Indian Journal of Science and Technology, Vol 8(36), DOI: 10.17485/ijst/2015/v8i36/88513, December 2015 ISSN (Print) : 0974-6846 ISSN (Online) : 0974-5645 Magnetic Pulse Welding of Two Dissimilar Materials with Various Combinations Adopted in Nuclear Applications S. Kudiyarasan1* and S. Arungalai Vendan2 AMET University and Technical Group, Bharatiya Nabhikiya Vidyut Nigam Limited (BHAVINI), Kalpakkam, Kancheepuram District - 603102, Tamil Nadu, India; kudiyarasan@rediffmail.com 2 Industrial Automation and Instrumentation Division, School of Electrical Engineering, VIT University, Vellore - 632014, Tamil Nadu, India 1 Abstract In this paper the joining of two dissimilar metals as Al-SS, Al-Cu and SS-Cu were studied. Commonly, MPW is considered as a non-melting process. Magnetic Pulse machine which is belong to Non-conventional technique instead of conventional technique. Magnetic Pulse Welding (MPW) is a joining process in which lap joint surfaces of cylindrical shape metals, such as pipes and tubes, are welded by impact, using electromagnetic forces. MPW is classified in the group of solid-state bonding processes together with Explosive Welding (EXW). The technique has become an unique and acknowledged welding process because it enables to join similar, as well as dissimilar metals, which is very difficult to weld by traditional methods such as GTAW or EBW due differences in melting points etc. MPW process is very fast, produces no Heat Affected Zone (HAZ) and may be performed without filler metals and protective gases. Nevertheless, it was detected a very thin film (10 to 50 µm) of two welded metals in the form of intermetallic phases, in which melting and solidification processes took place. These inter-metallic phases significantly affect the mechanical properties of the joint. The diffusion of elements in the intermetallic phase was studied for the pattern and the composition of the blended metals and formation of pores etc. The interface typically presents a wavy pattern and mutual diffusion of elements happens in the transition zone. The transition zone is composed of elements intermetallics, micro cracks and micro pores as expected in our study. The effect of the parameters on the morphology, configuration and structure of the interface has been thoroughly studied. The weld interface composition, structure and morphology were studied by optical and Scanning Electron Microscopy (SEM). Energy-Dispersive Spectrometry (EDS) was used in order to evaluate the local distribution of alloying elements at the joint interface and its vicinity and also nano-hardness tests were performed across the bonding zone at regular increments. The results of the joints were analysed for process parameters and based on the result , the process parameters has to be reviewed accordingly to yield best interface weld results. Keywords: Dissimilar Metals, Interfaces, Inter-Metallic Phases Transfer, Magnetic Pulse Welding, Welding 1. Introduction The Prototype Fast Breeder Reactor (PFBR) is a 500MWe sodium–cooled fast breeder nuclear reactor presently being constructed by Bharatiya Nabhikiya Vidyut Nigam Limited (BHAVINI) in Kalpakkam, India. The Indira Gandhi Centre for Atomic Research (IGCAR) is responsible for the design of this reactor. The cooling system of *Author for correspondence the reactor uses liquid sodium and requires additional safety measures to isolate the coolant from environment. The steam generator made of modified 91 steel, is connected to the intermediate heat exchanger, made of AISI 316LN stainless steel with the dissimilar metal weld. The schematic of the rector system is shown in Figure 1(a) and the steam generator with the dissimilar metal weld in Figure 1(b) currently the dissimilar metal Magnetic Pulse Welding of Two Dissimilar Materials with Various Combinations Adopted in Nuclear Applications power plants, an extensive failure analysis was carried out at IGCAR on dissimilar metal welds between 2.25Cr-Mo ferritic steel and AISI type 316 stainless steel with and without Inconel-82 buttering using non–destruction X-Ray Diffraction (XRD) technique and to assess the effectiveness of the buttering on the extent of reduction in the residual stress. To avoid the complex design, it is proposed the two dissimilar materials by Magnetic Pulse Welding. The Magnetic Pulse Welding (MPW) is solid-state joining (a) (a) process employed for both similar and dissimilar con(a) ductive metal combinations viz., aluminum, brass, and copper to steel, titanium, stainless, aluminum, magnesium copper etc. MPW system’s architecture consists of a dedicated AC power supply, bank of capacitors, a highspeed switching system and a coil (Figure 1(c)). The parts to be joined are inserted into the coil. The capacitor bank is charged and the high-speed switch is activated. A strong magnetic flux is created around the coil as per the principle of electromagnetic flux generated in a winding excited with an AC power supply. When the current is applied and as a result eddy currents are formed in the (b) parts. The eddy currents oppose the magnetic field in the (b) coil as per(c)Lenz Law of Electromagnetics and an opposFigure 1. (a) Schematic (b) of the rector system. (b) The steam generator with dissimilar Pulse Welding (c) metal weld. (c) Magnetic 1 ing force generated . This Power Supply Set Upof with bank.(b) The steam generator with dissimilar Figure 1. (a) Schematic the capacitor rector system. metalisweld. (c) Magnetic Pulse force Weldingdrives the materials Power Supply Set Up with capacitor bank. together at a tremendous high rate of speed and creates The schematic of the rector system is shown in Figure 1(a) and the steam generator with the dissimilar metal weld in Figure 1(b) weld (Figure Tungsten 2). theofdissimilar weld is a tri-metallic transition joint andgenerator uses a multi–pass Inert Gas welding Thecurrently schematic the rectormetal system is shown in Figure 1(a) and the steam with the dissimilar metal weld(TIG) in Figure 1(b) the When a filler highmaterial magnetic field BNi isandsuddenly genercomplex of the jointweld was is necessary to minimize thermal stresses. is an with 16% Cr 8% currently thedesign dissimilar metal a tri-metallic transition joint and uses ER16-8-2 a multi–pass Tungsten Inert Gas (TIG) welding the 2% Mo, usedoffor austenitic stainless steels, alloyER16-8-2 800 is anis Inconel withwith very good creep complex design the high joint temperature was necessary to minimize thermal stresses. an penetrated filler alloy material 16% Cr 8% Ni rupture andthe eddy currents ated and into metal, then 600temperature Inconel 182austenitic is an electrode in alloy dissimilar metal welds ofalloy stainless steel good joinedcreep to carbon 2%properties Mo, used above for high stainlessused steels, 800 is an Inconel with very rupturesteel (current passjoined through them experience with600 dissimilar weld has shown a considerable number ofstainless failures Ioccurred at a to very early stage in as a result, an properties above Inconelmetal 182 is an joints electrode used inthat dissimilar metal welds ofdensity steel carbon steeland service than powerhas plants, anthat extensive failure analysis carriedoccurred out at IGCAR onearly dissimilar metal experience with expected, dissimilarespecially metal weldinjoints shown a considerable number was of failures at aFvery stage inmainly on the base electromagnetic force of = I × B acts weldsthan between 2.25Cr-Mo ferritic steel plants, and AISI 316 stainless steel with without buttering using non– service expected, especially in power an type extensive failure analysis wasand carried out atInconel-82 IGCAR on dissimilar metal it is Inconel-82 accelerated away fromnon– thethecoil and collides destruction Diffraction technique and to assess the effectiveness ofand the buttering on the extent of reduction in welds betweenX-Ray 2.25Cr-Mo ferritic(XRD) steel and AISI type 316 stainless steelmetal with and without buttering using residual stress. destruction X-Ray Diffraction of the with buttering the extent of reduction in the current I and the (c)(XRD) technique and to assess the effectiveness rapidly theontarget metal. The eddy (c) residual stress. rector system. (b) The steam generator with dissimilar metal weld. (c) Magnetic Pulse Welding magnetic pressure p are given as following: avoid the complex it is proposed the two by Magnetic Pulse Welding. The Magnetic Pulse Figure 1. To (a) Schematic of design, the rector system. (b) Thedissimilar steam materials acitor bank. is solid-state process employed for both similar dissimilar conductive combinations To Welding avoid the(MPW) complex design, it isjoining proposed the two dissimilar materials byand Magnetic Pulse Welding.metal The Magnetic Pulseviz., the coil as per Lenz of Electromagnetics and an opposing force is generated1. T generator with(MPW) dissimilar metaljoining (c) Magnetic Pulse aluminum, brass, and copper to weld. steel,process titanium, stainless,for aluminum, magnesium copper etc. MPWLaw system’s architecture Welding is solid-state employed both similar and dissimilar conductive metalcombinations viz., ∂B consists tremendous high rate of speed and creates weld (Figure 2). tem is shown in Figure 1(a) and generator with dissimilar weld in aluminum, Figure 1(b)magnesium ofthea steam dedicated ACSet power supply, bank metal of capacitors, a high-speed switching system a coil (Figure parts to be ∆ × architecture i 1(c)). = −kThe aluminum, brass, and copper to steel, titanium, stainless, copper etc.and MPW system’s Welding Power Supply Upthe with capacitor bank. ∂consists flux is weld is a tri-metallic transition and a multi–pass Inert Gas bank (TIG) welding areuses inserted into supply, the Tungsten coil.bank The capacitor chargedthe and the high-speed activated. strong of joint ajoined dedicated AC power of capacitors, aishigh-speed switching systemswitch and a is coil (Figure A 1(c)). Themagnetic partst to be s necessary to minimize thermal stresses. ER16-8-2 is an filler material with Cr 8% Niand and created around the as perThe the principle of16% electromagnetic flux generated in a winding excitedAwith anmagnetic AC power supply. joined are inserted intocoil the coil. capacitor bank is charged the high-speed switch is activated. strong flux is rature austenitic stainless steels, alloy is transition anis Inconel alloy very good creep are rupture the800 current applied and aswith a and result eddy formed in the parts. The eddyexcited currents oppose thepower magnetic field in weld is a When tri-metallic joint uses acurrents multi–pass created around the coil as per the principle of electromagnetic flux generated in a winding with an AC supply. 182 is an electrode used in dissimilar metal welds ofand stainless steel joined to carbon steelin the parts. The eddy currents oppose the magnetic field in When the current is applied as a result eddy currents are formed Tungsten Inert Gasnumber (TIG) welding the al weld joints has shown that a considerable of failures occurred atcomplex a very earlydesign stage in ly in power plants, of an the extensive was carried out at IGCAR on dissimilar metal jointfailure was analysis necessary to minimize thermal stresses. ritic steel and AISI type 316 stainless steel with and without Inconel-82 buttering using non– ER16-8-2 is an filler material with 16% Cr 8% Ni and 2% (XRD) technique and to assess the effectiveness of the buttering on the extent of reduction in the Mo, used for high temperature austenitic stainless steels, 800 is an Inconel alloy with goodThe creep rupture it is proposed the alloy two dissimilar materials by Magnetic Pulsevery Welding. Magnetic Pulse joining process employed for both similar600 and Inconel dissimilar conductive combinations properties above 182 is anmetal electrode usedviz., in steel, titanium, stainless, aluminum, magnesium copper etc. MPW system’s architecture consists dissimilar metal welds of stainless steel joined to carbon ly, bank of capacitors, a high-speed switching system and a coil (Figure 1(c)). The parts to be . The capacitor banksteel is charged and the high-speed switch is activated. A strong experience with dissimilar metal weldmagnetic joints flux hasis the principle of electromagnetic flux generated in a winding excited with an AC power supply. shown that a considerable number of failures occurred at d as a result eddy currents are formed in the parts. The eddy currents oppose the magnetic field in a very early stage in service than expected, especially in Figure 2. Magnetic Pulse Welding (MPW) principle. Figure 2. Magnetic Pulse Welding (MPW) principle. 2 Vol 8 (36) | December 2015 | www.indjst.org When a high magnetic field B is suddenly generated and penetrated into metal, the Indian Journal of Science and Technology through them and as a result, an electromagnetic force of F = I × B acts mainly on th the coil and collides rapidly with the target metal. The eddy current I and the magneti S. Kudiyarasan and S. Arungalai Vendan p= (B d= 2 o − Bi2 2m ) = B (1 − e 2 o 2m −2 x / d )n 2 1 and k w = wk m LC Where K, µ, τ, Bo and Bi are the electrical conductivity, magnetic permeability, thickness, the magnetic flux density at lower and upper surfaces of Al, respectively. The depth of skin effect (δ) can be obtained by calculation of angular frequency (ω) and it is governed by the complete MPW system’s inductivity L and its capacity C. The skin depth becomes important parameter especially for thin metal bonding process. When the thickness of the base metal is the same as the skin depth, then magnetic pressure equals 85% of its maximum value and it reaches 97% when the base metal thickness is twice of the skin depth. The appropriate skin depth and higher magnetic pressure can be adjusted by the frequency of the discharge ­current2. At the moment of collision the colliding surfaces can be cleaned by a large kinetic energy getting before the collision. The velocities attained during this process range from 250 m/s to 500 m/s and the joining process completed within microsecond. Because of the short impact period, the extent of heating might be minimal along the joints3. Therefore, comparing to the traditional fusion welding process, no significant heat affected zones is produced in MPW joints and it can be noticed as a main advantage. The practical limitations of MPW relate to handling very high electrical currents. The major limitation of MPW equipment concerns the electrical connections between capacitors, switch, and coil. Very large metal components cannot be formed due to problems in design of very large coils4. It is very expensive equipment, just if able only by important mass production18. The experimental results and welding characteristics for several samples such as Al-Al and Al-Fe are reported in the available literatures already. However, Al-SS, Al-Cu and SS-Cu tubular combination which has greater demand in nuclear industries has been less reported with respect to MPW process. Moreover, the metallurgical characterization and non-destructive tests on MPW specimens in the available literatures are scanty. Hence, in this study, an attempt is being made to weld Al-SS, Al-Cu and SS-Cu tubular components using MPW process. Further, mechanical testing and metallurgical ­characterizations by destructive and non destructive methods are being ­carried out8. 2. Experimental Prior and Procedures The three specimens are employed in this study. However a typical one specimen consists of Cu (Driver) and Al (Flyer). The MPW equipment that is used in this study has a maximum charging energy of 10 kJ, Current of 12 kA and a Voltage of 10 kV. An outer Cu pipe was machined to be 2 mm thick, 80 mm long, and 40 mm in diameter. An inner SS pipe 9 mm thick, 90 mm long, and 36 mm in diameter was employed. For the pipe joint, the gap between the Cu and SS was 1mm. The specimens are ground using emery paper to remove marks sustained during machining. First, the voltage had to be charged according to the welding conditions. Then welding is carried out by electromagnetic force from discharged current through a working coil which develops a repulsive force between the induced currents flowing parallel and in the opposite direction in the tube14. Figure 3 shows few typical samples dimensional diagram, specimens after weld and cut cross section and inner weld view respectively. It may be observed that there is a reduction in diame8 Procedures 2. Experimental ter in the area of thePrior weldand . After welding, the work pieces are cross sectioned and prepared forstudy. examination by one specimen con The three specimens are employed in this However a typical MPW equipment that is used in this studysuch has a as maximum charging energy of 10 kJ, C standard metallographic procedures mechanical An outer Cu pipe was machined to be 2 mm thick, 80 mm long, and 40 mm in diamete polishing grit andForlight chemical long,down and 36 to mm1-micrometer in diameter was employed. the pipe joint, the gap between the C ground emerywere paper then to remove marks sustained during and machining. First, the vo etching. The using samples examined by optical welding conditions. Then welding is carried out by electromagnetic force from discharg scanning electron microscopy. develops a repulsive force between the induced currents flowing parallel and in the o shows few typical samples dimensional diagram, specimens after weld and cut cross sec Figure 3. MPW specimen dimensional diagram with cut cross section and inner weld vi Figure 3. MPW specimen dimensional diagram with cut It may be observed that there is a reduction in diameter in the area of the weld8. A cross section and inner weld view. sectioned and prepared for examination by standard metallographic procedures suc micrometer grit and light chemical etching. The samples were then examined by optical Vol 8 (36) | December 2015 | www.indjst.org Microanalysis by wavelength dispersive spectroscopy was utilized to evaluate the loca 3 Indian Journal of Science and Technology joint and its vicinity. 3. Results and Discussion Magnetic Pulse Welding of Two Dissimilar Materials with Various Combinations Adopted in Nuclear Applications (a) Microanalysis by wavelength dispersive spectroscopy was utilized to evaluate the local distribution of alloying elements at the joint and its vicinity. (a) 3. Results and Discussion The welded specimens are subjected to destructive and non destructive tests to evaluate its quality and strength. Metallurgical characterizations are performed to analyze the bond integrity and examined for presences of ­intermetallic phases5,6. 3.1 Tensile Test Specimen Description Al - SS Al - Cu SS - Cu Tensile Strength in kN 11.750 11.050 07.400* During the testing specimen got broken at weld joint * SS-Cu dissimilar metal configuration having failed in tensility, the improved configuration needs to be analyzed and tested; the base parameters tested with this configuration however has provided viable results, which would supplement further analyzing the same for testing again for tensility. The reports of the same are enumerated in the upcoming paragraphs. 3.2 Metallography Test For all the three welded samples, the optical microscopic examination was done and the results observed were as expected in all the aspects of perfections and integrity. First sample (Al-Cu), that was examined under optical microscope after etching and polishing then the bonding of two materials were verified with magnification ranging from 10X to 100X and observed that there is no imperfections and defects noticed and integrity of both the materials is intact6,7. 3.3 Radiography Test Radiography tests are performed for investigating the presence of pore/cluster of pores if any and also to ­examine 4 Vol 8 (36) | December 2015 | www.indjst.org (b) (b) Welded samples are tested on a standard tensile testing machine. In all cases, failure occurred in the region away from the weld area. The tensile results emphasizes that ductile failure of a welded Al-SS, Al-Cu and SS-Cu Rod/ Pipe occurs at a distant from the weld. There is no failure on the weld interface15. Sl. No. 1 2 3 (b) (a) (a) (b) (c) (c) (c) (d) (d) Figure 4. (a) Specimens after Tensile test. (b) Al-SS Tensile test graph. (c) Al-Cu Tensile test graph. (d) SS-Cu graph. Figure 4. (a) Specimens after Tensile test. (b) Al-SS Tensile dissimilar Tensile metal configuration failed in tensility, the improvedTensile configuration needs to be analyzed a test graph. (c)SS-Cu Al-Cu testhaving graph. (d) SS-Cu base parameters tested with this configuration however has provided viable results, which would supplement furt the same for testing again for tensility. The reports of the same are enumerated in the upcoming paragraphs. test graph. 3.2 Metallography Test (c) For all the three welded samples, the optical microscopic examination was done and the results observed were as e the aspects of perfections and integrity. First sample (Al-Cu), that was examined under optical microscope afte the effectiveness the fused dissimilar joints. X-rayranging mode polishingof then the bonding of two materials were verified with magnification from 10X to 100X and obser is no imperfections and defects noticed and integrity of both the materials is intact . with 150KV and 10mA source is used for this study. The 3.3 Radiography Test exposure time was about 100 seconds and ASME Sec V is Radiography tests are performed for investigating the presence of pore/cluster of pores if any and also to effectiveness of the fused(No dissimilar joints. X-ray modestandard with 150KV and 10mA sourcein is used for this study. The e the standardwas being used particular given about 100 seconds and ASME Sec V is the standard being used (No particular standard given in literatures). Fi the post radiographic examined samples. literatures). Figure 5 shows the post radiographic examined samples. The results of the radiography suggest that the quality is good and free from impurities/pores. Further, it illustrates good fusion in many samples. However, in few more Figure 5. Al/SS, Al/Cu and Cu/SS weldment specimen subjected to radiography. samples, the response appears to indicate lack of fusion. The results of the radiography suggest that the quality is good and free from impurities/pores. Further, it illustrate in many few more samples,radiography the response appears to indicate lack of It is important tosamples. noteHowever, the infact that, is not a fusion. It is important to that, radiography is not a suitable technique for solid state bonds as the thin line of interlayer’s formed at the weld identified generally by x-ray. suitable technique for solid state bonds as the thin line Micro-Structural Analysis of interlayer’s3.4 formed at the weldment are not ­identified Microstructures of cross sections of the different configurations of dissimilar welds are presented in Figure 6 (a), 6 generally by x-ray. 6,7 3.4 Micro-Structural Analysis Microstructures of cross sections of the different ­configurations of dissimilar welds are presented in Figure 6 (a), 6 (b) and 6 (c). There is a prominent difference in the quality of welding particularly for these configurations, and in general there is no bonding or minimal bonding in the corners and start-end zones, however the center of the welds showed a exemplary bonding or bond integrity. This may be regarded as the important feature or even the very unique feature of this type of welding. The inadequacy in bonding at the corners of the weld zone is a typical feature of MPW cylindrical parts and according to literature is not critical for many applications11,12. The minimally bonded Indian Journal of Science and Technology S. Kudiyarasan and S. Arungalai Vendan If the interface shows a wavy appearance, the i­ ntermetallics mainly concentrate in so called “melt pockets”, which are mostly located at the crests of the waves (Figure 6(a)). If EMP produces a wave less interface, the intermetallic phases form a film of byvarying thickness The wave pattern the side of the interface significantly depends on sample geometry and to parameters. Substantial utility of dissimilar specimen cylinders and relatively low pulse energ (Figure 6(b)). It is pointed out that the phase film appears Contrary, applying hollow dissimilar combines’ cylinders and high pulse energies pronounce (a) 5. the middle sectionany of the welds (Figure 6(c)). This geometrical influence is in accordance wi to be interrupted by regions without intermetallics. (a) Al/SS, Al/Cu and Cu/SS Weldment Specimen Subjected to Radiography. FigureFigure 5. Al/SS, Al/Cu and Cu/SS weldment specimen note that the wave formation process is not mandatory for a good bonding. It is furthermo There is a prominent difference in the quality of welding particularly for these configurations, and in general there is no bonding There is a prominent difference in the quality of welding particularly for these configurations, and in general there is no bonding or minimal bonding in the corners and start-end zones, however the center of the welds showed a exemplary bonding or bond For a thickness below 5 microns the intermetallics ­contain extent wave formation could also be observed in regions without bonding. Circumventing the subjected totheradiography. or minimal bonding in cornersintegrity. and start-end of the welds exemplary bonding or bond This zones, may behowever regardedthe as center the important featureshowed or evena the very unique feature of this type of welding. The inadequacy at the welding interface is impossible. The extent of interface depends on the process paramete integrity. This may be regarded as in thebonding important feature or even theweld veryzone unique this type of welding. The inadequacy at the corners of the is afeature typicaloffeature of MPW cylindrical parts and according to literature is not critical in bonding at the corners of the weld a typical feature. The of MPW cylindrical parts and according to specimen literature however is not critical any minimally bonded corners of the weld pose undesirabilityrarely and less adaptive in cracks, voids or pores. forzone manyisapplications structure of the interface. for many applications . The minimally bonded corners of the weld specimen however pose undesirability and less adaptive in 11,12 11,12 corrosive environments and in the case of recurrent cycled loads. corrosive environments and in the case of recurrent cycled loads. If the interface shows a wavy appearance, the intermetallics mainly concentrate in so called located at the crests of the waves (Figure 6(a)). If EMP produces a wave less interface, the i 3.5 Scanning Electron Microscopy (SEM) varying thickness (Figure 6(b)). It is pointed out that the phase film appears to be int intermetallics. For a thickness below 5 microns the intermetallics contain rarely any cracks, vo With Energy Dispersive Spectroscopy 3.5 Scanning Electron Microscopy (SEM) With Energy Dispersive Spectroscopy (EDS) (EDS) The SEM investigations present more information on bonding and phase formations. The SEM shown inmore Figure 7(a). Itinformation may be noted that the dearth ofon any diffusion layers leads to the postu The SEM investigations present involved in the phase formation and bonding process along the interface. bonding and phase formations. The SEM of the Al-Cu (a) (a) (b)(b) (b) There is a prominent difference in the quality of welding particularly for these configurations, and in general there is no bonding welded specimen is shown in Figure 7(a). It may be noted or minimal bonding in the corners and start-end zones, however the center of the welds showed a exemplary bonding or bond integrity. This may be regarded as the important feature or even the very unique feature of this type of welding. The inadequacy in bonding at the corners of the weld zone is a typical feature of MPW cylindrical parts and according to literature is not critical that the dearth of any diffusion layers leads to the postufor many applications . The minimally bonded corners of the weld specimen however pose undesirability and less adaptive in corrosive environments and in the case of recurrent cycled loads. lation that local melting is mainly involved in the phase The wave pattern by the side of the interface significantly depends on sample geometry and to a negligible degree on the process formation along the interface. parameters. Substantialand utility of bonding dissimilar specimen process cylinders and relatively low pulse energies inhibited the wave formation. Contrary, applying hollow dissimilar combines’ cylinders and high pulse energies pronounced waves are visible, especially in to the middle section of thelow welds (Figure 6(c)). This energies geometrical influencethe is in accordance with findings in . It is imperative As for pulse intermetallic phases note that the wave formation process is not mandatory for a good bonding. It is furthermore worth mentioning that to some extent wave formation could also be observed in regions without bonding. Circumventing the formation of intermetallic phases consist primarily ofextentaluminum, itprocess is parameters deduced that at the welding interface is impossible. The of interface depends on the and is fairly connectedsolely with the (c) structure of the interface. (c)(c)viewed under the optic microscope. (b) SS-Al specimen viewed under the optic microscope. (c) Figure 6. (a) Cu-SS specimen aluminum but not copper was molten during low energy If the interface shows a wavy appearance, the intermetallics mainly concentrate in so called “melt pockets”, which are mostly Cu-Al specimen viewed under the optic microscope. located at the crests of the waves (Figure 6(a)). If EMP produces a wave less interface, the intermetallic phases form a film of Figure 6. (a) Cu-SS specimen viewed under the optic microscope. (b) SS-Al specimen viewed under the optic microscope. (c) varying thickness (Figure 6(b)).phases It is pointed out that formed the phase film appears to be interrupted by regions any MPW. Al-rich are under strong nonwithout equiCu-Al specimen 6. viewed under microscope.specimen viewed under the optic Figure (a)the optic Cu-SS intermetallics. For a thickness below 5 microns the intermetallics contain rarely any cracks, voids or pores. (b) librium conditions. the sharp and(EDS) stepwise transition microscope. (b) SS-Al specimen viewed under the optic 3.5 Scanning Electron Microscopy (SEM)From With Energy Dispersive Spectroscopy 13 accordance with Carpenter and Wittman who deduced thatmetals solidis state diffusion is not i The SEM investigations present more information on bonding and phase formations. The SEM of welded specimen (a)the­pAl-Cu in chemical composition between the two arent microscope. (c) Cu-Al specimen viewed under the optic shown in Figure 7(a). It may be noted that the dearth of any diffusion layers leads to the postulation that local melting is mainly the process of MPW aluminum to copper. involved in the phase formation and bonding process along the interface. microscope. 11,12 11 corners of the weld specimen however pose undesirability and less adaptive in corrosive environments and in the (c) case of recurrent cycled loads. Figure 6. (a) Cu-SS specimen viewed under the optic microscope. (b) SS-Al specimen viewed under the optic microscope. (c) Cu-Al specimen viewed under the optic microscope. The wave pattern by the side of the interface significantly depends on sample geometry and to a negligible degree on the process parameters. Substantial utility of dissimilar specimen cylinders and relatively low pulse energies inhibited the wave formation. Contrary, applying hollow dissimilar combines’ cylinders and high pulse energies pronounced waves are visible, especially in the middle section of the welds (Figure 6(c)). This geometrical influence is in accordance with findings in11. It is imperative to note that the wave formation process is not mandatory for a good bonding. It is furthermore worth mentioning that to some extent wave formation could also be observed in regions without bonding. Circumventing the formation of intermetallic phases at the welding interface is impossible. The extent of interface depends on the process parameters and is fairly connected with the structure of the interface. Vol 8 (36) | December 2015 | www.indjst.org The Sum spectra of the welded specimen clearly illustrates the % composition of Co shown in Figure 7(b). The proportionate quantity of Aluminium is remarkably more region and copper dominates to the right of the curve, the AL-Cu in equal proportion shown in Figure 7(c). The mixing of the dissimilar metals at the welded joint for the 30u the perfection of the mixing of dissimilar metals. Al vs SS shows a moderate to low mixing of metals at the weld joint as shown in Figur as the unique quality of MPW is clearly depicted in Figure 7(d) and similar studies has b (a) The bonding (b)(b)for the 10um to 20um width of the (a) of the SS vs Al at the welded joint bonding in compared to Cu Vs SS. As for low pulse energies the intermetallic phases consist primarily of aluminum, it is dedu copper was molten during low energy MPW. Al-rich phases are formed under strong non equi and stepwise transition in chemical composition between the two parent metals and the fo (b) As for low pulse energies the intermetallic phases consist primarily of aluminum, it is deduced that solely aluminum but not copper was molten during low energy MPW. Al-rich phases are formed under strong non equilibrium conditions. From the sharp and stepwise transition in chemical composition between the two parent metals and the formed intermetallic phases it is in (c) (c) Indian Journal of Science and Technology 5 Magnetic Pulse Welding of Two Dissimilar Materials with Various Combinations Adopted in Nuclear Applications (c) prevalent at the intermetallic region shown in Figure 7(c). The mixing of the dissimilar metals at the welded joint for the 30um to 40um width of the specimen shows the perfection of the mixing of dissimilar metals. Al vs SS shows a moderate to low mixing of metals at the weld joint as shown in Figure 7(d). The wavy pattern of bonded area as the unique quality of MPW is clearly depicted in Figure 7(d) and similar studies has been already taken12,13,16,17. The bonding of SS-Cu found to be imperfect, due to the applied energy being Theinadequate bondingforofthis theconfiguration, SS vs Al athowever the welded joint for the bonding in the range 5um-10um is observed and to make the bonding even more efficient and in line with others, the 10um tothe20um width of concentrated the specimen improvement and further study is required. The bonding was prevalent throughout specimen however in theshows the little or narrow region, which is inadequate for the tensility point of view. The bonded zone is analyzed with in SEM methodology and theVs SS. moderate bonding compared to Cu (d) 7(e). same can be viewed in Figure (d) The bonding of SS-Cu found to be imperfect, due to the applied energy being inadequate for this configuration, however bonding in the range 5um-10um is observed and to make the bonding even more efficient and in line with others, the improvement and further study is required. The bonding was prevalent throughout the specimen however concentrated in the narrow region, which is inadequate for the tensility point of view. The bonded zone is analyzed with SEM methodology and the same can be viewed in Figure 7(e). The later studies of MPW would be in this area to further the equally distributed bonding of this SS-CU specimens at the lower KeV as applied for the other ­samples. Owing to short bonding time and the finite rates of solid-state phase transformations, there is prospectus that a thin layer on the low-melting point material fused and alloyed with the more refractory metal. Rapid melting and solidification explain the formation of intermetallic (e) phases. (e) Figure 7. (a) SEM of the Al-Cu welded specimen. (b) Sum spectra view of proportionate quantity of metals in the welded Figure 7. (a) SEM of the Al-Cu welded specimen. (b) portion. (c) Graphical analysis of dissimilar metals in intermetallic phase region. (d) Wavy pattern and line scanning of Al vs SS. Sum spectra of proportionate quantity of metals in the (e) SEMview and EDS analysis of SS vs Cu. 3.6 Nano Indentation welded portion. (c) Graphical analysis of dissimilar metals The later studies of MPW would be in this area to further the equally distributed this SS-CU specimens at the lower For bonding MPW ofjoint at the discharge voltage of 10kV, the in intermetallic phase region. (d) Wavy pattern and line KeV as applied for the other samples. nano indentation test was carried out to measure the scanning of Al vs SS. (e) SEM and EDS analysis of SS vs Cu. Owing to short bonding time and the finite rates of solid-state phase transformations, there is prospectus that a thin layer on micro hardness across the transition the zone by using Nano low-melting point material fused and alloyed with the more refractory metal. Rapid melting and solidification explain the Indeniter XP equipment. Five points near the interfaces and the formed intermetallic phases it is in accordance formation of intermetallic phases. 13 on both basic metals and one point on the transition zone with Carpenter and Wittman who deduced that solid 3.6 Nano Indentation were chosen for the test. state diffusion is not involved as active bonding mechaFor MPW joint at the discharge voltage of 10kV, the nano indentation test was carried out to measureand the micro hardness acrossof the micro hardThe magnitude the distribution nism in the process of MPW aluminum to copper. the transition zone by using Nano Indeniter XP equipment. Five points near the interfaces on both basic metals and one point on ness are given in Figure 8 (a) and (b). It is illustrated that ThetheSum spectra of the welded clearly illustransition zone were chosen for thespecimen test. The magnitude and the distribution of the micro hardness are given 8 (a)hardness and (b). It isvalue illustrated hardness value in that thethetransition zone is the highest trates the % composition of Copper and Aluminium inin Figurethe in the transition zone is the highest and the values decrease with increasing the distance away from the zone or the interface. It and the values decrease with increasing the weld shownto in 7(b).deformation The proportionate can joints be attributable the Figure sharp plastic along the interfaces that causes the gradient of work hardening near the the distance away interface. from the zone or the interface. It can be attributable to the quantity of Aluminium is remarkably more in the left hand sharp plastic deformation along the interfaces that causes side of the intermetallic region and copper dominates to the gradient of work hardening near the interface. the right of the curve, the AL-Cu in equal proportion is 6 Vol 8 (36) | December 2015 | www.indjst.org Indian Journal of Science and Technology (b) Figure 8. (a) Indentation hardness of Al/Cu. (b) Indentation modulus of Al/Cu. S. Kudiyarasan and S. Arungalai Vendan Similarly in combination of SS/Cu also the intermediate compounds produced in the tran hardness than the basic metals which is shown Figure 9 (a), (b) and (c). (a) (a) (a) Both the plastic deformation and the hardness reduce with increasing the distance from the interfaces. In addition, the intermediate compounds might be produced in the transition zone that is fragile and has higher hardness than the basic metals16, which will be analyzed deeply. (a) (a) Both the plastic deformation and the hardness reduce with increasing the distance from the interfaces. In addition, the intermediate compounds might be produced in the transition zone that is fragile and has higher hardness than the basic metals16, which will be analyzed deeply. (b) (b) (b) (b) (b) (b) Figure (a) Indentationhardness hardness ofofAl/Cu. (b)(b) Indentation modulus of Al/Cu. Figure 8. (a)8.Indentation Al/Cu. Indentation modulus of Al/Cu. Similarly in combination of SS/Cu also the intermediate compounds produced in the transition zone that is fragile and has higher hardness than the basic metals(b) which is shown Figure 9 (a), (b) and (c). 8. (a) Indentation hardnessand of Al/Cu. (b) Indentation modulus of Al/Cu. BothFigure the plastic deformation the hardness reduce (c)(c) with increasing the distance from the interfaces. In addi(c) Figure (a) Indentation in Side start from interface. Indentation Hardness of SS/Cu in combination of SS/Cu also the intermediate compounds in the9. transition zone that is fragile and has higher Figure (a) 9.Indentation inSSSS Side start from (b) interface. tion, theSimilarly intermediate compounds might be produced in produced Figure 9. (a) Indentation in SS Side start from interface. (b) Indentation Hardness of SS/Cu hardness than the basic metals which is shown Figure 9 (a), (b) and (c). (b) Indentation Hardness of SS/Cu. (c) (c) Indentation Modulus the transition zone that is fragile and has higher hardness 16 of SS/Cu. than the basic metals , which will be analyzed deeply. Figure 9. (a) Indentation in SS Side start from interface. (b) Indentation Hardness of S Similarly in combination of SS/Cu also the intermediate compounds produced in the transition zone that (a) is fragile and has higher hardness than the basic metals which is shown Figure 9 (a), (b) and (c). (a) (a) Similarly in combination of Al/SS also the interme(a) diate compounds produced in the transition zone that (a)(a) is fragile and has higher hardness than the basic metals which is shown Figure 10 (a), (b) and (c). 4. Reliability Analysis The Magnetic Pulse Welding (MPW) is one of the ­reliable methods that can be used for the dissimilar metal joints. The Magnetic Pulse Welding (MPW) provides an excellent tool for achieving of conductive metals such as aluminum, brass, or copper to steel, titanium, stainless, aluminum, magnesium copper and most other metals joints19. The Vol 8 (36) | December 2015 | www.indjst.org (b) (b) Indian Journal of Science and Technology 7 (b) Magnetic Pulse Welding of Two Dissimilar Materials with Various Combinations Adopted in Nuclear Applications c­ racking and spallation. The Cu-SS requires further study in the betterment of bonding. 6. Acknowledgements The authors sincerely thank SERB, Dept. of Science and Technology, India for providing the financial assistance vide order # FTYSS: SR/FTP/ETA-0134/2011 to carry out this research and IGCAR, India for testing and analysis. 7. References (c) (c) Figure 10. (a) Indentation in Al/SS side start from interface. (b) Indentation hardness of Al/SS. (c) Indentation modulus of 10. (a) Indentation in Al/SS side start Al/SS. from 1. Pulsar Ltd: Magnetic pulse welding Figure solutions. Raanana, interface. (b) Indentation hardness of Al/SS. (c) Indentation Israel: Pulsar Ltd; 2006. Available from: Similarly in combination of Al/SS also the intermediate compounds produced in the transition zone that is fragile and has higher http://www.pulsar. modulus of Al/SS. hardness than the basic metals which is shown Figure 10 (a), (b) and (c). co.il/systems/?did=30 2. Glouschenkov VA, Grechnikov FV, Mayshev BS. Pulsemagnetic processing technology when making parts units structure of an interphase region was ­investigated using a The Magnetic Pulse Welding (MPW) is one of the reliable methods that canofbeaerospace used for theengineering. dissimilar metal joints. The Journal de Physique 4. 1997; microscope and scanning Magnetic Pulse Welding microscope, (MPW) providesChemical an excellent compotool for achieving of conductive metals such as aluminum, brass, or copper to steel, titanium, stainless, aluminum, magnesium copper and most other7(C3):C3-45–48. metals joints19. The structure of an interphase sition was determined by a spectroscope. The Magnetic region was investigated using a microscope and scanning microscope, Chemical composition was determined by a process spectroscope. 3. Austin W. The cold welding is being used for more Pulse Welding (MPW) is reliable and wellandsuited to to high-volume The Magnetic Pulse Welding (MPW) is reliable well suited production (MTBF typically 1-5 million and more high-volume applications. Assembly Magazine; 20 welds) . high-volume production (MTBF typically 1–5 million 2002. 20 welds) . 5. Conclusion 4. Aizawa T, Kwang-Jin L, Shinji K, Takashi A. Interfacial microstructure and strength of steel/aluminum alloy Magnetic Pulse Welding of three dissimilar configurations of metals is performed and a detailed comparative study between the jointheat fabricated by magnetic pressure seam welding. specimens is done. Specific Observations include the dissimilar metals generateslap enough at the interface to enhance plenty 5. Conclusion of mass transfer for the precipitation of intermetallic phases. However, the relative amounts of these and phasesEngineering remained smallA. 2007; 471(1-2): Materials Science compared to fusion welding processes because the observed transition region is narrow and discontinuous. The type and 95–101. chemical composition created intermetallics depend on the pulse parameters chosen. This behavior is endorsed to different Magnetic Pulse Weldingofofthethree dissimilar configurations 5. Masumoto I, Tamaki K, Kojima M. 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Wave formation mechanism in magnetic pulse weldthe pulse parameters chosen. This behavior is endorsed to ing. International Journal of Impact Engineering. 2010; different temperature-time system of the process leading 37:397–404. to varying amounts of melting of the two base materials. 9. Marya M, Marya S, Priem D. On the characteristics of elecTo impound detrimental effects on the mechanical propertromagnetic welds between aluminum and other metals ties of the joints the thickness of the formed ­intermetallics and alloys. Welding in the World. 2005; 49:74–84. should not exceed few microns. 10. Carpenter SH, Wittman RH. Explosive welding. Annu Hardness of the welded specimen at the joint region Reviews Mater Sci. 1975; 5:177–99. is observed to be the maximum in compared to the 11. Tsujino J, Ueoka T. Ultrasonic butt welding of aluminum, either side of transition zones having dissimilar metals. anticorrosive aluminum and copper plate specimens. 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Journal of Manufacturing Processes. 2012; 14(3):372–7. 15. Van Wonterghem M, Vanhulsel P. Magnetic pulse crimping of mechanical joints. Ghent. 2011 Jun. 16. Hai-Ping Y, Zhi-Dan X, Hong-Wei J, Zhi-Xue Z, Chun-Feng L. Magnetic pulse joining of aluminum alloy-carbon steel tubes. Trans Nonferrous Met Soc China. 2012; 22:548−52. Vol 8 (36) | December 2015 | www.indjst.org 17. Korea SD, Datea PP, Kulkarnib SV. Electromagnetic impact welding of aluminum to stainless steel sheets. Journal of Materials Processing Technology. 2008; 208:486–93. 18. Jassim AK. Magnetic pulse welding technology. R&D, the state company for iron and steel-ministry of industry. Iraq J Electrical and Electronic Engineering. 2011; 7(2):2011. 19. Ivanas V. Reliability estimation of the austenitic steels welded joints. Materials Science (Medziagotyra). Vilnius, Lithuania: Department of Welding and Material Science, Vilnius Gediminas Technical University, Basanaviciaus 28. 2007; 13(2). ISSN: 1392–1320. 20. Magnetic Pulse Welding. Available from: http://www.bmax. com/technology/magnetic-pulse-welding/ Indian Journal of Science and Technology 9