Acoustic GHz-Microscopy: Potential, Challenges and Applications A Joint Development of PVA TePLa Analytical Systems GmbH and Fraunhofer IWM-Halle Dr. S ebas tian Brand (Ph.D.) Fraunhofer CAM Fraunhofer Institute for Mechanics of Materials Department of Microelectronics and Microsystems Characterization of Microsystems Acous tic Micros copy Walter-Huelse-Str. 1 06120 Halle/S. Germany ( * www + 49 (0) 345 5589-193 + 49 (0) 345 5589-101 Sebastian.Brand@iwmh.fraunhofer.de www.iwmh.fraunhofer.de © Fraunhofer-Institut für Werkstoffmechanik IWM Agenda The Acoustic GHz-Microscope - Features and Requirements - Microscope Hardware and Technical Background Potential and Challenges - Tray & Stitch Mode - V(z) and Time-integrated Mode - Time-resolved Acquisition - Wave Modes and their Use - Challenges Selected Applications Summary and Outlook © Fraunhofer-Institut für Werkstoffmechanik IWM The GHz-SAM and the Acoustic High-Resolution Lens A Joint Development of PVA TePLa Analytical Systems GmbH and Fraunhofer IWM-Halle © Fraunhofer-Institut für Werkstoffmechanik IWM Parameter Value Resolution > 0.65 µm Frequency Range Penetration Depth Line Frequency 0.4 – 2 GHz approx. 1.5 λ < 50 Hz Focussing f#: 0.57 – 1 Refractive Index approx. 7.5 acous tic GHz-lens © Fraunhofer-Institut für Werkstoffmechanik IWM The Acoustic GHz-Lens Purpose : - Active element (piezo) excites elastic wave - Plane wave spherically focussed (cavity) - Wavelength and geometry of cavity define shape of sound field - Achievable lateral resolution dependent on sound field SF in 2D lateral cut through SF in focus © Fraunhofer-Institut für Werkstoffmechanik IWM axial cut through SF GHz-SAM – Technical Background Communication TRIGGER Gate l na l na si g eo si g rf- vi d z - STAGE y - STAGE x - STAGE PULSE Fast High-Precision Scanner Receiver Unit Motion Controller Pulser Unit RECEIVE SIGNAL Control Center sample © Fraunhofer-Institut für Werkstoffmechanik IWM GHz-SAM – Technical Background Device developed by and CAM © Fraunhofer-Institut für Werkstoffmechanik IWM The GHz - SAM - Scanner mounted on optical microscope - Scan line repetition frequency (LRF) up to 50 Hz - Extremely fast frame acquisition (15s – 30s) - Scan range can be defined freely 50 µm – 2 mm - Scan resolution can be defined freely down to 100 nm - Combined with precise X-/Y-stage for sample positioning - Automated scan sequencies © Fraunhofer-Institut für Werkstoffmechanik IWM Additional Features / Options of the GHz-SAM Alternativ e ex citation S ignal by Arbitrary Wav eform Generation - Spike excitation - Chirp signals for high axial resolution - Customized broad-band pluses Acquis ition of the unproces s ed RF-data - Signal analysis using SAMNALYSIS - Extraction / Identification of Wavemodes - Estimation of wave velocities © Fraunhofer-Institut für Werkstoffmechanik IWM Potential and Challenges © Fraunhofer-Institut für Werkstoffmechanik IWM Tray - Scan - Max. Lateral Range of Scanner : 2 mm @ 30 Hz LRF - Sample re-positioning by precise X/Y- stage - Fully automated scan sequence - Scan field extension by TRAY – Scan - Resulting data stitched to form global image © Fraunhofer-Institut für Werkstoffmechanik IWM V(z) - Scan - 2D-Scan repeated at multiple z-Positions - Max. z-Range of Scanner : 2 mm - Advantage of defocus sequence - Acquisition of optimum image - Excitation of SAW - Fully automated scan sequence © Fraunhofer-Institut für Werkstoffmechanik IWM Wave Modes in GHz-SAM longitudinal mode direction of density/wave component change direction of wave propagation transverse mode direction of density/wave component change direction of wave propagation Materials that support both modes also support Rayleigh waves Rayleigh Wave: Surface Acoustic Wave with longitudinal and transverse components Animation courtesy of Dr. Dan Russell, Kettering University © Fraunhofer-Institut für Werkstoffmechanik IWM GHz-SAM – V(x, y, z) Scan Sequence © Fraunhofer-Institut für Werkstoffmechanik IWM Use of V(z) Approach V(z) curve at a broad band excitation 10 V(z) curve at a single frequency 20 amplitude [dB] 10 frequency [MHz] 30 Δz 0 -10 40 50 60 -20 70 -30 80 90 -40 -7 -6.5 -6 -5.5 rel. defocus position [µm] z sin(R ) 0 2(1 cos(R )) v0 vR V0 = sound velocity of coupling vR = Rayleigh wave velocity θR = Rayleigh angle © Fraunhofer-Institut für Werkstoffmechanik IWM -6.8 -6.6 -6.4 -6.2 -6 rel. defocus position [µm] -5.8 -5.6 Challenges in Acoustic GHz-Microscopy - acoustic attenuation - penetration depth (lens aperture, focussing) - resolution (wavelength depending on sound velocity) - requires scanning - requires coupling fluid (impedance matching) acous tic attenuation x 1 ; yn x1 ; y1 x2 ; y1 x2 ; yn x3; y1 x3; yn xn; yn xn; y1 2D-s can required © Fraunhofer-Institut für Werkstoffmechanik IWM Selected Applications © Fraunhofer-Institut für Werkstoffmechanik IWM GHz-SAM Inspection of a microbolometer device 40 µm leg Potential problem area (void?) contact window leg contact window © Fraunhofer-Institut für Werkstoffmechanik IWM GHz-SAM Inspection of a microbolometer device microbolometer decive cut - A - transfer bonded thermistor onto read-out-integrated-circuit cut - A cut - B - Imaging through layer of 2 µm SiO2/Si/TiAl/SiO2 - voids 2.5 µm beneath surface cut - B Bonding interface pixel leg reflector thermistor © Fraunhofer-Institut für Werkstoffmechanik IWM GHz-SAM Inspection of Induced µ-crack - artificial defects induced by nano-indentation - GHz-SAM inspection in V(x,y,z) mode optical micrograph GHz-SAM micrograph (in focus) GHz-SAM micrograph (de-focussed) 40 µm © Fraunhofer-Institut für Werkstoffmechanik IWM 40 µm Defocus Sequence in GHz-SAM – V(x,y,z) minor subsurface crack large, obvious crack features way beneath surface (10 µm) © Fraunhofer-Institut für Werkstoffmechanik IWM GHz-SAM Inspection of sub-surface µ-crack surface GHz-SAM - micrograph SE- micrograph 50 µm PFIB - cut 40 µm defocussed GHz-SAM - micrograph clear indication for crack © Fraunhofer-Institut für Werkstoffmechanik IWM defocussed GHz-SAM - micrograph Void Inspection on TSV‘s GHz-SAM near surface image V(x, z) of TSV – „A“ V(x, z) of TSV – „B“ sample courtesy by J. Wolf, Fraunhofer ASSID © Fraunhofer-Institut für Werkstoffmechanik IWM - contrast in defocussed GHz-SAM image correlates With voids found in TSV‘s - dimensions of TSV larger than theoretical penetration depth - likely interface wave excited between TSV and Si - further research required for clarification Transient Simulation of Wave Propagation in GHz-SAM - 1 GHz -> enormous computational effort Mode conversion, reflection, diffraction, interference Computation of received acoustic signal @ 1GHz Identification of individual modes TS V w ith edge delam ination Lens Lens H2 O Si couplant Air Lens H2 O void Si TS V w ith v oid Si © Fraunhofer-Institut für Werkstoffmechanik IWM S ound intens ity in S i s ubs trate w ith v oid GHz-SAM visualization of sub-surface features µ-Bumps BCB (5 µm) Silicon (800 µm) interconnect wiring 20 µm © Fraunhofer-Institut für Werkstoffmechanik IWM GHz-SAM visualization of sub-surface features 30 µm -30 -40 20 µm z [µm] -50 -60 -70 -80 -90 © Fraunhofer-Institut für Werkstoffmechanik IWM 20 40 60 80 x [µm] 100 120 140 GHz-SAM in Life Science © Fraunhofer-Institut für Werkstoffmechanik IWM GHz-SAM in Life Science Cell Thickness Estimation Cell Thicknes s © Fraunhofer-Institut für Werkstoffmechanik IWM S ound Velocity Summary and Outlook Summary Developed an acoustic GHz microscope fast an precise scanner; stable RF-chain combined with optical microscope successfully employed in first applications Outlook Quantitative parameter estimation (Z, E, G, ν) Signal Analysis for parametric imaging Application specific and Coded Excitation Design of application specific GHz-lenses Optimized Matching Layers improve wave transmission Numerical simulation for investigating the propagation behaviour in specific structures and geometries © Fraunhofer-Institut für Werkstoffmechanik IWM Acoustic GHz-Microscopy: Potential, Challenges and Applications A Joint Development of PVA TePLa Analytical Systems GmbH and Fraunhofer IWM-Halle Dr. S ebas tian Brand (Ph.D.) Fraunhofer CAM Fraunhofer Institute for Mechanics of Materials Department of Microelectronics and Microsystems Characterization of Microsystems Acous tic Micros copy Walter-Huelse-Str. 1 06120 Halle/S. Germany ( * www + 49 (0) 345 5589-193 + 49 (0) 345 5589-101 Sebastian.Brand@iwmh.fraunhofer.de www.iwmh.fraunhofer.de © Fraunhofer-Institut für Werkstoffmechanik IWM