Document Owners: Release Date: 8/20/10 MTW Facilities Management, MTW EH&S MacroTechnology Works Document Title: Document No: Document Rev: 0 Equipment Decontamination Purpose – The purpose of this document is to provide a uniform procedure to ensure that all ASU equipment that is removed from service or is relocated at the MacroTechnology Works is reviewed for compliance with Facilities Management and EH&S decontamination requirements. Removing or relocating any equipment MUST BE completed in a manner designed to minimize or eliminate the opportunity for harm to personnel, to the facility, and to the environment. Any piece of equipment, component, or sub-assembly that has been exposed to or contained any hazardous or toxic material must be decontaminated (cleaned) to the greatest extent possible. The determination of appropriate methods and means to accomplish this task will be determined on a case-by-case basis. Tenants/lessees are required to adopt their own standards for the handling of tenant/lessee-owned equipment. Tenant/lessee-owned equipment may be inspected by ASU personnel to ensure the safety of ASU personnel and the MacroTechnology Works facility. Scope – This document applies to all ASU equipment located at the ASU MacroTechnology Works (ASUMTW or MTW) including research and development, production, laboratory, point-of-use abatement, metrology, test, and other equipment that can present an electrical, radiation, mechanical, environmental, fire, ventilation, or chemical hazard. In addition, this document applies to equipment that is connected to or provides facility services such as house exhaust, waste drains, chemical dispense systems, toxic gas monitoring, fire protection, house air/vacuum systems, and other systems that have been or may be contaminated. This document covers the removal and decontamination of any component of a piece of equipment that may be or may have been contaminated. Facilitysupport equipment such as exhaust ductwork, vacuum interconnection piping, drain piping, chemical distribution systems, etc. are included in the scope of this document. This document applies to all aspects of all ASU operations at the ASU-MTW and only to activities at the MTW. Reference Documents – EHS 104 Laboratory Use of Hazardous Chemicals EHS 105 Personal Protective Equipment EHS 113 Radiation Safety in Research and Teaching EHS 403 Chemical Release Emergency Response EHS 405 Laboratory Check-in/Check-out Arizona State University – MacroTechnology Works Hardcopy may not be current document. Page 1 of 9 Document Owners: Release Date: 8/20/10 MTW Facilities Management, MTW EH&S MacroTechnology Works Document Title: Document No: Document Rev: 0 Equipment Decontamination Regulatory and Safety Drivers and Resources – SEMI S12 Guidelines for Equipment Decontamination SEMI S16 Environmental, Health and Safety Guidelines for Semiconductor Manufacturing Equipment Disposal 49CFR171-178 Department of Transportation (DOT) 40CFR260-271 Resource Conservation & Recovery Act (RCRA) 29CFRI910 Occupational Health & Safety Administration (OSHA) Procedure – 1.0 EQUIPMENT DECONTAMINATION GUIDELINES: This section describes the guidelines for the decontamination of process-related equipment/tools, research equipment, point-of-use abatement, metrology, test, and laboratory equipment/tools and the individual components of such equipment. An approval/review/sign-off requirement for the decontamination procedures to be used to perform the decontamination process is included in this guideline to ensure applicable regulations are met. Included in the equipment decontamination process are the following equipment/tool situations: Relocation (for re-installation within same bay/room or within site boundaries) Moved to storage/staging on-site for possible future use Sent off-site (transferred/sold to another company; sent for refurbishment, repair or maintenance) Sent off-site for final disposal Exception: this protocol does not cover parts being removed to be sent to parts clean operations or for vacuum pump repairs - provided that a written procedure has been developed regarding the safe handling/shipping of equipment with residual contamination And in addition, if the equipment/tool has any one of the following features: Uses, contains, or comes in contact with a hazardous chemical Connects to a facility system such as house exhaust, waste drains, chemical feed, toxic gas monitoring, fire alarm and/or suppression, and house air/vacuum systems Contains any ionizing or non-ionizing radiation source (i.e. laser, RF, microwave, X-ray, etc.). NOTE: Transportation, safety, and environmental regulations prohibit the improper transportation and disposal of hazardous materials. Contaminated equipment and support facilities must be decontaminated prior to removal. When sufficient decontamination is not attained or is unfeasible, equipment and/or support materials will be packaged, labeled, transported, and disposed-of as regulated waste. The costs of such handling and disposal will be the responsibility of the tool/equipment owner. Arizona State University – MacroTechnology Works Hardcopy may not be current document. Page 2 of 9 Document Owners: Release Date: 8/20/10 MTW Facilities Management, MTW EH&S MacroTechnology Works Document Title: Document No: Document Rev: 0 Equipment Decontamination ASU and state regulations govern radiation sources and they must be properly managed and inventoried when removed or relocated. See “EHS 113: Radiation Safety in Research and Teaching” for further information. The tool/equipment owner must identify any components such as batteries, capacitors, lamps, mercury switches, etc. or any materials contained in the equipment (PCBs, dioxins, mercury, lead, lubricants, coolants, etc.) that require special disposal procedures. These items must be handled as required by various environmental laws and regulations. The tool/equipment owner must identify all components such as flow controllers, chemical source tanks or controllers, etc. and any materials contained in the equipment (reactives, corrosives, flammables, pyrophorics, etc.) that require special decontamination or disposal procedures. These items must be handled as required by various environmental laws and regulations. Visible and detectable contamination, as evidenced by odors, residues, liquids, powders, flakes, or films on or in equipment should be assumed to be hazardous contamination that must be removed unless determined to be otherwise. If possible, equipment should be decontaminated “in place” in order to take advantage of exhaust systems, drains, and other support facilities that are available. If “in place” decontamination is not possible, proper protection of workers, the facility, the environment, neighbors, etc. must be provided. Any equipment still containing hazardous materials after decontamination has been attempted must be treated as hazardous waste and disposed of accordingly. All liquid residues must be removed from all pipes, tanks, etc. or said pipes, tanks, etc. must be capped, plugged or otherwise sealed. Arizona State University – MacroTechnology Works Hardcopy may not be current document. Page 3 of 9 Document Owners: Release Date: 8/20/10 MTW Facilities Management, MTW EH&S MacroTechnology Works Document Title: Document No: Document Rev: 0 Equipment Decontamination 1.1 Equipment Engineer/Tool Owner Responsibilities to Prepare Decontamination Plan: 1. Identify equipment/tool and/or tool components that are to be removed and the intended final disposition of tool or part (sale, salvage, scrap, reuse, storage, repair, etc.). Begin documentation process including ASU asset transfer. Begin preparation of checklist. 2. Meet with ASU-MTW Facilities Management Director, ASU-MTW EH&S Director, Lab Director/Manager, and lab/department EH&S Compliance Officer to determine scope of project. 3. Collect available data to determine what chemicals and chemical byproducts are or were present in equipment or components to be removed. 4. Determine appropriate means and methods to remove contamination. This may include the use of water, solvents, acids, neutralizers, etc. or physical means (wipes, bead blasting, etc.) to clean the equipment or components. Note that approval for any new chemicals to be used is required per MacroTechnology Works protocols and proper disposal methods for used cleaning solutions/materials must be identified. Perform Job Hazard Analysis if appropriate. Identify methods and means to minimize hazards. 5. Identify the proper location for such cleaning activities (in place, in a hood, etc.). Consider the possibility of outgassing and unplanned reactions that might occur during the cleaning process. Describe preventative measures to be taken to ensure no exposure of surrounding employees/area to hazards during decontamination. 6. Determine and procure proper Personal Protective Equipment (PPE) required to safely perform the decontamination process. 7. Identify proper means and methods to prove that the decontamination process/procedure has been successful and that the item can be safely dispositioned. 8. Identify proper personnel (contractors, employees, etc.) to perform decontamination process and identify and provide appropriate training, if necessary. 9. Meet with ASU-MTW Facilities Management Director, ASU-MTW EH&S Director, Lab Director/Manager, and lab/department EH&S Compliance Officer to review items 3-8 above and the checklist. 10. Once approval has been granted, obtain PPE, chemicals, tools, containers, etc. to be used for decontamination work and waste collection. 11. Once the above steps have been completed, decontamination work may proceed, with proper supervision of the work at all times. Arizona State University – MacroTechnology Works Hardcopy may not be current document. Page 4 of 9 Document Owners: Release Date: 8/20/10 MTW Facilities Management, MTW EH&S MacroTechnology Works Document Title: Document No: Document Rev: 0 Equipment Decontamination 1.2 Equipment Engineer/Tool Owner Responsibilities to Perform Decontamination: 1. Verify that all preparatory tasks listed above have been completed and that tool and/or tool components that are to be removed are ready for decontamination. This may include purging, capping of lines, etc. Provide a copy of the checklist to the person(s) performing the decontamination tasks. 2. Supervise decontamination of tool/component following the procedures in the checklist. If unplanned events are observed, STOP work immediately. 3. Supervise/perform tests described in the decontamination verification protocol identified above to prove that the decontamination process/procedure has been successful and the item can be safely dispositioned. If the decontamination process has not removed all contamination, STOP. 4. Once the decontamination process has been successfully completed, contact ASU Facilities Management and ASU EH&S to review all data, including decontamination verification test data. Once approval has been granted, decontaminated equipment or components may be packaged for disposition. 5. Provide copies of all completed checklists, etc. to ASU EH&S to be stored in site documents file. 6. Once affected equipment has been removed from lab, inspect area for any repairs needed. Contact ASU Facilities Management for final inspection upon completion of project. 7. Comply with requirements of EHS 403, Laboratory Check-in/Check-out, as appropriate. 1.3 Person(s) Performing Decontamination Activities: 1. Verify that all preparatory tasks listed above have been completed and that tool and/or tool components that are to be removed are ready for decontamination. This may include purging, capping of lines, etc. See checklist. 2. Verify that you understand proper procedures to perform decontamination. Use PPE as directed. 3. Begin decontamination of tool/component following the procedures in the checklist. If there are unexpected problems, STOP work immediately and contact the tool owner and EH&S. 4. Perform tests identified above to prove that the decontamination process/procedure has been successful. If the decontamination process has not removed all contamination, Arizona State University – MacroTechnology Works Hardcopy may not be current document. Page 5 of 9 Document Owners: Release Date: 8/20/10 MTW Facilities Management, MTW EH&S MacroTechnology Works Document Title: Document No: Document Rev: 0 Equipment Decontamination STOP. Contact tool owner for further instructions. 5. Once the decontamination process has been successfully completed, clean up all materials, supplies, tools, PPE, etc. used for the decontamination process. Dispose of used material properly. Dispose of excess cleaning materials as necessary. 6. Once decontamination verification approval has been granted, decontaminated equipment or components may be prepared/packaged for disposition. 1.4 Lab/Department Management/EH&S Compliance Officer Responsibilities: 1. Provide assistance to equipment/tool owner in preparation of equipment decontamination plan and checklist. 2. Review and approve completed equipment decontamination plan and checklist prior to plan initiation. 3. Provide necessary resources/assistance to equipment/tool owner to ensure safe operation. 1.5 MTW Facilities Management/EH&S Responsibilities: 1. Provide assistance to equipment/tool owner in preparation of equipment decontamination plan and checklist. 2. Review and approve completed equipment decontamination plan and checklist prior to plan initiation. 3. Review decontamination verification data. 4. Inspect space once equipment has been removed and ensure that all necessary repairs are completed. Arizona State University – MacroTechnology Works Hardcopy may not be current document. Page 6 of 9 Document Owners: Release Date: 8/20/10 MTW Facilities Management, MTW EH&S MacroTechnology Works Document Title: Document No: Document Rev: 0 Equipment Decontamination Equipment Decontamination Checklist Equipment/Component Information: Manufacturer: Serial Number: Location, Room Number: Date: Model Name/Number: ASU Asset Number: Bay, Floor, Column: Description: Chemical Information: List all chemicals used in equipment and all byproducts formed in equipment: Briefly describe process: Decontamination Protocol Information: Recommended Decontamination Process/Procedure: Recommended Decontamination Chemicals to be Used: Recommended Location for Decontamination Process to be Performed: Recommended Disposal Method for Used Decontamination Chemicals: Recommended Personal Protective Equipment Required: Recommended Personnel to Perform Decontamination: Describe Decontamination Verification Tests to be Performed: Arizona State University – MacroTechnology Works Hardcopy may not be current document. Page 7 of 9 Document Owners: Release Date: 8/20/10 MTW Facilities Management, MTW EH&S MacroTechnology Works Document Title: Document No: Document Rev: 0 Equipment Decontamination Describe, in detail, exact procedures to be used to perform decontamination and verification of successful decontamination: Reviewed/Approved: Tool Owner: Date: Lab Director/Manager: ASU EH&S Compliance Officer: ASU Facilities Management: ASU EH&S Management: Arizona State University – MacroTechnology Works Hardcopy may not be current document. Page 8 of 9 Document Owners: Release Date: 8/20/10 MTW Facilities Management, MTW EH&S MacroTechnology Works Document Title: Document No: Document Rev: 0 Equipment Decontamination Equipment Decontamination Verification Equipment/Component Information: Date: Model Name/Number: Manufacturer: Serial Number: ASU Asset Number: Location, Room Number: Bay, Floor, Column: Description: Chemical Information: List all chemicals used in equipment and all byproducts formed in equipment: Briefly describe process: Decontamination Protocol Information: Decontamination Process/Procedure Used: Decontamination Verification Tests Performed: Decontamination Verification Test Results: Decontamination Has Been Successfully Completed: Name of Tool Owner: Signature of Tool Owner: Name of Person(s) Performing Decontamination: Signature(s) of Person(s) Performing Decontamination: ASU EH&S Approval: Arizona State University – MacroTechnology Works Hardcopy may not be current document. Page 9 of 9