A WIRELESS ULTRAVIOLET SENSOR FOR HARSH ENVIRONMENTS By RACHEL DUDUKOVICH Submitted in partial fulfillment of the requirements for the degree of Master of Science Department of Electrical Engineering and Computer Science CASE WESTERN RESERVE UNIVERSITY January, 2015 CASE WESTERN RESERVE UNIVERSITY SCHOOL OF GRADUATE STUDIES We hereby approve the thesis/dissertation of Rachel Dudukovich candidate for the degree of Master of Science Committee Chair Christos Papachristou Committee Member Daniel Saab Committee Member Frank Merat Date of Defense November 3, 2014 2 Contents Introduction ......................................................................................................................... 8 Motivation .................................................................................................................................................. 8 Problem Statement .................................................................................................................................. 9 Outline ......................................................................................................................................................... 9 Chapter 1 - Background..................................................................................................... 12 Current combustion control methods ............................................................................................. 12 SiC for Harsh Environments ............................................................................................................. 13 UV Sensing Capabilities of SiC ...................................................................................................... 14 Related Work ......................................................................................................................................... 15 Dual-SiC Photodiode Devices for Simultaneous Two-Band Detection .................... 15 Chapter 2 - Approach ........................................................................................................ 18 Use of Frequency Modulation to Convey Sensor Signal ........................................................ 18 Oscillator Circuits ................................................................................................................................ 19 Relaxation Oscillator ........................................................................................................................... 19 Differential Oscillator ......................................................................................................................... 21 Colpitts Oscillator ................................................................................................................................ 22 Clapp Oscillator .................................................................................................................................... 23 Chapter 3 - Simulation....................................................................................................... 24 Clapp Oscillator .................................................................................................................................... 24 Chapter 4 - Device Characterization ................................................................................. 27 Chapter 5 - Implementation ............................................................................................... 29 Silicon Prototype Design ................................................................................................................... 29 Sensor Selection and Characterization .......................................................................................... 30 Development of Silicon Carbide Based Oscillators .................................................................. 32 SiC Relaxation Oscillator Design ................................................................................................... 34 Sensitivity Characterization .............................................................................................................. 38 Circuit Power Consumption .............................................................................................................. 40 Telemetry Design ................................................................................................................................. 40 Summary ................................................................................................................................................. 44 Chapter 6 - Conclusion ...................................................................................................... 45 3 Bibliography ...................................................................................................................... 46 4 List of Figures Figure 1. System View of UV Sensor Components .......................................................... 18 Figure 2. Relaxation Oscillation ........................................................................................ 20 Figure 3. Differential Oscillator ........................................................................................ 21 Figure 4. Colpitts Oscillator .............................................................................................. 22 Figure 5. Clapp Oscillator ................................................................................................. 23 Figure 6. Simulated Clapp Oscillator Circuit .................................................................... 25 Figure 7. Clapp Oscillator Simulation Output ................................................................... 25 Figure 8. Clapp Oscillator Fourier Transform ................................................................... 26 Figure 9. SiC Photodiode I-V Characteristics Under Illumination ................................... 27 Figure 10. Cadmium Sulfide Photoresistor I-V Characteristics Under Illumination ........ 28 Figure 11. Silicon relaxation oscillator and photodiode sensor ........................................ 30 Figure 12. Difference between photodiode capacitance under illumination and at dark. . 31 Figure 13. Current versus voltage of diode under UV illumination. ................................. 31 Figure 14. Cadmium-sulfide photocell I-V characteristics under illumination ................. 32 Figure 15. Clapp oscillator based UV sensor. ................................................................... 33 Figure 16. SiC differential oscillator. ................................................................................ 33 Figure 17. Final SiC relaxation oscillator based UV sensor. ............................................ 35 Figure 18. Relaxation oscillator circuit with Cree SiC MESFETs. ................................... 36 Figure 19. Initial ramp-up of relaxation oscillator. ........................................................... 37 Figure 20. The change in frequency under UVA, UVC, and darkness. ............................ 37 Figure 21. Relaxation oscillator output frequencies as a function of UV photon flux.. .... 38 Figure 22. Clapp oscillator output frequencies as a function of UV photon flux. ............ 39 5 Figure 23. The SiC relaxation oscillator frequency change under illumination................ 39 Figure 24. Receiver circuit design. .................................................................................... 41 Figure 25. The major components of the AD650 frequency to voltage converter . ......... 43 6 A Wireless Ultraviolet Sensor For Harsh Environments Abstract By RACHEL DUDUKOVICH This thesis discusses the development of an ultraviolet sensor for use in harsh environments, in particular high temperature environments. The sensor is constructed of silicon carbide components for this reason. The sensor creates a frequency modulated signal that is based on the change in light spectrum. The signal is transmitted wirelessly to a receiver circuit. Background information related to the sensor design is presented, as well as design considerations that were explored during the sensor development. The process of building the sensor is discussed, as well the resulting signal output characteristics of the sensor when it is exposed to ultraviolet radiation. 7 Introduction The subject of this thesis is a SiC-based wireless sensor that is designed to monitor the combustion efficiency in jet turbines and combustion engines. In this type of environment, the temperature may exceed 600 ˚C, and can be very corrosive, as well as subject to noise. For these reasons, silicon carbide based components were selected for use in the sensor circuit. Silicon carbide is a wide energy bandgap semiconductor and it use in this type of environment has been well documented [1]. The sensor can be used to determine the efficiency of combustion based on the ultraviolet emission intensity. The circuit is comprised of a relaxation oscillator with silicon carbide metal–semiconductor field effect transistors (MESFET) as the active components and a silicon carbide photodiode as the sensing element. The photodiode is embedded within the oscillator circuit and acts as a resistive element. As the light spectrum changes, the resistance of the photodiode changes, thereby changing the frequency of oscillation. The sensor frequency modulated RF signal is then transmitted using a dipole antenna. The signal is received and converted to a DC voltage using a frequency to voltage converter so that it can easily be measured with a standard data acquisition unit. Motivation The efficiency of combustion systems can be improved by implementing a feedback based control loop, rather than open loop control [2]. In order to achieve closed loop control of combustion processes, sensors capable of monitoring the exhaust gases, UV and visible light emissions from the flame and other pertinent parameters must be developed. The use of a feedback controller would allow for more efficient fuel consumption and therefore reduce pollution and operation costs. 8 UV emissions can be used in combustion control systems to monitor fuel efficiency. Chemiluminescence signals given off during chemical reactions taking place during combustion could be used to estimate the fuel-air ratio of the combustion process and could be used to control the injection of fresh gases to a desired set point [2]. Development of a sensor which takes advantage of the relationship between UV emissions and the quality of gases being burned could be used to improve combustion control methods. Problem Statement The goal of this thesis is to develop a wireless SiC-based UV sensor for use in harsh environments, such as a combustion engine. This sensor could be mounted near the combustion source, so it should be designed to be rugged and small in size. It is desired to keep the number of circuit components to a minimum to allow for a simple design and small footprint. The use for this sensor would be to allow for onboard monitoring of combustion efficiency. Outline Chapter 1 - Background • Current combustion control methods - This section discusses the benefits of closed loop control and the role sensors play in this. • Suitability of SiC for harsh environments – The properties of silicon carbide as they pertain to high temperature and pressure electronics are explained. • UV sensing capabilities of SiC – The UV sensing properties of silicon carbide are discussed. 9 • Related Work – Several other projects regarding silicon carbide photosensors and silicon carbide oscillators are included as background material. Chapter 2 - Approach • Use of frequency modulation to convey sensor signal – The rationale of using frequency modulation to transmit the sensor signal is explained. • Oscillator Circuits – The theory of different types of oscillator circuits is presented. • Selection of UV sensitive components – The appropriateness of different types of photosensors as it pertains to the circuit being developed is explored. Chapter 3 - Simulation • Comparison of different oscillator types – A brief discussion of simulations of oscillator circuits is presented. Chapter 4 - Device Characterization This section provides data on the I-V characteristics of the different photodetectors considered for use in the sensor circuit. Chapter 5 - Implementation • Silicon Prototype Design – The development of a silicon based prototype is explained. • Sensor Selection and Characterization – This section discusses the rationale behind the photodetector selected for use in the circuit. • Development of Silicon Carbide Based Oscillators – Work that was completed to develop an operational silicon carbide based oscillator is presented. • SiC Relaxation Oscillator Design – The final design of the silicon carbide based relaxation oscillator is discussed. • Sensitivity Characterization – The sensor’s response under UV light is demonstrated. 10 • Circuit Power Consumption – The power consumption of the circuit is discussed, as well as possible methods for supplying power. • Telemetry Design – The receiver circuit design is presented. Chapter 6 – Conclusion The topics discussed in this paper and the results of the sensor development are summarized. References 11 Chapter 1 – Background An overview of the use of optical sensors for combustion control methods is given. The type of environment such a sensor would operate in is likely to exceed the operating temperature of standard electronics. For this reason silicon carbide is an ideal candidate for the circuit components of such a sensor. The properties are silicon carbide related to operating temperature is discussed. Silicon carbide is also well known as a photodetector and its properties as a UV radiation detector are detailed. Finally, related work in high temperature silicon carbide oscillators is explored, as the RF generator is a major component of the sensor circuit. Current combustion control methods Many combustion control processes still operate in an open loop method without the feedback of relevant parameters to the injection system. Future advances to the efficiency and performance of these systems could benefit greatly from a closed loop system employing sensors to provide controllers with information to make operating adjustments. Applications that would benefit from such feedback-based control include automotive engines, biomass combustion systems and gas turbines. In gas turbines in particular, a significant reduction of nitrogen oxide emissions has been achieved by using a premixed mode of operation that allows the flame temperature to be reduced and the level of nitrogen oxide be thereby also reduced. However, premixed combustion requires a precise determination of the air-fuel ratio. Real-time measurements of the airfuel ratio would allow for improvements to this process [2]. Optical sensors may be used to monitor the light emitted by a flame. The light 12 spectrum from the flame is produced by chemical reactions occurring as the result of combustion. This process called chemiluminescence produces electronically excited radicals in the UV and visible range. Each radical produces a particular spectrum that is related to its quantum properties and can be used as a means of identification [2]. In addition, optical sensors have the advantage of not requiring direct contact with the flame, can selectively sense a desired wavelength, are fast, and able to gather data even in extremely hostile environments [3]. SiC for Harsh Environments In most optical sensor applications, the sensor must be mounted within the line of sight of the radiation source. If a sensor is to be mounted on-board in close enough proximity to observe the combustion flame, the sensor must be designed to withstand high temperatures. Most commercial and industrial sensors and electronics are rated to operate up to a temperature of around 85 to 100 C. It is therefore necessary to utilize components designed specifically with higher operating temperatures such as silicon carbide based transistors and diodes. Silicon carbide is very frequently used in high temperature applications due to several of its characteristics [1]. Silicon carbide has a wide bandgap, mechanical strength, high thermal conductivity, high melting point and inertness to exposure in corrosive environments [4]. SiC does not melt, rather is sublimes at about 1800 ˚C. Silicon carbide is very scratch and wear resistant and a Mohs hardness of 9. This is nearly as hard as diamond, which is rated as a 10. Silicon carbide is also resistant to most acids. Due to all of these qualities silicon carbide is often chosen for use in harsh environments. Applications for SiC sensors include radio frequency devices, pressure sensors able to withstand high vibration 13 due to its hardness and strength, accelerometers in airplane engines and motors in harsh environments, and optical sensors for control of light [1]. UV Sensing Capabilities of SiC Silicon carbide has a wide bandgap (Eg=3.0 and 3.2 eV for 6H and 4H SiC), low dark noise and low impact ionization ratio [1]. This makes it an excellent candidate for photo detection. 3C-SiC has a bandgap of 2.3 eV which also it to be used to detect photon in the 200-500nm range. 4H-SiC has an indirect bandgap of 3.23 eV which makes in suitable to detect photons in the 220-380 nm range [4]. Electromagnetic radiation interacts with semiconductors through absorption processes. Absorption is the relative decrease of the irradiance Ф, per unit length, δΦ( x) Φ = αδx . The solution of this equation is given by Φ( x) = Φ 0 e −αx , where Φ 0 is the incident irradiance, α is the absorption coefficient and x is a path length variable [5]. The photoelectric affect dominates for the ultraviolet spectrum (< 50 keV). Absorption by the photoelectric effect results in a complete transfer of the electromagnetic radiant energy from an incident photon to the interacting atom, which interjects a photoelectron. The minimum photon energy required is approximately equal to the semiconductor bandgap. Carriers already within the conduction band may absorb photons with energy below the bandgap. However the probability of this is low. Photoelectric absorption depends on the density of occupied states at the initial energy, the density of available states at the final energy, and the transition probability. The absorption coefficient for 14 3 direct transition is α (hv ) = A * (hv − E g ) 2 where A* = q 2 (2mr )1.5 /(nch 2 me *) and 1 / mr = 1 / me * +1 / mh *. The electron, hole and reduced effective masses are given by me *, mh *, mr respectively, n is the index of refraction, and E g is the bandgap [5]. Related Work The related work presented in this section discusses the development of silicon carbide photodiodes for UV detection and the use of silicon carbide transistors in high frequency oscillators. This related work shows that silicon carbide MESFETs can be used to create high frequency oscillators that are capable of operating at temperatures exceeding 200 C. The circuit designs discussed below were instrumental in achieving oscillation in the relaxation oscillator developed in this thesis. The designs below were explored to gain knowledge about the biasing and start up conditions of a SiC based oscillator. Dual-SiC Photodiode Devices for Simultaneous Two-Band Detection Silicon carbide is frequently used for UV detectors due to its large bandgap and its ability to withstand harsh environments such as gas turbines [6]. Research conducted by the GE Global Research group in Niskayuna, New York attempted to improve on standard SiC photodiodes by making a single device with separate sensing components which respond to multiple wavelength bands concurrently. 6H p-type substrates were purchased from Cree Research. These substrates were approximately 350 µm thick, having a resistance of approximately 1 Ω/cm. Epitaxy was then added with a 1 µm, ptype layer , a second p-type layer, 5 µm thick, and an n-type layer, 0.35 µm thick. In 15 order to create separate sensing components, reactive ion etching was first performed to form trenches 1 µm deep between adjacent device components. As the p-n junction was located approximately 0.25 µm below the surface, the trenches reduce unwanted electrical cross talk between the filtered and unfiltered parts of the chip. Light-blocking strips made from opaque layers of metal were then added to reduce absorption of UV in the areas between adjacent fingers. Optical filters were then deposited directly over the diodes and selectively etched to filter incident light to at least one of the device components. The materials used for the filters were and, deposited in thin layers, for a total thickness of approximately 3 µm [6]. An interdigitated geometry was employed to reduce sensitivity to chip misalignment when placed in an optical system. Square chip sizes of 1, 1.5, and 2 mm on a side were fabricated in order to determine the effect of area on overall performance [6]. The spectral responsivity curves of both diodes were measured using a 150 W Xe lamp. A monochrometer was used to obtain individual response measurements with a wavelength bandwidth less than 2 nm in the range between 200 and 400 nm. The unfiltered diode had a peak responsivity of 290 nm and the filtered diode reached a peak response at 320 nm that rapidly decreases at shorter wavelengths. 1-GHz, 200 C, SiC MESFET Clapp Oscillator This paper discusses the design of an oscillator for use in high temperature environments. The oscillator is intended for use as an RF signal generator in a frequency modulated sensor circuit. The circuit uses Cree SiC MESFETs, ceramic chip capacitors, gold bond wires and spiral inductor on an alumina substrate. The design is based on a Clapp 16 oscillator, which was selected since the frequency of oscillation is easily modulated based on sensor capacitance. The circuit was tested at 30 C to 200 C [7]. High Temperature Performance of a SiC MESFET Based Oscillator A differential oscillator was developed using Cree SiC MESFETs for pressure sensors for use in high temperature environments. The oscillator consists of two crosscoupled SiC MESFETS, two LC tank circuits made of spiral inductors and chip capacitors on an alumina substrate. The oscillator operates in the UHF band. The substrate was placed on top of a ceramic heater and heated from 30 to 475 C while RF measurements were taken. The biasing conditions were changed as needed to allow the oscillator to function reliably up to 475 C [8]. 17 Chapter 2 – Approach The UV sensor design concept consists of an oscillator circuit and a UV photo detector. The photo detector's resistance or capacitance will change when exposed to UV light versus ambient light. This change in resistance or capacitance will cause a change in the frequency of the oscillator. A dipole antenna is used to transmit the frequency signal to a wireless receiver. The use of frequency modulation, oscillator design and photo detector selection are discussed below. Figure 1. System View of UV Sensor Components Use of Frequency Modulation to Convey Sensor Signal Frequency modulation was determined to be the best way to convey that the sensor has detected UV light. The sensor changes the output frequency based on exposure to darkness, ambient light, UVA and UVC spectrums. Frequency modulation is more resilient to noise since most noise is amplitude based. Frequency modulation is also more resistant to signal strength variations [9]. Both of these advantages allow for a simpler circuit design. An oscillator circuit with relatively few components can be used for the basis of the sensor circuit design. The effects of UV radiation on the sensing component 18 can then change the frequency of the oscillator. A simple dipole antenna can be used to transmit the signal. Oscillator Circuits There are many types of oscillator circuits. For the purpose of creating a sensor, the oscillator frequency would need to change with respect to changes in either a resistive of capacitive component. The reason for this is that most photosensitive elements either display a change in their resistance or capacitance. Several types of oscillators were considered. Relaxation Oscillator The relaxation oscillator is a rather simple circuit consisting of two transistors, three resistors, a capacitor and voltage source, as shown in Figure 2. Capacitor C1 and resistor R2 control the frequency of oscillation. The basic principle of the relaxation oscillator is the charging and discharging of C1. It is designed such that a current charges the capacitor until a positive voltage threshold is obtained and the direction of the current is reversed. Next, the negative threshold voltage is reached and the current changes direction again. The process is repeated over and over again to produce the oscillations [10]. In relaxation oscillators, the transistors act like on-off switches. Two regions of operation determine the timing of the oscillation period. The first occurs when the devices are operating in the active region or negative conductance region. The waveform 19 displays an exponential growth, rather than a slower growing sinusoid. This response is referred to as the ‘regenerative-switching’ mode. The second stage of operation is called the recovery mode. In this case, both transistors are in the normal operating region. A small voltage or current excitation is plied to the base of J1 and is amplified by J1 with a phase change. This is coupled directly to the base of J 2 where another amplification and phase change occurs which leads to positive feedback at the base of J 1. Regenerative build-up occurs if the loop gain is greater than one until one of the transistor leaves its active region and enters saturation or cutoff. Regenerative switching is generally very fast, and the voltages of the coupling capacitors do not change significantly. When one of the transistors is cutoff, the biasing of the circuit attempts to return to the state of the circuit without capacitors. This time regenerative switching will occur in the opposite direction due to the fact that the saturated transistors re-enter the active region and the loop gain is again greater than unity. This causes another and restarts the entire the cycle. This cycling will produce a steady-state oscillation [11]. R1 R3 732 2.7k V1 4.5V J2 C1 68p J1 R2 69.1k 0 Figure 2. Relaxation Oscillation 20 Differential Oscillator The tail-current biased differential LC oscillator consists of a differential pair, which commutates a tail current and creates an effective negative resistance across a resonator. The differential inductors provide a higher Q while taking up less area than single-ended inductors. Oscillation occurs when energy in the inductor is balanced by the energy in the capacitor. The frequency of oscillation is determined by the resonator [12]. The amplitude of oscillation is proportional to the tail current. However if the current source is increased until the transistor is driven into the triode region, the oscillation amplitude is clipped at 2 Vdd. At this point, the current source is supplying as much current as the oscillator can support. When this happens the current source can be thought of as a short to ground. This region of operation is called supply limited. The linear region of operation is called current limited [12]. L2 L4 60uH C2 60uH C4 3p V2 4Vdc 3p C1 C3 3p J2 3p J3 L1 L5 10uH 10uH R1 10 V3 7.5Vdc 0 Figure 3. Differential Oscillator 21 Colpitts Oscillator The Colpitts oscillator is a fairly simple and robust oscillator. It frequency of oscillation is determined by two capacitors and one inductor. A voltage divider made by the two capacitors provides the feedback that is necessary for oscillation. In a Colpitts oscillator, the transistor conducts for a very short duration, which causes an impulse of negative resistance current. The amplitude builds up in a Colpitts oscillator as follows: When M1is off, the current source charges C1until the gate-source voltage of M1exceeds VT . M1 then conducts and the resulting current reaches C1and C2. C2 recharges and the transistor is shut off. This results in a train of narrow current pulses that are T seconds apart, where T is the period of oscillation [12]. VCC_WAVE L1 M1 VCC C1 M2 VCC_BAR C2 Figure 4. Colpitts Oscillator 22 Clapp Oscillator Vd L2 4 Vdc 0.5uH L1 CT 0.5uH 15p LT 0.5uH J1 15p C2 3p Vg 6 Vdc C3 C1 J2N3819 R1 50 3p 0 Figure 5. Clapp Oscillator The Clapp oscillator is a variable frequency oscillator that is tuned with a series LC tank rather than with a parallel tank as in the Colpitts or Hartley oscillator. The Clapp oscillator is related to the Colpitts oscillator but it has an additional capacitor placed in series with the inductor. A typical Clapp oscillator consists of a single inductor and three capacitors. Two of the capacitors (C1 and C2) form a voltage divider that determines the feedback voltage applied to the transistor input. A Clapp oscillator has some advantages over the Colpitts oscillator when used as a variable frequency oscillator. In the Colpitts circuit, the voltage divider contains the variable capacitor. This also causes the feedback voltage to be variable, making it difficult to achieve oscillation over a portion of the desired frequency range. This problem can be avoided by using fixed capacitors in the voltage divider and a variable capacitor (CT) in series with the inductor for the LC tank [12]. 23 Chapter 3 – Simulation Simulations were performed to help to determine a suitable oscillator design and determine component values. Orcad PSpice was used to develop the simulations [13]. The circuit simulations were used to develop prototype silicon oscillators prior to developing a silicon carbide based implementation. This was done so that cheaper, readily available components such as silicon JFETs could be used until a promising design was found that would then later be developed with more expensive, longer lead time silicon carbide MESFETs. The JFETs used in the simulations were J2N4393. The circuits selected for simulation were a Clapp oscillator and a relaxation oscillator. Clapp Oscillator A Clapp oscillator simulation was developed and produced. The oscillator frequency is around 60 kHz. Possible options for placement of the photodiode were in series with L2 and C1, or in series with R1. However, this circuit was deemed unsuitable since the resistance of R1 required a high value of 1 Mohm or greater to produce oscillations, further more changes in this resistance did not significantly impact the frequency of oscillation. The diode’s capacitance does not change enough under UV illumination to produce changes in oscillation. Figure 6 shows the Clapp oscillator circuit that was simulated. A voltage source with a short pulse in the initial start up was used to help set up the oscillations in circuit. 24 V1 L1 TD = .01u TF = .01u 10uHPW = 1 PER = 2 V1 = 0 TR = .01u V2 = 5 -1.066e-30V 1u L2 0V 1uH V J1 0V J2N4393 R1 10M 0 Figure 6. Simulated Clapp Oscillator Circuit Figure 7. Clapp Oscillator Simulation Output The waveform in Figure 7 has a time scale of 2 us per division on the x axis and 1 V per division on the y axis. Figure 8 shows the Fourier transform of the oscillator frequency output. The x axis based on 20 kHz per division and the y axis is 0.5 V per division. 25 Figure 8. Clapp Oscillator Fourier Transform While several LC type oscillators were simulated successfully, the RC based relaxation oscillator could not be made to produce oscillations in PSPICE. This is thought to be due to the fact that the necessary start up conditions for oscillation cannot be achieved in PSPICE. Several attempts were made to start up the oscillations with an initial pulse of the power supply, as well as modifying the initial conditions of the capacitor. It is sometimes suggested the circuit noise helps to start the oscillations in an actual circuit, which is lacking in the SPICE simulation. It should be noted that the actual circuit was built and oscillates with the parameters used in the simulation, simply oscillation through the simulation process itself could not be achieved. 26 Chapter 4 - Device Characterization Photodiodes and photoresistors where characterized under darkness, UVA and UVC illumination. The differences in the I-V characteristics are shown below. It can be seen that the SiC photodetector is more sensitive to the changes in the UV spectrum and also can distinguish between ambient and white light better than the photoresistor. For this reason, as well as the fact that the SiC photodetector is much more tolerant of high temperature environments, it was determined that the photodetector was the better choice for use in the UV detector circuit. Figure 9. SiC Photodiode I-V Characteristics Under Illumination 27 Figure 10. Cadmium Sulfide Photoresistor I-V Characteristics Under Illumination 28 Chapter 5 – Implementation This section discusses the general design of the UV sensor as well as preliminary work such as the development of a silicon based prototype design and circuits built as a study of SiC oscillators. The final oscillator design is discussed, as well as the wireless transmitter and receiver circuits. It was determined that the relaxation oscillator was the most suitable as a basis for the sensor since it had few components, was a simple design and the frequency is dependent on a resistive component. Silicon Prototype Design A prototype of the relaxation oscillator was first constructed with silicon JFETs. JFETS were selected due to their similarity to the MESFETs that would eventually be used in the SiC design. This prototype provided approximate values for the input voltage, resistors and capacitor suitable for the SiC relaxation oscillator design. The prototype was also used to experiment with where to embed the photosensor within the circuit. SiC photodiodes, cadmium sulfide photo-resistors, and silicon photocells were tested for UV sensitivity in the relaxation oscillator circuit. It was found that the largest frequency differential could be obtained by placing the SiC photodiode between the gate of the JFET in the first stage of the circuit and ground. This allowed the time constant of the oscillator to change appreciably but not so much as to cause the oscillations to become unstable. Once the prototype was constructed in silicon, several attempts to transform the design to SiC were made. It was found that the biasing conditions necessary to produce oscillations in the SiC design were quite different from those of the silicon relaxation 29 oscillator. Figure 11 shows the schematic for the original silicon prototype. R1 732 V1 4Vdc 68p R2 2.7k C1 Figure 11. Silicon relaxation oscillator and photodiode sensor Sensor Selection and Characterization Several options for the ultra-violet sensing component were explored. The first choice was a silicon carbide photodiode. The diode’s change in capacitance while in darkness and under UV illumination was compared. The difference was less than a picofarad as can be seen in Figure 12. The diode showed much greater sensitivity when used as a resistive component as shown in the I-V characteristics when in darkness and when illuminated by a MAPP (methylacetylene-propadiene propane)torch. MAPP gas produces approximately the same amount of UV radiation as the combustion of jet fuel, so it was selected as a suitable approximation. 30 Figure 12. Difference between the UV photodiode capacitance under illumination and at dark. Figure 13. Current versus voltage of the same diode under the UV illumination at dark and a MAPP torch at 5 cm: the difference is quite large. The UV illumination had 4eV photon energy. A cadmium sulfide photocell was also characterized and tested in the oscillator circuits. However, as it was more sensitive to ambient light and not made of silicon carbide it was deemed unsuitable for UV sensing in high temperature environments. 31 Figure 14. Cadmium-sulfide photocell I-V characteristics under illumination and at dark. Development of Silicon Carbide Based Oscillators The proper operating conditions were found by constructing a Clapp oscillator [7] and a differential oscillator [8] using a SiC MESFETs from Cree, Inc. The Clapp oscillator can operate with gate voltages approximately between 5 and -8 volts and drain voltages between 1.2 and 5 volts. Its frequency varies between approximately 6 and 50 MHz depending on biasing conditions. The differential oscillator operated at a drain voltage of approximately 1.5 to 6 volts and a gate voltage of approximately -4.5 to -10 volts. Its frequency varies from approximately 2 to 10 MHz, and also is dependent on the applied voltages. The Clapp oscillator design in shown in Figure 15 and the differential oscillator in shown in Figure 16. 32 Figure 15. Clapp oscillator based UV sensor. L2 L4 60uH C2 60uH C4 3p V2 4Vdc 3p C1 C3 3p J2 3p J3 J2N3819 L1 J2N3819 L5 10uH 10uH R1 10 V3 7.5Vdc 0 Figure 16. SiC differential oscillator. These designs produced very stable oscillations when the gate and drain voltages were adjusted to a suitable level. Experimenting with the differential oscillator confirmed that a second power supply is necessary to apply a negative voltage to the MESFET gate in order to produce oscillations and to control the drain current level. Both of these circuits were eventually abandoned however, in favor of the relaxation oscillator due to 33 the fact that the frequency of oscillation is controlled by the tank capacitor CT in both designs. The SiC photodiode junction capacitance does not change sufficiently to produce a significant change in frequency. Also, as the designs are based on an LC tank, parasitics tended to dominate the oscillations which produced poor sensitivity to changes in the tank capacitance. It was determined that the RC based relaxation oscillator would be more sensitive to UV emissions due to the photodiode’s larger change in resistance rather than capacitance when under illumination. SiC Relaxation Oscillator Design With the knowledge gained from the Clapp and differential oscillators, the Si based relaxation oscillator was redesigned for SiC and is shown below. A negative voltage was applied to the gate of both transistors. The two stages of the circuit were coupled using 830 nF blocking capacitors at the gate of each MESFET. It was also necessary to considerably reduce the resistors R1 and R2. Oscillations occur with a gate voltage of -6 to -8 V and a drain voltage of 6 to 10 V. When suitable biasing conditions have been met, the gate voltage can be used to pinch off the MESFETs and keep the drain current at a lower level, reducing heat output from the components. 34 V1 7.5Vdc R1 R2 15 28 C1 C3 68p 830n C2 SiC Photodiode 15k SiC MESFET SiC MESFET 830n R3 R4 51 V2 8Vdc Figure 17. Final SiC relaxation oscillator based UV sensor and antenna for wireless transmission. When the proper biasing resistor values were found and stable oscillations were achieved, a printed circuit board was designed. All of the traces where made 0.04” inches wide to easily account for a current of up to 0.5 A. All of the surface mount resistors where replaced with two resistors of the same value in parallel to account for this as well. The printed circuit board was manufactured by ExpressPCB according to the drawing provided [14]. The completed circuit board is shown in Figure 18. The board was first tested without the photodiode to ensure that the oscillator was functioning properly. 35 Figure 18. Relaxation oscillator circuit with Cree SiC MESFETs. The sensor was tested by exposing it to ambient light, darkness, UVA, and UVC. The device is contained in a metal package to block electromagnetic interference, with a small opening to allow UV illumination of the sensing elements. The light source was positioned 3 cm from the photodiodes. The sensor was exposed to each type of illumination for a period of approximately 2 minutes before transitioning to the next type of light in order to capture the rise and fall times associated with the changing light spectrum. It was found that during the first fifteen minutes of operation the oscillator’s frequency must ramp up and stabilize before reliable sensing can occur as shown in Figure 18. The change in frequency under exposure to ambient light and UVC are shown in Figure 19. The sensor was first exposed to ambient light for 20 seconds, then UVC at a 36 distance of 5 cm for 20 seconds. The light sources are then switched back successively in 20 second intervals. It can be seen that exposure to UVC causes the frequency to increase by 20 to 30 kHz during each interval. Relaxation Oscillator Turning On 23.35 Frequency (MHz) 23.30 23.25 23.20 23.15 23.10 23.05 23.00 22.95 22.90 22.85 1 46 91 136 181 226 271 316 361 406 451 496 541 586 631 676 721 766 Timed (s) Figure 19. Initial ramp-up of relaxation oscillator. Relaxation Oscillator Sensing UV Illumination 22.88 22.87 UVA UVC MHz 22.86 22.85 22.84 22.83 Darkness Darkness 22.81 1 29 57 85 113 141 169 197 225 253 281 309 337 365 393 421 449 477 505 533 561 589 617 645 673 701 729 22.82 Time (s) Figure 20. The change in frequency under UVA, UVC, and darkness. 37 Sensitivity Characterization The sensor was tested by illuminating it with ambient light, darkness, UVA, and UVC. The sensor is packaged in a metal box with a cutout large enough to expose the sensing elements in order to block electromagnetic interference. The light source was positioned 1 inch from the photodiodes. The sensor was exposed to each spectrum of light for a period of approximately 2 minutes before transitioning to the next type of light in order to capture the rise and fall times associated with changing light frequency. Figures 21 and 22 show the relaxation and Clapp oscillator output frequencies as a function of UV photon flux. The UV photon flux is shown in log scale in both cases. The relaxation oscillator’s frequency shift has a linear dependence on the photon flux. 62.85 F req u en cy (kH z). 62.80 62.75 E p h = 4 eV 62.70 62.65 62.60 62.55 62.50 62.45 62.40 1E +15 1E +16 1E +17 U V P h o to n F lu x (1/cm 2.s.) 1E +18 Figure 21. Relaxation oscillator output frequencies as a function of UV photon flux. The UV photon flux is shown in log scale. The frequency shift has linear dependence on the photon flux. 38 8.06 Frequency (MHz) . 8.05 Eph =4 eV 8.04 8.03 8.02 8.01 8.00 1E+14 1E+15 1E+16 1E+17 1E+18 UV Photon Flux (1/cm2.s.) Figure 22. Clapp oscillator output frequencies as a function of UV photon flux. Figure 23 shows the UV detector’s operation in conjunction with the wireless transmitter and receiver. A UVC source placed 5 cm away from the sensor produces a 20 kHz increase in the oscillator’s frequency. This corresponds to a 125 mV increase in the final DC output signal from the receiver. Figure 23. The SiC relaxation oscillator frequency changes by 20 kHz when illuminated by UVC. This produces a 125 mV change in the wireless receiver’s output voltage. 39 Circuit Power Consumption The current draw of the circuit is typically around 0.150 A, while operating around 6 to 8 volts. This level of power consumption could likely be reduced by optimizing the circuit. If the power consumption could be reduced, this would open several possibilities for powering the circuit. It is highly desirable to utilize properties of the sensor installation environment for potential energy harvesting. However, most energy harvesting technologies are much lower power and would be impractical to meet the power requirements of the present circuit design. Optimization of the power consumption of the circuit would have to be completed to make use of such energy harvesting capabilities. This has been left as future work and has not been implemented in the scope of this project. Of the several types of energy harvesting capabilities available, thermoelectric technologies on average produce about 40 µW/cm3, vibration technologies produce about 116 µW/cm3 and solar cells can generate about 15 mW/cm3 [14]. While heat is highly available in the combustion environment, thermoelectric technologies are not very efficient and produce considerably less than the UV sensor circuit requires, even if an optimization was completed to minimize the power consumption. Solar cells have the highest efficiency and may be a promising method if light from the combustion flame could be used to produce power. Telemetry Design The wireless transmission system was designed to minimize the size of the footprint of the primary sensor/transmitter component. As such, all that is required to 40 transmit the FM signal is a small dipole antenna. The receiver consists of a dipole antenna, variable gain amplifier, frequency divider, and frequency-to-voltage converter. The receiver’s input is initially a 40 mV, 22 MHz FM signal. It is then amplified by a National Semiconductor LM386 variable gain amplifier. This increases the amplitude to approximately 5 V. The signal is demodulated by the Analog Devices’ AD650. The AD650 is a voltage-to-frequency converter, but it can be wired to function as a frequency-to-voltage converter. A schematic is shown below. +5V +5V 250u 250u 0.05 u 0.1u 0.05 u 0.1u LM386 LM386 10u 10u Vin 10k 10k Rint -15V Cint 11.11k 0.1u 3u Cos Vout 88u SN54LS294 AD650 20k D1N914 0.1u 250k +5V 2k R4 1k 500 +15V 560p Fin +5V Figure 24. Receiver circuit design. The maximum input frequency the AD650 is capable of processing is 1 MHz, so a 41 SN74LS294N frequency divider from Texas Instruments is used to divide the input frequency by a factor of 32. The SN74LS29N is programmed by specifying the desired frequency divisor value on the four programming inputs, pins 2, 1, 15, and 14 respectively. To divide the input frequency by 32, or 25, the input 0101 (binary 5) is chosen. Consequently, pins 2 and 15 are tied low and 1 and 14 are high. This will produce and output frequency of 22 MHz/32 or 687.5 kHz, which is well within the range of the AD650’s input range [15]. The signal can then be converted by the AD650. Analog Devices provides an article detailing the use of the AD650 voltage-to-frequency converter as a frequency-tovoltage converter [16]. The major components of the AD650 are shown in Figure 25. It consists of a comparator, a one-shot with a switch, a constant current source, and a lossy integrator. An input signal at the comparator triggers the one-shot. The one-shot actuates a single-pole-double-throw switch which determines when the current source is applies to the summing junction or the output of the lossy integrator. When the one-shot is on, there is current applied to the input of the integrator and its output increases. At the end of the one-shot period, the current enters the output of the integrator. Since the output has a low impedance, the current has no effect and the circuit is essentially turned off. During this time the output falls due to the discharge of the Cint capacitor through the resistor Rint. When the comparator is triggered constantly, the integration capacitor will maintain to a steady value due to charging and discharging. 42 Figure 25. The major components of the AD650 frequency to voltage converter as explained in the application note “Using the AD650 Voltage-to-Frequency Converter As a Frequency-to-Voltage Converter” [13]. The values of the feedback resistor Rint, the integration capacitor Cint, and oneshot timing capacitor Cosmust be determined as follows. The input frequency fin has a constant amplitude α and period tos. The average output voltage is given by the equation: Voutavg = tos× Rint×α×fin. Thus, a suitable value for Rintcan be found by selecting the desired output voltage for a given signal with frequency fin and amplitude α. Cos determined by the relationship: Cos= !!" !!.!µ! !.!!" ! . This equation is simply rearranged from the equation for the one-shot timing period t !" as given in the AD650 datasheet [15].Cint !"#$%&'#%( !"#$%&#" !"#$ is given by the equation: Cint= !×!!"# where N is the number of time constants needed to settle and the mechanical response time is that of the switch actuated by the one-shot shown in Figure 25. 43 Summary The initial silicon based design had to be modified significantly in order to function with SiC transistors. The input voltages and the amount of current drawn increased, as well. Comparable output voltages were achieved, however the SiC MESFET circuits operated with frequencies several orders of magnitude greater than that of the Si JFETS. The use of the relaxation oscillator design provided superior sensing performance over the Clapp and differential oscillators. This is due to the fact the period of the oscillation is controlled by an RC time constant in the relaxation oscillator, rather than a LC tank as in the Clapp and differential oscillators. The SiC photodiode exhibits a must greater sensitivity to UV illumination when used as a resistive element rather than a capacitive element. The output signal of the oscillator was strong enough to be sent via a simple dipole antenna to a receiver circuit that converts the change in frequency to a change in voltage. There is a 125 mV difference in the output voltage of the receiver when the sensor is illuminated by UV as compared to when it is under ambient light. This is a more than sufficient change to be detected by most data acquisition modules and could easily be integrated into a computer based system for data logging or control. 44 Chapter 6 – Conclusion In closing, this thesis discusses the design and implementation of a silicon carbide UV sensor for use in high temperature environments. This type of sensor has applications in the aero and space industries, or in any industry where the combustion of fuels may give off NO and other pollutants. The sensor prototypes a particularly useful design in that it possesses an on board wireless transmission system and a remote receiver for ease of integration into a monitoring system. Future work that would be beneficial to this design would be to perform an optimization of the power consumption of the circuit. This would potentially allow the sensor to make use of various energy harvesting technologies. The trade-offs between different types of energy harvesting methods could be explored and there practicality for use in high temperature environments could also be studied. 45 Bibliography [1] Rebecca Cheung, Silicon Carbide Microelectromechanical Systems for Harsh Environments. Edinburgh: University of Edinburgh, 2006. 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