Indiana University Northwest Chemistry/Physics Lab Report Style Guide How to Write a Formal Lab Report Foreword: What’s the Deal with Technical Writing? A lot of the experience you’ve had with papers has probably been in the form of English assignments rather than Chemistry assignments. Writing is incredibly important across both the arts and the sciences, but there are key differences in the goals of that writing. These are accomplished with varying levels of technical writing and creative writing. Technical writing is performed with the goal that everyone reading the passage has the same ideas being put into their head. Instructions on how to construct a new bookshelf are almost exclusively technical writing, so that everyone can have a sturdy and stable product at the end. Creative writing is meant to be inspirational, where new and different ideas come about due to unique interpretations. A moving speech uses elements of creative writing to arouse emotion and connect with different people in different ways. The purpose of laboratory reports in the sciences is to train you how to share scientific data and findings with your peers. Because of the importance of reproducibility, this goal is primarily served with technical writing. You want your colleagues to be able to perform your experiment and confirm your results without any deviation. Technical writing works to ensure that the same ideas will be communicated to the person reading your report, and that they can repeat the experiment in exactly the same way you did. Technical writing is a skill that is commonly not well developed in High School environments. One facet of this document is to help you build technical writing skills and apply them to your Chemistry lab reports. It will also detail the various sections of lab reports to help you understand their importance in science communication. By understanding the purpose of these various sections, you will be able to figure out what your lab instructor expects and thus achieve better grades on your reports. Technical Writing Basics In this section, some important rules and guidelines for technical writing that you may not be familiar with are outlined. These rules and guidelines should be followed for all of your Chemistry lab reports. Intended Audience Because technical writing is about communicating the same idea across multiple people, it is important to think about whom the people you are actually trying to communicate with. Instructions you would give a toddler are often simpler than instructions you’d give to a high school student, for example. In the case of lab reports, you can think of your audience as being your current classmates. You should use important vocabulary terms from your textbook or lab manual, and describe the material at the same kind of level of understanding. Write it in terms they should understand, having read the same material that you have. “Everything Should be Made as Simple as Possible, but not Simpler.” The above is a quote from Albert Einstein, and it describes a very important part of technical writing. Communicating an idea in a way everyone can understand requires detail, but it becomes harder to understand with unnecessary language and pompous-sounding words. Consider the following three statements: 1) “Water was added to the flask.” 2) “Thirty mL of water was added to the flask containing the reaction mixture.” 3) “Thirty mL of dihydrogen monoxide was carefully discharged into the 350 mL reaction vessel that incorporated the three reagents in the midst of a solvent.” All three statements are conveying the same idea with varying levels of success. Statement one is vague and has too few details to ensure that anyone repeating the experiment would perform the same procedure. Statement two provides needed information (30 mL) and some potentially helpful clarification (flask containing the reaction mixture). Statement three provides unnecessary levels of detail and uses forms of words that work more to confuse than to clarify. A thesaurus is not a particularly helpful tool in technical writing. Your report should strive to be like statement two; it needs to have the necessary information written in the simplest possible way. Remember that the object is to communicate, not to win a contest for the ‘smartest-sounding’ person in the lab or largest page count. It often has the opposite effect, making it look like you are covering up a lack of knowledge of the material. Past Tense Your lab report is written about an experiment you previously performed, therefore your report should be written in past tense. 3rd Person and Passive Voice Because a key component of science is reproducible data, these data are shared without any personal or unique connections. The report should not include any first-person perspective (I, We, etc.). The idea is that these results would be the same regardless of who performed the experiment. Mentioning yourself implies a level of personal connection to the results, which would further imply that only you can obtain them and that other people could not reproduce them. Similarly, the passive voice is predominant in technical writing because it places emphasis on what is occurring rather than whom or what is performing an action. Depending on your English background, you may not have a clear idea what defines an active or passive voice. Consider the following examples. (Active): The instructor added the unknown to the reaction mixture. (Passive): The unknown was added to the reaction mixture by the instructor. In most non-scientific writing, the passive voice is avoided because the person acting is usually of the most importance in the sentence. In lab reports, it is the object you are acting upon, and how you are acting upon it, that is of the most importance. Using a passive voice is preferred in this setting because it separates the experiment and data from yourself, implying that the results will occur whoever performs the experiment. Your word-processing program may indicate a grammar issue with passive sentences, but rest assured, that is the correct phrasing for scientific writing. Formatting Recommendations Your instructors have the final say in the formatting they want to see in your lab reports, which can usually be found in the syllabus or is announced in class. In the absence of specific directions, the following is a helpful list of guidelines that will make your report easier to read. o 12-point sans-serif style font – Crazy fonts and sizes are distracting and harder to read. o Double-space – Provides more room for grading comments from your instructor. o Justify – Makes your lines equal in length. o Page Numbers in Lower Right Corner – Allows easier referencing. Parts of the Lab Report The following are the necessary pieces to a successful chemistry lab report. More detail is provided in the individual sections below. While the order and specific composition may change, these general areas are important parts of nearly any scientific reporting of data. Abstract – Brief Overview of Everything Introduction – Details Necessary Background Experimental – Laboratory Instructions Figures** – Pictures or Non-Paragraph Additions to Other Sections Results and Discussion – Lists and Explains the Outcomes Conclusion – Final Summation References – Giving Proper Credit for Ideas Abstract The Abstract is a short paragraph that provides a brief overview of everything contained within the lab report. Its purpose is to let a scientist know whether an article is of interest to them and their work, without committing them to reading the entire multi-page document. An Abstract typically covers what the experiment was about, why it is scientifically important, how it was performed, and what the final results were. In a way, an abstract is set up like a 30-second local TV news story. Imagine you received an award from the President, and you were watching the event covered on the local news. They would introduce the story by telling what happened (a local student received an award), and they would briefly say why you were receiving the reward. They then might go into how you won the award, or how the President was the one who gave you the award at a special ceremony. Finally, they could tie the story up by announcing what sum of money you won with the award. In your abstract, you want to talk about all the important points of your experiment. A common question is “how do I know what is important?” This is a question that will depend upon the specific lab, and will really showcase what you understand about the experiment. In the local news example, the name or type of award you were given would definitely be considered important, and likely mentioned by the newscaster. Where you received the award may or may not be important enough to mention (e.g. The White House versus your old high school auditorium). The fact that Dorothy Brown of 1923 High Street was in the audience at you award ceremony is unlikely to be important. In the end, you will have to decide what is and isn’t important enough to be included in your abstract. There may even be topics important in one experiment but not another. Making these determinations can be difficult at first, but with proper scientific understanding, and some feedback from your instructor, you should start getting the hang of it. Introduction The introduction is a section that takes all the important background information and presents it in a manner that logically leads to the purpose of your experiment. It should present enough information for any of your classmates to read it and understand the experiment and any results you present. The entirety of the Introduction can be described as triangular in content, starting with big ideas that are gradually focused into the experiment that was performed. Broad Theories, Ideas, and Concepts How Theories Interact in Real Settings Purpose and Importance of Specific Experiment Following the triangle above helps ensure your introduction stays coherent. The introduction often takes several paragraphs, but must be logically constructed. There should be clean transitions between paragraphs where possible; this means that somebody reading the last line of a paragraph and the first line of the following paragraph could tell you how they tie together. Additionally, avoid the phrase “in this lab” wherever possible. A good way of thinking about this section is to imagine a friend who has been sick for a week; they have to make up the lab material despite missing the relevant lecture, and are relying on your introduction to understand what is going on in the experiment. You start with the main ideas, talk about how the practical consequences of those ideas, and finally go into how the specific experiment will demonstrate those ideas and/or what you accomplish by doing the experiment. Experimental The experimental section of a lab report is where the specific procedure followed during the experiment is recorded. This is done in narrative paragraph form rather than as a list of instructions, and should be 3rd person, past tense, and in the passive voice. You should write what procedure you followed, especially including any alterations you may have made from the procedure written in the lab manual. In particular, this should not be a copy of what is written in the lab manual. Sometimes there are additional parts to an experimental section, such as tables of reagents or specific subsections concerning the materials used. Be sure to check with your instructor if there are additional parts required. Figures Figures are non-sentence additions to a lab report that either assist understanding or present data in a new fashion. Graphs, charts, tables, equations, and images all fall into this category. There is not a specific section for figures in a lab report, they are just included in the section in which they are most relevant. As an example, the Lewis Structure of a molecule may be included in the introduction to help emphasize connection to a physical property that was studied in the experiment. The following are some helpful descriptions, links, or guidelines to the best presentation for different kinds of figures. - Excel Graphs o Graphing is one of the most important ways that scientists look at large amounts of data. A tutorial on making graphs can be found at the following link. We will primarily use Scatter Plots (marker only) and Trendlines in Chemistry labs. o http://www.excel-easy.com/examples/scatter-chart.html o http://www.excel-easy.com/examples/trendline.html - Math and Chemistry Equations o We will commonly reference math and chemistry equations that don’t fit well in-line with our normal text. In Microsoft Word, we can use the equation editor to better represent these math and chemistry equations. The equations can be numbered and referred to within the text (equation 1, eq. 2, etc.). o http://www.wikihow.com/Insert-Equations-in-Microsoft-Word - Tables o Sometimes a table of data is more useful than a graph. In those cases, we can use word to directly insert the table into the text. Double-check with your instructor on what kind of rules/formatting they would like you to use. o https://support.office.com/en-us/article/Insert-or-create-a-tablede20e78c-ede3-4043-a9fb-27f0b73fb447 - Images o Sometimes a picture helps explain complicated ideas better than words can. Images can be added into your document near a description that references the image, with a short caption that explains the image by itself. If you did not personally create the image, it must be a public domain image and you must make sure you properly cite the source in a caption. (see Reference section). o http://www.wikihow.com/Add-an-Image-in-Word - ChemDraw o For Organic Chemistry, structural drawings, arrow-pushing diagrams, and reaction schemes are essential to explaining the experimental transformations. ChemDraw is the main program used to create these figures. o Use the ACS 1996 Document Settings to ensure the correct standard of bond length and angle in your figures. o The instructions for using ChemDraw are too detailed for this Style Guide. Check with your Organic Chemistry lab instructor for further tutorials and specific requirements. Results and Discussion Although commonly found grouped together, the Results and Discussion are actually two different aspects of the lab report. The results are the raw data and calculated values that are obtained from the experiment, while the discussion is any further theoretical analysis of the results. The results can be numbers, values, or observations, whereas the discussion tries to explain how or why the specific results were achieved. The final solution temperature is a result, the explanation of why the temperature of the solution increased is an element of the discussion. An important feature to writing the discussion section of a report is a thorough and scientific analysis of the results. This can be difficult for students, as it requires taking a step back and looking at the larger scientific picture. Consider the following examples as discussions of a specific result, leaves changing color in the fall: 1) As summer ends and autumn begins, the leaves change from green to yellow and photosynthesis decreases. 2) Plants produce pigments responsible for the color found in leaves. Chlorophyll provides the green pigment during summer months and is responsible for photosynthesis. As summer ends and autumn begins, the days get shorter and the trees respond to the diminishing sunlight by decreasing chlorophyll production. When this occurs, carotenoid, a yellow pigment becomes visible and the trees begin to use stored glucose for energy produced over the summer months. In the first example, there is little actual connection of the result to science, and a very superficial explanation is presented. In the second example, the result is thoroughly connected to the processes that are occurring, providing a good explanation for the color change. Although it is longer than the first example, every part of the second example plays an important role in describing what happens to cause the color change. For IUN General Chemistry Lab courses, the lab manual worksheet pages of the associated experiment cover the Results and some of the Discussion section of your lab report. A short discussion of the results beyond the worksheets is required. In particular, you should look to analyze your results in relation to the grand purpose of the experiment. For IUN Organic Chemistry Lab courses, both of these sections are the responsibility of the students themselves. See your instructor for further preparation for these sections. Conclusion In some ways the conclusion is like an expanded abstract, summarizing the experiment over a few paragraphs rather than a few sentences. The conclusion can be described with a useful acronym, RERUN. - R.E.R.U.N. o Restate o Explain o Results o Uncertainties o New Ideas The conclusion section should restate and purpose of the experiment, while also explaining how the experiment relates to important theories. The final results and their statistical deviations should also be reported and briefly commented upon. The conclusion is also where any errors or uncertainties can be discussed. Any errors need to be clearly linked to the results through logical explanation. Listing “human error” or “some sample was spilled” is insufficient explanation; you must establish a specific chain of cause and effect between the error and your result. Finally, you should show how the results or ideas studied in the experiment relate to other important areas of science or life. Demonstrate how the concepts in the experiment can be applied to other problems. For example, the measurement of density can be used to predict the outcomes of chemical spills for insoluble compounds such as oil in bodies of water. While you might not yet be at a level to radically change the world, show that you can use the ideas of the experiment outside of the experiment itself. References In all scientific work, we are building on top of the ideas of others that have come before us. Proper citation of someone’s work is important to give credit where it is due but also to allow readers to further inform themselves individually. Your lab reports are expected to be primarily original works, created by your knowledge and your experimental results. You cannot copy sections from anyone else’s report, even your lab partner. Any part that comes directly from another source must be identified as such. It is very common to seek other sources to help understand aspects of your lab experiments, but you must properly credit any of these outside sources in your report. To pass off the words (or even ideas) of others as your own is plagiarism, and has serious grade and disciplinary penalties. In lab reports, you can provide a citation by adding a numerical superscript to the idea, as seen at the end of this sentence.1 Then, after the conclusion section, reference selection includes a numbered list of your sources. References should be ordered according to appearance in your written report. For lab reports at IUN, we require the ACS format for the reference section. This will list, in a consistent form, all of the information required to look up the reference and see the origination. Some examples of ACS formatting are given below. Follow the examples, including italics and bolding. Lab Manual Form Author(s) Last-Name, First Initial, Lab Manual Title, Year of Publication, Experiment Title, Page numbers. Example Wozniewski, L., C126 Lab Manual, 2013, Titrations of Acids and Bases, 5763. Textbook Form Author(s) Last, First, Book Title, Publisher, City of Publication, State, Year, page numbers. Example Tro, N., Chemistry: Structure and Properties, Pearson, Upper Saddle River, NJ, 2015, 626-635. Scientific Journal Article Form Author(s) Last-Name, First Initial, Article Title, Journal Abbreviation, Year of Publication, Volume Number, Page numbers. Example Thuéry, P., Harrowfield, J., A New Form of Triple-Stranded Helicate Found in Uranyl Complexes of Aliphatic α,ω-Dicarboxylates. Inorg. Chem., 2015, 54, 10539-10541. Internet sources, while convenient, are generally looked down upon in scientific works, due to the anonymity and lack of reliability involved. You should double-check with your instructor if they will allow any internet-based sources for citations. If allowed, you will likely be limited to sources from .edu websites. Final Note: A Guide, not a Grading Rubric This guide was put together to help students understand how to write lab reports for chemistry labs at IUN, especially students who have not had this kind of experience in other classes. While all of the lab instructors have participated in the writing of this guide, the specific grading criteria are in the hands of the instructors themselves, not this document. Be sure you listen to your instructors and read any further criteria they share as it pertains to writing your lab reports.