Cellulose based insulation materials for oil immersed transformers Dipl. Ing. (FH) Frank Kübler KREMPEL GmbH TRANSFORM Partner Introduction Name : Frank Kübler Education: Electrical Engineer Fachhochschule Esslingen - University of Applied Sciences Position: Head of Technical Service at KREMPEL GROUP Member of IEC TC 15: “Solid electrical insulation materials” since 2009. Frank Kübler, KREMPEL GmbH 06.06.2013 Page 2 Content • From wood to paper – the paper manufacturing process • Introduction of cellulose based materials: - Insulating (Kraft) paper - Presspaper - Pressboard - Laminated pressboard • Introduction of IEC standards • Applications • Characteristics of cellulose based materials Frank Kübler, KREMPEL GmbH 06.06.2013 Page 3 Paper manufacturing From wood to cellulose Composition of wood: ≈ 45% Cellulose ≈ 15% Hemicellulose ≈ 35% Lignin, Resin ≈ 5 % Minerals Pine wood Only the pure cellulose fibres can be used for manufacturing of high grade insulation papers. In a special process known as Kraft- or sulphate process the cellulose fibres are extracted from the wood. Frank Kübler, KREMPEL GmbH 06.06.2013 Page 4 Paper manufacturing Chemical structure of the cellulose fibres Cellulose is a polymer made of repeating glucose molecules Degree of polymerisation (DP): • Length of the molecule chains • DP value of new presspaper: approx. 1200 • End of life is reached at a DP value of 200 • Test standard: IEC 60450 In cellulose fibres many polymers are connected by hydrogen bonding Frank Kübler, KREMPEL GmbH 06.06.2013 Page 5 Paper manufacturing Schematic paper manufacturing process Pulper (cellulose loosening) Continous crusher (grinding) Vats (interim storage) Finishing Reel cutter (Edge cutting) Calender Mixer vat (additives) Machine vat (suspension) Cleaner Paper machine PM – dryer or Hot press PM – wet part (sheet forming) Further processing Reel cutter (narrow reel) Transverse cutter (format products) Frank Kübler, KREMPEL GmbH 06.06.2013 Page 6 Insulating paper Manufacturing of insulating paper Principle of a “Fourdrinier” paper machine: Drying Flow box • Production of a single paper layer • Typical density of the papers: 0.8 – 1.1 g/cm³ • Special type: crepe paper Frank Kübler, KREMPEL GmbH 06.06.2013 Page 7 Insulating paper Insulating paper – material standards IEC Standard Title IEC 60554-1 Specification for cellulosic papers for electrical purposes - Part 1: Definitions and general requirements IEC 60554-2 Cellulosic papers for electrical purposes Part 2: Methods of test IEC 606554-3-1 Specification for cellulosic papers for electrical purposes - Part 3: Sheet 1: General purpose electrical paper IEC 606554-3-2 Specification for cellulosic papers for electrical purposes - Part 3: Sheet 2: Capacitor paper IEC 606554-3-3 Specification for cellulosic papers for electrical purposes - Part 3: Sheet 3: Crepe paper IEC 606554-3-4 Specification for cellulosic papers for electrical purposes - Part 3: Sheet 4: Electrolytic capacity paper IEC 606554-3-5 Frank Kübler, KREMPEL GmbH Specification for cellulosic papers for electrical purpose - Part 3: Sheet 5: Special papers 06.06.2013 Page 8 Insulating paper Typical application for insulating paper in transformers: • Conductor insulation for the so called CTC (Continuously Transposed Cable) • Layer insulation • Insulation of internal wiring made with crepe paper tubes • Other application: - capacitors - measurement transformers - transformer bushings Frank Kübler, KREMPEL GmbH Picture: Essex Germany GmbH 06.06.2013 Page 9 Presspaper Manufacturing of presspaper Principle of a presspaper machine: Wet felt Drying Cylindrical sieves • Production of multilayer (3 – 7) paper • Typical density of the papers: 0.95 – 1.3 g/cm³ • Produced thicknesses: 0.04mm – 0.5mm Frank Kübler, KREMPEL GmbH 06.06.2013 Page 10 Presspaper Presspaper types produced by KREMPEL Designation Krempel Type IEC Type Colour Transformer presspaper RPT 3055 P.2.1 B IEC 60641-3-2 natural Low density transformer presspaper RPT 3055 SL P.4.1 A IEC 60641-3-2 natural RPT 3055-2 P.2.1 B IEC 60641-3-2 natural Maschine presspaper RPG 3020 P.6.1 A IEC 60641-3-2 orangebrown High grade presspaper EPR 3040 P.6.1 B IEC 60641-3-2 grey-black DPP - natural; red resin 2-layer transformer presspaper Krempel DPP Frank Kübler, KREMPEL GmbH 06.06.2013 Page 11 Presspaper Presspaper – material standards IEC Standard Title IEC 60641-1 Specification for pressboard and presspaper for electrical purposes – Part 1: Definitions and general requirements IEC 60641-2 Pressboard and presspaper for electrical purposes Part 2: Methods of test IEC 60641-3-2 Pressboard and presspaper for electrical purposes –Part 3: Sheet 2: Requirements for presspaper, types P.2.1, P.4.1, P.4.2, P.4.3 and P.6.1 Frank Kübler, KREMPEL GmbH 06.06.2013 Page 12 Presspaper KREMPEL-DPP • Manufactured from presspaper with a diamond-pattern resin coating. The epoxy resin is still in the reactive B-stage. • After application of heat and pressure for a certain time, the partial resin coating of KREMPEL-DPP leads to bonding of the electrical conductors with the layer insulation and mutual bonding of the insulation material layers. The large axial and radial mechanical forces arising in the case of a short circuit are safely tolerated by this internal strengthening of the coil. • At the same time the partial coating leaves empty spaces between the insulation and the electrical conductors: - Air and moisture can be removed more easily. - Faster oil impregnation. Frank Kübler, KREMPEL GmbH 06.06.2013 Page 13 Presspaper Application in oil filled distribution transformers Layer insulation Diamond dotted paper Presspaper Cooling channels Corrugated pressboard Ladder ducts and ladder grids Strips Internal wiring: Crepe paper tubes HV coil Frank Kübler, KREMPEL GmbH LV coil 06.06.2013 Page 14 Pressboard Manufacuring of pressboard: Principle of a pressboard machine: Drying Cylindrical sieves • Production of multi layer pressboard: • Typical density of the board: 0.95 – 1.3 g/cm³ • Produced thicknesses: 1.0 mm – 8.0 mm Frank Kübler, KREMPEL GmbH 06.06.2013 Page 15 Pressboard Pressboard types produced by KREMPEL Designation IEC Type Colour Hot pressed pressboard POWERBOARD AK B.3.1 A Natural Calendered pressboard PSP 3050 B.2.1 B Natural Mouldable pressboard PSP 3051 B.4.1 Natural Machine pressboard PSP 3010 B.6.1 A OrangeBrown POWERBOARD AK LB.3.1 A.1 LB.3.1 A.2 Natural Laminated pressboard Frank Kübler, KREMPEL GmbH Krempel Type 06.06.2013 Page 16 Pressboard Pressboard – Material standards IEC Standard Title IEC 60641-1 Specification for pressboard and presspaper for electrical purposes – Part 1: Definitions and general requirements IEC 60641-2 Pressboard and presspaper for electrical purposes Part 2: Methods of test IEC 60641-3-1 Pressboard and presspaper for electrical purposes –Part 3: Sheet 1: Requirements for pressboard, types B.0.1, B.0.3, B.2.1, B.2.3, B.3.1, B.3.3, B.4.1, B.4.3, B.5.1, B.5.3 and B.6.1 Frank Kübler, KREMPEL GmbH 06.06.2013 Page 17 Pressboard POWERBOARD AK • Precompressed pressboard type B.3.1A according to IEC 60641-3-1 • Produced in our factory in Zwönitz / Germany • Natural coloured, made from 100 % unbleached cellulose • POWERBOARD AK offers: - high purity - very good mechanical strength - low shrinkage - high oil absorption capacity • Thicknesses: 1 - 8mm • Master sheet size: 4.2m x 2.2m Frank Kübler, KREMPEL GmbH 06.06.2013 Page 18 Pressboard Major production steps of POWERBOARD AK: Frank Kübler, KREMPEL GmbH 06.06.2013 Page 19 Laminated Pressboard Laminated Board Laminated board is produced by bonding several layers of KREMPEL POWERBOARD AK with different type of bonding agents. Our laminated board is produced according to the IEC 60673-3-1 3 types of Laminated Board are available: •POWERBOARD AK-CG Glued with an aqueous casein glue according to type LB.3.1A.1 •POWERBOARD AK-PG Glued with a polyester resin according to type LB.3.1A.2 •POWERBOARD AK-PHG Glued with a phenolic resin similar to type LB.3.1A.2 Frank Kübler, KREMPEL GmbH 06.06.2013 Page 20 Laminated Pressboard Laminated pressboard – material standards IEC Standard Title IEC 60763-1 Laminated pressboard for electrical purposes – Part 1: Definitions, classification and general requirements IEC 60763-2 Specification for laminated pressboard – Part 2: Methods of test IEC 60763-3-1 Frank Kübler, KREMPEL GmbH Laminated pressboard for electrical purposes –Part 3: Sheet 1: Requirements for laminated precompressed pressboard, Types LB 3.1A.1 and LB 3.1A.2 06.06.2013 Page 21 Pressboard Application of pressboard Frank Kübler, KREMPEL GmbH 06.06.2013 Page 22 Fibre Structure Fibre structure of presspaper and pressboard: • All fibres are oriented either in machine direction or in cross machine direction. • Due to the production process the amount of fibres oriented in machine direction is higher than the amount in cross direction. 1 mm Thickness • Different behaviour in the three major directions: - Tensile strength, elongation - Shrinkage d CMD Frank Kübler, KREMPEL GmbH 06.06.2013 Page 23 Drying and Shrinkage Shrinkage MD and CMD of POWERBOARD AK Almost a linear relation between moisture content and shrinkage of pressboard Higher shrinkage in cross direction due to fibre orientation. Dimensional change [%] 0,80 0,70 0,60 Machine Direction (3mm) Cross Machine Direction (3mm) 0,50 0,40 0,30 0,20 0,10 0,00 0,00 Frank Kübler, KREMPEL GmbH 1,00 2,00 3,00 4,00 Moisture content [%] 5,00 06.06.2013 6,00 Page 24 Drying and Shrinkage Shrinkage MD and CMD of POWERBOARD AK Almost a linear relation between moisture content and shrinkage of pressboard Higher shrinkage in cross direction due to fibre orientation. Dimensional change [%] 0,80 0,70 0,60 Machine Direction (3mm) Cross Machine Direction (3mm) 0,50 0,40 0,30 0,20 0,10 0,00 0,00 Frank Kübler, KREMPEL GmbH 1,00 2,00 3,00 4,00 Moisture content [%] 5,00 06.06.2013 6,00 Page 25 Drying Time Drying of POWERBOARD AK 30 Drying time depends mostly on thickness of pressboard Measuring parameter: - Temperature: 105 °C - Sample size: 300 mm x 50 mm - Moisture content before drying: approx. 5% Drying time [h] 25 20 15 10 5 0 1 mm 3 mm 5 mm 8 mm Thickness of Pressboard Frank Kübler, KREMPEL GmbH 06.06.2013 Page 26 Drying and water absorption Storage parameter: - Temperature: 23 °C / 50 % r.h. - Sample size: 300 mm x 50 mm 6,0 5,0 Change in weight [%] Drying parameter: - Hot air drying at: 105°C - Sample size: 300 mm x 50 mm 4,0 3,0 Drying (1mm) Storage at 23°C/50% r.h. (1mm) Drying (3mm) Storage at 23°C / 50% r.h. (3mm) 2,0 1,0 0,0 0 5 10 15 20 25 30 35 40 45 50 Storage time[h] Frank Kübler, KREMPEL GmbH 06.06.2013 Page 27 Influence of moisture Influence of moisture to an oil / paper insulation regarding PD and breakdown voltage* Moisture in pressboard insulation means: • Reduced dielectric strength • Lower PD inception voltage • Accelerated degradation of the cellulose fibres Influence of moisture and temperature to aging of oil / paper insulation* Moisture content *Reference: Kahle, M.: Elektrische Isoliertechnik. Berlin, Heidelberg, New York, London, Paris, Tokyo: Springer-Verlag 1989. Frank Kübler, KREMPEL GmbH 06.06.2013 Page 28 Conclusion • The different production methods of cellulose based insulating materials cause different properties and make them suitable for various applications. • Due to the fibre orientation presspaper and pressboard are anisotropic materials which have different properties in machine direction and cross direction. • Due to the highly hygroscopic behaviour of cellulose based materials it is recommended to protect dried parts from picking up moisture again. • An optimized drying process for all pressboard insulation parts used in a transformer is essential to ensure a long life in service. Frank Kübler, KREMPEL GmbH 06.06.2013 Page 29