA, MÜ,
OP, RM, WA
DIN EN ISO 13395: 1996-12 (D 28)
DIN 38405-D 9-2 / 9-3: 1979-05
DIN 38405-D 29: 1994-11
DIN EN ISO 11885: 1998-04 (E 22)
Total phosphorus
DIN EN 1189: 1996-12 (D 11)
Ortho phosphorus
AL, HA, MÜ,
OP
AL, HA, MÜ,
OP1, WA
DIN EN ISO 10304-1: 1995-04 (D 19)
DIN EN ISO 10304-2: 1996-11 (D 20)
DIN EN 1189: 1996-12 (D 11)
DIN 38405-D 4: 1985-07
Fluoride (in solution and total)
DIN EN ISO 10304-1: 1995-04 (D 19)
AL, HA, MÜ,
OP
AL, HA, MÜ,
OP, WA
AL, HA, MÜ,
RM, WA
DIN 38405-D 1: 1985-12
DIN EN ISO 10304-1: 1995-04 (D 19)
Chloride
DIN EN ISO 10304-2: 1996-11 (D 20)
AL, HA, MÜ,
OP, RM WA
AL, HA, MÜ,
OP, RM, WA
DIN EN ISO 10304-4: 1999-07 (D 25)
DIN EN ISO 15682: 2002-01 (D 31)
1
only Ofw and Grw
Period of validity: 01.10.2012 to 13.09.2016
Translation
52/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
Test method
Abw Ofw Grw
AL, HA, MÜ,
OP, RM, WA
AL, HA, MÜ,
OP, RM, WA
DIN EN ISO 10304-1: 1995-04 (D 19)
Sulfate
Sulfite
Sulfide (easily liberatible)
DIN EN ISO 10304-2: 1996-11 (D 20)
DIN 38405-D 5: 1985-01
DIN EN ISO 10304-3: 1997-11 (D 22),
Part 5
AL
AL, HA, MÜ,
OP, WA
AL, HA, MÜ
AL, HA, MÜ
AL, MÜ, OP,
WA
DIN 38405-D 27: 1992-07
DIN 38405-D 13-2: 1981-02
DIN 38405-D 14-2: 1988-12
Cyanide (easily liberatible)
Sites
DIN EN ISO 14403: 2002-07 (D 6)
DIN 38405-D 7: 2002-04
AL, HA, MÜ
AL, HA, MÜ
AL, MÜ, OP,
WA
DIN 38405-D 13-1: 1981-02
DIN 38405-D 14-1: 1988-12
Cyanide (total)
DIN EN ISO 14403: 2002-07 (D 6)
DIN 38405-D 7: 2002-04
AL, HA, MÜ,
OP, RM, WA
DIN 38405-D 24: 1987-05
Chromium VI
Oxygen
DIN EN ISO 10304-3: 1997-11 (D 22),
chapter 5 (dissolved chromate)
AL, BE, BO,
HA, MÜ, OP,
RM, WA
DIN EN 25814: 1992-11 (G 22)
Part 3: Elemental analysis
Parameter
Test method
Abw Ofw Grw
DIN EN ISO 11885: 1998-04 (E 22)
Aluminium
Sites
AL, HA, MÜ,
OP
DIN EN ISO 12020: 2000-05 (E 25)
DIN 38406-E 29: 1999-05
AL, HA, RM,
WA
DIN EN ISO 15586: 2004-02 (E 4)
Period of validity: 01.10.2012 to 13.09.2016
Translation
53/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
Test method
DIN EN ISO 11969: 1996-11 (D 18)
DIN EN ISO 11885: 1998-04 (E 22)
Arsenic
DIN 38406-E 29: 1999-05
Abw Ofw Grw
Sites
AL, HA, MÜ,
OP
AL, HA, RM,
WA
DIN EN ISO 15586: 2004-02 (E 4)
DIN 38406-E 6: 1998-07
DIN EN ISO 11885: 1998-04 (E 22)
Lead
AL, HA, MÜ,
OP
DIN 38406-E 16: 1990-03
DIN 38406-E 29: 1999-05
AL, HA, RM,
WA
DIN EN ISO 15586: 2004-02 (E4)
DIN EN ISO 5961: 1995-05 (E19)
DIN EN ISO 11885: 1998-04 (E22)
Cadmium
AL, HA, MÜ,
OP
DIN 38406-E 16: 1990-03
DIN 38406-E 29: 1999-05
AL, HA, RM,
WA
DIN EN ISO 15586: 2004-02 (E 4)
DIN EN ISO 11885: 1998-04 (E 22)
AL, HA, MÜ,
OP
DIN 38406-E 3: 2002-03
Calcium
DIN EN ISO 7980: 2000-07 (E 3)
DIN 38406-E 29: 1999-05
AL, HA, RM,
WA
DIN EN ISO 14911: 1999-12 (E 34)
DIN EN ISO 11885: 1998-04 (E 22)
AL, HA, MÜ,
OP
DIN EN 1233: 1996-08 (E 10)
Chromium
DIN 38406-E 29: 1999-05
AL, HA, RM,
WA
DIN 38406-E 22: 1988-03
DIN EN ISO 15586: 2004-02 (E 4)
Period of validity: 01.10.2012 to 13.09.2016
Translation
54/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
Test method
Abw Ofw Grw
DIN EN ISO 11885: 1998-04 (E 22)
Iron
DIN 38406-E 1: 1983-05
Sites
AL, HA, MÜ,
OP
AL, HA, MÜ,
WA
DIN 38406-E32: 2000-05
DIN EN ISO 15586: 2004-02 (E 4)
DIN 38406-E 13: 1992-07
DIN EN ISO 11885: 1998-04 (E 22)
Potassium
DIN 38406-E 29: 1999-05
AL, HA, MÜ,
OP
AL, HA, RM.
WA
DIN EN ISO 14911: 1999-12 (E 34)
DIN EN ISO 11885: 1998-04 (E 22)
Copper
AL, HA, MÜ,
OP
DIN 38406-E 7: 1991-09
DIN 38406-E 16: 1990-03
DIN 38406-E 29: 1999-05
AL, HA, RM,
WA
DIN EN ISO 15586: 2004-02 (E 4)
DIN EN ISO 11885: 1998-04 (E 22)
Manganese
DIN 38406-E 29: 1999-05
AL, HA, MÜ,
OP
AL, HA, RM,
WA
DIN 38406-E33: 2000-06
DIN EN ISO 15586: 2004-02 (E 4)
DIN EN ISO 14911: 1999-12 (E 34)
DIN 38406-E 14: 1992-07
DIN EN ISO 11885: 1998-04 (E 22)
Sodium
DIN 38406-E 29: 1999-05
AL, HA, MÜ,
OP
AL, HA, RM,
WA
DIN EN ISO 14911: 1999-12 (E 34)
Period of validity: 01.10.2012 to 13.09.2016
Translation
55/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
Test method
Abw Ofw Grw
DIN EN ISO 11885: 1998-04 (E 22)
Sites
AL, HA, MÜ,
OP
DIN 38406-E 11: 1991-09
Nickel
DIN 38406-E 29: 1999-05
AL, HA, RM,
WA
DIN 38406-E 16: 1990-03
DIN EN ISO 15586: 2004-02 (E 4)
DIN EN 1483: 1997-08 (E 12)
Mercury
AL, HA, MÜ,
OP
DIN EN 12338: 1998-10 (E 31)
DIN EN 13506: 2002-04 (E 35)
DIN EN ISO 11885: 1998-04 (E 22)
Zinc
AL, HA, MÜ,
OP
DIN 38406-E 8-1: 1980-10
DIN 38406-E 16: 1990-03
DIN 38406-E 29: 1999-05
AL, HA, RM,
WA
DIN EN ISO 15586: 2004-02 (E 4)
DIN EN ISO 11885: 1998-04 (E 22)
Tin
According to: DIN EN ISO 5961:
1995-05 (chapter 3) (E 19)
According to: DIN EN ISO 11969:
1996-11 (D 18)
(Digestion according to chapter
8.3.1)
DIN 38406-E 29: 1999-05
DIN EN ISO 11885: 1998-04 (E 22)
Boron
AL, HA, MÜ,
OP
AL, HA, RM,
WA
AL, HA, MÜ,
OP
DIN 38405-D 17: 1981-03
DIN 38406-E 29: 1999-05
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL, HA, RM,
WA
56/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
Test method
Abw Ofw Grw
DIN EN ISO 11885: 1998-04 (E 22)
Magnesium
Sites
AL, HA, MÜ,
OP
DIN 38406-E 3: 2002-03
DIN EN ISO 7980: 2000-07 (E 3a)
AL, HA, RM,
WA
DIN 38406-E 29: 1999-05
DIN EN ISO 14911: 1999-12 (E 34)
Part 4: Group parameters and sum parameters (section 1)
Parameter
Test method
Abw Ofw Grw
Biochemical oxygen demand
BOD5
DIN EN 1899-1: 1998-05 (H 51)
AL, HA, MÜ,
OP
AL, HA, OP
HA
AL, MÜ
AL, HA, MÜ,
OP, WA
AL, HA, MÜ
AL, MÜ, OP,
WA
AL, HA, MÜ,
OP, WA
AL, HA, OP,
WA
AL, HA, MÜ,
OP, RM, WA
DIN 38409-H 41: 1980-12
Chemical oxygen demand
(COD)
DIN 38409-H 44: 1992-05
DIN ISO 15705: 2003-01 (H 45)
Low volatile lipophile
compounds
Phenol index (with and
without distillation)
DEV H 56 (46. delivery 2000)
DIN 38409-H 16: 1984-06
DIN EN ISO 14402: 1999-12 (H 37)
DIN 38409-H 2: 1987-03
Filtratable compounds
DIN EN 872: 1996-03 (H 33)
Acid and base-neutralizing
capacities
Sites
DIN 38409-H 7: 2004-03
Part 5: Group parameters and sum parameters (section 2)
Parameter
Test method
Total organic carbon (TOC)
DIN EN 1484: 1997-08 (H 3)
Dissolved organic carbon
(DOC)
DIN EN 1484: 1997-08 (H 3)
Total bound nitrogen (TNb)
DIN ENV 12260: 1996-06 (H 34)
DIN EN 12260: 2003-12 (H 34)
DIN 38409-H 27: 1992-07
DIN EN ISO 11905-1: 1998-08 (H 36)
Period of validity: 01.10.2012 to 13.09.2016
Abw Ofw Grw
Translation
Sites
AL, HA, MÜ,
OP, RM
AL, HA, MÜ,
OP, RM
OP
OP
HA
57/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
Test method
Abw Ofw Grw
Hydrocarbons
DIN EN ISO 9377-2: 2001-07 (H 53)
Adsorbable organically bound DIN EN 1485: 1996-11 (H 14)
halogens (AOX)
DIN 38409-H 22: 2001-02
Sites
AL, HA, MÜ,
OP, RM, WA
AL, HA, MÜ,
OP, RM
AL, HA, MÜ
Part 6: Gas chromatography methods
Parameter
Test method
Highly volatile halogenated
hydrocarbons
DIN EN ISO 10301: 1997-08 (F 4)*
Benzene and derivatives
DIN 38407-F 9: 1991-05*
Organochlorine insecticides
Abw Ofw Grw
DIN EN ISO 12673: 1999-05 (F 15)
AL, HA, MÜ,
OP, RM
AL, HA, MÜ,
OP, RM
AL, BO1, OP
AL, MÜ, OP
AL, BO
AL, BO, MÜ,
OP
AL, BO, HA,
MÜ, OP, RM,
WA
AL, HA, MÜ,
OP, RM
AL, OP
AL, MÜ, OP
AL, MÜ
DIN EN ISO 10695: 2000-11 (F 6) *
AL, BO
DIN EN ISO 6468: 1997-02 (F 1)*
DIN 38407-F 2: 1993-02*
DIN EN ISO 6468: 1997-02 (F 1)*
DIN 38407-F 2: 1993-02*
Polychlorinated biphenyls
DIN 38407-F 3: 1998-07
Mono- and dichlorobenzene
Tri- bis Hexachlorobenzene
Chlorophenoles
Organic nitrogen and
phosphorus compounds
Sites
DIN EN ISO 10301: 1997-08 (F 4)*
DIN EN ISO 6468: 1997-02 (F 1)*
DIN 38407-F 2: 1993-02*
* MS Detection is allowed
Part 7: HPLC- methods
Parameter
Polycyclic aromatic
hydrocarbons (PAH)
1
Test method
DIN 38407-F 18: 1999-05
DIN EN ISO 17993: 2004-03 (F 18)
Abw Ofw Grw
Sites
AL, OP
AL, HA, MÜ,
OP, RM
only Ofw and Grw
Period of validity: 01.10.2012 to 13.09.2016
Translation
58/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
Plant treatment agents and
pesticides
Test method
Abw Ofw Grw
Sites
AL, HA, MÜ
DIN EN ISO 11369: 1997-11 (F 12) *
* MS Detection is allowed
Part 8: Microbiological methods
Parameter
Colony count
Total quantity of coliform
organisms
Quantity of fecal coliform
organisms
Intestinal enterococci
Test method
Abw Ofw Grw
Sites
DIN EN ISO 6222: 1999-07 (K 5)
AL, OP, WA
DIN 38411-K 6: 1991-06 in
conjunction with DIN EN ISO 9308-1:
AL, OP, WA
2001-07 (K 12)
DIN EN ISO 9308-1: 2001-07 (K 12)
AL, OP, WA
DIN EN ISO 9308-1: 2001-07 (K 12)
AL, OP, WA
DIN EN ISO 9308-3: 1999-07 (K 13)
AL, OP, WA
DIN EN ISO 7899-2: 2000-11 (K 15)
AL, OP, WA
DIN EN ISO 7899-1: 1999-07 (K 14)
AL
Part 9: Biological methods, Biotests
Parameter
Saprobic index
Test method
DIN 38410-M 2: 2004-10
Chlorophyll a
DIN 38412-L 16: 1985-12
Phaeophytin
DIN 38416-L 16: 1985-12
Fish eggs test
DIN 38415-T 6: 2003-08
Luminescent bacteria test
DIN 38412-L 34: 1997-07 in
Connection with DIN 38412-L 34-1:
1993-10
DIN EN ISO 11348-1: 1999-04 (L 34-1)
DIN EN ISO 11348-2: 1999-04 (L 34-2)
Abw Ofw Grw
Sites
AL
AL
AL
AL
AL
AL
DIN EN ISO 11348-3: 1999-04 (L 34-3)
Daphnia test
DIN 38412-L 30: 1989-03
Algea test
Umu-Test
DIN 38412-L 33: 1991-03
DIN 38415-T 3: 1996-12
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL
AL
59/141
Annex to the Accreditation Certificate D-PL-14162-01-00
5
List of test methods for Technical Module SOIL AND CONTAMINATES SITES
As of: 20.10.2000
Fields of testing 1: Solids, anorganic parameters
Parameter
Procedure
Method
Sites
Sampling
Bores by hand
DIN 19671 Page 1; 1964
E DIN ISO 10381-2
Chapter 8.5.6; 02.96
Sampling within the
analysis of contaminated
sites
Core piling
DIN 4021, 10.90
samples in undisturbed
situation
E DIN ISO 10381-2
Chapter 8.3; 02.96
DIN 19672, Part 1; 1968
E DIN ISO 10381-4; 02.96
Sampling within the
analysis of natural and
near-natural sites
Pedological mapping
guidance 4th print run,
1994, reprint 1996
VDLUFA-Book of
methods Part 1
E DIN ISO 10381-3; 02.96
Operational safety for
sampling
ZH 1/183: 1997
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL, BE, BO,
BOi, HA,
MA, MÜ,
OP, WA
AL, BE, BO,
HA, MÜ,
OP, WA
AL, BE, BO,
HA, MÜ,
OP, WA
AL, BE, BO,
BOi, HA,
MA, MÜ,
OP, WA
BE, BO, HA,
OP, MÜ,
WA
AL, BE, BO,
BOi, HA,
MA, MÜ,
OP, WA
AL, BE, BO,
BOi, HA,
MA, MÜ,
OP, WA
BE, BO, HA,
MÜ, OP,
WA
AL, BE, BO,
BOi, HA,
MA, MÜ,
OP, WA
AL, BE, BO,
BOi, HA,
MA, MÜ,
OP, WA
60/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
Procedure
Method
Sites
On-site
Pedological mapping
guidance 4th print run,
1994, reprint 1996
Particle size distribution
Finger test on site
DIN 19682-2; 04.97
AL, BE, BO,
BOi, HA,
MA, MÜ,
OP, WA
AL, BE, BO,
BOi, HA,
MA, MÜ,
OP, WA
Laboratory
Sample pretreatment,
Sample preparation
Dry matter content
DIN ISO 11464; 12.96
Fresh or air-dried soil
samples
Organic carbon and total
carbo after dry
Air-dried soil samples
combustion
Fresh or air-dried soil
pH- value (CaCl2)
samples,
c(CaCl2): 0,01 mol/l
1) Sieving, dispersion,
Pipett-analysis
Particle size distribution
2) Sieving, dispersion,
areometer-method
Bulk density
Aqua regia soil extract
Drying of soil samples at
105 °C, reweighing
From milled samples
(grain size < 150 µm)
Ammonium nitrate
extract
Arsenic (As)
DIN ISO 11465; 12.96
DIN ISO 10694;08.96
BO, HA, OP,
WA
DIN ISO 10390, 05.97
AL, HA, MÜ,
OP, WA
E DIN ISO 11277; 06.94
DIN 19683-2; 04.97
DIN 18123; 11.96
E DIN ISO 11277; 06.94
AL
AL
E DIN ISO 11272; 01.94
DIN 19683-12; 04.73
DIN ISO 11466; 06.97
DIN 19730; 06.97
ICP - AES
DIN EN ISO 11885; 04.98
ICP - MS
DIN 38406-29; 05.99
Extraction with aqua regia ET - AAS
According to
E DIN ISO 11047; 06.95
Hydrid AAS
DIN EN ISO 11969; 11.96
Period of validity: 01.10.2012 to 13.09.2016
AL, HA, MÜ,
OP, WA
AL, BO, HA,
MÜ, OP,
WA
Translation
AL, OP
AL, HA, MÜ
OP, WA
AL, HA, MÜ
AL, HA, MÜ,
OP
AL, HA, WA
61/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
Cadmium (Cd)
Chromium (total)
Chromium (VI)
Copper (Cu)
Nickel (Ni)
Lead (Pb)
Thallium (Tl)
Mercury (Hg)
Procedure
Method
Laboratory
AAS
E DIN ISO 11047; 06.95
ICP - AES
Extraction with aqua regia
DIN EN ISO 11885; 04.98
ICP - MS
DIN 38406-29; 05.99
AAS
E DIN ISO 11047; 06.95
ICP - AES
Extraction with aqua regia
DIN EN ISO 11885; 04.98
ICP - MS
DIN 38406-29; 05.99
Extraction with
spectrophotometric
phosphate-buffered
method
solution of aluminium
DIN 19734; 01.99
sulfate
AAS
E DIN ISO 11047; 06.95
ICP - AES
Extraction with aqua regia
DIN EN ISO 11885; 04.98
ICP - MS
DIN 38406-29; 05.99
AAS
E DIN ISO 11047; 06.95
ICP - AES
Extraction with aqua regia
DIN EN ISO 11885; 04.98
ICP - MS
DIN 38406-29; 05.99
AAS
E DIN ISO 11047; 06.95
ICP - AES
Extraction with aqua regia
DIN EN ISO 11885; 04.98
ICP - MS
DIN 38406-29; 05.99
AAS
E DIN ISO 11047: 06.95
ICP-AES (ICP-MS possible)
DIN EN ISO 11885: 04.98
AAS- cold-vapour-method
DIN EN 1483; 08.97
Extraction with aqua regia
Reduction with Sn(II)Drying temperature ≤ 400
chlorid oder NaBH4
°C
Period of validity: 01.10.2012 to 13.09.2016
Translation
Sites
AL, HA, MÜ,
OP
AL, HA, WA
AL, HA, MÜ,
OP
AL, HA, WA
AL, HA, MÜ
AL, HA, MÜ,
OP
AL, HA, WA
AL, HA, MÜ,
OP
AL, HA, WA
AL, HA, MÜ,
OP
AL, HA, WA
AL, HA, MÜ,
OP, WA
AL, HA, MÜ,
OP
62/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
Zinc (Zn)
Procedure
Method
Laboratory
AAS
E DIN ISO 11047; 06.95
ICP - AES
Extraction with aqua regia
DIN EN ISO 11885; 04.98
ICP - MS
DIN 38406-29; 05.99
Cyanide
E DIN ISO 11262; 06.94
Sites
AL, HA, MÜ,
OP
AL, HA, WA
AL, HA, MÜ,
OP
Field of testing 2: Solids, organic parameters
Parameter
Procedure
Method
Sites
Sampling
Bores by hand
DIN 19671 Page 1; 1964
E DIN ISO 10381-2
Chapter 8.5.6; 02.96
Sampling within the
analysis of contaminated sites
Core piling
DIN 4021; 10.90
samples in undisturbed
situation
E DIN ISO 10381-2
Chapter 8.3; 02.96
DIN 19672, Part 1; 1968
E DIN ISO 10381-4; 02.96
Sampling within the
analysis of natural and
near-natural sites
Pedological mapping
guidance 4th print run,
1994, reprint 1996
VDLUFA-Book of
methods Part 1
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
AL, BE, BO,
HA, MÜ, OP,
WA
AL, BE, BO,
HA, MÜ, OP,
WA
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
BE, BO, HA,
MÜ, OP, WA
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
BE, BO, HA,
MÜ, OP, WA
63/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
Procedure
Method
Sites
Sampling
E DIN ISO 10381-3; 02.96
Operational safety for
sampling
ZH 1/183: 1997
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
On site
Particle size distribution
Pedological mapping
guidance 4th print run,
1994, reprint 1996
Finger test on site
E DIN 19682-2; 04.97
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
Laboratory
Sample pretreatment,
Sample preparation
Dry matter content
E DIN ISO 14507; 02.96
Fresh or air-dried soil
samples
Organic carbon and total
carbon after dry
air-dried soil samples
combustion
Fresh or air-dried soil
pH-Value (CaCl2)
samples, c(CaCl2): 0,01
mol/l
Particle size distribution
Bulk density
1) Sieving, dispersion,
Pipett-analysis
2) Sieving, dispersion,
areometer-method
Drying of soil sample at
105 °C, reweighing
Period of validity: 01.10.2012 to 13.09.2016
DIN ISO 11465; 12.96
AL, HA, MÜ,
OP, WA
AL, BO, HA,
MÜ, OP, WA
DIN ISO 10694; 08.96
BO, HA, OP,
WA
DIN ISO 10390; 05.97
AL, HA, MÜ,
OP, WA
E DIN ISO 11277; 06.94
DIN 19683-2;04.97
DIN 18123; 11.96
E DIN ISO 11277; 06.94
AL
AL
E DIN ISO 11272; 01.94
DIN 19683; 04.73
Translation
AL
64/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
Polycyclic aromatic
hydrocarbons (PAHs)
16 PAH (EPA)
Benzo(a)pyren
Note:
Acenaphthylene cannot
be determinated with
fluorescence detektion
Hexachlorobenzene
Pentachlorophenol
Aldrine, DDT,
HCH-mixture
Procedure
Method
Laboratory
1) Soxhlet-extraction with GC - MS
acetone/toluene or
Bulletin No.1 des
acetone/ cyclohexane,
LUA-NRW, 1994
chromatographic Clean-up
2) Extraction with
HPLC-UV/DAD/F*
tetrahydro-furane oder
Bulletin No. 1 des
acetonitrile
LUA-NRW, 1994*
3) Extraction with acetone, HPLC - UV/F
addition of light
E DIN ISO 13877; 06.95
petroleum, removal of
acetone, chromatographic GC - MS, HPLC purification of light
UV/DAD/F
petroleum extract,
dissolving in acetonitrile
VDLUFA-Book of
4) Extraction with
methods, part VII,
water/acetone/light
3.3.3.1
petroleum mixture in the
Handbook contaminated
presence of NaCl
sites vol. 7, LfU Hesse
Extraction with acetone/
cyclohexane or
acetone/light petroleum, if
GC - ECD, GC - MS
applicable
E DIN ISO 10382; 02.98
chromatographic
purification after removal
of acetone
Soxhlet-extraction with
heptane or
GC - ECD, GC - MS
acetone/heptane (50:50);
E DIN ISO 14154; 10.97
derivatisation with aceticanhydride
1) Extraction with light
GC - ECD, GC - MS
petroleum or Acetone/
E DIN ISO 10382; 02.98
light petroleum mixture,
chromatographic
GC - ECD, GC - MS
purification
2) Extraction with water/ VDLUFA-Book of
methods, part VII, 3.3.2
acetone/light petroleum
mixture
Period of validity: 01.10.2012 to 13.09.2016
Translation
Sites
AL, HA, MÜ,
OP
HA, MÜ
WA
AL, MÜ, OP
AL, MÜ
AL, MÜ, OP
65/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
PCB
Procedure
Method
Laboratory
1) Extraction with heptane
E DIN ISO 10382; 02.98
or Acetone/ light
petroleum,
DIN 38414-20; 01.96
chromatographic
purification
2) Soxhlet-extraction with
heptane, hexane or
pentane, chromatographic
purification over AgNO3/
VDLUFA-Book of
silica gel column
methods, part VII, 3.3.2
3) Extraction with water/
acetone/light petroleum
mixture in the presence of
NaCl
Sites
AL, BO, HA,
MÜ, WA
AL, BO, HA,
MÜ, OP, WA
Fields of testing 3: Solids, dioxines und furanes
Parameter
Procedure
Methode
Sites
Sampling
Bores by hand
DIN 19671 Page 1; 1964
E DIN ISO 10381-2
Chapter 8.5.6; 02.96
Core piling
Sampling within the
analysis of contaminated
sites
samples in undisturbed
situation
DIN 4021; 10.90
E DIN ISO 10381-2
Chapter 8.3; 02.96
DIN 19672, Part 1; 1968
E DIN ISO 10381-4; 02.96
Sampling within the
analysis of natural and
near-natural sites
Pedological mapping
guidance 4th print run,
1994, reprint 1996
VDLUFA-Book of
methods Part 1
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
AL, BE, BO,
HA, MÜ, OP,
WA
AL, BE, BO,
HA, MÜ, OP,
WA
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
BE, BO, HA,
MÜ, OP, WA
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
BE, BO, HA,
MÜ, OP, WA
66/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
Procedure
Methode
Sites
Sampling
E DIN ISO 10381-3; 02.96
Operational safety for
sampling
ZH 1/183: 1997
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
On-site
Particle size distribution
Pedological mapping
guidance 4th print run,
1994, reprint 1996
Finger test on site
E DIN 19682-2; 04.97
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
Laboratory
Sample pretreatment,
Sample preparation
Dry matter content
E DIN ISO 14507; 02.96
Fresh or air-dried soil
samples
Organic carbon and total air-dried soil samples
carbon after dry
combustion
Fresh or air-dried soil
pH-Value (CaCl2)
samples, c(CaCl2): 0,01
mol/l
1) Sieving, dispersion,
Pipett-analysis
Particle size distribution 2) Sieving, dispersion,
areometer-method
DIN ISO 11465; 12.96
DIN ISO 10694; 08.96
BO, HA, OP
DIN ISO 10390; 05.97
HA, MÜ, OP
E DIN ISO 11277; 06.94
DIN 19683-2; 04.97
DIN 18123; 11.96
E DIN ISO 11277; 06.94
Bulk density
Polychlorinated
dibenzo-p-dioxins and
polychlorinated
dibenzofurans
Drying of soil sample at
105 °C, reweighing
Freeze dried samples,
Soxhlet-extraction of the
fresh sample with
Toluene, internal
standard,
chromatographic
purification
Period of validity: 01.10.2012 to 13.09.2016
AL, HA, MÜ,
OP
AL, HA, MÜ,
OP
AL
AL
E DIN ISO 11272; 01.94
DIN 19683; 04.73
GC- MS according to
Klärschlammverordnung
considering
DIN 38414- 24;04.98
VDI-rule 3499,
Page 1: 03.90
GC - MS with internal
standard
Translation
AL
AL
AL
AL
67/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Fields of testing 4: Groundwater, leakwater, surface water
Parameter
Methode
Sampling
AL, BE, BO,
HA, MÜ, OP,
WA
AL, BE, BO,
HA, MÜ, OP,
WA
DIN EN ISO 25667, Part 2
DIN 38402-13; 1985
Sampling of groundwater Working committee WATER of the states of the
Federal Republic of Germany(LAWA):
Directive groundwater, Part 3; 03.93
AQS-Bulletin P 8/2; 01.96
German Association for Water Resources
Management and Soil Engineering (DVWK):
DVWK-Rule 128/92
DVWK-Bulletin 245/1997
Sampling of leakage
water
To date no standard method available
DIN 38402-15; 07.86
Sampling of surface
water (flowing water)
AQS-Bulletin P 8/3; 05.98
Sampling of surface
water (stagnant water)
Sites
DIN 38402-12; 06.85
AL, BE, BO,
HA, MÜ, OP,
WA
AL, BE, BO,
HA, MÜ, OP,
WA
AL, BE, BO,
HA, MÜ, OP,
WA
AL, BE, BO,
HA, MÜ, OP,
WA
AL, BE, BO,
HA, MÜ, OP,
WA
AL, BE, BO,
HA, MÜ, OP,
WA
On-site
Temperature
DIN 38404-4; 12.76
pH-Value
DIN 38404-5; 01.84
Oxygen content
DIN EN 25814; 11.92
Period of validity: 01.10.2012 to 13.09.2016
AL, BE, BO,
HA, MÜ, OP,
WA
AL, BE, BO,
HA, MÜ, OP,
WA
AL, BE, BO,
HA, MÜ, OP,
WA
Translation
68/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
Procedure
Methode
Sites
On-site
Electrical conductivity
Leaching method 1
(Bodensättigungsextrakt)
Leaching method 2
(modified S 4-method)
Leaching method 3
column test or
lysimeter-test
DIN EN 27888; 11.93
AL, BE, BO,
HA, MÜ, OP,
WA
According to BBodSchV (Annex 1, 3.1.2)
AL, HA, MÜ,
OP
DIN 38414-4; 10.84 considering the notes of the
BBodSchV (appendix 1, 3.1.2)
AL, HA, MÜ,
OP
To date no standard method available; execution of
state of the art column test or lysimeter-test
ICP - AES based on DIN EN ISO 11885; 04.98
Antimony (Sb)
ICP - MS DIN 38406-29; 05.99
AL, MÜ
AL, HA, MÜ,
OP
AL, HA, WA
Hydride - AAS E DIN 38405-32; 11.96
Laboratory
ICP - AES based on DIN EN ISO 11885; 04.98
Arsenic (As)
ICP - MS DIN 38406-29; 05.99
AL, HA, MÜ,
OP
AL, HA, WA
Hydride - AAS DIN EN ISO 11969; 11.96
ICP - AES based on DIN EN ISO 11885; 04.98
Lead (Pb)
ICP - MS DIN 38406-29; 05.99
AL, HA, MÜ,
OP
AL, HA, WA
AAS - E DIN 38406-6; 06.97
ICP - AES based on DIN EN ISO 11885; 04.98
Cadmium (Cd)
ICP - MS DIN 38406-29; 05.99
AL, HA, MÜ,
OP
AL, HA, WA
AAS DIN EN ISO 5961; 05.95
ICP - AES based on DIN EN ISO 11885; 04.98
Chromium (Cr) total
ICP - MS DIN 38406-29; 05.99
AL, HA, MÜ,
OP
AL, HA, WA
AAS DIN EN 1233; 08.96
Chromium (Cr VI)
Cobalt (Co)
Spectrophotometric method DIN 38405-24; 05.87
ICP - AES based on DIN EN ISO 11885; 04.98
AL, HA, MÜ,
OP, WA
AL, HA, MÜ,
OP
AAS DIN 38406-24; 03.93
Period of validity: 01.10.2012 to 13.09.2016
Translation
69/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
Procedure
Laboratory
Methode
ICP - AES based on DIN EN ISO 11885; 04.98
Copper (Cu)
ICP - MS DIN 38406-29; 05.99
Sites
AL, HA, MÜ,
OP
AL, HA, WA
AAS DIN 38406-7; 09.91
Molybdenum (Mo)
ICP - AES based on DIN EN ISO 11885; 04.98
ICP - MS DIN 38406-29; 05.99
ICP - AES based on DIN EN ISO 11885; 04.98
Nickel (Ni)
ICP - MS DIN 38406-29; 05.99
AL, HA, MÜ,
OP
AL, HA, WA
AL, HA, MÜ,
OP
AL, HA, WA
AAS DIN 38406-11; 09.91
Mercury (Hg)
AAS – cold vapour method DIN EN 1483; 08.97
ICP - AES based on DIN EN ISO 11885; 04.98
Selenium (Se)
ICP - MS DIN 38406-29; 05.99
AL, HA, MÜ,
OP
AL, HA, MÜ,
OP
AL, HA, WA
AAS DIN 38405-23; 10.94
ICP - AES based on DIN EN ISO 11885; 04.98
Zinc (Zn)
ICP - MS DIN 38406-29; 05.99
AL, HA, MÜ,
OP
AL, HA, WA
AAS DIN 38406-8; 10.80
Tin (Sn)
Cyanide, total
ICP - AES based on DIN EN ISO 11885; 04.98
ICP - MS DIN 38406-29; 05.99
Spectrophotometric method
DIN 38405-13; 02.81
E DIN EN ISO 14403; 05.98
Cyanide (easily
liberatible)
Fluoride
BTEX
Spectrophotometric method
DIN 38405-13; 02.81
Fluoride sensitive electrode
DIN 38405-4; 07.85
Ion chromatography
DIN EN ISO 10304-1; 04.95
GC - FID DIN 38407-9; 05.91
(considering the matrix)
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL, HA, MÜ,
OP
AL, HA, WA
AL, HA, MÜ
AL, MÜ, OP,
WA
AL, HA, MÜ,
OP
AL, HA, MÜ,
OP
AL, HA, MÜ,
WA
AL, HA, MÜ,
OP
70/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
Procedure
Laboratory
Methode
Easily liberatible
halogenated
hydrocarbons (LHKW)
Aldrine
GC - ECD, GC - MS possible DIN 38407-2; 02.93
DDT
GC - ECD, GC - MS possible DIN 38407-2; 02.93
Phenoles
GC - ECD ISO DIS 8165-2; 01.97
Chlorphenoles
GC - ECD, GC - MS E DIN EN 12673; 02.97
Chlorbenzenes
Polychlorinated
biphenyls (PCB): 6 PCBcongeners (No. 28, 52,
101, 138, 163, 180
according to
Ballschmiter)
GC - ECD, GC - MS possible DIN 38407-2; 02.93
16 PAH (EPA)
HPLC - F DIN 38407-18; 05.99
Naphthalene
GC - FID, GC - MS DIN 38407-9; 05.91
Petroleum hydrocarbons
Extraction with light petroleum; gaschromatographic
determination according to ISO/TR 11064; 06.94
GC - ECD DIN EN ISO 10301; 08.97
GC - ECD, GC - MS DIN 38407-2; 02.93
Sites
AL, BE, HA,
MÜ, OP
AL, MÜ, OP
AL, MÜ, OP
AL, MÜ, OP
AL, MÜ, OP
AL, BO, MÜ,
WA
AL, BO, HA,
MÜ, OP
E DIN 38407-3; 10.95
AL, HA, MÜ
OP
AL, HA, MÜ,
OP
AL, HA, MÜ,
OP, WA
Fields of testing 5: Soil air, landfill gas
Parameter
Method
Sampling
Association of German Engineers (VDI)
VDI-rule 3865 page 2, chapter 4.4.3
Sampling of soil air
VDI-rule 3865 page 2, chapter 4.4.4
VDI-rule 3865 page 2, chapter 4.4.5
Period of validity: 01.10.2012 to 13.09.2016
Translation
Sites
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
71/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
Method
On-site
Carbon dioxide (CO2)
Displaying measuring instrument
Methane (CH4)
Displaying measuring instrument
Hydrogen sulfide (H2S)
Displaying measuring instrument
Oxygen (O2)
Displaying measuring instrument
Sum parameters
trace gases
Displaying measuring instrument
BTEX
Easily liberatible
halogenated
hydrocarbons (LHKW)
Sites
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
Laboratory
VDI-rule 3865 page 3, chapter 3.2
MÜ, OP, RM
VDI-rule 3865 page 3, chapter 3.2
MÜ, OP, RM
Fields of testing 6: Dry and wet deposition
Parameter
Procedure
Method
Sites
Sampling
Precipitation with
particles
Sampling of rain
water
Bergerhoff-device
VDI 2119, Page 2; 09.96
(standard- method)
Collecting device ARS
VDI 3870, Page 10; 12.96
721
Laboratory
Be, Cd, Co, Cr, Cu, Fe,
Mn, Ni, Pb, Sb, V, Zn
Thallium
Lead und Cadmium
pH-Value
For ion-meager waters
Chloride, nitrate, sulfate
Chloride
titrimetric
Period of validity: 01.10.2012 to 13.09.2016
AL, BO, OP
VDI 2267, Page 5; 12.96
AL, OP
VDI 2267, Page 7; 11.88
VDI 2267, Page 4; 03.87
VDI 3870, Page 10; 12.96
DIN 38404-C5; 01.84
VDI 3870, Page 11; 12.96
DIN EN ISO 10304-1; 04.95
DIN 38405-D1; 12.85
AL, OP
AL
Translation
AL
AL, OP
AL
72/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parameter
Procedure
Laboratory
photometric
DIN 38405-D9; 05.79
Gran-method
VDI 3870, Page 13; 12.96
titrimetric or
potentiometric according
to the Gran-method and
DIN EN ISO 9963-1; 02.96
by means of two point
titration (pH 4,5 / pH 4,5)
respectively
DIN EN 27888; 11.93
DIN 38409-H3-1; 06.83
VDIN EN 12260; 06.96
photometric
molybdenum-blueDIN EN 1189; 12.96
method
Ion chromatography
DIN EN ISO 10304-1; 04.95
DIN 38406-E 5-1; 10.83
DIN 38406-E 23-1; 12.93
DIN 38406-E 13
DIN 38406-E 14
DIN 38406-E 3-1; 09.82
DIN EN 12338 (E 31), 07.98
DIN EN 1483, 08.97
Nitrate
free acidity
Alkalinity
Elektrical conductivity
TOC
Ntotal
PO4- P
NH4
Na, K
Ca, Mg
Hg
Al, Na, K, Ca, Mg, Mn, Fe,
Cu, Zn, Pb, Co, Cd, Mo, S,
Cr, Ni, Pgesamt
Fields of testing 7:
Method
Sites
AL
AL
AL
AL
AL
AL, OP
DIN 38406-E22; 03.88
DIN EN ISO 11885 (E 22)
AL, OP
Investigation of forest soil
Testing field not requested
Fields of testing 8:
Investigations for appraisement of the terrestrial ecological toxicity of
hazardous substances
Testing field not requested
Period of validity: 01.10.2012 to 13.09.2016
Translation
73/141
Annex to the Accreditation Certificate D-PL-14162-01-00
6
List of test methods fort he Technical Module WASTE
As of: 01.08.2005
Fields of testing 1: Sewage sludge
Parts/
Parameters
Bases/
Test methods
AbfKlärV
1.1 Sampling
Annex 1 AbfKlärV
Sampling of sludge
DIN 38414-S 1 (11.86)
Collecting sample preparation and
sample division
Annex 1 No. 1.1 AbfKlärV
Sample preparation, homogenization,
centrifugation, lyophilisation
Annex 1 No. 1.2 AbfKlärV
1.2 Heavy metalse
§ 3 Abs. 5 AbfKlärV
Aqua regia digestion
Lead
(from aqua regia digestion)
Cadmium
(from aqua regia digestion)
Chromium
(from aqua regia digestion)
Copper
(from aqua regia digestion)
Nickel
(from aqua regia digestion)
Mercury
(from aqua regia digestion)
Period of validity: 01.10.2012 to 13.09.2016
Sites
AL, BE, BO,
HA, MÜ, OP,
WA
AL, BE, HA,
MÜ, OP, WA
AL, HA, MÜ,
OP, WA
DIN 38414-S 7 (01.83)
DIN EN 13346 (S 7a) (04.01)
DIN 38406-E 6 (05.81)
DIN 38406-E 6 (07.98)
DIN EN ISO 11885 (E 22) (04.98)
DIN 38406-E 22 (03.88)
DIN 38406-E 19 (07.80)
DIN EN ISO 5961 E 19 (05.95)
OP
AL, HA, OP
DIN EN ISO 11885 E 22 (04.98)
DIN 38406-E 22 (03.88)
AL, HA, OP
DIN 38406-E 10 (06.85)
DIN EN 1233 (E 10) (08.96)
DIN EN ISO 11885 E 22 (04.98)
DIN 38406-E 22 (03.88)
DIN 38406-E 7 (09.91)
DIN EN ISO 11885 E 22 (04.98)
DIN 38406-E 22 (03.88)
DIN 38406-E 11 (09.91)
DIN EN ISO 11885 E 22 (04.98)
DIN 38406-E 22 (03.88)
DIN 38406-E 12 (07.80)
DIN EN 1483 E 12 (08.97)
Translation
AL, HA, OP
AL, HA, OP
AL, HA, OP
AL, HA, OP
AL, HA, OP
74/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parts/
Parameters
Zinc
(from aqua regia digestion)
Bases/
Test methods
DIN 38406-E 8 (10.80)
DIN EN ISO 11885 E 22 (04.98)
DIN 38406-E 22 (03.88)
1.3 Adsorbable organically bound
halogens
§ 3 Abs. 5 AbfKlärV
AOX (from dry residues)
DIN 38414-S 18 (11.89)
1.4 Physical parameters, nutrients
§ 3 Abs. 5 AbfKlärV
DIN 38414-S 2 ( 11.85 )
Dry residue
Organic substance from ignition loss
(from dry residue)
pH value
Aqua regia digestion
Basic-active materials as CaO
Ammoniacal nitrogen (NH4-N)
Total nitrogen (Ntot.)
Phosphorus P2O5
(from aqua regia digestion)
Potassium K2O
(from aqua regia digestion)
Magnesium
(from aqua regia digestion)
Period of validity: 01.10.2012 to 13.09.2016
DIN EN 12880 S 2a (02.01)
DIN 38414-S 3 ( 11.85 )
DIN EN 12879 (S 3a) (02.01)
DIN 38414-S 5 ( 09.81 )
DIN EN 12176 S 5 (06.98)
DIN 38414-S 7 (01.83)
DIN EN 13346 S 7a (04.01)
Annex 1 AbfKlärV
Calculation using % CaO = (50-x-2y) •
1,402
DIN 38406-E 5 (10.83)
DIN 19684-4 (02.77) distilling method
DIN ISO 11261 b (05.97)
DIN 38414-S 12 (11.86)
DIN 38406-E 22 (03.88)
DIN EN ISO 11885 E 22 (04.98)
DEV E 13 (5. Lfg. 68)
DIN 38406-E 13 (07.92)
DIN 38406-E 22 (03.88)
DIN EN ISO 11885 E 22 (04.98)
DIN 38406-E 3 (09.82)
DIN EN ISO 7980 E 3a (07.00)
DIN 38406-E 22 (03.88)
DIN EN ISO 11885 E 22 (04.98)
Translation
Sites
AL, HA, OP
AL, HA, OP
BO
AL, BO, HA,
OP
BO
AL, HA, OP
AL, HA, OP
AL, HA, OP
AL, HA, OP
AL, HA, OP
AL, HA, OP
AL, HA, OP
AL, HA, OP
AL, HA, OP
AL, HA, OP
75/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parts/
Parameters
Bases/
Test methods
Persistent organic pollutants
§ 3 Abs. 6 AbfKlärV
1.5
1.6
Polychlorinated biphenyls
(PCB)
Polychlorinated
Dibenzodoxines/-furans
(PCDD/PCDF)
Annex 1, No. 1.3.3.1 AbfKlärV
DIN 38414-S 20 (01.96)
Annex 1 No. 1.3.3.2 AbfKlärV
Sites
AL, BO,
AL, BO, HA,
OP
AL
Fields of testing 2: Soil
Parts/
Parameters
2.1 Sampling and sample
preparation
Bases/
Test methods
AbfKlärV and BioAbfV
§ 3 Abs. 2 AbfKlärV and § 9 BioAbfV
Sampling, preparation of the average
sample
Annex 1, No. 2.1 AbfKlärV
Sample preparation
Annex 1, No. 2.1 AbfKlärV
Screening < 2 mm
Annex 1, No. 2.1 AbfKlärV
Crushing< 0,1 mm
Annex 1, No. 2.1 AbfKlärV i.V. with
DIN 38414-S 7 (01.83)
2.2 Heavy metals, pH value and soil
texture
§ 3 Abs. 2 AbfKlärV
§ 9 Abs. 2 BioAbfV
Aqua regia digestion
Lead
(from aqua regia digestion)
Cadmium
(from aqua regia digestion)
Period of validity: 01.10.2012 to 13.09.2016
Sites
DIN 38414-S 7 (01.83)
DIN EN 11466 (06.97)
DIN 38406-E 6 (07.98)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
DIN 38406-E 22 (03.88)
DIN EN ISO 5961 E 19 (05.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
DIN 38406-E 22 (03.88)
Translation
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
AL, HA, MÜ,
OP, WA
AL, HA, MÜ,
OP, WA
AL, HA, MÜ,
OP, WA
AL
AL, HA, OP
AL, HA, OP
AL, HA, OP
76/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parts/
Parameters
Chromium
(from aqua regia digestion)
Copper
(from aqua regia digestion)
Nickel
(from aqua regia digestion)
Mercury
(from aqua regia digestion)
Zinc
(from aqua regia digestion)
Soil texture
pH value
2.3 Physical parameters, nutrients
pH value
Clay content/ soil texture
Period of validity: 01.10.2012 to 13.09.2016
Bases/
Test methods
DIN EN 1233 E 10 (08.96)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
DIN 38406-E 22 (03.88)
DIN 38406-E 7 (09.91)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
DIN 38406-E 22 (03.88)
DIN 38406-E 11 (09.91)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
DIN 38406-E 22 (03.88)
DIN 38406-E 12 (07.80)
DIN EN 1483 E 12 (08.97)
DIN 38406-E 8 (10.80)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
DIN 38406-E 22 (03.88)
DIN 18123 (1983)
DIN 18123 (11.96)
VDLUFA-Book of methods I
D 2.1 (1991)
DIN 19684-1 (02.77)
DIN ISO 10390 (05.97)
VDLUFA-Book of methods I
A 5.1.1 (1991)
Sites
AL, HA, OP
AL, HA, OP
AL, HA, OP
AL, HA, OP
AL, HA, OP
AL
OP
AL, HA
AL, OP
§ 3 Abs. 4 AbfKlärV, § 9 Abs. 2
BioabfV
DIN 19684-1 (02.77)
DIN ISO 10390 (05.97)
VDLUFA- Book of methods I
A 5.1.1 (1991)
DIN 18123 (1983)
DIN 18123 (11.96)
VDLUFA- Book of methods I
D 2.1 (1991)
Translation
AL, HA
AL, OP
AL
OP
77/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parts/
Parameters
Phosphorus P2O5 CA/DL *
Potassium K2O CA/DL *
Magnesium Mg CaCl2 *
Bases/
Test methods
VDLUFA- Book of methods
A 6.2.1.1; A 6.2.1.2 (1991)
VDLUFA- Book of methods
A 6.2.1.1; 6.2.1.2 (1991)
VDLUFA- Book of methods 6.2.4.1
(1991)
* only for AbfKlärV, not binding in BioAbfV
Sites
AL, HA, OP
AL, HA, OP
AL, HA, OP
Fields of testing 3: Biowaste
Parts/
Parameters
3.1 Sampling
Sampling of solid biowaste
Bases/
Test methods
§ 4 Abs. 5 BioAbfV,
Anhang 3 BioAbfV
Book of methods Compost (1994)
LAGA RL PN 2/78 (12.83)
Sampling of liquid, pasty and sludgy
waste
LAGA RL PN 2/78 K (12.83)
LAGA PN 98 (12.01)
Sites
AL, BOi, HA,
MÜ, OP, WA
AL, BOi, HA,
MÜ, OP, WA
AL, BOi, HA,
MÜ, OP, WA
AL, BOi, HA,
MÜ, OP, WA
Sample preparation and sampling of a
portion of the residue, screening< 10
mm, crushing
< 0,25 mm
Annex 3 No. 1.2 BioAbfV
AL, HA, MÜ,
OP, WA
Dry substance
DIN 38414-S 2 (11.85)
AL, HA, MÜ,
OP
3.2 Heavy metals
§ 4 Abs. 5 BioAbfV
Aqua regia digestion
Lead
(from aqua regia digestion)
Period of validity: 01.10.2012 to 13.09.2016
DIN 38414-S 7 (01.83)
DIN EN 13657 (01.03)
DIN 38406-E 6 (05.81)
DIN 38406-E 6 (07.98)
DIN 38406-E 22 (03.88)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
Translation
AL, OP
AL, OP
AL, OP
78/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parts/
Parameters
Cadmium
(from aqua regia digestion)
Chromium
(from aqua regia digestion)
Copper
(from aqua regia digestion)
Nickel
(from aqua regia digestion)
Mercury
(from aqua regia digestion)
Zinc
(from aqua regia digestion)
Bases/
Test methods
DIN EN ISO 5961 E 19 (05.95)
DIN 38406-E 22 (03.88)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
DIN EN 1233 E 10 (08.96)
DIN 38406-E 22 (03.88)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
DIN 38406-E 7 (09.91)
DIN 38406-E 22 (03.88)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
DIN 38406-E 11 (09.91)
DIN 38406-E 22 (03.88)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
DIN 38406-E 12 (07.80)
DIN EN 1483 E 12 (08.97)
DIN 38406-E 8 (10.80)
DIN 38406-E 22 (03.88)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
3.3 Physical parameters, extraneous
materials
Dry residue
pH-value
Salt content
Period of validity: 01.10.2012 to 13.09.2016
Sites
AL, OP
AL, OP
AL, OP
AL, OP
AL, OP
AL, OP
§ 4 Abs. 5 BioAbfV
DIN ISO 11465 (12.96)
DIN ISO 10390 (05.97)
VDLUFA-Book of methods
Volume I A 5.1.1 (1991)
Annex 3 No. 1.3.4 BioAbfV
VDLUFA- Book of methods
Volume I (1991)
Translation
AL, BO, OP
AL, BO
AL, OP
AL
AL, OP
79/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parts/
Parameters
Organic substance from ignition loss
(from dry residue)
Bases/
Test methods
DIN 19684-3 (02.77)
DIN 19684-3 (08.00)
Annex 3 BioAbfV, No. 1.3.3
Extraneous matters (stones, glass,
plastics, metals)
Book of methods Compost
Federal Technical Association
Compost
3.4 Hygienic control of epidemics
§ 3 Abs. 4 BioAbfV
Salmonella (product tests)
Annex 2 No. 2.3.1.2 BioAbfV
Sites
AL, BO, OP
AL
AL, OP
AL
Annex 2 No. 2.3.1.1 BioAbfV
via Plastikampullen 2ml
Salmonella senftenberg W 775 (H2S-neg.)
Annex 2 No. 2.3.1.1 BioAbfV
(process tests)
via diffusion germ carriers according
to RAPP
3.5 Phytohygiene
§ 3 Abs. 4 BioAbfV
Germinable seeds and plant parts
capable of shooting (product tests)
Annex 2 No. 2.3.2 und 2.3.2.5 BioAbfV
Incl. salt content
Plasmodiophora brassicae (Kohlhernie)
(process tests)
Tomatoe seeds (process tests)
Book of methods Compost
Federal Technical Association
Compost
Annex 2, No. 2.3.2.1 and 2.3.2.3
BioAbfV, Test according to BRUNS and
KNOLL et. al. (1990, 1994)
Annex 2, No. 2.3.2.1 and 2.3.2.4
BioAbfV, Test according to
POLLMANN and STEINER (1994)
AL
AL
Fields of testing 4: Used oils, insulating liquids
Parts/
Parameters
Bases/
Test methods
§ 5 AltölV / § 8 Abs. 3 DepV
4.1 Sampling
§ 5 Abs. 2 AltölV
Sampling preparation, protocol
Smapling of liquid substances
Period of validity: 01.10.2012 to 13.09.2016
Annex 2 AltölV in conjunction with
DIN 51750-1 (08.83)
Annex 2 AltölV in conjunction with
DIN 51750-2 (03.84)
Translation
Sites
AL, BO, HA,
MÜ, OP, WA
AL, BO, HA,
MÜ, OP, WA
80/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parts/
Parameters
Bases/
Test methods
4.2 PCB and halogen (according
to AltölV) or PCB (according
to DepV)
§ 5 Abs. 2 AltölV and
Annex 4 No. 3 DepV
PCB *
PCB **
Total halogen *
DIN EN 12766-1 (11.00)
in conjunction with
DIN EN 12766-2 (12.01)
IEC 61619 (04.97)
EN 12766-1 (11.00)
Annex 2, No. 3.1, 3.2, 3.3.1 AltölV EdRFA according to DIN 51577-4 (02.94)
Annex 2, No. 3.1, 3.2, 3.3.2.2 AltölV:
Wd-RFA according to DIN 51577-2
(01.93) or DIN 51577-3 (06.90)
Annex 2, No. 3.1, 3.2, 3.3.2.1 AltölV:
Wickbold according to DIN EN ISO
24260 (05.94) and DIN 51408-1
(06.83)
Annex 2, No. 3.1, 3.2, 3.3.2.1 AltölV:
Wickbold according to DIN EN ISO
24260 (05.94) and DIN 38405-D 1
(12.85)
Annex 2, No. 3.1, 3.2, 3.3.2.1 AltölV:
Wickbold according to DIN EN ISO
24260 (05.94) and DIN EN ISO 103041 D 19 (04.95)
* only for AltölV
** only for DepV
Sites
AL, BO, HA
AL
AL, BO, HA
BO
Fields of testing 5: Waste for deposition
Parts/
Parameters
Bases/
Test methods
§ 8 Abs. 3 DepV
5.1 Sampling, sample preparation
Annex 4 No. 2 and No. 3.1.1 DepV
Sampling of liquid, pasty and sludgy
waste
LAGA PN 98 (12.01)
Sample preparation: reduction, crushing
and grinding of solid samples for
Annex 4 No. 3.1.1 DepV
laboratory samples
Period of validity: 01.10.2012 to 13.09.2016
Translation
Sites
AL, BE, BO,
BOi, HA, MA,
MÜ, OP, WA
AL, BE, BO,
HA, MÜ, OP,
WA
81/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parts/
Parameters
Sample preparation: reduction, grinding
of pasty and sludgy samples for
laboratory samples
5.2 Sample preparation, general
parameters
Dissolution method (aqua regia)
Bases/
Test methods
Annex 4 No. 3.1.1 DepV
E DIN EN 13657 (10.99)
DIN EN 13657 (01.03)
Eluate preparation
DIN EN 12457-4 (01.03) i.V. Annex 4
No. 2.4 AbfAblV
pH value soil characteristics
DIN ISO 10390 (05.97)
pH value of the eluate
DIN 38404-C 5 (01.84)
Conductance of the eluate
DIN EN 27888 C 8 (11.93)
Dry residues (soil characteristics)
DIN ISO 11465 (12.96)
E DIN EN 14346 (02.02)
Dry residues (waste)
DIN EN 12880 S 2a (02.01)
Ignition loss of the dry residue in the
original substance
DIN 38409-H 1-2 (01.87)
DIN 38414-S 3 (11.85)
DIN EN 12879 ( 02.01)
E DIN ISO 11262 (06.94)
Cyanide, total
ISO 11262 (09.03)
Cyanide, easily liberatable
(from eluate)
Period of validity: 01.10.2012 to 13.09.2016
AL, BE, OP,
WA
Annex 4 No. 3 DepV
DIN EN 13346 S 7a (04.01)
Water-soluble part of the dry residue in
the original substance (determined by
the filtrate dry residue of the eluate)
Sites
DIN 38405-D 14-2 (12.88)
For sulfide containing waste DIN
38405-D 13-2 (02.81)
DIN EN ISO 14403 D 6 (07.02)
Translation
AL, HA, MÜ
AL, HA, MÜ,
OP
AL, HA, MÜ,
OP
AL, HA, MÜ,
OP
AL, HA, MÜ,
OP
AL, HA, MÜ,
OP
AL, HA, MÜ,
OP
AL, BO, HA,
MÜ
AL, BO, HA,
MÜ, OP
AL, HA, MÜ,
OP
BO, OP
AL, BO, HA,
MÜ
AL, HA, MÜ,
OP
AL, HA, MÜ,
OP
AL, HA, MÜ
AL, HA, MÜ
AL, MÜ, OP
82/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parts/
Parameters
Bases/
Test methods
DIN 38405-D 4-1 (07.85)
Fluoride (from eluate)
DIN EN ISO 10304-1 D 19 (04.95)
Ammonia nitrogen (NH4-N) (from
eluate)
DIN 38406-E 5-1 (10.83)
DIN EN ISO 11732 E 23 (09.97)
DIN EN ISO 11732 E 23 (05.05)
5.3
Annex 4 No. 3 DepV
Arsenic and other heavy metals
Arsenic
(from aqua regia digestion)
Sites
AL, HA, MÜ,
OP
AL, BO, HA,
MÜ
AL, HA, MÜ
MÜ, OP
DIN EN ISO 11969 D 18 (11.96)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
AL, HA, MÜ,
OP
DIN EN ISO 11969 D 18 (11.96)
Arsenic (from eluate)
Lead
(from aqua regia digestion)
DIN EN ISO 11885 E 22 (04.98)
DIN 38406-E 6 (07.98)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
Lead (from eluate)
AL, HA, MÜ,
OP
DIN 38406-E 2 (07.98)
DIN 38406-E 6 (07.98)
DIN EN ISO 11885 E 22 (04.98)
Cadmium
(from aqua regia digestion)
AL, HA, MÜ,
OP
AL, HA, MÜ,
OP
DIN EN ISO 5961 E 19 (05.98)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
AL, HA, MÜ,
OP
DIN EN ISO 5961 E 19 (05.98)
Cadmium (from eluate)
Chromium
(from aqua regia digestion)
Period of validity: 01.10.2012 to 13.09.2016
DIN EN ISO 11885 E 22 (04.98)
AL, HA, MÜ,
OP
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
Translation
AL, HA, MÜ,
OP
83/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parts/
Parameters
Bases/
Test methods
Chromium-VI (from eluate)
DIN 38405-D 24 (05.87)
Copper
(from aqua regia digestion)
Sites
AL, HA, MÜ,
OP
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
AL, HA, MÜ,
OP
DIN 38406-E 7 (09.91)
Copper (from eluate)
Nickel
(from aqua regia digestion)
Nickel (from eluate)
DIN EN ISO 11885 E 22 (04.98)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
Mercury (from eluate)
Zinc
(from aqua regia digestion)
AL, HA, MÜ,
OP
DIN 38406-E 11 (09.91)
DIN 38406-E 22 (03.88)
DIN EN ISO 11885 E 22 (04.98)
Mercury
(from aqua regia digestion)
AL, HA, MÜ,
OP
DIN EN 1483 E 12 (08.97)
AL, HA, MÜ,
OP
AL, HA, MÜ,
OP
DIN EN 12338 E 31 (10.98)
DIN 38406-E 12 (07.80)
DIN EN 1483 E 12 (08.97)
AL, HA, MÜ,
OP
DIN EN 12338 E 31 (10.98)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
AL, HA, MÜ,
OP
DIN 38406-E 8-1 (10.80)
Zinc (from eluate)
5.4
Group and sum parameters
DIN EN ISO 11885 E 22 (04.98)
Annex 4 No. 3 DepV
Matter soluble in organically bound
halogens (EOX)
DIN 38414-S 17 ( 11.89)
Adsorbable organically bound halogens
(AOX) (from eluate)
DIN EN 1485-H 14 (11.96)
Period of validity: 01.10.2012 to 13.09.2016
AL, HA, MÜ,
OP
Translation
AL, HA, MÜ,
OP
AL, HA, MÜ,
OP
84/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parts/
Parameters
Total carbon (TOC) of the dry residue in
the original substance
Bases/
Test methods
Annex 4 No. 2.2.2 AbfAblV
DIN 38409-H 3 (06.83)
DIN EN 1484 H 3 (08.97)
DIN EN 13137 (12.01)
Total carbon (TOC) (from eluate)
DIN EN 1484 H 3 (08.97)
Matter soluble in lipophilic substances
Annex 4 No. 2.3 AbfAblV
Phenols (from eluate)
DIN 38409-H 16-3 (06.84)
DIN EN ISO 14402 H 37 (12.99)
Hydrocarbons
E DIN EN 14039 (12.00) i.V. with LAGA
KW/04 (11.04)
DIN EN 14039 (01.05)
5.5
Organic single substances
Sites
BO, OP
BO, HA, OP
AL, HA, MÜ,
OP
AL, HA, MÜ,
OP
AL, HA
AL, MÜ, OP
AL, HA, MÜ,
OP
AL, HA, MÜ,
OP
Annex 4 No. 3 DepV
Handbuch Altlasten Bd. 7, HLUG
(1998)
Polycyclic aromatic hydrocarbons (PAH)
Bulletin 1 LUA NRW (1994)
AL, HA, MÜ,
OP
DIN 38414-S 21 (02.96)
DIN 38414-S 23 (02.02)
Volatile halogenated hydrocarbons
(VHHC)
DIN EN ISO 10301 F 4 (08.97)
Benzene and derivatives, highly volatile
monoaromatic hydrocarbons (BTEX)
DIN 38407-F 9 (05.91)
Polychlorinated biphenyls (PCB)
DIN 38414-S 20 (01.96)
5.6
Annex 4 No. 3 DepV
Strength
Shear strength
Axial deformation
Uniaxial compressive strength
DIN 4096 (05.80)
DIN 18136 (08.96)
DIN 18136 (08.96)
5.7
§ 6 Part 4 DepV
Biological degradability
Respiration activity during 4 days (AT4)
Rate of gas generation by fermentation
test during 21 days (GB21)
Period of validity: 01.10.2012 to 13.09.2016
Annex 4 No. 2.5 AbfAblV
Annex 4 No. 2.6 AbfAblV i.V. with DIN
38414-S 8 (06.85)
Translation
AL, HA, MÜ,
OP
AL, HA, MÜ,
OP
AL, HA, MÜ,
OP
AL, BO, HA,
MÜ, OP
AL
AL
85/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Fields of testing 6: Waste wood
Parts/
Parameters
Bases/
Test methods
§ 6 Part 6 AltholzV
6.1 Sampling, sample preparation
Annex IV No. 1.1-1.3, 1.4.1 AltholzV
Sampling of wood chips
Annex IV No. 1.1 AltholzV
Preparation of the laboratory sample,
sample division
Annex IV No. 1.2 AltholzV with
DIN 51701-3 (08.85)
Sample preparation: homogenization,
drying and crushing < 2 mm
Annex IV No. 1.3
Moisture contents
DIN 52183 (11.77)
6.2 Metals
Annex IV No. 1.4.3 AltholzV
Aqua regia digestion
Arsenic (from aqua regia digestion)
Lead
(from aqua regia digestion)
Cadmium
(from aqua regia digestion)
Chromium
(from aqua regia digestion)
E DIN EN 13657 (10.99)
DIN EN 13657 (01.03)
DIN EN ISO 11969 D 18 (11.96)
DIN 38406-E 6 (07.98)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
DIN EN ISO 5961 (05.95)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
DIN EN 1233 E 10 (08.96)
Mercury
(from aqua regia digestion)
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
DIN EN 12338 E 31 (10.98)
DIN EN 1483 E 12 (08.97)
6.3 Halogen
Annex IV No. 1.4.2 AltholzV
Oxidative dissolution
DIN 51527 (06.01)
Period of validity: 01.10.2012 to 13.09.2016
AL, BO, HA,
MÜ, OP, WA
AL, BO, HA,
MÜ, OP, WA
AL, BO, HA,
OP, WA
AL, BO, HA,
OP, WA
AL, HA, OP
AL, HA, OP
AL, HA, OP
DIN ISO 11047 (06.95)
DIN ISO 11047 (05.03)
DIN EN ISO 11885 E 22 (04.98)
DIN 38406-E 7 (09.91)
Copper
(from aqua regia digestion)
Sites
Translation
AL, HA, OP
AL, HA, OP
AL, HA, OP
BO, OP, WA
86/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Parts/
Parameters
Fluorine (ion chromatography by
oxidative dissolution)
Chlorine (ion chromatography by
oxidative dissolution)
Pentachlorophenol (PCP)
Polychlorinated biphenyls (PCB)
7.1
Sites
DIN EN ISO 10304-1 D 19 (04.95)
BO, WA
DIN EN ISO 10304-1 D 19 (04.95)
BO, OP, WA
Annex IV No. 1.4.4. and 1.4.5
AltholzV
6.4 Organic parameters
7
Bases/
Test methods
Annex IV No. 1.4.4 AltholzV, (GC/ECD
after acetylation)
Annex IV No. 1.4.5 AltholzV in
connection with DIN 38414-S 20
(01.96)
AL
AL, BO, HA,
OP
Sampling and analysis of pollutants in the air
Determination of indoor air pollutants
DIN ISO 16000-3
2002-08
Indoor air - Part 3: Determination of formaldehyde and
other carbonyl compounds; Active sampling method
in conjunction with:
DIN EN ISO 16000-1
2006-06
DIN EN ISO 16000-5
2007-05
DIN ISO 16000-6
2004-12
AL (SA),
BE (SA),
BOi (SA),
HA (SA, AN),
MA (SA),
Indoor air - Part 1: General aspects of
MÜ (SA),
sampling strategy
OP (SA),
WA (SA)
Indoor air - Part 5: Sampling strategy
for volatile organic compounds (VOCs)
Indoor air - Part 6: Determination of volatile organic
compounds in indoor and test chamber air by active
sampling on Tenax TA sorbent, thermal desorption and gas
chromatography using MS/FID
in conjunction with:
DIN EN ISO 16000-1
2006-06
Indoor air - Part 1: General aspects of
sampling strategy
DIN EN ISO 16000-5
2007-05
Indoor air - Part 5: Sampling strategy
for volatile organic compounds (VOCs)
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL (SA, AN),
BE (SA),
BOi (SA),
HA (SA),
MA (SA),
MÜ (SA),
OP (SA)
87/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN ISO 16000-16
2009-12
VDI 2100 Page 2
2010-11
Indoor air - Part 16: Detection and enumeration of moulds - AL (SA),
Sampling by filtration
BOi (SA),
HA (SA),
in conjunction with:
MA (SA),
MÜ (SA),
DIN EN ISO 16000-1
Indoor air - Part 1: General aspects of OP (SA)
2006-06
sampling strategy
VDI 4300 Page 10
2008-07
Measurement of indoor air pollution Measurement strategies for
determination of mould fungi in indoor
environment
Determination of gaseous compounds in ambient air;
Determination of indoor air pollutants - Gas
chromatographic determination of organic compounds Active sampling by accumulation on activated charcoal;
Solvent extraction
in conjunction with:
VDI 2267 Page 8
2000-03
VDI 2100 Page 1
2008-06
Gaseous ambient air pollution
measurement - Indoor air pollution
measurement - Gas chromatographic
determination of organic compounds Fundamentals
DIN EN ISO 16000-1
2006-06
Indoor air - Part 1: General aspects of
sampling strategy
DIN EN ISO 16000-5
2007-05
Indoor air - Part 5: Sampling strategy
for volatile organic compounds (VOCs)
Determination of suspended particles in ambient air Measurement of the mass concentration of mercury Sampling by sorption as amalgam and determination by
atomic absorption spectrometry (AAS) with cold vapour
technique
AL (SA),
BE (SA),
BOi (SA),
HA (SA),
MA (SA),
MÜ (SA),
OP (SA),
WA (SA)
OP (SA, AN)
in conjunction with:
DIN EN 13211
2001-06
Period of validity: 01.10.2012 to 13.09.2016
Air quality - Stationary source emissions
- Manual method of determination of
the concentration of total mercury
Translation
88/141
Annex to the Accreditation Certificate D-PL-14162-01-00
VDI 2464 Page 1
2009-09
Ambient air measurement - Indoor air measurement Measurement of polychlorinated biphynyls (PCBs); GC/MS
method for PCB 28, 52, 101, 138, 153, 180
(Analysis analogously DIN 51527-1: withdrawn standard)
(AL: Analysis analogously DIN EN 61619)
in conjunction with:
DIN EN ISO 16000-1
2006-06
AL (SA, AN),
BE (SA),
BOi (SA),
HA (SA),
MA (SA),
MÜ (SA)
OP (SA)
WA (SA)
Indoor air - Part 1: General aspects of
sampling strategy
VDI 3482 Page 4
1984-11
Measurement of gaseous immissions - Gas chromato-graphic BE (SA)
determination of organic compounds using capillary columns RM (AN)
- Sampling by enrichment on activated carbon; desorption OP (AN)
with solvent
(Variation for RM: Extraction with benzyl alcohol
and headspace analysis; GC-MS)
(Variation for OP: Measurement with GC-MS)
(withdrawn standard)
VDI 3482 Page 5
1984-11
Measurement of gaseous immissions - Gas chromato-graphic BE (SA)
determination of aromatic hydrocarbons - Sampling by
RM (AN)
enrichment on activated carbon; desorption with solvent
(Variation for RM: Extraction with benzyl alcohol, headspace
analysis; GC-MS)
(withdrawn standard)
VDI 3484 Page 1
2001-11
Gaseous ambient air measurements - Indoor-air pollution
measurements - Test gases measurements; Measurement of
the formaldehyde concentration with the sulphite
pararosaniline method
BE (SA)
BO (SA)
HA (AN)
OP (SA)
In conjunction with:
VDI 3498 Page 2
2002-07
DIN EN ISO 16000-1
2006-06
Indoor air - Part 1: General aspects of
sampling strategy
DIN EN ISO 16000-2
2006-06
Indoor air - Part 2: Sampling strategy
for formaldehyde
Ambient air measurement - Indoor air measurement Measurement of polychlorinated dibenzo-p-dioxins and
dibenzofurans; Method using small filters
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL (AN)
BE (SA)
89/141
Annex to the Accreditation Certificate D-PL-14162-01-00
AL, BE, BOi,
HA, MA, MÜ,
OP
VDI 4300 Page 8
2001-06
Measurement of indoor air pollution Sampling of house dust
VDI 4301 Page 2
2000-06
Indoor air pollution measurement - Measurement of
AL (SA, AN)
pentaclorphenol (PCP) and <gamma>-hexachlorcyclohexane BE (SA)
(lindane) - GC/MS-method
BOi (SA)
HA (SA)
(Variation: Use of native standards)
MA (SA)
(Additionally: more organochlorine insecticides and
MÜ (SA)
chlorobenzenes)
OP (SA)
WA (SA)
in conjunction with:
DIN EN ISO 16000-1
2006-06
Indoor air - Part 1: General aspects of
sampling strategy
VDI 4300 Page 4
1997-08
Indoor air pollution measurement Measurement strategy for
pentachlorophenol (PCP) and <gamma>hexachlorocyclo-hexane (lindane) in indoor
air
VDI 6022
2006-04
Hygiene requirements for ventilation and air-conditioning
systems and units
AL, HA, OP
NIOSH 5506
1998-01
Determination of polycyclical aromatic hydrocarbons using
HPLC
AL (SA, AN)
BE (SA)
BOi (SA)
HA (SA)
MA (SA)
MÜ (SA)
OP (SA)
in conjunction with:
DIN EN ISO 16000-1
2006-06
DFG No. 1
1991
Indoor air - Part 1: General aspects of
sampling strategy
Analytical methods to test chemical agents/air analyses
detrimental to health, pentachlorophenol
in conjunction with:
VDI 4300 Page 4
1997-08
Period of validity: 01.10.2012 to 13.09.2016
Indoor air pollution measurement Measurement strategy for pentachlorophenol (PCP) and χ-hexachloro-cyclohexane
(lindane) in indoor air
Translation
AL (SA, AN)
BE, (SA)
BOi (SA)
HA (SA)
MA (SA)
MÜ (SA)
OP (SA)
90/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DFG 1
1978-12
Chlorinated biphenyls (PCB)
(Variation WA: Detection by GC-MS)
in conjunction with:
PCB-Guide
DIN EN ISO 16000-1
2006-06
Indoor air - Part 1: General aspects of
sampling strategy
VDI 4300 Page 2
1997-12
Indoor-air pollution measurement - Measurement strategy for polycyclic aromatic
hydrocarbons (PAHs), polychlorinated
dibenzo-p-dioxins (PCDDs), polychlorinated
dibenzofurans (PCDFs) and polychlorinated
bibhenyle (PCBs)
Directive for assessment and remediation of PCBcontaminated building materials and building components
in conjunction with:
WES 103
1996
7.2
DIN EN ISO 16000-1
2006-06
Indoor air - Part 1: General aspects of
sampling strategy
VDI 4300 Page 2
1997-12
Indoor-air pollution measurement Measurement strategy for polycyclic
aromatic hydrocarbons (PAHs),
polychlorinated dibenzo-p-dioxins (PCDDs),
polychlorinated dibenzofurans (PCDFs) and
polychlorinated bibhenyle (PCBs)
GC-MS - Analysis in water, soil and soil gas (Extraction and
headspace analysis)
AL (AN)
BE (SA)
HA (AN)
WA (AN)
AL (SA)
BE (SA)
BOi (SA)
HA (SA)
MA (SA)
MÜ (SA)
OP (SA)
WA (SA)
AL, OP, RM
Analysis of building materials and other material samples, test chamber analyses
DIN ISO 16000-3
2002-08
Indoor air - Part 3: Determination of formaldehyde and other AL (SA)
carbonyl compounds; Active sampling method
HA (AN)
DIN ISO 16000-6
2004-12
Indoor air - Part 6: Determination of volatile organic
AL (SA, AN)
compounds in indoor and test chamber air by active sampling
on Tenax TA sorbent, thermal desorption and
gas chromatography using MS/FID
DIN EN ISO 16000-9
2008-04
Indoor air - Part 9: Determination of the emission of volatile
organic compounds from building products and furnishing Emission test chamber method
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL
91/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN EN ISO 16000-11
2006-06
Indoor air - Part 11: Determination of the emission of volatile AL
organic compounds from building products and furnishing Sampling, storage of samples and preparation of test
specimens
DIN EN 717-1
2005-01
Wood-based panels - Determination of formaldehyde release - AL
Part 1: Formaldehyde emission by the chamber method
DIN EN 717-3
1996-05
Wood-based panels - Determination of formaldehyde release - HA
Part 3: Formaldehyde release by the flask method
WES 101
1999
Sampling of building substance
(Material sampling of building materials to test for chemical
and biological pollutants)
7.3
AL, BE, BOi,
DR, HA, MA,
MÜ, OP
Sampling of soil gas and determination of hazardous substances in soil air and landfill gases
DIN EN ISO 10301
1997-08
(A)
Water quality - Determination of highly volatile halogenated
hydrocarbons - Gas-chromatographic methods
(Variation for soil air: determination after desorption of
activated carbon with GC/MS)
BE
DIN ISO 10381-7
2007-10
(A)
Soil quality - Sampling - Part 7: Guidance on sampling of soil
gas
AL, BE, BOi,
HA, MA, MÜ,
OP, WA
DIN EN 24260
1994-05
Petroleum products and hydrocarbons; determination of
HA (AN)
sulfur content; Wickbold combustion method
(Additionally: Determination of chlorine and fluorine)
(Variation: Determination of chloride-, fluoride- and sulphate
ions by ion chormatography)
VDI 2469 Page 1
2005-02
Gaseous emission measurement - Measurenment of nitrous
oxide - Manual gas chromatographic method
HA (AN)
VDI 3496 Page 1
1982-04
Gaseous emission measurement; determination of basic
nitrogen compounds seizable by absorption in sulphuric acid
BO (AN)
HA (AN)
VDI 3860 Page 1
2006-05
Measurement of landfill gas - Principles
AL (SA)
BE (SA)
BO (SA)
HA (SA, AN)
MÜ (SA)
OP (SA)
RM (SA)
WA (SA)
Period of validity: 01.10.2012 to 13.09.2016
Translation
92/141
Annex to the Accreditation Certificate D-PL-14162-01-00
VDI 3860 Page 2
2008-02
Measurement of landfill gas - Measurements in the gas
collection system - Determination of methane, carbon dioxide,
nitrogen, oxygen, hydrogen, hydrogen sulphide, carbon
monoxide, ethane, propane, butane, pentane
AL (SA)
BE (SA)
BO (SA)
HA (SA, AN)
MÜ (SA)
OP (SA)
RM (SA)
WA (SA)
E VDI 3860 Page 4
2009-06
Measurement of landfill gas - Measurements in the subsoil
HA (AN)
VDI 3865 Page 1
2005-06
(A)
Measurement of organic soil pollutants - Planning of
measurements for the determination of volatile organic
compounds in soil gas
AL (SA)
BE (SA)
BO (SA)
BOi(SA)
HA (SA)
MA (SA)
MÜ (SA)
OP (SA)
WA (SA)
VDI 3865 Page 2
1998-01
(A)
Measurement of organic soil pollutants - Techniques of active AL (SA)
sampling of soil gas
BE (SA)
BO (SA)
BOi (SA)
HA (SA)
MA (SA)
MÜ (SA)
OP (SA),
WA (SA)
VDI 3865 Page 3
1998-06
(A)
Measurement of organic soil pollutants - Gas chromatographic MÜ (AN)
determination of volatile organic compounds in soil gas OP (AN)
Direct measurement
RM (AN)
(Variation: Extraction with benzyl alcohol, Headspace-Analysis;
GC-MS or GC-FID for determination of LHKW, benzene and
derivates as well as vinyl chloride)
VDI 3865 Page 4
2000-12
(A)
Measurement of organic soil pollutants, gas chromatographic
determination of low boiled organic compounds is soil air by
direct metering
(Additionally: determination from gas sampling containers)
(Variation: GC-MS or GC-FID for the determination of LCHC,
benzene and derivatives as well as vinyl chloride)
(Additionally for MU: alkane and test spirit)
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL (AN),
HA (AN),
MÜ (AN),
OP (AN),
RM (AN)
93/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN 38407-9 (F 9)
1991-05
(A)
Determination of benzene and several derivatives using Gas
chromatography by steam chamber analysis
(Variation for soil air: determination after desorption of
activated carbon with GC/MS)
DIN 51396-1
2005-08
Testing of lubricants - Determination of wear elements - Part HA
1: Direct determination by inductively coupled plasma optical
emission spectroscopy (ICP-OES)
DIN 51857
1997-03
Gaseous fuels and other gases - Calculation of calorific value,
density, relative density and Wobbe index of pure gases and
gas mixtures
HA
WES 104
1996
Determination of von permanent gases methane, oxygen,
carbon dioxide by GC-WLD
AL (AN),
MÜ (AN),
OP (AN)
WES 191
2006
Determination of soil air and landfill gases: methane, oxygen, AL, BE, BO,
carbon dioxide, hydrogen sulphide, sum parameters, trace
BOi, HA, MA,
gases; direct metering
MÜ, OP
7.4
BE
Fields of testing subject to administrative regulation on pollution protection, here: technical
fields („fields“)
The listed test methods for the respective fields of testing as follows are seen only as examples.
Within the listed fields of testing the laboratory in the area of pollution protection is permitted to
use standard test methods or test methods equivalent to them.
Fields /
Identification
Fields of testing A: inorganic gases, determination of emissions
Components
Standard Title
SO2
SO2
1
Gaseous emission
measurement; determination
of sulphur dioxide
concentration; infrared
absorption units UNOR 6 and
URAS
Gaseous emission
measurement; determination
of sulphur dioxide
concentration; infrared
absorption
SRM
Quality
Document
Note
Site
VDI 2462
Page 4
1975-08
(z)1
---
SOP
„Emi-Kont“
BO (SA),
BE (SA),
RM (SA)
VDI 2462
Page 4
1975-08
(z)*
---
SOP
„Emi-Kont“
RM (SA)
CEM
Only restricted suitable for monitoring limit values
Period of validity: 01.10.2012 to 13.09.2016
Translation
94/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Fields /
Identification
Fields of testing A: inorganic gases, determination of emissions
Components
Standard Title
SO2
Stationary source emissions Determination of mass
--concentration of sulphur
dioxide - Reference method
NOx
Stationary source emissions Reference method for
determination of the sum of
--nitrogen monoxide and
nitrogen dioxide - Ion
chromatography method
NOx
Stationary source emissions Determination of mass
DIN EN
concentration of nitrogen
14792
oxides (NO<(Index)x>) 2006-04
Reference method:
Chemiluminescence
NOx
Gaseous emission
VDI 2456
measurement; determination
Page 6
of the sum of NO and NO2 as
1978-05 (z)*
NO by using a convertor
Stationary source emissions Manual method of
determination of HCl - Part 1:
Sampling of gases
HCl
Stationary source emissions Determination of mass
concentration of gaseous
chlorides expressed as HCl Standard reference method
Period of validity: 01.10.2012 to 13.09.2016
Quality
Note
Document
Site
SOP „EmiDIN EN
Abs“
BO (SA),
14791
SOP „UAL
BE (SA),
2006-04
WL IC-Luft RM (SA),
ion chromaChlorid
AL (AN),
tographic
Nitrat
BO (AN)
method
Sulfat “
SOP
„NOx_Disk_
BO (SA),
Pn“
BE (SA),
VDI 2456
SOP „UAL
RM (SA),
2004-11
WL IC-Luft
AL (AN),
Chlorid
BO (AN)
Nitrat
Sulfat “
CEM
SRM
DIN EN
14792
2006-04
SOP „EmiKont“
BE (SA)
BO (SA)
RM (SA)
SOP
„Emi-Kont“
BE (SA)
BO (SA)
SOP
„Emi-Abs.“
BE (SA)
BO (SA)
RM (SA)
DIN EN
1911-1
1998-07
--DIN EN 1911
2010-12
Translation
95/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Fields /
Identification
Fields of testing A: inorganic gases, determination of emissions
Components
Standard Title
CEM
Stationary source emissions Manual method of
determination of HCl - Part 2:
Gaseous compounds
absorption
HCl
SRM
Note
Site
SOP
„Emi-Abs. “
BE (SA)
BO (SA)
RM (SA)
DIN EN
1911-2
1998-07
---
Stationary source emissions Determination of mass
concentration of gaseous
chlorides expressed as HCl Standard reference method
Stationary source emissions Manual method of
determination of HCl - Part 3:
Absorption solutions analysis
and calculation
HCl
Quality
Document
DIN EN 1911
2010-12
DIN EN
1911-3
1998-07
---
Stationary source emissions Determination of mass
concentration of gaseous
chlorides expressed as HCl Standard reference method
SOP
„UAL WL ICAL (AN)
Luft Chlorid,
BO (AN)
Nitrat,
Sulfat“
DIN EN 1911
2010-12
HF
Gaseous emission
measurement; measurement
of gaseous fluorine
--compounds; absorption
method
VDI 2470
Page 1
1975-10
SOP
„Emi-Abs“
SOP
„UAL WL
Fluorid_Luft
“
CO
Stationary source emissions Determination of the mass
concentration of carbon
--monoxide (CO) - Reference
method: Non-dispersive
infrared spectrometry
DIN EN
15058
2006-09
SOP
„Emi-Kont“
Period of validity: 01.10.2012 to 13.09.2016
Translation
BO (SA)
BE (SA)
RM (SA)
AL (AN)
BO (AN)
BO (SA)
BE (SA)
RM (SA)
96/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Fields /
Identification
Components
Fields of testing C: Inorganic gases, check of the correct installation, function and
calibration of continuously working emission measuring equipment
Note
Standard Title
CEM
SRM
Quality Document
Site
SOP
Stationary source emissions „Funktionsprüfung
DIN EN
Quality assurance of
automatischer
BE (SA)
14181
automated measuring
2004-11 Messeinrichtunge
systems
n nach DIN“
SOP
“Funktionsprüfung
_ autom.
Messeinr.“ SOP
„Funktionsprüf_Ka
Stationary source emissions librierung_ autom
Quality assurance of
VDI 3950 Messeinr 0505“
BE (SA)
automated measuring and
2006-12
electronic data evaluation
SOP
systems
„Funktionsprüf_
Ordnungsgemäßer
Einbau_autom.
Messeinr“
Basic test methods already listed in the fields of testing A (SRM) are not listed here.
Fields /
Identification
Components
Fields of testing D: Dust, dust constituents and chemical compounds absorbed on
dust, determination of emissions
Quality
Note
Standard Title
CEM
SRM
Document
Site
Dust,
tubular filter
device
Particulate matter
measurement - Dust
measurement in flowing gases
--- Gravimetric determination of
dust load / tubular filter device
(4 m³/h, 12 m³/h)
VDI 2066
Page 1
2006-11
SOP „Emi
Staub”
BO (SA)
BE (SA)
RM (SA)
Dust
table filter
Stationary source emissions Determination of low range
mass concentration of dust Part 1: Manual gravimetric
method
DIN EN
13284-1
2001-01
SOP „Emi
Staub”
BO (SA)
BE (SA)
RM (SA)
Period of validity: 01.10.2012 to 13.09.2016
---
Translation
97/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Fields /
Identification
Fields of testing D: Dust, dust constituents and chemical compounds absorbed on
dust, determination of emissions
Quality
Note
Components
Standard Title
CEM
SRM
Document
Site
SOP „Emi Met“
SOP „UOP IL
Metals /
Stationary source emissions BO (SA)
DIN EN
Mikro-wellensemimetals
Determination of the total
BE (SA)
--14385
Aufschlussparticulate and emission of As, Cd, Cr, Co, Cu,
RM (SA)
2004-05
Emissions-filter
filtrable
Mn, Ni, Pb, Sb, TI and V
OP (AN)
SOP „UOP MET
KÖWA“
SOP
„Emi Met”
SOP „UOP IL
DIN EN
Aufschluss von
Air quality - Stationary source
13211
Filter-blättern BO (SA)
emissions - Manual method of
2001-06
für Hg BeBE (SA)
Hg
--determination of the
and
RM (SA)
stimmung“
OP (AN)
concentration of total mercury
correction
SOP
2005-06
“UOP MET“
Quecksilber in
Luft und
Gasproben”
SOP
Stationary source emissions BO (SA)
“Emi-PAK”
Determination of polycyclic
VDI 3874
BE (SA)
PAH
--SOP
aromatic hydrocarbons (PAH) 2006-12
RM (SA)
„UAL GC VDI
GC/MC method
AL (AN)
PAK”
Stationary source emissions SOP “GEF_PNBO (SA)
Measurement of inorganic
VDI 3861 VDI-FAS”
Fibrous
BE (SA)
fibrous particles in exhaust gas --Page. 2
SOP
particles
RM (SA)
- Scanning electron microscopy
2008-01
„UBO REM VDI
BO (AN)
method
3492
Period of validity: 01.10.2012 to 13.09.2016
Translation
98/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Fields/
Identification
Components
Fields of testing F: Dust, dust constituents and chemical compounds absorbed on
dust, check of the correct installation, function and calibration of continuously
working emission measuring equipment
Quality
Not
Standard Title
CEM
SRM
Document
Site
SOP
„FunktionsStationary source emissionsDIN EN
prüfung autoQuality assurance of
--14181
matischer
BE SA)
automated measuring systems
2004-09
Mess-einrichtungen nach
DIN“
SOP
„Funktionsprüfung_auto
m. Messeinr.“
SOP
„FunktionsStationary source emissionsprüf_Kalibrier
Quality assurance of
VDI 3950
ung_autom
automated measuring and
--BE (AN)
2006-12
Messeinr
electronic data evaluation
0505“
systems
SOP
„Funktionsprü
f_Ordnungsgemäßer
Einbau_auto
m. Messeinr“
Stationary source emissions Determination of low range
DIN EN
mass concentration of dust --13284-2
BE (AN)
Part 2: Automated measuring
2004-12
systems
Basic test methods already mentioned in D (SRM) are not listed here.
Period of validity: 01.10.2012 to 13.09.2016
Translation
99/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Fields/
Identification
Fields of testing I: Organic chemical compounds, determination of emissions
Components
Standard Title
Benzene,
toluene, xylene,
ethyl benzene,
tetrachlorethyl
ene,
trichlorethen
Stationary source emissions Determination of the mass
concentration of individual
gaseous organic compounds Activated carbon and solvent
desorption method
Quality
Note
Documents
Site
SOP
“EMI Ads”
BO (SA)
SOP
“uop gc lhkw BE (SA)
und btex in
RM (SA)
aktivkohle
OP (AN)
mittels
headspace”
CEM
SRM
---
DIN EN
13649
2002-05
prEN 13649
2011-05
DIN EN
12619
1999-09
DIN EN
12619
1999-09
prEN 12619
2011-02
---
VDI 3862
Page 2
2000-12
SOP
“Emi Abs”
SOP
“UHA LC ALD
Luft”
BO (SA)
BE (SA)
RM (SA)
HA (AN)
PAH
Stationary source emissions Determination of polycyclic
--aromatic hydrocarbons (PAH) GC/MC method
VDI 3874
2006-12
SOP
“Emi-PAK”
SOP
„UAL GC VDI
PAK”
BO (SA)
BE (SA)
RM (SA)
AL (AN)
Total
hydrocarbon
Stationary source emissions Determination of the mass
concentration of total gaseous
organic carbon in flue gases
from solvent using processes Continuous flame ionisation
detector method
DIN EN
13526 200205
Total
hydrocarbon
Aldehydes /
ketones
Gaseous emission
measurement Determination of volatile
organic compounds, especially
solvents, flame ionization
detector (FID)
Gaseous emission
measurement - Measurement
of aliphatic and aromatic
aldehydes and ketones by
DNPH method - Impinger
method
Period of validity: 01.10.2012 to 13.09.2016
Translation
SOP
„Emi kont“
SOP
„Emi kont“
BO (SA)
BE (SA)
RM (SA)
BO (SA)
BE (SA)
RM (SA)
100/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Fields/
Identification
Components
Fields of testing L: Organic chemical compounds, check of the correct installation,
function and calibration of continuously working emission measuring equipment
Standard Title
CEM
SRM
Quality
Note
Document
Site
SOP
“FunktionsStationary source emissions DIN EN prüfung automatischer
BE (SA)
Quality assurance of automated
14181
measuring systems
2004-09 Messeinrichtungen nach
DIN“
Stationary source emissions SOP
Quality assurance of automated
“Funktionsprü
measuring and electronic data
fung_autom.
evaluation systems
Messeinr.“
SOP
„Funktionsprüf_Kalibrier
VDI 3950
ung_autom
BE (SA)
2006-12
Messeinr
0505“
SOP
„Funktionsprüf_Ordnung
sgemäßer
Einbau_auto
m. Messeinr“
Test methods already mentioned in I are not listed here
Period of validity: 01.10.2012 to 13.09.2016
Translation
101/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Fields/
Identification
Components
PCDD/PCDF
PCB
Fields of testing M1 (M3): Highly toxic organic chemical compounds in extremely
low concentrations (dioxins and furans), determination of emissions sampling,
analysis by a foreign institute
Quality
Note
Standard Titel
CEM
SRM
Document
Site
Stationary source emissions Determination of the mass
concentration of PCDDs/PCDFs
DIN EN
and dioxin-like PCBs - Part 1:
1948
Sampling of PCDDs/PCDFs
Teil 1
SOP
BO (SA),
--2006-06
“EMI_194 BE (SA)
Stationary source emissions 8”
Determination of the mass
DIN EN 1948
concentration of PCDDs/PCDFs
Teil 4 2010-12
and dioxin-like PCBs - Part 4:
Sampling and analysis of dioxinlike PCBs
Period of validity: 01.10.2012 to 13.09.2016
Translation
102/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Fields/
Identification
Components
Fields of testing M2: Highly toxic organic chemical compounds in extremely low
concentrations (dioxins and furans), determination of emissions
analysis
Quality
Note
Standard Titel
CEM
SRM
Document
Site
Stationary source emissions Determination of the mass
concentration of
PCDDs/PCDFs and dioxin-like
PCBs - Part 2: Extraction and
clean-up of PCDDs/PCDFs
PCDD/PCDF
PCB
Stationary source emissions Determination of the mass
concentration of
PCDDs/PCDFs and dioxin-like
PCBs - Part 3: Identification
and quantification of
PCDDs/PCDFs
---
DIN EN
1948
Part 2 and
3
2006-06
DIN EN
1948 Part
4 2010-12
Stationary source emissions Determination of the mass
concentration of
PCDDs/PCDFs and dioxin-like
PCBs - Part 4: Sampling and
analysis of dioxin-like PCBs
PCDD/PCDF
Ambient air measurement Indoor air measurement Measurement of
polychlorinated dibenzo-pdioxins and dibenzofurans;
Method using large filters
Period of validity: 01.10.2012 to 13.09.2016
---
VDI 3498
Page 1
2002-07
Translation
SOP „UAL HSL
Probenvorbereit
ung PCDD“
SOP „UAL HSL
Messung PCDD“
AL (SA)
SOP „UAL HSL
Qualitätssicheru
ng PCDD“
SOP
„UAL HSL
Probenvorbereitung
PCDD“
SOP
„UAL HSL
Messung PCDD“
SOP
„UAL HSL
Qualitätssicherung PCDD“
AL (SA)
103/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Fields/
Identification
Components
PCDD/PCDF
PCDD/PCDF
PCB
Fields of testing M2: Highly toxic organic chemical compounds in extremely low
concentrations (dioxins and furans), determination of emissions
analysis
Quality
Note
Standard Titel
CEM
SRM
Document
Site
SOP
„UAL HSL
ProbenAmbient air measurement vorbereitung
Indoor air measurement PCDD“
VDI 3498
Measurement of
SOP
--Page 2
AL (SA)
polychlorinated dibenzo-p„UAL HSL
2002-07
dioxins and dibenzofurans;
Messung PCDD“
Method using small filters
SOP
„UAL HSL
Qualitätssicherung PCDD“
SOP
„UAL HSL
Ambient air measurement Probenvorbereit
Deposition measurement of
VDI 2090
ung PCDD“
low volatile organic
Page 1
SOP
AL (SA)
compounds - Determination
--2001-01
„UAL HSL
of PCDD/F deposition;
Messung PCDD“
Bergerhoff sampling device
SOP
„UAL HSL
and GC/HRMS analysis
Qualitätssicherung PCDD“
Fields/
Identification
Group IV
Component
Standard Titel
Determination
of the
minimum
temperature
(Combustion
chamber
temperature)
Measurement of combustion
conditions of refuse
incinerators
Period of validity: 01.10.2012 to 13.09.2016
CEM
SRM
Quality
Document
Note
Site
SOP
„NachBE (AN,
verbrenn_Beding SA)
“
---
Translation
104/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Further applicable documents
DIN EN 15259
2008-01
7.5
Air quality - Measurement of stationary source emissions Requirements for measurement sections and sites and for the
measurement objective, plan and report
Methods for the determination and assessment of concentrations of dangerous air
constituents at working places
The listed test methods for the respective fields of testing as follows are seen only as examples.
Within the listed fields of testing the laboratory in the area of workplace mesurements is permitted
to use standard test methods or test methods equivalent to them.
Group 1
Aerosols
(without fibrous
dust)
Component
Standard Titel
Quality
Document
SRM
VA /AA
SOP „A-Staub“
BGIA No. 6068
SOP „Grav-Fil“
2003-10
SOP „Grav-Fil-A“
SOP „E-Staub“
BGIA No. 7284
SOP „Grav-Fil“
2003-10
SOP „Grav-Fil-A“
A dust
Alveolar dust fraction
E dust
Inhaleable dust
fraction
Chromium
Chromium
BGIA No. 6645 SOP„E-Staub“
2001-10
SOP „UOP MET KÖWA“
Cobalt
Cobalt
BGIA No. 6690 SOP „E-Staub“
1990-10
SOP „UOP MET KÖWA“
Nickel and nickel
Nickel
compounds
Chromate
Chromium (VI)
Cristalline
mineral dusts
Quartz
DME
Diesel engine
emissions
Period of validity: 01.10.2012 to 13.09.2016
BGIA No. 8095
1997-04
SOP „E-Staub“
SOP „UOP MET KÖWA“
BGIA 6665
2006-10
SOP „E-Staub“
SOP „UAL WL Chrom VI
Leder Luft“
BGIA No. 8522
2005-04
BGI 505-44 V2
1995
Translation
Note
Site
BE (SA, AN),
BO (SA, AN),
RM (SA, AN)
BE (SA, AN),
BO (SA, AN),
RM (SA, AN)
BE (SA),
BO (SA),
RM (SA),
OP (AN)
BE (SA),
BO (SA),
RM (SA),
OP (AN)
BE (SA),
BO (SA),
RM (SA),
OP (AN)
AL (AN),
BE (SA),
BO (SA),
RM (SA)
SOP „A-Staub“
RM (SA)
SOP „A-Staub“
BE (SA),
BO (SA)
105/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Group 2
Fibrous dust
Component
Asbestos fibres
and other
inorganic fibres
Group 3
Inorganic gases
and vapours
Component
Halogenated
hydrogens and
other inorganic
acids
Standard Titel
SRM
Method for the
seperate
determination of
respirable asbestos
fibers and other
inorganic fibers REM-method
BGI 505-46
1991-01
Standard Titel
SRM
Quality
Document
VA /AA
SOP
„PN-ZH-Fas“
SOP
“UBO REM BGI505.46”
Quality
Document
Hydrogen chloride
BGIA No. 6172
2007-04
Hydrocyanic acid
BGIA No. 6725
2000-03
Sulfuric acid
BGIA No. 6173
aerosol oder gaseous 2010-12
Other volatile
hydrides
Ammonia
Period of validity: 01.10.2012 to 13.09.2016
BGIA No. 6150
2009-05
VA /AA
SOP “E-Staub-”
SOP „UAL WL IC Chlorid
Nitrat Sulfat”“
SOP “GEF Abs”
SOP „UAL WL
Cyanwasser-stoff”
SOP “E-Staub”
SOP „UAL WL IC Chlorid
Nitrat Sulfat“
SOP “E-Staub”
SOP “UAL WL
Ammonium”
Translation
Note
Site
BO (AN, SA)
Note
Site
AL (AN)
BO (AN, SA)
AL (AN),
BO (SA)
AL (AN),
BO (AN, SA)
AL (AN),
BO (AN, SA)
106/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Group 4
Organic gases
and vapours
Component
Standard Titel
Phenols
Note
Site
VA /AA
BGIA No. 7732
2005-04
SOP “GEF-Ads”
SOP „UOP GC
Loesemittel Luft“
Aromatic compounds BGIA No. 7733,
2005-04
(e.g. Benzol)
SOP “GEF-Ads”
SOP „UOP GC
Loesemittel Luft“
LHKW (e.g.
dichloromethane)
BGIA No.6600
2006-10
SOP “GEF-Ads”
SOP „UOP GC
Loesemittel Luft“
Ketones (e.g.
acetone)
BGIA No. 7708
2005-04
SOP “GEF-Ads”
SOP „UOP GC
Loesemittel Luft“
Ester
(e.g. ethyl acetate)
BGIA No. 7322
2009-05
SOP “GEF-Ads”
SOP „UOP GC
Loesemittel Luft“
Phenols
BGIA No. 8330
1991-04
SOP “GEF-Ads”
SOP „UOP GC
Loesemittel Luft“
Aliphatic compounds
(e.g. Hexan)
Simple solvents
(Aliphatics,
aroma-tics,
LCHC, ketones,
esters)
Quality
Document
SRM
2-Butanol
Alcohols
Methanol
BE (SA)
BO (SA)
RM (SA)
OP (AN)
BE (SA)
BO (SA)
RM (SA)
OP (AN)
BE (SA)
BO (SA)
RM (SA)
OP (AN)
BE (SA)
BO (SA)
RM (SA)
OP (AN)
BE (SA)
BO (SA)
RM (SA)
OP (AN)
BO (SA)
OP (AN)
BE (SA)
SOP “GEF-Ads”
BGIA No. 6386
BO (SA)
SOP „UOP GC Loesemittel
1997-04
RM (SA)
Luft“
OP (AN)
BE (SA)
SOP “GEF-Ads”
BGIA No. 7810
BO (SA)
SOP „UOP GC
1997-04
RM (SA)
Loesemittel Luft“
OP (AN)
Aldehydes
Aldehydes
BGIA No. 6045
2009-11
SOP “GEF-Ads”
SOP „UHA LC ALD Luft“
BE (SA)
BO (SA)
HA (AN)
Organic acids
Formic acid
BGIA No. 6070
1993-10
SOP “GEF-Ads”
BE (SA)
Period of validity: 01.10.2012 to 13.09.2016
Translation
107/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Group 5
Selected
parameters
Component
Standard Titel
SRM
Quality Document
Note
Site
VA /AA
Cooling
lubricants
Cooling lubricants
BGIA No. 7750
1997-01
SOP “E-Staub“
BE (SA)
BO (SA)
Isocyanate
Diisocyanate, monomer
(2,4-TDI, 2,6-TDI, 2,4’-MDI,
2,6’-MDI, HDI, IPDI und
NDI), Isocyanate
BGIA No. 7120
2010-12
BGIA No. 7670
2009-05
SOP „E-Staub“
SOP “UHA LC ICN
Luft”
HA (AN)
BE (SA)
BO (SA)
Mineral oils
Mineral oils, vapour and
aerosols
BGIA 8000
1997-11
SOP „E-Staub“
BO (SA)
Phthalates
Phthalates
BGIA 8387
2009-11
SOP “GEF-Ads”
RM (SA)
Further applicable documents
Dangerous Substances Directive, respectively valid version
Guideline "Grundsätzliche Anforderungen an akkreditierte Messstellen zum Vollzug des
Gefahrstoffrechts" (2005-09)
IFA workbook (Expositionsermittlung bei chemischen und biologischen Einwirkungen)
TRGS 402 respectively valid version
Manual of analytical Methods of NIOSH (national Institute for occupational safety and health)
8
Sampling and tests of inorganic fibrous particles using scanning electron microscopy *
BGI 505-46
(ZH1/120.46)
2004-04
Test methods for the determination of respirable
asbestos fibres and other inorganic fibres - REM test
methods
BO(AN)
BO(SA)
VDI 3492
2004-10
Indoor air measurement - Ambient air measurement Measurement of inorganic fibrous particles - Scanning
electron microscopy method
AL (SA)
BE (SA)
BO (AN)
BOi (SA)
HA (SA)
MA (SA)
MÜ (SA)
OP (SA)
RM (SA)
WA (SA)
Period of validity: 01.10.2012 to 13.09.2016
Translation
108/141
Annex to the Accreditation Certificate D-PL-14162-01-00
VDI 3866 Page 1
2000-12
Determination of asbestos in technical products Principle - Sampling and sample preparation
in conjunction with:
TRGS 519
2007
TRGS 521
2008
AL (SA)
BE (SA)
BOi (SA)
HA (SA)
MA (SA)
Asbestos, demolition, decontamination MÜ (SA)
or maintenance works
OP (SA)
Fibrous dusts
VDI 3866 Page 5
2004-10
Determination of asbestos in technical products Scanning electron microscopy method
BO (AN)
E VDI 3877 Page 1
2009-09
Indoor air pollution - Measurement of fibrous dust on
settled on surfaces - Sampling and analysis (REM/EDXA)
AL (SA)
BOi (SA)
HA (SA)
MA (SA)
MÜ (SA)
OP (SA)
in conjunction with
TRGS 521
2008
Fibrous dusts
WES 082
2008
Identification and determination of the asbestos
BO (AN)
contamination in dust and soil samples, semiquantitative;
scanning electron microscopy method
WES 085
2008
Testing of unknown dust and solid material samples for
chemical composition; scanning electron microscopy
method
9
BO (AN)
Determination of polyhaloginated dioxines and furanes by HRGC/HRMS *
Flexible accreditation area: AL*
BIA 120 245
1994
Halogenated dibenzodioxins and dibenzofurans at work
place.
AL
DIN 38407-3 (F 3)
1998-07
Determination of polychlorinated biphenyls (F3)
AL
V DEV F 33
2002
Determination of polychlorinated dioxins (PCDD) and
polychlorinated dibenzofurans (PCDF)
AL
Period of validity: 01.10.2012 to 13.09.2016
Translation
109/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN 38414-24 (S 24)
2000-10
(A)
Determination of polychlorinated dioxins (PCDD) and
polychlorinated dibenzofurans (PCDF)
(Additionally for soil: Extraction of air dried or freeze
dried samples)
AL
EPA method 1613
1994-10
Tetra-through Octa-Chlorinated Dioxins and Furans by
Isotope Dilutions HRGC/HRMS
(Variation AL, BO: detection by MS/MS)
(Additionally for AL, BO: dioxin- like PCB)
(Additionally for AL: swab samples)
AL, BO
in conjunction with:
AbfKlärV
Annex 1, Part 1.3.3.
1997-03
VDI 3499 Page 1
2003-07
(A)
COMMISION
REGULATION (EC) No
1883/2006
Laying down methods of sampling and
analysis for the official control of levels
of dioxins and dioxin-like PCBs in
certain foodstuffs
Commission Directive
2002/70/EG of
26 July 2002
Establishing requirements for the
determination of levels of dioxins and
dioxin-like PCBs in feeding stuffs
Commission Directive
2005/7/EG of 27
January 2005
Modification of the Commission
Directive 2002/70/EG for the
establishing requirements for the
determination of levels of dioxins and
dioxin-like PCB in feeding stuff.
Determination of polychloride dibenzodioxins (PCDDs)
and polychloride dibenzofurans (PCDF)
Emission measurement - Determination of
polychlorinated dibenzo-p-dioxins (PCDDs) and
dibenzofurans (PCDFs) - Dilution method
AL
AL
10 Biological tests in surface, ground, leachate and waste water, waste, organic fertilizers, soil
improvers, substrates, compost and eluates as well as determination of the biodegradation of
chemical substances
DIN EN ISO 6341 (L 40)
1996-06
Water quality - Determination of the inhibition of the
mobility of Daphnia magna Straus (Cladocera,
Crustacea) - Acute toxicity test
AL
DIN EN ISO 8692
2005-01
Water quality- Freshwater algal growth test with
unicellular green algae
AL
Period of validity: 01.10.2012 to 13.09.2016
Translation
110/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN EN ISO 9888
1999-11
Water quality- Evaluation of ultimate aerobic
biodegradablity of organic compunds in aqueous
medium, Static test (Zahn- Wellens method)
DIN EN ISO 11348-2
(L 34)
2009-05
Water quality - Determination of the inhibitory effect of AL
water samples on the light emission of Vibrio fischeri
(Luminescent bacteria test) - Part 2: Method using liquiddried bacteria
DIN EN ISO 15088
2009-06
Water quality - Determination of the acute toxicity of
waste water to zebrafish eggs (Danio rerio)
AL
DIN 38415 (T 3)
1996-12
Determination of the genotype potential of water and
waste water components with the umu-test (T3)
MS
DIN 38410-1 (M 1)
2004-10
Biological- ecological analysis of water (group M)- Part 1: AL
Determination of the saprobic index in running waters
(M1)
DEV L 3
1966
Determination of toxicity of waste water and waste
AL
water constituents after dehydrogenase activity using 2,
3, 5-triphenyltetrazolium chloride (TTC)
(withdrawn standard)
DIN 38412-3 (L 3)
2010-10
Toxicity test for assessing the inhibition of the
dehydrogenase activity of activated sludge
microorganism (TTC- Test) (L3)
AL
DIN 38412-16 (L 16)
1985-12
Determination of chlorophyll a in surface water (L16)
AL
DIN 38412-30 (L 30)
1989-03
Determining the tolerance of Daphnia to the toxicity of
waste water by way of dilution series (L30)
AL
DIN 38412-31 (L 31)
1989-03
Determining the tolerance of fish to the toxicity of waste AL
water by way of a dilution series
DIN 38412-33 (L 33)
1991-03
Determining the tolerance of green algae to the toxicity AL
of waste water (Scenedesmus chlorophyll fluorescence
test) by way of dilution series
DIN 38412-34 (L 34)
1997-07
Determination of inhibitory effect of water samples on
the light emission of Photobacterium phosphoreum
(Luminescent bacteria test)
(withdrawn standard)
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL
AL
111/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN 38414-8 (S 8)
1985-06
Determination of the amenability to anaerobic digestion AL
(S8)
Book of methods BGK
e. V. chapter II A3.1
2009-09
Maximum grain size
AL
Book of methods BGK
e. V. chapter II A 4
2009-09
Bulk density
AL, OP
Book of methods BGK
e. V. chapter II C
2009-09
Undesired / foreign particles
AL, OP
Book of methods BGK
e. V. chapter IV A1
2009-09
Degree of digestion in the auto-heating test
AL
Book of methods BGK e. V.
chapter IV A2
2009-09
Respiration activity
AL
Book of methods BGK
e. V. chapter IV A3
2009-09
Plant compatibility in the seedlings test with
spring barley
AL
Book of methods BGK
e. V. chapter IV A4
2009-09
Gaseous phytotoxins in the seedlings test
cress
AL
BioAbfV
Annex 2
1998-09
Germinable seeds and plant parts capable of shooting
AL
DepV
2009-04
Biodegradabilitiy oft he dry residue oft the original
substances breathability (AT4)
AL
DepV
2009-04
Gas production (GB21)
AL
Laboratory methods to
assess the biological soil
decontamination,
determination of the actual
microbial activity, Dechema
1992-01
Actual respiration activity in soil (Sapromat)
AL
Period of validity: 01.10.2012 to 13.09.2016
Translation
112/141
Annex to the Accreditation Certificate D-PL-14162-01-00
Laboratory methods to
assess the biological soil
decontamination,
determination of the actual
microbial activity, Dechema
1992-01
Potential respiration activity in soil (Sapromat)
AL
VDI 3475 Page 4
2010-08
Emission control- Agricultural biogas facilities - Digestion AL
of energy crops and manure
VDI 4630
2006-04
Fermentation of organic materials - Characterisation of
the substrate, sampling, collecting of material data,
fermentation tests
AL
OECD 471
Ames-test methods
MS
11 Test of foodstuffs, animal feeding stuffs, drinking water, mineral and table water, commodity
goods, cosmetics, air, organic fertilizers, soil improvement materials, substrates and compost
11.1 Sampling
ASU L 00.00-7 (EG)
2004-07
Tests of foodstuffs - Sampling methods to check the
maintenance of the maximum residue levels - MRLS in
pesticide residues in and products of vegetal or animal
origin
BE
11.2 Microbiological methods **; Culture tests (aerobic and anaerobic)
11.2.1 Cast iron plate, surface spatulate, titre, MPN, concentration method by membrane filtration
and sedimentation techniques
Flexibel accriditation area: AL**, OP**, WA**
ISO 4832
2006-02
Horizontal method for the enumeration of coliforms Colony count technique
ISO 11290-2
2005-01
Horizontal method for the detection and enumeration of AL, WA
Listeria monocytogenes Part 2: Enumeration method
DIN ISO 16000-17
2010-06
Indoor air- Part 17: Detection and enumeration of
moulds- Culture-based method
Period of validity: 01.10.2012 to 13.09.2016
Translation
OP, WA
AL, OP, WA
113/141
Annex to the Accreditation Certificate D-PL-14162-01-00
ISO 16649-2
2009-12
Horizontal method for the enumeration of ßglucoronidase-positive Escherichia coli - Part 2: Colonycount technique at 44°C using 5-bromo-4-chloro-3indolyl β-D-glucoronide
AL, OP, WA
ISO 18415
2007-12
Cosmetics- Microbiology- Detection of specified and
nonspecified microorganisms
AL, WA,
ISO 21527-1
2008
Microbiology of food and animal feeding stuffs AL, WA
Horizontal method for the enumeration of yeasts and
moulds - Part 1: colony count technique in products with
water activity greater than 0,95
ISO 21527-2
2008
Microbiology of food and animal feeding stuffs AL, WA
Horizontal method for the enumeration of yeasts and
moulds - Part 2: colony count technique in products with
water activity less than or equal to 0,95
ISO 21528-2
2009-12
Horizontal method for the detection and enumeration of AL, OP, WA
Enterobacteriaceae - Part 2: Colony-count method
ISO 26323
2009-07
Milk products- Determination of the acidification activity WA
of dairy cultures by continuous pH measurement (CpH)
DIN EN ISO 4833
2003-06
Microbiology of food and animal feeding stuffsHorizontal method fort he enumeration of
microorganisms- Colony count technique at 30 °C
DIN EN ISO 6222 (K 5)
1999-07
Water quality - Enumeration of culturable microAL, MS, OP,
organisms Colony count by inoculation in a nutrient agar WA
culture medium
(colony count at 22 oC and 36 oC)
DIN EN ISO 6579
2007-10
Horizontal method for the detection of Salmonella spp.
(ASU L 00.00-20, 2008-12)
AL, OP, WA
DIN EN ISO 6887-2
2004-01
Preparation of test samples, initial suspension and
decimal dilutions for microbiological examination- Part
2: Specific rules fort he preparation of meat an meat
products (ASU L 06.00-16, 2004-12)
AL, OE, OP,
WA
DIN EN ISO 6887-5
2011-01
Preparation of test samples, initial suspension and
AL, OE, OP,
decimal dilutions for microbiological examination- Part 5 WA
Specific rules fort he preparation of milk and milk
products (ASU L 01.00-1, 2002-05)
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL, OE, OP,
WA
114/141
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DIN EN ISO 6888-1
2003-12
Horizontal method fort he enumeration of coagulaseAL, OE, OP,
positive staphylococci (Staphylococcus aureus and other WA
species) Part 1: Technique using Baird-Parker agar
medium
(ASU L 00.00-55, 2004-12)
DIN EN ISO 6888-2
2003-12
Horizontal method fort he enumeration of coagulaseAL, OE, OP,
positive staphylococci (Staphylococcus aureus and other WA
species) Part 2: Technique using rabbit plasma
fibrinogen agar medium
(ASU L 00.00-56, 2004-12)
DIN EN ISO 6888-3
2005-07
Horizontal method fort he enumeration of coagulaseWA
positive staphylococci (Staphylococcus aureus and other
species) Part 3: Detection and MPN technique for low
numbers
DIN EN ISO 7899-1 (K 14)
1999-07
Water quality - Detection and enumeration of intestinal AL
enterococci in surface and waste water - Part 1:
Miniaturized method (most probable number) by
inoculation in liquid medium
DIN EN ISO 7899-2 (K 15)
2000-11
Water quality - Detection and enumeration of intestinal AL, MS, OP,
enterococci - Part 2: Membrane filtration method
WA
DIN EN ISO 7932
2005-03
Horizontal method fort he enumeration of presumptive AL, OP, WA
Bacillus Cereus- Colony-count technique at 30°C (ASU L
00.00-33, 2006-09)
DIN EN ISO 8261
2001-10
General guidance for the preparation of test samples,
initial suspensions and decimal dilutions for
microbiological examination
(ASU L 01.00-1, 2002-05)
DIN EN ISO 9308-1 (K 12)
2001-07
Correction 2009-07
Water quality- Detection and enumeration of Escherichia AL, MS, OP,
coli soliform bacteria- Part 1: Membrane filtration
WA
method
DIN EN ISO 9308-3 (K 13)
1999-07
Water quality - Detection and enumeration of
Escherichia coli and coliform bacteria in surface and
waste water - Part 3: Miniaturized method (most
probable number) by inoculation in liquid medium
AL, WA
DIN EN ISO 10272-1
2006-04
Horizontal method for detection and enumeration of
Campylobacter spp. - Part 1: Detection method
AL, OP, WA
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL, OE, OP,
WA
115/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN EN ISO 11290-1
2005-01
Horizontal method for the detection and enumeration of AL, OP, WA
Listeria monocytogenes- Part 1: Detection method
(ASU L 00.00-32, 2006-09)
DIN EN ISO 11290-2
2005-01
Horizontal method for the detection and enumeration of AL, OP, WA
Listeria monocytogenes - Part 2: Enumeration method
(ASU L 00.00-22, 2006-09)
DIN EN ISO 11731-2
2008-06
Water quality - Detection and enumeration of
AL, MS, OP,
Legionella- Part2: Direct membrane filtration method for WA
waters with low bacterial counts
DIN EN ISO 13843 (K 2)
2001-12
Water quality - Guidance on validation of microbiological AL, OP, WA
methods
DIN EN ISO 16266
2008-05
Water quality - Detection and enumeration of
Pseudomonas aeruginosa- Method by membrane
filtration
AL, MS, OP,
WA
DIN EN ISO 19458
2006-12
Water quality - Sampling for microbiological analysis
AL, OP, WA
DIN EN 26461-2 (K 7)
1993-04
Detection and enumeration of the spores of sulfitereducing anaerobes (clostridia); Part 2: method by
membrane filtration
AL, MS, WA
DIN 10103
1993-08
Microbiological analysis of meat products;
AL, OP, WA
determination of mesophilic sulfite reducting clostridia;
method with poured plates (reference method) (ASU L
06.00-39, 1994-05)
DIN 10106
1991-09
Microbiological analysis of meat and meat products;
determination of enterococcus faecalis and
enterococcus faecim; spatula method (reference
method) (ASU L 06.00-32, 1992-06)
AL, OP, WA
DIN 10109
1991-09
Microbiological analysis of meat products;
determination of aerobic grown latic acid bacterian;
spatula method (reference method) (ASU L 06.00-35,
1992-12)
AL, OE, OP,
WA
DIN 10110
1994-08
Microbiological analysis of meat and meat products Fluorescence optical colony count method using
membranes; spatula method - spatula method
(reference method)
(ASU L 06.00-36, 1996-02)
AL, WA
Period of validity: 01.10.2012 to 13.09.2016
Translation
116/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN 10113-1
1997-07
Determination of surface colony count on fitment and
OP
utensils in foodareas- Part 1: Quantitative swab method
(ASU L 80.00-1, 1998-01)
DIN 10113-2
1997-07
Determination of surface colony count on fitment and
utensils in foodareas- Part 2: Semiquantitative swab
method (ASU B 80.00-2, 1998-01)
OP, WA
DIN 10113-3
1997-07
Determination of surface colony count on fitment and
utensils in foodareas- Part 3- Semiquantitative method
with culture media laminated taking up equipment
(squeeze method)
(ASU L 80.00-3, 1998-01)
OP
DIN 10164-1
1986-08
Microbiological examination of meat and meat products; AL, OE, OP,
determination of Enterobacteriaceae by the spatula
WA
method (reference method)
(ASU L 06.00-24, 1987-11)
DIN 10198-1
2010-07
Determination of presumptive Bacillus cereus- Colony
count technique at 37 °C
(ASU L 00.00-25, 1992-12)
DIN 10198-2
Determination of presumptive Bacillus cereus in Milk
WA, AL
and milk products; technique for selective accumulation
(ASU L 01.00-53, 1992-12)
DIN 38411-6 (K 6)
1991-06
Determination of Escherichia coli and coliforms
AL, MS, WA
ASU L 01.00-3
1987-03
Determination of coliforms in milk, milk products,
butter, cheese and ice cream
OP
ASU L 01.00-37
1991-12
Enumeration of yeasts and moulds in milk and milk
products (reference method)
AL, OE, OP,
WA
ASU L 06.00-18
1984-05
Enumeration of aerobic organisms at 30°C in meat and
meat products; spatula method and method with
poured plates (in combination with DIN EN ISO 4833
(2003-06) Horizontal method fort he enumeration of
microorganisms- Colony-count technique at 30 C
AL, OE, OP,
WA
ASU L 06.00-43
1998-09
Enumeration of Pseudomonas spp. in meat and meat
products
OP
ASU L 59.00-2
1988-05
Detection of faecal Streptoccucus in natural mineral
AL, WA
water, spring water and table water, (reference method)
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL, OP, WA
117/141
Annex to the Accreditation Certificate D-PL-14162-01-00
ASU L 59.00-3
1988-05
Detection of Pseudomonas aeruginosa in natural mineral AL, WA
water, spring water and table water, (reference method)
Colilert-18/Quantitray/
IDEXX
Alternitive process
according to drinking water
Ordiance 2001
Quantitative Determination von E.coli and coliforms
OP, WA
BioAbfV
Annex 2 No 2.3.1.2
1998-09
Salmonellae
AL
UBA-method
Bundesgesbl. 11/2000, 43
S. 911-15
Detection of Legionella in drinking water and water of
baths
AL, MS, OP,
WA
Book of methods BGK e. V.
Chapter IV C1
2009-09
Hygiene of epedemics: product testing of Salmonellae
AL
Ph. Eur. - method 2.6.12
Respectively valid version
Testing of microbiological contamination of nonsterile
products: Enumeration of all augmentable aerobe
bacteria
AL, WA
Ph. Eur. - method 2.6.13
valid vision
Microbiological testing of nonsterile products: detection AL, WA
of specified microorganisms
Ph. Eur. method 5.1.3
valid vision
Testing of adequate preservation
VDI 4253 Page 2
2004-06
Measurement of airborne microorganisms and viruses in AL, OP
ambient air- Culture based method fort he
determination of the concentration of mould in airIndirect method after sampling with
gelatine/polycarbonate filters
VDLUFA 28.1.1 to 28.1.4
2007
aerobe bacteria, yeast and moulds in feeding stuffs
Bundesgesbl. 10/1995
S. 385-96
Microbiological test method of natural waters for
AL, OP, WA
swimming purposes according to directives for natural
waters for swimming purposes 76/160/EWG
Detection of Salmonellae in natural water for swimming
purposes
(withdrawn standard)
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL, WA
AL
118/141
Annex to the Accreditation Certificate D-PL-14162-01-00
TrinkwV, Annex 1
1990-04
Determination of the microbial colony number
(withdrawn standard)
AL, OP, WA
Drinking water Ordiance
1990-12
Detection of Escherichia coli and coliforms by
enrichment in a liquid medium
(withdrawn standard)
AL, MS
Drinking water Ordiance
1990-12
Detection of faecal Streptococcus by enrichment in a
liquid medium
(withdrawn standard)
AL, MS
Drinking water Ordiance
1990-12
Detection of sulfite reducing and sporogenic anaerobes
(Clostridia) by enrichment in a liquid medium
(withdrawn standard)
AL, MS
TRBA 430
2001-08
Method to determine the concentrations of mould fungi AL, OP, WA
and yeast in the air at the workplace
(withdrawn standard)
WES 006
2007
Determination of the Total Viable Count from Chewing
Gum
AL
WES 008
2003-01
aerobe and anaerobe sporns in food
AL, OE, WA
WES-017
2009-06
Identification of isolated microorganisms
(biochemical und microscopic)
WA
WES 018
2003
Determination of Escherichia Coli from Chewing Gum
AL
WES-537
2003
Determination of Yeasts and Moulds from Chewing Gum AL
WES 551
2010
Total bacteria count in food (TEMPO)
AL
WES 552
2010
Escherichia coli in food (TEMPO)
AL
WES 553
2010
Coliforms in food (TEMPO)
AL
WES 554
2010
Enterobacteriaceae in food (TEMPO)
AL
Period of validity: 01.10.2012 to 13.09.2016
Translation
119/141
Annex to the Accreditation Certificate D-PL-14162-01-00
WES 555
2010
Staphylococcus in food (TEMPO)
AL
WES 556
2010
Latic acid bacteria in food (TEMPO)
AL
WES 557
2010
Yeast and moulds in food (TEMPO)
AL
11.2.2 Agardiffusions-method
DIN EN 1104
2005-11
Paper and board intended to come into contact with
foodstuffs - Determination of the transfer of
antimicrobial constituents
AL
ASU L 01.00-6
1997-01
Detection of inhibitors in the agar diffusion method
(leaf tests)
AL, WA
Meat hygiene Ordiance
1986
Annex 1 (2, 4)
WES 033
Inhibitors in muscles and kidneys (three plates test with AL, WA
TMP)
11.2.3 Microbiological technique for detection of vitamins
WES 547
2010
Microbiological testing in micro-well plates for
quantitative determination of vitamin B1 (thiamine)
AL
WES 548
2010
Microbiological testing in micro-well plates for
quantitative determination of vitamin B2 (riboflavin)
AL
WES 549
2010
Microbiological testing in micro-well plates for
quantitative determination of vitamin B6 (pyridoxin)
AL
11.3 Determination of constituents and contaminants using high-pressure liquid chromatography
(HPLC) using the UV/VIS-, DAD-, RI-, LF fluorescence and MS/MS detector **
Flexible accreditation area: AL**, BE**
DIN EN 12014-2
1997-08
Determination of nitrate and/or nitrite content-Part 2: AL
HPLC/IC method for the determination of nitrate
content of vegetables and vegetables products
(replacing the previous official methods L 26.00-1 und L
48.03.05-2)
Period of validity: 01.10.2012 to 13.09.2016
Translation
120/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN EN 12856
1999-07
Determination of acesulfame- K, aspartame and
saccharin- High performance liquid chromatographic
method
(ASU L 00.00-28, 2001-07)
AL
DIN EN 12857
1999-07
Determination of cyclamate- Method by high
performance liquid chromatography
(ASU L 00.00-29, 2006-12)
AL
DIN EN 14177
2004-03
Determination of clear and cloudy apple juice and puree- BE
HPLC method with liquid/liquid partition clean-up
(Variation: application to other fruit puree)
DIN EN 14352
2004-10
Determination of fumonisin B1 and B2 in maize based
foods- HPLC method with immunoaffinity column clean
up
DIN EN 14362-1
2003-12
Textiles- Method for determination of certain aromatic AL
amines derived from azo colorants- Part 1: Detection of
the use of certain azo colorants accessible without
extraction (replacing the previous official method ASU B
82.02-2, 2004-06)
DIN EN 15055
2006-08
Determination of chlormequat and mepiqaut- LCMS/MS method
(ASU L 00.00-76, 2008-12)
BE
DIN EN 15662
2009-02
Foods of plant origin- Determination of pesticide
residues using GC-MS and/or LC-MS/MS following
acetonitrile extraction/partitioning and clean-up by
dispersive SPE - QuEChERS-method
BE
DIN CEN/TS 13130-13
2005-05
Materials and articles in contact with foodstuffs- Plastics AL
substances subject to limitation- Part 13: Determination
of 2,2-Bis(4-Hydroxyphenyl) Propan (Bisphenol A) in
food simulants
DIN 10751-3
2002-02
Analysis of hones- Determination of the content of
hydroxymethylfurfural- Part3: High performance liquid
chromatographic method
DIN 10777-2
2000-06
Analysis of coffee and coffee products- Determination of AL
coffeine content- Part2: rapid method (ASU L 46.00-3,
2000-07)
Period of validity: 01.10.2012 to 13.09.2016
Translation
BE
BE
121/141
Annex to the Accreditation Certificate D-PL-14162-01-00
DIN 10801-2
1995-01
Analysis of tea- Determination of coffeine contentHPLC- method
(ASU L 47.00-6, 1996-02)
AL
ASU L 00.00-9
1984-11
Determination of preserving agents in non-fatty foods
AL
ASU L 00.00-34
1999-11
Analysis of food modular multimethod for determination BE
of Pesticide Residues in food (extended revision of the
DFG-method S 19)
ASU L 00.00-113
2007-12
Analysis of food modular multimethod for determination BE
of Pesticide Residues in food by LC-MS/MS after
extraction with methanol and purification on
diatomaceous earth
ASU L 00.00-115
2007-12
Analysis of food modular multimethod for determination BE
of Pesticide Residues in vegetable food by GC-MS(/MS)
or LC-MS/MS after extraction with acetonitril,
/distribution and purification by dispersive
SPE (QuEChERS1)
ASU L 01.00-55
1993-08
Determination of chloramphenicol in milk
(Additionally: Analysis other foods of animal origin)
BE
ASU L 18.00-16
1999-11
Determination of theobromin and caffeine in pastry
AL
ASU L 43.08-1
1996-02
Determination of glycyrrhizine in liquorice and liquorice- AL
containing sugar products - use of reversed phase high
performance liquid chromatography
VDLUFA volume III, chapter. Determination of aflatoxin B1, B2, G1 and G2 in feeding AL
16.1.4
stuff
1993
VDLUFA volume III, chapter. Determination of deoxynivalenol in feeding stuffs
16.12.1
AL
A. Tellmann, W. Weber: DLR Determination of ochratoxin A in food - HPLC-method
93 (1), 1997, S. 1-3
with immunoaffinity column cleanup
AL
DFG 261-1
1987
Determination of benomyl, carbendazime and
thiophanate-methyl (altogether as carbendazime) and
thiabendazole in foodstuffs using LC-MS/MS
BE
VO (EG) 152/2009
Determination of vitamin A and E in feeding stuff
AL
Period of validity: 01.10.2012 to 13.09.2016
Translation
122/141
Annex to the Accreditation Certificate D-PL-14162-01-00
WES 042
2006
Determination of nitrofuran metabolits in foods of
animal origin by LC-MS/MS
BE
WES 044
2006
Determination of liposoluble azocolourants and
triphenylmethan dye in food by LC-MS/MS
BE
WES 045
2006
Determination of watersoluble azocolourants in food by BE
LC-MS/MS
WES-046
2006
Determination of natural colouring in food by LC-MS/MS BE
WES 063
2006
Determination of sugar and sugar substitutes, glycerin
and 1,2 propandiol in food (HPLC)
AL
WES 072
2001
Determination of deoxynivalenol in food
AL
WES 076
WES 221
2008
Determination of perfluorooctanoic acid (PFOA) und
perfluorooctanoic acid (PFOS) in food
BE
WES 128
2005
Determination of zearalenon in food and feeding stuff
AL
WES 138
2002
Determination of sucralose
AL
WES 205
2007
Determination of inulin in food
AL
WES 251
2004
Determination of amitrol in water by HPLC-MS/MS
BE
WES 274
2005
Determination of dithianon in food by HPLC-MS/MS
BE
WES 404
2008
Determination of melamine in food and feeding stuff by BE
HPLC-MS/MS
WES 461
2009
Determination of ethephon in food by LC-MS/MS
BE
WES 490
2009
Determination of fosetyl-aluminium in food by LCMS/MS
BE
Period of validity: 01.10.2012 to 13.09.2016
Translation
123/141
Annex to the Accreditation Certificate D-PL-14162-01-00
WES 495
2009
Determination of taurine in food by LC-MS-MS
BE
11.4 Determination of constituents and contaminants using gas chromatography (GC)**
Flexible accreditation area: AL**, BE**
DIN ISO 16000-6
2004-12
Indoor air- Part 6: Determination of volatile organic
AL
compounds in indoor and test chamber air by active
sampling on TENAX TA® sorbent, thermal desorption and
gas chromatography using MS/FID (only for analytics)
DIN EN 12396-2
1998-12
Non-fatty foods - Determination of dithiocarbamate and BE
thiuram disulfide residues - Part 2: Gas chromatographic
method
(ASU L 00.00-49/2, 2002-12)
DIN EN 13191-1+2
2000-10
Determination of inorganic bromide in food
(ASU L 00.00-36/1+2, 2004-07)
BE
DIN EN 15662
2009-02
Foods of plant origin - Determination of pesticide
residues using GC-MS and/or LC-MS/MS following
acetonitrile extraction/partitioning and clean-up by
dispersive SPE - QuEChERS-method
BE
ASU L 00.00-34
1999-11
Analysis of food - multimethod for determination of
BE
pesticide residues in foods (extended new version of the
DFG-method, Page 19)
ASU L 00.00-115
2007-12
Analysis of food - multimethod for determination of
pesticide residues in vegetable food using GC-MS(/MS)
or LC-MS/MS after extraction with acetonitril,
/distribution and purification using dispersive
SPE (QuEChERS1)
BE
ASU L 17.00-12
1999-11
Determination of butyric acid in food
AL
ASU L 18.00-10
2006-12
Corrigenda 2011-01
Determination of cholesterol content in starchy foods GC-method after acidic and alkaline solubilisation
AL
ASU L 52.02-1
1995-01
Determination of 3-chlor-1,2-propandiol (3-MCPD) in
BE
seasoning (hydroylsates of proteins) (PBA-method) using
GC/MS
Period of validity: 01.10.2012 to 13.09.2016
Translation
124/141
Annex to the Accreditation Certificate D-PL-14162-01-00
E. Schulte, Fat. Sci. Technol.
91 (1989) 181
Determination of trans-fatty acids in fats, oils and
foodstuffs
FDA
2004-05
Determination of furan in liquid foodstuff by headspace BE
GC/MS
WES 005
2006
Determination of acrylamide in foodstuffs
BE
WES 025
2001
Determination of cholesterol in egg-based farinaceous
products and pastries
AL
WES 035
2006
Determination of nicotine in egg products and other
foodstuffs
BE
WES 047
2006
Determination of acrylamide in coffee
BE
WES 048
2006
Determination of acrylamide in cocoa products
BE
WES 049
2006
Determination of acrylamide in cane sugar and sugar
molasses
BE
WES 132
2000
Determination of Menthol in Gum Base and Chewing
Gum
AL
WES 133
1998
Determination of menthol in sweets
AL
WES 137
2001
Determination of thujone and bisabolol in candies
AL
WES 142
2007
Determination of phthalates in plastic using GC-MS
BE
WES 143
2007
Bestimmung von Phthalaten in Lebensmitteln und
Bedarfsgegenständen mittels GC-MS
BE
WES 183
2007
Determination of pentachlorophenol (PCP) in foodstuffs AL, BE
by GC-MS
(Additionally: also in food additives (e.g. guar flour))
WES 285
2007
Determination of the fatty acid spectrum in fats and oils AL
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL
125/141
Annex to the Accreditation Certificate D-PL-14162-01-00
WES 341
2007
Determination of polycyclic aromatic hydrocarbons
(PAH) in foodstuffs by GC-MS
BE
WES 415
2008
Determination of 3-methylindole (skatole) in pepper by
GC-MS
BE
WES 451
2009
Determination of dimethylfumarates in leather and
textiles
BE
WES 486
2006
Determination of chloroform residues in polyactide
coated stents by GC-MS
BE
WES 487
2006
Determination of solvent residues in foodstuufs and
feeding stuffs after THV by GC-MS
BE
WES 488
2008
Determination of esters of 3-monochloropropane-1,2diol (3-MCPD-esters) in fats and oils by GC-MS
BE
WES 489
2008
Determination of esters of 3-monochloropropane-1,2- BE
diol (3-MCPD-esters) in foodstuffs containing fat by GCMS
11.5 Atomic absorption spectrometric determination of heavy metal residues and metals using
graphite furnace and FIAS measurements as well as CV technology *
DIN EN 13805
2002-06
Determination of element traces in foodstuffs - Part 1:
Decomposition under pressure
(ASU L 00.00-19/1, 2003-12)
AL
DIN EN 13806
2002-11
Determination of element traces in foodstuffs - Part 4:
Determination of mercury with atomic absorption
spectrometry (AAS) - cold vapour technology after
decompo-sition under pressure
(ASU L 00.00-19/4, 2003-12)
AL, HA
11.6 Determination of constituents using enzymatic methods (photometric, enzyme-test-kit) *
DIN 10335
2010-09
Determination of the content of L- and D-lactic acid in milk AL
and milk products; enzymatic method
(ASU L 01.00-26, 2004-07)
DIN 10344
1982-08
Determination of the lactose and galactose content of
milk and milk products; enzymatic method
(ASU L 01.00-17, 2010-09)
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL
126/141
Annex to the Accreditation Certificate D-PL-14162-01-00
ASU L 05.00-2
1987-11
Correction 2002-12
Determination of L-lactic acid, succinic acid and D-3AL
hydroxybutyric acid in eggs and egg products - enzymatic
method
ASU L 07.00-13
2008-06
Determination of citric acid in meat products
AL
ASU L 07.00-25
1983-05
Determination of starch in meat products
AL
ASU L 48.01-5
1985-05
Determination of starch in partly adapted baby food on
milk basis
AL
Appl. r-Biopharm
Determination of ascorbic acid in foodstuffs
AL
Appl. r-Biopharm
Determination of sucrose, D-glucose and D-fructose in
foodstuffs
AL
11.7 Photometric determination of constituents **
DIN EN 717-3
1996-05
Wood-based panels - Determination of formaldehyde
AL
release - Part 3: Formaldehyde release by the flask method
DIN EN 1141
1994-12
Fruit and vegetable juices - Spectrometric determination
of proline content
(ASU L 31.00-7, 1997-01)
ASU L 00.00-6
1995-01
Correction
2002-12
Analysis of foodstuffs - Determination of primary aromatic AL
amines in aqueous simulants
ASU L 06.00-8
1980-09
Correction
2010-09
Determination of the hydroxyproline content in meat and AL
meat products
ASU L 06.00-9
1992-12
Correction
2009-06
Determination of the total phosphate content in meat and AL
meat products
S. Littmann-Nienstedt:
Deutsche Lebensm.
Rundsch. 97 (2) 2001,
S. 60 ff.
Detection and Determination of hydrolysed gelatine in
AL
meat and meat products and additives for meat products
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL
127/141
Annex to the Accreditation Certificate D-PL-14162-01-00
11.8 Thin-layer chromatographic detections of constituents *
ASU L 06.00-15
1982-11
Correction
2002-12
Detection of condensed phosphates in meat and meat
products
AL
ASU L 08.00-12
1980-09
Detection of foodstuff colours in surface-treated sausages AL
for boiling and smoked goods
11.9 Titrimetric determination of the content of constituents *
Flexible accreditation area: AL*, BR*
DIN EN ISO 5943
2007-01
Cheese and processed cheese products - Determination of AL
chloride content - Potentiometric titration method
(ASU L 03.00-11,2007-12)
DIN EN 12147
1997-02
Fruit and vegetable juices - Determination of titrable
acidity (ASU L 31.00-3, 1997-09)
AL, BR
ASU L 06.00-7
2007-04
Determination of the raw protein content in meat and
meat products
AL
ASU L 17.00-6
1988-12
Correction
2009-06
Determination of chloride for the calculation of common
salt in bread, including small pastries made of bread
doughs
AL
ASU L 20.01/02-2
1980-05
Determination of the total acid content in mayonnaise
and emulgated sauces
AL
ASU L 26.04-3
1987-06
Determination of pH value in liquid foodstuffs
AL, BR
ASU L 26.04-4
1987-06
Determination of titrable acidity (total acid) in foodstuffs
AL, BR
ASU L 46.02-1
1988-12
Determination of the water content according to Karl
Fischer; Method for roasted coffee
AL
GAFTA method 4:0
2003-01
Determination of crude protein in feeding stuffs
AL
Bundesgesbl. 40/1997
S. 412 ff.
Determination of peroxide residues in synthetic materials AL
Period of validity: 01.10.2012 to 13.09.2016
Translation
128/141
Annex to the Accreditation Certificate D-PL-14162-01-00
11.10 Gravimetric determination of constituents *
Flexible accreditation area: AL*
ASU L 06.00-6
1980-09
Determination of the total fat content in meat and meat
products
AL
ASU L 16.01-1
2008-12
Determination of the content of moisture in flour
AL
ASU L 16.01-2
2008-12
Determination of the content of ash in flour
AL
ASU L 17.00-1
1982-05
Correction
2002-12
Determination of the drying loss in bread, including small AL
pastries made of bread doughs
GAFTA method 2:1
2005-03
Determination of water content in feeding stuffs
AL
GAFTA method 3:0,
2003-01
Determination of fat in feeding stuffs
AL
GAFTA method 12:0
2003-01
Determination of crude ash in feeding stuffs
AL
GAFTA method 13:0
2003-01
Determination of hydrochloric acid insoluble ash in
feeding stuffs
AL
Richtl. z.
Füllmengenprüfung von
Fertigpackungen
1983-06
Determination of the capacity in pre-packages
AL, BE, BR,
WA
Richtl. z.
Füllmengenprüfung von
Fertigpackungen
1983-06
Determination of the drip-off weight
AL, BR, WA
Ph. Eur., 4. Volume.
2002
Determination of the content of ethereal oils in drugs and BE
spices
Bundesgesbl. 25/1982
S. 911-12
Determination of volatile organic compounds in
commodities
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL
129/141
Annex to the Accreditation Certificate D-PL-14162-01-00
11.11 Determination of chemical-physical parameters *
Flexible accreditation area: AL*
DIN EN ISO 660
2005-11
Determination of the acid number and acidity in fats and
oils (ASU L 13.00-5, 2007-04)
DIN EN ISO 14891
2002-07
Determination of nitrogen content - Routine method using AL
combustion according to the Dumas principle
ASU L 06.00-2
1980-09
Measurement of the pH-value in meat and meat products AL, BR, OE
ASU 06.00-20
2003-12
Determination of nitrogen content in meat and meat
products
AL
ASU L 13.00-6
1991-06
Determination of the peroxide number in fats and oils
AL
ASU L 26.04-3
1987-06
Determination of pH value in liquid foodstuffs
BR
ASU L 30.00-2 (EG)
1993-08
Refractometer method for determination of the soluble
siccative content in products processed from fruits and
vegetablevs
AL, BR
ASU L 36.00-3a
1989-12
Determination of the relative density d 20/20 of worth
and beer; flexural resonators method
AL
DGF C-IV 2d (02),
DIN 53217 Teil 5
2002-05
Density of fats and oils
AL
DGF-Einheitsmethoden
C-V 3 (77)
2002-05
Determination of the saponification number in fats and
oils
AL
VDLUFA Volume. III, 4.1.2
2004
Determination of crude Protein in feeding stuff according AL
to Dumas principle- combustion method
Applikation Rotronic für
HygroLab 2
Determination of water activity (aw-value) in foodstuffs
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL
OE
130/141
Annex to the Accreditation Certificate D-PL-14162-01-00
11.12 Sensory analysis
Flexible accreditation area: AL*
DIN ISO 8587
2010-08
Sensory analysis - Methodology - Ranking
(ASU L 00.90-4, 2011-01)
AL
DIN EN 1622 (B 3)
2006-10
Determination of the threshold odour number (TON) and AL
threshold flavour number (TFN)
DIN EN ISO 4120
2007-10
Sensory analysis - Methodology - Triangle test
(ASU L 00.90-7, 2007-12 )
AL
DIN EN ISO 5495
2007-10
Sensory analysis - Methodology - Paired comparison test
(ASU L 00.90-8, 2007-12)
AL
DIN 10950-2
2000-10
Sensory analysis - Part 2: Basic principles
(ASU L 00.90-1, 2007-04)
AL, BR, OE,
WA
DIN 10959
1998-07
Sensory analysis - Determination of sensitivity of taste
(ASU L 00.90-9, 1999-11)
AL
DIN 10961-2
1997-09
Training of assessors for sensory analysis
AL
DIN 10964
1996-02
Sensory testing methods - Simple descriptive test
(ASU L 00.90-6, 1997-09 )
AL, BE, BR,
WA
11.13 Determination by ELISA of constituents and contaminants *
ASU L 06.00-47
1999-11
Correction
2004-07
Immunoenzymatic detection of the kind of animal for
heated meat and meat products, ELISA method in the
microtitre system
AL
WES 037
2005
Determination of gluten using enzymimmunoassay
AL
WES 038
2005
Immunoenzymatic determination of histamine
AL
WES 039
2005
Immunoenzymatic determination of ß-lactoglobuline
AL
WES 040
2005
Immunoenzymatic determination of deoxynivalenol (DON) AL
Period of validity: 01.10.2012 to 13.09.2016
Translation
131/141
Annex to the Accreditation Certificate D-PL-14162-01-00
WES 050
2003
Detection of Salmonella in foodstuffs by enzyme immuno- AL
assay (ELISA)
WES 051
2005
Detection of Bacillus Diarrhoeal Enterotoxin (ELISA)
AL
WES-052
2005
Detection of Staphylococcal Enterotoxin (ELISA)
AL
WES 053
2005
Immunoassay determination of casein in foodstuffs
(ELISA)
AL
WES 054
2005
Immunoassay determination of egg protein (ELISA)
AL
WES 055
2005
Immunoassay determination of hazelnut content in
foodstuffs (ELISA)
AL
WES 056
2005
Immunoassay determination of crustaceen content in
foodstuffs (ELISA)
AL
WES 057
2005
Immunoassay determination of almond content in
foodstuffs (ELISA)
AL
WES 058
2005
Immunoassay determination of sesame protein in
foodstuffs (ELISA)
AL
WES 059
2005
Immunoassay determination of soy protein in foodstuffs
(ELISA)
AL
WES 060
2006
Immunoassay determination of Durum wheat in
foodstuffs (ELISA)
AL
WES 071
2005
Immunoassay determination of risk material
AL
WES 136
2005
Determination of peanut protein in foodstuffs by enzyme AL
immunoassay (ELISA)
WES 550
2010
Enzyme-linked immunosorbent assay for quantitative
determination of vitamin B12
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL
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11.14 Microscopic examination of foodsuffs and feeding stuffs*
ASU L 06.00-13
1989-12
Histological examination of meat
AL
Microscopic examination of Microscopic detection of alginate
vegetable food stuff and
feeding stuff, G. Gassner, B.
Hohmann, Behr's Verlag,
2007, Chapter 11
AL
RL 2003/126/EG
2003-12
AL
Microscopic examination of feeding stuffs
11.15 Tests of commodity goods
DIN EN ISO 17070
2007-01
Leather - Chemical tests - Determination of
pentachlorophenol content
DIN EN ISO 17075
2008-02
Leather - Chemical tests - Determination of chromium (VI) AL
content
DIN EN 71-3
2002-11
Safety of toys - Part 3: Migration of certain elements
DIN EN 1811
2008-09
Reference test method for release of nickel from all post HA
assemblies which are inserted into pierced parts of the
human body and articles intended to come into direct and
prolonged contact with the skin
(ASU B 82.02-06, 2009-11)
DIN EN 14362-2
2003-12
Textiles - Methods for determination of certain aromatic
amines derived from azo colorants - Part 2: Detection of
the use of certain azo colorants accessible by extracting
the fibres (ASU B 82.02-4, 2004-06)
(Variation Confirmatory test by GC-MS)
AL
DIN 53160-1
2010-10
Determination of the colourfastness of articles for
common use - Part 1: Test with artificial saliva
(ASU B 82.92. 2011-12)
AL
DIN 53160-2
2010-10
Determination of the colourfastness of articles for
common use - Part 2: Test with artificial sweat
(ASU B 82.02-13. 2011-12)
AL
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL
AL, HA
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Annex to the Accreditation Certificate D-PL-14162-01-00
ASU B 80.03-2 (EG)
2007-03
Analysis method for the determination of lead and
cadmium release
AL, HA
ASU B 80.30-1 ff (EG)
1998-01
Overall migration
AL
ASU K 84.00-7 (EG)
1991-09
Detection and quantitative determination of the free
form-aldehyde
AL
BGVV - 24. BfR
Recommendation to
materials with food contact
IX
2010-01
Testing of coloured commodity goods made of plastics
and other polymers for colourfastness
AL
11.16 Molecular-biological tests - detection of specific DNA segments using PCR in foodstuffs and
animal feeding stuffs **
DIN EN ISO 21569
2005-09
Methods of analysis for the detection of genetically
modified organisms and derived products - Qualitative
nucleic acid based methods
DIN EN ISO 22174
2005-05
Microbiology of food and animal feeding stuffs AL
Polymerase chain reaction (PCR) for the detection of foodborne pathogens - General requirements and definitions
(ASU L 00.00-45, 2006-12)
DIN 10135
1999-11
Method for detection of salmonella with polymerase
chain reaction (PCR) (ASU L 00.00-52, 2000-07)
DIN 58967-60
2001-10
Diagnostics of infectious diseases and diseases of the
AL
immune system in serology and molecular biology - Part
60: Polymerase chain reaction (PCR); Terminology, general
method-specific requirements
ASU L 00.00.31
2001-07
Correction
2002-12
Screening method for the detection of genetically
AL
modified DNA sequences in foodstuffs by the detection of
DNA sequences which are often to be found in genetically
modified organisms
ASU L 02.02-4
1997-09
Detection of a genetic modification of Streptococcus
thermophilus in yoghurt by amplification of the modified
DNA sequence by PCR (Polymerase chain reaction) and
hybridisation of the PCR product with a DNA sample
Period of validity: 01.10.2012 to 13.09.2016
Translation
AL
AL
AL
134/141
Annex to the Accreditation Certificate D-PL-14162-01-00
ASU L 08.00-44
1997-01
Correction 2002-12
Detection of a genetic modification of Lactobacillus
curvatus in raw sausage by amplification of the modified
DNA sequence by PCR (Polymerase chain reaction)
AL
ASU L 11.00-7
2002-12
Correction 2003-12
Identification of the fish species in raw and heated
products
AL
ASU L 15.05-1
2002-05
Detection of genetic modifications in maize (Zea mays L.)
by PCR (Polymerase chain reaction) and restriction
analysis or hybridisation of the PCR product
AL
ASU L 23.01.22-1
1998-03
Detection of genetic modification of soy beans by
AL
amplification of the modified DNA sequence by PCR
(Polymerase chain reaction) and hybridisation of the PCRproduct with a DNA sample
ASU L 24.01-1
1997-01
Correction 2002-12
Detection of genetic modification of potatoes by
AL
amplification of the modified DNA sequence by PCR
(Polymerase chain reaction)and hybridisation of the PCRproduct with a DNA sample
ASU L 25.03.01-1
1999-11
Detection of genetic modification of potatoes by
AL
amplification of the modified DNA sequence by PCR
(Polymerase chain reaction)and hybridisation of the PCRproduct with a DNA sample or restriction analysis of the
PRC product
Schweiz. Lebensmittelbuch, Methods in molecular biology
Kapitel 52 b
2009
AL
WES 073
2009
Detection of Salmonella using polymerase chain reaction
(Realtime-PCR)
AL
WES 074
2007
Determination of verotoxin-forming Escherichia coli in
foodstuffs (online-PCR)
AL
WES 135
2003
Detection of Serpula lacrymans (echter dry rot) by PCR
AL
WES 442
2009
Gender determination of meat by PCR
AL
WES 479
2009
Detection of Listeria monocytogenes in foodstuffs using
polymerase chain reaction (Realtime-PCR)
AL
Period of validity: 01.10.2012 to 13.09.2016
Translation
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Annex to the Accreditation Certificate D-PL-14162-01-00
11.17 Molecular biological analysis fort he detection of pathogens and non- pathogenic
microorganisms using PCR (thermal cycler with integrated detection) in foodstuffs, feeding
stuffs and cosmetics**
WES 073
2009
Salmonella spp.
WA
WES 479
2009
Listeria monocytogenes
WA
WES 493
2009
Cronobacter spp.
WA
11.18 Microbiological analysis in accordance with international pharmacopoeias in the
respectively valid version of proprietary medicinal products, raw materials, excipients and
active substances, food supplements, foodstuffs and feeding stuffs*
Ph. Eur. 2.6.1
Testing for sterility
MS
Ph. Eur. 2.6.12
Microbiological testing of non-sterile products Enumeration of all propagatable aerobic germs
MS
Ph. Eur. 2.6.13
Microbiological testing of non-sterile products Detection of specified microorganisms
MS
Ph. Eur. 2.6.14
Testing for bacteria - endotoxins (Turbidity and gel-clot)
MS
Ph. Eur. 2.6.31
Microbiological testing of herbal medicinal products for
internal use
MS
Ph. Eur. 2.7.2
Microbiological evaluation of antibiotics
MS
Ph. Eur. 5.1.2
Assessment of bioindicators for the sterilisation
MS
Ph. Eur. 5.1.3
Testing for sufficient conservation
MS
Ph. Eur. 5.1.4
Microbiological quality of non-sterile pharmaceutical
preparations and substances for pharmaceutical use
MS
Ph. Eur. 5.1.8
Microbiological quality of herbal medicinal products for
internal use
MS
Period of validity: 01.10.2012 to 13.09.2016
Translation
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Annex to the Accreditation Certificate D-PL-14162-01-00
11.19 Chemical-physical analysis in accordance with international pharmacopoeias in the
respectively valid version of proprietary medicinal products, raw materials, excipients and
active substances, food supplements, foodstuffs and feeding stuffs*
Ph. Eur. 2.2.3
pH value - potentiometric method
MS
Ph. Eur. 2.2.5
Relative density
MS
Ph. Eur. 2.2.6
Refractive index
MS
Ph. Eur. 2.2.7
Optical rotation
MS
Ph. Eur. 2.2.10
Rotationsviskosimetrie (Brookfield) (Viscosity -Rotating
Viscosimeter Method)
MS
Ph. Eur. 2.2.20
Potentiometry
MS
Ph. Eur. 2.2.24
Infrared spectroscopy
MS
Ph. Eur. 2.2.25
UV-visible spektroskopy
MS
Ph. Eur. 2.2.27
Thin layer chromatography
MS
Ph. Eur. 2.2.29
Liquid chromatography
MS
Ph. Eur. 2.2.32
Drying loss
MS
Ph. Eur. 2.2.38
Conductivity
MS
Ph. Eur. 2.2.44
Total organic carbon (TOC) in water for pharmaceutical
use
MS
Ph. Eur. 2.2.60
Melting point - instrumental method
MS
Ph. Eur. 2.3.1
Identification reactions of ions and functional groups
MS
Ph. Eur. 2.4.8
Heavy metals
MS
Ph. Eur. 2.4.14
Sulphated ash
MS
Ph. Eur. 2.4.16
Total ash
MS
Ph. Eur. 2.5.1
Acid value
MS
Ph. Eur. 2.5.2
Ester value
MS
Ph. Eur. 2.5.3
Hydroxyl value
MS
Period of validity: 01.10.2012 to 13.09.2016
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Annex to the Accreditation Certificate D-PL-14162-01-00
Ph. Eur. 2.5.4
Iodine value
MS
Ph. Eur. 2.5.5
Peroxide value
MS
Ph. Eur. 2.5.6
saponification value
MS
Ph. Eur. 2.5.7
unsaponifiable dues
MS
Ph. Eur. 2.5.12
Water - Semi- micro determination
(Karl-Fischer method)
MS
Ph. Eur. 2.8.1
Acid insoluble substances
MS
Ph. Eur. 2.9.19
Partikel kontamination - subvisible partikles
MS
Period of validity: 01.10.2012 to 13.09.2016
Translation
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Annex to the Accreditation Certificate D-PL-14162-01-00
The methods listed in section 7 comply with the requirements for the „Fachkundenachweis für
Ermittlungen im Bereich des Immissionsschutzes“ (“Special knowledge proofs for investigations
in the field of immission control”) („Modul Immissionsschutz“ - Module Immission Control) as
amended on 16.10.2003.
The competence is confirmed for the technical task areas
A, C, D, F, I, L, M1 (M3), M2, N2, groups I, II, III and IV.
The methods listed in section 7 comply with the „Grundsätzliche Anforderungen an akkreditierte
Messstellen zum Vollzug des Gefahrstoffrechts“ (“General requirements for accredited gauging
stations for the implementation of the law on hazardous substances”) (LASI publication LV 2.2,
updated in September 2005).
Together with the checking of the submitted reports available in a suficient number for the individual
groups, the competence is attested for the detection and assessment of concentrations of hazardous
airborne substances according to the Hazardous Substances Ordinance § 9, section 6 and annex III No
2:
Site Bochum
Group 1
Group 2
Group 3
Group 4
Group 5 (Cooling lubricants, mineral oils, isocyanides)
Site Berlin
Group 1
Group 3
Group 4
Group 5 (Cooling lubricants, isocyanides)
Site Rhein-Main (Weiterstadt)Group 1
Group 4
Group 5 ( phithalic acid ester)
Period of validity: 01.10.2012 to 13.09.2016
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Annex to the Accreditation Certificate D-PL-14162-01-00
1) Technical responsibility:
Herr Dipl.-Ing. Stephan Kottmann, Bochum
Areas:
(Area A, D, I, M1)
2) Technical responsibility:
Herr Dipl.-Ing. Michael Naumann, Berlin
Areas:
(Areas A, C, D, F, I, L, Group IV)
3) Technical responsibility:
Herr Dipl.-Ing. Matthias Post, Altenberge
Areas:
(Area M2, N2)
Deputy of 1):
Herr Dipl.-Chem. Christian Kauke, Bochum
Herr Dipl.-Ing. Gunnar Fette, Bochum
Herr Dr. Bayer-Beck, Weiterstadt
Herr Christian Knorr, Berlin
Frau Dipl.-Chem. Monika Schmidt, Berlin
Areas:
(Areas A, D, I, M1)
(Areas A, D, I, M1)
(Areas A, D, I, M1)
(Areas A, D, I, M1)
(Areas A, D, I)
Deputy of 2):
Herr Dipl.-Chem. Christian Kauke, Bochum
Herr Dipl.-Ing. Gunnar Fette, Bochum
Herr Dr. Bayer-Beck, Weiterstadt
Herr Christian Knorr, Berlin
Frau Dipl.-Chem. Monika Schmidt, Berlin
Herr Dipl.-Ing. Gunnar Fette, Bochum
Herr Stephan Kottmann, Bochum
Areas:
(Areas A, D, I)
(Areas A, D, I)
(Areas A, D, I)
(Areas A, D, I)
(Areas A, D, I)
(Areas A, C, D, F, I, L)
(Areas Group IV)
Deputy of 3):
Herr Dipl.-Ing. Michael Eißing. Altenberge
Herr Dipl.-Ing. Roland Jordan, Altenberge
Herr Dipl.-Ing. Carsten Lammers, Altenberge
Areas:
(Areas M2, N2)
(Areas M2, N2)
(Areas M2, N2)
Used abbreviations:
AbfAblV
AbfKlärV
AQS-bulletin
ASU
Period of validity: 01.10.2012 to 13.09.2016
Abfall-Ablagerungsverordnung
Klärschlammverordnung
AQS-Merkblätter der Länderarbeitsgemeinschaft
Wasser für die Wasser-, Abwasser- und
Schlammuntersuchungen
Amtlichen Sammlung von Untersuchungsverfahren
nach §64 LFGB
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Annex to the Accreditation Certificate D-PL-14162-01-00
BGI 505
BGIA
DFG
DIN
DVWK
EN
EPA
Fat Sci Technol
GAFTA
ISO
J. appl. Bact.
LAGA
LFGB
LÖLF
LUA
LWA
Book of methods BGK e. V.
NIOSH
OFD H
Ph. Eur.
TrinkwV
VDI
VDLUFA
WES
ZH
Period of validity: 01.10.2012 to 13.09.2016
Von den Berufsgenossenschaften anerkannte
Analysenverfahren zur Feststellung der
Konzentrationen krebserzeugender Arbeits-stoffe in
der Luft in Arbeitsbereichen
Berufsgenossenschaftliches Institut für
Arbeitssicherheit
Deutsche Forschungsgemeinschaft
Deutsches Institut für Normung
Deutscher Verband für Wasserwirtschaft und
Kulturbau
Europäische Norm
Environmental Protection Agency, USA
Fat Science Technology
The Grain and Feed Trade Association
International Organization for Standardization
Journal of applied Bacteriology
Länderarbeitsgemeinschaft Abfall
Lebensmittel-, Bedarfsgegenstände- und
Futtermittelgesetzbuch
Landesanstalt für Ökologie, Landschaftsentwicklung
und Forstplanung Nordrhein-Westfalen (nach
Umstrukturierung LUA)
Landesumweltamt Nordrhein-Westfalen
Landesamt für Wasser und Abfall NordrheinWestfalen (nach Umstrukturierung LUA)
Methodenbuch (Bundesgütegemeinschaft
Kompost) zur Analyse organischer Düngemittel,
Bodenverbesserungsmittel und Substrate
National Institute of Occupational Safety and Health
Oberfinanzdirektion Hannover
Europäisches Arzneibuch
Trinkwasserverordnung
Verein Deutscher Ingenieure e. V.
Verband Deutscher Landwirtschaftlicher
Untersuchungs- und Forschungsanstalten
Inhouse-methode of WESSLING GmbH
Zentralstelle für Unfallverhütung und
Arbeitsmedizin
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