Genuine Restek Replacement Parts Shimadzu GCs More Parts & Accessories for More GC Systems Agilent • Bruker/Varian • PerkinElmer • Shimadzu • Thermo Scientific • And More! Pure Chromatography www.restek.com More Parts & Accessories for More GC Systems Agilent • Bruker/Varian • PerkinElmer • Shimadzu • Thermo Scientific • And More! Table of Contents Dear Colleague, Restek’s GC Accessories Team is devoted to bringing you the highest-quality products, delivered on time every time, to help you maximize data reproducibility and minimize instrument downtime— regardless of which brand of instrument you use. From our exceptionally inert Sky® inlet liners on the right to the invaluable Restek Electronic Leak Detector on page 12, Genuine Restek Replacement Parts are designed to meet or even exceed GC manufacturers’ already-strict specifications and performance requirements. And of course, as with all Restek products, we also offer exemplary Plus 1 service before and after you order. Sky® Inlet Liners ....................................................1–5 Other Deactivations .................................................6 Other Inlet Liners .................................................7–8 Inlet Liner Packing Materials.................................9 Inlet Liner Accessories.......................................... 10 O-Rings, Septa, Seals ............................................ 11 Do you have a product suggestion or question about Restek’s GC accessories? Feel free to contact one of our team members or your Restek representative today. We look forward to hearing from you! Leak Detector ......................................................... 12 Sincerely, Scott Adams Super-Clean Gas Filters ........................................ 14 GC Accessories Product Marketing Manager Tools.....................................................................15–16 Flowmeter ............................................................... 13 Ferrules ...............................................................17–19 Connectors ........................................................20–23 Vial Accessories....................................................... 24 Vials ......................................................................25–28 Syringes ..................................................................... 29 Scott Grossman GC Accessories Chemist Rob Lindquist GC Accessories Associate Product Marketing Manager Kelli Steindl GC Product Line Manager Scott Adams GC Accessories Product Marketing Manager e-mail us at gcaccpmm@restek.com ? Gas Regulators & Accessories.....................30–31 Fittings ................................................................32–33 Fitting Kits ................................................................. 33 How can we help you today? Contact us… customer service: 1-814-353-1300 (ext. 3) | e-mail: csreps@restek.com technical service: 1-814-353-1300 (ext. 4) | e-mail: support@restek.com sales representatives: 1-814-353-1300 | e-mail: salesreps@restek.com 3 ways to order: 1. CALL: 1-800-356-1688 (ext. 3) or 1-814-353-1300 (ext. 3) Monday–Friday 8:00 a.m.–6:00 p.m. Eastern Time 2. FAX: 1-814-353-1309 24 hours a day 3. ONLINE: www.restek.com 24 hours a day Outside the U.S.? Find a distributor at www.restek.com/distributor Page Header Patent pending True Blue Performance • Increase accuracy and reproducibility with state-of-the-art deactivation. • Achieve lower detection limits for a wide range of active compounds. • Use wool with confidence—quartz wool is deactivated after packing, preventing the loss of sensitive analytes. When faced with complex choices, simple solutions stand out. Sky® inlet liners from Restek use a comprehensive, state-of-the-art deactivation and are the only blue liners on the market—makSky® liners give you the ing them an easy-to-recognize solution to common inlet problems. inertness you need for more accurate tracelevel results. The innovative deactivation used for Sky® liners results in exceptional inertness for a wide range of analyte chemistries. By reducing active sites and enhancing analyte transfer to the column, these liners increase accuracy and precision, allowing lower detection limits for many active compounds. In addition to improved data quality, you’ll benefit from fewer liner changes and less downtime for maintenance. Selecting the right liner for your application can be a challenging task. Sky® inlet liners make the choice simple; the comprehensive deactivation, distinctive color, and availability in popular configurations mean Sky® liners are the best choice for optimizing chromatographic performance. Regardless of your application, Sky® liners provide reliable inertness and assured performance, day-after-day and analysis-after-analysis. The Story Behind Sky® Liners For over 25 years, Restek’s vision has been to be the company chromatographers trust. This philosophy is the cornerstone of our business, and it’s the reason our chemists and engineers are dedicated to developing innovative, best-in-class products like Sky® liners. As chromatographers, we understand your needs and strive to develop and deliver products that make your life easier. With Sky® liners, our goal was to create a state-of-the-art deactivation that provides superior performance. But why did we make them blue? Restek has always been associated with the color blue; to us, it signifies strength, innovation, and excellence. We made Sky® liners blue because it represents the technological advancements and unmatched quality that define Restek products. Choose blue—the best choice for dependable results. 1-800-356-1688 or 1-814-353-1300 www.restek.com 1 Sky® Inlet Liners Simple Solutions: Inert Sky® Inlet Liners Improve Accuracy and Precision for a Wide Range of Analytes Many chromatographic problems, such as poor response and missing or tailing peaks, are caused by activity in the inlet liner. These effects complicate quantification and can be particularly problematic for sensitive analytes. Sky® inlet liners from Restek offer exceptional inertness, ensuring enhanced transfer of analytes to the column, good response, and highly symmetric peaks. The inertness of these liners is due to a state-of-the-art deactivation process that completely passivates the liner and wool so that they are inert to a wide variety of active analytes. Some deactivations, such as base deactivation, are effective only for particular target compound chemistries. In contrast, the balanced deactivation of Sky® liners prevents interactions with many chemical classes. As shown on the following pages, complex pesticide probes, as well as both acidic and basic compounds have strong responses and excellent peak shapes, demonstrating the inertness of Sky® liners. With Sky® inlet liners, you will see improved sensitivity, accuracy, and reproducibility liner-to-liner, which allows you to quantify challenging compounds at trace levels with confidence. Reduced Breakdown Improves Trace Analyses Endrin and DDT are important analytes for the environmental and food safety industries, and they also serve as excellent general probes for liner inertness. Both compounds are sensitive to different modes of activity due to their chemical structures and their being analyzed at very low concentrations. As shown in Figure 1, Sky® liners are significantly more inert than comparable competitor liners, showing 3–4 times less endrin and DDT breakdown. Figure 1: Endrin and DDT breakdown is significantly reduced with Sky® liners, demonstrating higher inertness. 1. 2. 3. 4. 5. 6. Peaks DDE* Endrin DDD* Endrin aldehyde* DDT Endrin ketone* *breakdown products GC_EV1200_1202 Column: Rxi®-5Sil MS, 15 m, 0.25 mm ID, 0.25 μm (cat.# 13620); Sample: Endrin (50 ng/mL) and DDT (100 ng/mL) in hexane; Injection: Inj. Vol.: 1 μL splitless (hold 0.75 min); Liner: Comparison of Sky® Single Taper Liner with Wool (cat.# 23303.5) and Agilent Single Taper Liner with Wool (cat.# 5062-3587); Inj. Temp.: 250 °C.; Detector: μ-ECD @ 300 °C. did you know? Sky® inlet liners from Restek are extensively tested to ensure consistent product quality. The color and label have been shown not to interfere with analyses or contribute to background. Choose blue—the best liner for sensitive applications. 2 www.restek.com 1-800-356-1688 or 1-814-353-1300 Sky® Inlet Liners Greater Inertness Results in Higher Analyte Response Another common probe used to illustrate inertness is 2,4-dinitrophenol (2,4-DNP), which functions as an indicator of acid compound interactions. It is used to monitor system suitability in semivolatiles methods, which benefit from the use of wool to assist in sample vaporization. As shown in Figure 2, the response of 2,4-DNP with the Sky® inlet liner, even at low concentrations, is superior to a competitor's liner. The competitor liner with wool has active sites that adsorb 2,4-DNP and reduce its response. In contrast, an excellent response is achieved using the Sky® liner, even in the presence of wool. Figure 2: The state-of-the-art deactivation used for Sky® liners with wool results in higher responses for active acid compounds, such as 2,4-DNP. Peaks 1. Acenaphthene (IS) 2. 2,4-DNP Column: Rxi®-5Sil MS, 15 m, 0.25 mm ID, 0.25 µm (cat.# 13620); Sample: 10 µg/mL each 2,4-dinitrophenol and acenaphthene standard in methylene chloride; Injection: Inj. Vol.: 1 µL splitless (hold 1 min); Liner: Comparison of Sky® Single Taper Inlet Liner with Wool (cat.# 23303.5) and Agilent Single Taper Inlet Liner with Wool (cat.# 5062-3587); Inj. Temp.: 250 °C; Detector: FID @ 300 °C. GC_EV1204 Comprehensive Deactivation Ensures Excellent Peak Shape In addition to providing excellent results for active pesticides and acidic compounds, Sky® inlet liners are also highly inert to active basic compounds, such as underivatized amphetamines. The exceptional inertness of Sky® liners produces much better peak shape than is typically seen on other liners, resulting in simpler quantification and more accurate results (Figure 3). Figure 3: Sky® liners are completely passivated. Even when using wool, peak shape for highly active underivatized amphetamine is excellent. Amphetamine Sky® liners reliably provide excellent peak shape and response for active basic compounds. Restek Sky® Inlet Liners SGE Peaks 1. Amphetamine Column: Rxi®-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623); Sample: Amphetamine; Diluent:1-chlorobutane; Conc.: ~10 µg/mL; Injection: Inj. Vol.: 1 µL splitless (hold 1 min); Liner: Comparison of Sky® Single Taper with Wool (cat.# 23303.5) and SGE Single Taper with Wool (cat.# 092019); Inj. Temp.: 250 °C; Purge Flow: 20 mL/min; Oven Temp: 45 °C to 250 °C at 20 °C/min; Carrier Gas: He, constant flow; Flow Rate: 2 mL/min; Detector: FID @ 350 °C.; Make-up Gas Flow Rate: 45 mL/ min; Make-up Gas Type: N2; Instrument: Agilent 7890A GC GC_CF1151 1-800-356-1688 or 1-814-353-1300 www.restek.com 3 Sky® Inlet Liners Liner-to-Liner Reproducibility: A Measure of Consistent Quality It’s not good enough to have one quality liner. You have to be confident that every liner will give the same level of performance. We test Sky® liners extensively to ensure that each one is exceptionally inert and will provide optimal results. Using endrin breakdown as a measure of reproducibility, the data in Figure 4, based on multiple lots, illustrate that Sky® liners are more consistently inert than competitor products. Sky® liners provide exceptional inertness across a wide range of active analytes. The consistent, comprehensive deactivation process results in the accuracy and precision you need for reliable trace-level analyses. Simplify liner selection with Sky® liners from Restek—choose blue, the best choice for dependable results. Figure 4: Sky® inlet liners from Restek consistently show less endrin breakdown than comparable liners from other sources. 35.00% Average % Endrin Breakdown 30.00% 25.00% 20.00% 15.00% Restek Sky® liners SGE liners 10.00% Agilent liners 5.00% 0.00% Liner by Vendor Error bars represent 3 standard deviations. Sky® inlet liners are easily recognizable for your reordering convenience. All Sky® liners come in specially marked boxes and are packaged in ultra-clean blister packs. 4 www.restek.com 1-800-356-1688 or 1-814-353-1300 Sky® Inlet Liners Sky® Inlet Liners for Shimadzu GCs Split Liners for Shimadzu 17A, 2010, and 2014 GCs ID OD x Length Similar to Shimadzu part # Sky 3.5 mm Split 3.5 mm 5.0 mm x 95 mm 221-41444-01 Sky 3.5 mm Split w/Wool ea. cat.# 5-pk. 25-pk. 23318.1 23318.5 23318.25 3.5 mm 5.0 mm x 95 mm 23319.1 23319.5 23319.25 3.5 mm 5.0 mm x 95 mm 23320.1 23320.5 Sky 3.5 mm Precision Liner w/Wool 3.5 mm 5.0 mm x 95 mm 23455.1 23455.5 Single Taper Precision Liner w/Wool NEW! 3.5 mm 5.0 mm x 95 mm 23456.1 23456.5 Cyclosplitter NEW! ea. cat.# 5-pk. 25-pk. 23321.1 23321.5 23321.25 Splitless Liners for Shimadzu 17A, 2010, and 2014 GCs ID OD x Length Similar to Shimadzu part # Sky 3.5 mm Single Taper 3.5 mm 5.0 mm x 95 mm 221-48335-01 3.5 mm 5.0 mm x 95 mm 23322.1 23322.5 Sky 3.5 mm Single Taper w/Wool 3.5 mm 5.0 mm x 95 mm 23457.1 23457.5 Double Taper ea. cat.# 5-pk. 25-pk. 23458.1 23458.5 23458.25 ea. cat.# 5-pk. 25-pk. 23435.1 23435.5 23435.25 ea. cat.# 5-pk. 23459.1 23459.5 Split/Splitless Liners for Shimadzu 17A, 2010, and 2014 GCs Split/Splitless w/Wool Liners for Shimadzu 17A PTV GCs PTV w/Wool DI Liners for Shimadzu 17A, 2010, and 2014 GCs Uniliner w/Wool ID OD x Length Similar to Shimadzu part # 3.5 mm 5.0 mm x 95 mm 221-41444-00 ID OD x Length Similar to Shimadzu part # 1.6 mm 4.0 mm x 95 mm 225-09212-01 ID OD x Length 3.5 mm 5.0 mm x 95 mm NEW! NEW! NEW! NEW! Also Available for Agilent, PerkinElmer, Thermo Scientific, and Bruker/Varian GCs www.restek.com/sky Patent pending 1-800-356-1688 or 1-814-353-1300 www.restek.com 5 Other Deactivations Intermediate Polarity (IP)–Deactivation • Phenylmethyl-deactivated surface for better recovery of polar and nonpolar compounds. • Compatible with most common solvents. • Our standard deactivation—every clear Restek liner is IP deactivated unless otherwise requested. Siltek®-Deactivation For Siltek®-deactivated inlet liners, add the corresponding suffix number to the liner catalog number. • • • • • • Siltek®-Deactivated Inlet Liners Maximizes the inertness of the sample pathway with proprietary deactivation. Minimizes breakdown. Low bleed. Thermally stable. “Clean and green”—manufactured without the use of harmful organic solvents. Ideal for chlorinated pesticides. The patented Siltek® deactivation process for liners produces a highly inert glass surface that features high temperature stability, extreme durability, and low bleed. Try Siltek® liners, guard columns, and connectors for better recovery of sample analytes. qty. each 5-pk. 25-pk. Siltek Liner -214.1 addl. cost -214.5 addl. cost -214.25 addl. cost Siltek Liner w/Wool -213.1 addl. cost -213.5 addl. cost -213.25 addl. cost Siltek Liner w/CarboFrit -216.1 addl. cost -216.5 addl. cost -216.25 addl. cost Base-Deactivation For base-deactivated inlet liners, add the corresponding suffix number to the liner catalog number. qty. each 5-pk. 25-pk. Base-Deactivated Liner -210.1 addl. cost -210.5 addl. cost -210.25 addl. cost Base-Deactivated Liner w/ Base-Deactivated Wool -211.1 addl. cost -211.5 addl. cost -211.25 addl. cost Base-Deactivated Liner w/CarboFrit -229.1 addl. cost -229.5 addl. cost -229.25 addl. cost Don’t Forget Routine Maintenance Inlet liners are the key to good injection port maintenance; changing them regularly helps prevent problems such as: Looking for the Best Solution? Sky® inlet liners, featuring a state-of-the-art deactivation, give you the inertness you need for accurate, reproducible trace-level results. • • • • • Sample degradation resulting in poor response. Sample adsorption resulting in poor peak shape (tailing). Sample discrimination. Irreproducibility. Extraneous peaks from contamination or cored septum particles. Finally, be sure to condition your liners at 20 °C higher than the operating inlet temperature for a minimum of 10 minutes to prepare them for use. By following these basic tips, you can avoid inlet problems and improve chromatographic performance. See pages 1–5 for details. 6 www.restek.com 1-800-356-1688 or 1-814-353-1300 Other Inlet Liners Split Liners for Shimadzu 14A GCs ID* OD x Length Similar to Shimadzu part # 3.5 mm 5.0 mm x 99 mm 221-32544-01 ea. cat.# 5-pk. 25-pk. 20860 20861 20862 3.5 mm 5.0 mm x 99 mm 20870 20871 3.5 mm 5.0 mm x 99 mm 20868 20869 high MW compounds Splitless Liners for Shimadzu 14A GCs Benefits/Uses: ID* OD x Length Similar to Shimadzu part # ea. cat.# 5-pk. 25-pk. 20864 20865 trace samples 3.5 mm 5.0 mm x 99 mm 20863 3.5 mm Splitless 221-32544-00 Split Liners for Shimadzu 17A, 2010, and 2014 GCs Benefits/Uses: ID* OD x Length Similar to Shimadzu part # ea. cat.# 5-pk. 25-pk. 20976 20977 20978 22283 22284 22285 Split Cyclosplitter Laminar Cup Splitter 1 mm Split 3.5 mm Split Benefits/Uses: universal, for most common analyses dirty samples, many injections before cleaning required purge & trap, fast GC universal, for most common analyses 1.0 mm 5.0 mm x 95 mm 3.5 mm 5.0 mm x 95 mm 221-41444-01 2.0 mm dirty samples, trace samples 5.0 mm x 95 mm 22171 22172 2 mm Split Precision Liner w/Deact. Wool 3.5 mm dirty samples, trace samples 5.0 mm x 95 mm 21020 21021 3.5 mm Split Precision Liner w/Deact. Wool 3.5 mm dirty samples, trace samples 5.0 mm x 95 mm dirty samples, many injections 3.5 mm before cleaning required 5.0 mm x 95 mm 22173 22174 22072 22073 ea. cat.# 5-pk. 22276 22277 22286 22287 22274 22275 ea. cat.# 5-pk. 25-pk. 20955 20956 20957 3.5mm Single Taper Precision Liner w/Deact. Wool Cyclosplitter Splitless Liners for Shimadzu 17A, 2010, and 2014 GCs Benefits/Uses: ID* OD x Length 3 mm Single Taper Splitless universal, trace samples 2.0 mm 5.0 mm x 95 mm 3.5 mm Single Taper Splitless universal, trace samples reduces backflash and catalytic decomposition Double Taper Splitless Split/Splitless Liners for Shimadzu 17A, 2010, and 2014 GCs Split/Splitless w/Deact. Wool Benefits/Uses: universal, for most common analyses 3.5 mm 5.0 mm x 95 mm Similar to Shimadzu part # 221-48335-01 3.5 mm 5.0 mm x 95 mm ID* OD x Length Similar to Shimadzu part # 3.5 mm 5.0 mm x 95 mm 221-41444-00 *Nominal ID at syringe needle expulsion point. All liners are shipped with intermediate polarity (IP) deactivation unless otherwise requested. See page 6. 1-800-356-1688 or 1-814-353-1300 www.restek.com 7 Other Inlet Liners SPME Liner for Shimadzu 17A, 2010, and 2014 GCs SPME Liner Liners for Shimadzu 17A PTV GCs Benefits/Uses ideal for low volume SPME applications Benefits/Uses trace, dirty, high & low MW active samples 17A PTV Liner w/Deact. Wool DI Liners for Shimadzu 17A, 2010, and 2014 GCs (0.25/0.32/0.53 mm ID) Uniliner w/Deact. Wool Open-Top Drilled Uniliner (hole near top) Open-Top Drilled Uniliner (hole near bottom) Single Taper Drilled Uniliner (hole near top) Single Taper Drilled Uniliner (hole near bottom) Benefits/Uses trace, dirty, high MW active samples, high recovery & linearity trace, active samples, high recovery & linearity trace, active samples, high recovery & linearity trace, active samples, high recovery & linearity trace, active samples, high recovery & linearity ID* OD x Length ea. cat.# 5-pk. 22278 22279 ea. cat.# 5-pk. 25-pk. 21705 21706 21707 ea. cat.#/price 5-pk. 3.5 mm 5.0 mm x 95 mm 21713 21719 3.5 mm 5.0 mm x 95 mm 21285 21286 3.5 mm 5.0 mm x 95 mm 21287 21288 3.5 mm 5.0 mm x 95 mm 21289 21290 3.5 mm 5.0 mm x 95 mm 21291 21292 0.75 mm 5.0 mm x 95 mm ID* OD x Length Similar to Shimadzu part # 1.6 mm 4.0 mm x 95 mm 225-09212-01 ID* OD x Length *Nominal ID at syringe needle expulsion point. All liners are shipped with intermediate polarity (IP) deactivation unless otherwise requested. See page 6. tech tip Drilled Uniliner® Liners Use the Drilled Uniliner® liner with the hole near the bottom for semivolatile analysis or when compounds of interest could be affected by a tailing solvent peak. Use the Drilled Uniliner® liner with the hole near the top for chlorinated pesticides analysis, aqueous injections, as well as analyses in which the compounds of interest elute away from the solvent peak. Restek can provide any of the liners shown deactivated by one of three processes, including highly inert Siltek® coating. Ordering information is on page 6. Packing materials, including wool and CarboFrit® inserts, can be provided in any liner—subject to the liner ID and geometry. Ordering information is on page 9. Siltek® Treated Liners Siltek® Treated Metal Inlet Liners for Shimadzu GCs • Won’t crack, chip, or break like glass liners. • Excellent response for pesticides, phenols, and other active compounds. Liner Type (3.5 mm ID x 5.0 mm OD x 95 mm) 95 mm Split/Splitless w/Deact. Wool, Siltek, Metal 8 www.restek.com qty. 5-pk. cat.# 21003 price 1-800-356-1688 or 1-814-353-1300 Inlet Liner Packing Materials CarboFrit® Inlet Liner Packing Material Deactivated Wool 24324 • More inert than our traditional fused silica wool. • Use to vaporize a sample in a liner prior to introduction into a capillary column. Description Deactivated Wool qty. 10 grams cat.# 24324 • Highly inert. • Extends analytical column lifetime. • Enhances reproducibility of split and splitless injections. • Uniform pore size and consistent packing density guarantee consistent flow through the liner. • Easy to install in any liner with an ID > 3.5 mm when using puller-inserter tool listed below.* Add the corresponding suffix number to the liner catalog number. qty. ea. 5-pk. 25-pk. suffix -209.1 -209.5 -209.25 addl. cost addl. cost addl. cost *Liners with IDs less than 3.5 mm are difficult to pack. We will pack them on a custom basis (minimum neck ID of 2 mm required). Replacement CarboFrit® Inserts Description Frits for liner ID ≤ 4 mm Frits for liner ID > 4 mm qty. 10-pk. 10-pk. cat. # 20295 20294 20999 Base-Deactivated Wool Ideal for amines and other basic compounds. Description Base-Deactivated Wool qty. 10 grams cat.# 20999 21642 Prepacked Inlet Liners Let Restek do the work! Just add the appropriate suffix to the liner catalog number. qty. ea. 5-pk. 25-pk. Wool -200.1 -200.5 -200.25 CarboFrit† -209.1 -209.5 -209.25 addl. cost addl. cost addl. cost CarboFrit® Puller/Inserter Tool • Hook end for removing CarboFrit® inserts. • Bent end (90°) for inserting CarboFrit® inserts. Description CarboFrit Puller/Inserter Tool qty. ea. cat.# 21642 †CarboFrit® inserts require a neck greater than 2 mm. tech tip Use of Packings With an Autosampler We recommend using an injection port liner with wool or CarboFrit® packing when making injections with an autosampler. If there is no packing material in the liner, the solvent droplets act like water on a hot iron: they bounce around until vaporized (Leidenfrost phenomenon). Because autosamplers make rapid injections, samples can be incompletely vaporized, leading to nonreproducible peak response and tailing. You can prevent this by using wool or CarboFrit® packing material in the splitless liner to provide a surface for the solvent droplets to “sit” on until the heat from the injector vaporizes them. 1-800-356-1688 or 1-814-353-1300 www.restek.com 9 Inlet Liner Accessories 20181 20114 No more burned fingers! Inlet Liner Removal Tool Mini Wool Puller/Inserter Insert and remove wool plugs easily. Order a spare pack so you’ll always have one available. • Easily remove liner from injector—no more burned fingers. • Made from high-temperature silicone. • Won’t chip or crack the liner. Description Inlet Liner Removal Tool Description Mini Wool Puller/Inserter qty. 2-pk. qty. 3-pk. cat.# 20114 cat.# 20181 26262 26261 Eliminates user variation! The Claw and The Claw Holder Kit Inlet Liner Packing Tool • Easily removes hot liners from injection ports. • 4 mL vials (not included) can be replaced when dirty. • Position wool reproducibly every time. • Accurate to a specific, measured depth. • Can be used with all manufacturers' liners. Never again will you burn your fingers removing a hot injection port liner. The Claw safely and cleanly removes liners, O-rings, or other small objects from the injection port. You can then place the hot objects in a clean 4 mL vial situated in The Claw holder until ready for reuse. Description The Claw The Claw Holder Kit (includes The Claw and holder) WISP 48 Snap Seal Vial Loosen the nut on the side of the tool and adjust the gauge to the manufacturer’s recommended depth. Place a plug of loosely bound wool at the top of the inlet liner. Description Inlet Liner Packing Tool Recommended for inlet liners with an ID ≥ 2 mm. 10 www.restek.com Insert the liner packing tool into the liner until the tool bottoms out. Remove the tool. The wool is now positioned correctly in the liner and the liner is ready for use. qty. ea. cat.# 20339 qty. ea. kit 100-pk. cat. # 26261 26262 24658 tech tip Injector Maintenance Approximately ninety percent of “bad” chromatography is traceable to problems in the injection port. These problems include contaminated carrier gas, incorrect injector flows, active or dirty sites on inlet seals and liners, improper use of wool, leaks, backflash, discrimination, incorrect injector temperature, poor column installation, and use of the wrong injection technique. To minimize injection port problems, set up a routine maintenance schedule and be sure to investigate the injector first when troubleshooting. 1-800-356-1688 or 1-814-353-1300 O-Rings, Septa, Seals Septum Nut for Shimadzu 17A, 2010, and 2014 GCs Viton® O-Rings for Shimadzu 17A, 2010, and 2014 GCs Description Max. temp. Similar to Shimadzu part # qty. cat.# Viton O-Rings for Shimadzu 17A, 2010, and 2014 GCs 250 °C 036-11203-84 10-pk. 24899 Graphite O-Rings for Split Liners Graphite O-Rings for Splitless Liners Max. temp. 450 °C 450 °C qty. cat.# 221-41286-00, 22144584-00 ea. 22079 qty. kit cat.# 21895 kit 22331 Injector Nut Kit for Shimadzu 17A, 2010, and 2014 GCs for Shimadzu 2010 and 2014 GCs Description Similar to Shimadzu part # Description Septum Nut for Shimadzu 17A, 2010, and 2014 GCs Graphite O-Rings Similar to Shimadzu part # 221-48393-91 221-47222-91 qty. cat.# 5-pk. 5-pk. 20243 20244 Includes 17A injector nut, 0.4 mm graphite ferrule, and 1/16-inch stainless steel capillary nut. Description Injector Nut Kit for Shimadzu 17A, 2010, and 2014 GCs Siltek Treated Injector Nut Kit for Shimadzu 17A, 2010, and 2014 GCs Capillary Nut for Shimadzu 17A, 2010, and 2014 GCs Septa (Plug) for Shimadzu GCs Thermolite Septa usable to 340 °C inlet temp. qty. cat.# 25-pk. 27153 50-pk. 27154 100-pk. 27155 • One-piece design for ease of installation and removal. • Made of clear anodized aluminum and high-quality stainless steel. IceBlue Septa usable to 250 °C inlet temp. qty. cat.# 50-pk. 27170 100-pk. 27171 Premium Non-stick BTO Septa* usable to 400 °C inlet temp. qty. cat.# 50-pk. 27098 100-pk. 27099 *Minimum recommended operating temperature for Premium Non-Stick BTO septa is 250 °C. Note: Due to differences in inlet design, the actual septum temperature for a given inlet setpoint can vary by manufacturer. Merlin Microseal Septa for Shimadzu GCs • Compatible with Shimadzu models GC-2010 and GC-2025 only. • 450 °C maximum injection port temperature. • For use with 23-gauge (0.63 mm, 0.025") needle or probe with blunt, truncated conical tip. 1-800-356-1688 or 1-814-353-1300 Description Capillary Nut for Shimadzu 17A, 2010, and 2014 GCs Similar to Shimadzu part # qty. cat.# 221-41533-00 2-pk. 22688 Restek Enhanced Capillary Nut for Shimadzu 17A, 2010, and 2014 GCs • Restek’s design eliminates the slot, increasing lifetime and durability. • Meets or exceeds original manufacturer's performance. no slot Description Restek Enhanced Capillary Nut for Shimadzu 17A, 2010, and 2014 GCs Similar to Shimadzu part # qty. cat.# 221-41533-00 2-pk. 20375 qty. 10-pk. cat.# 21121 qty. cat.# 10-pk. 10-pk. 10-pk. 24827 24828 24829 5 mm Ferrules for Shimadzu 17A GCs A Merlin Microseal septum provides several distinct advantages: elimination of septum coring, long lifetime, and consistently low needle-insertion force. The Microseal septum incorporates two separate sealing mechanisms; these sliding seals prevent septum coring and the associated accumulation of septum crumbs in the injection port liner. Installation is simple, requiring no modification of the injection port. Description General Purpose Kit for Shimadzu GCs (3 to 100 psi) Includes: Nut, Adapter, O-Ring, & 2 General-Purpose (#410) Microseals Replacement Microseals General Purpose Microseal (most applications, 3 to 100 psi) Low-Pressure Microseal (1 to 45 psi) Microseal for SPME Applications (3 to 100 psi) slot Meets original manufacturer's performance. Merlin # cat.# 61-12 22972 410 22812 310 21-01 22815 22782 • For use with packed columns. • Graphite construction. Description 5 mm Ferrules for Shimadzu 17A GCs Graphite Ferrules for Shimadzu 17A, 2010, and 2014 GCs • Graphite 2-piece construction. • Available in 0.4, 0.5, and 0.8 mm sizes. • Packaged on mandrel for easy handling. Ferrule ID Fits Column ID 0.4 mm 0.5 mm 0.8 mm 0.25 mm and less 0.32 mm 0.53 mm Similar to Shimadzu part # 220-90765-00 221-32126-05 221-32126-08 www.restek.com 11 Leak Detector Restek Electronic Leak Detector Don’t let a small leak turn into a costly repair—protect your instrument and analytical column by using a Restek Leak Detector. Features & benefits include: • • • • • • • • • Optimized sample flow path. Ergonomic, handheld design. Rugged side grips for added durability. Handy probe storage for cleanliness and convenience. Long-lasting battery; up to 6 hours of continuous use. Automatic shutoff. A convenient carrying and storage case. Easy-to-clean probe assembly. A universal charger set (U.S., European, UK, and Australian plugs included). Backed by a 1-year warranty, the Restek Leak Detector is the industry standard for performance and affordability in handheld leak detectors. 22839 restek recommends When your Leak Detector batteries need to be replaced, send the unit to us for a routine maintenance review to ensure continued sensitivity and reliability. We will replace not only the batteries, but also the probe and internal/external tubing. We will also recertify your unit. Contact Customer Service to send in your Leak Detector for maintenance (cat. #22839-R). Leak Detector Facts Detectable Gases: Battery: Operating Temperature Range: Humidity Range: Warranty: Certifications: Compliance: Helium, nitrogen, argon, carbon dioxide, hydrogen Rechargeable Ni-MH internal battery pack (6 hours normal operation) 32–120 °F (0–48 °C) 0–97% One year CE, Ex, Japan WEEE, RoHS Limits of Detection These gases can be detected with the Restek Electronic Leak Detector at the following leak rates: Minimum Detectable Gas Limits and Indicating LED Color: • Helium, 1.0 x 10-5, red LED • Hydrogen*, 1.0 x 10-5, red LED • Nitrogen, 1.4 x 10-3, yellow LED • Argon, 1.0 x 10-4, yellow LED • Carbon Dioxide, 1.0 x 10-4, yellow LED Gas detection limits measured in atm cc/sec Carrying/storage case included with purchase of unit. Description Leak Detector With Hard-Sided Carrying Case and Universal Charger Set (U.S., UK, European, Australian) Leak Detector Routine Maintenance Review Soft-Side Storage Case Small Probe Adaptor qty. cat.# ea. 22839 ea. ea. ea. 22839-R 22657 22658 Avoid using liquid leak detectors on a GC! Liquids can be drawn into the system. *Caution: The Restek Electronic Leak Detector is designed to detect trace amounts of hydrogen in a noncombustible environment. It is NOT designed for determining leaks in a combustible environment. A combustible gas detector should be used for determining combustible gas leaks under any condition. When using it to detect hydrogen, the Restek Electronic Leak Detector may only be used for determining trace amounts in a GC environment. Checking for leaks maintains the integrity of a GC system. 22658 Verify hard-to-reach leaks using the small probe adaptor (sold separately). 12 www.restek.com 1-800-356-1688 or 1-814-353-1300 Flowmeter Restek ProFLOW 6000 Electronic Flowmeter State-of-the-art features include: • Measures volumetric flow for gases across a range of 0.5–500 mL/min. • NIST traceable calibration. • Ex rating (electrical apparatus for explosive gas atmospheres) for hydrogen and related gas types. • Accuracy of ± 2% of flow reading or ± 0.2 mL/min, whichever is greater. • Over-range warning indicator. • Auto shutoff feature. • Use as a benchtop or handheld unit. • Ergonomic design and side grips for comfort. • Measures most gas types.* • Convenient carrying/storage case included. • Uses 2-AA batteries (included). • Data output via USB port. • 1-year warranty. • Recalibration service available. Flowmeters that can measure flammable gases are becoming mandatory, due to the increased use of hydrogen in chromatography. With its Ex rating, the Restek ProFLOW 6000 Flowmeter is designed specifically with explosive and flammable gases in mind. The Restek ProFLOW 6000 is the only flowmeter you need for any type of chromatography gas measurement because of its wide range of capabilities. The ProFLOW 6000 is an electronic device capable of measuring volumetric flow for most gases. Real-time measurements can be made for various types of flow paths, including continually changing gas types. This portable unit is designed for easy handheld use, and the stand adds benchtop convenience. Flowmeter Facts: Type of Flowmeter: Battery: Operating Temp. Range: Warranty: Certifications: Compliance: 22656 restek recommends Recalibrate your ProFLOW 6000 Flowmeter once every year. Prolonged failure to recalibrate your unit may result in increased error. To always get the most accurate flow measurements, contact Customer Service to send in your flowmeter for recalibration (cat.# 22656-R). Volumetric 2-AA 32–120 °F (0–48 °C) One year CE, Ex WEEE, RoHS Description Restek ProFLOW 6000 Electronic Flowmeter With Hard-Sided Carrying Case ProFLOW 6000 Recalibration Service Soft-Side Storage Case qty. ea. ea. ea. cat.# 22656 22656-R 22657 *The flowmeter is designed to measure clean, dry, non-corrosive gases. 1-800-356-1688 or 1-814-353-1300 www.restek.com 13 Super-Clean Gas Filters Restek Super-Clean Gas Filters • • • • • High-purity output ensures 99.9999% pure gas (at max. flow of 2 L/min). “Quick connect” fittings for easy, leak-tight cartridge changes. Glass inside to prevent diffusion; polycarbonate housing outside for safety. All traps measure 10 5/8" x 1 3/4" (27 x 4.4 cm). Each base plate unit measures 4" x 4" x 1 7/8" (10.2 x 10.2 x 4.8 cm). Table I: Each Super-Clean gas filter provides high-purity outlet gas. 22022 did you know? All Restek SuperClean gas filter cartridges (except hydrocarbon filter cat.# 22030) feature easy-to-read indicators. The indicator code is shown on every trap, so there is no confusion about when to replace it. Type of Filter Outlet Gas Quality (%) Maximum Pressure/ Maximum Flow Rates Use for: Inert carrier gas Air Hydrogen Yellow/orange to clear 7.2 — — >2 Indicator Color Change H2O (g) Estimated Capacity Lifetime O2 (mL) Hydrocarbons (g) (years) Moisture cat.# 22028 >99.9999 11 bar 159 psi/ 7 L/min Oxygen cat.# 22029 >99.9999 11 bar 159 psi/ 7 L/min Inert carrier gas Green to grey NA 1,000 — >2 Hydrocarbons cat.# 22030 >99.9999 11 bar 159 psi/ 7 L/min Inert carrier gas Air Hydrogen No indicator NA — 123 >2 Fuel Gas1 cat.# 22022 >99.9999 11 bar 159 psi/ 7 L/min Inert carrier gas Air Hydrogen Yellow/orange to clear 3.5 — 243 >1.5 Triple2 cat.# 22020 >99.9999 11 bar 159 psi/ 7 L/min Inert carrier gas Yellow/orange to clear Green to grey 1.8 500 43 >1 Helium Specific2 cat.# 21982 >99.9999 11 bar 159 psi/ 7 L/min Helium Yellow/orange to clear Green to grey 1.8 500 — >1 Removes hydrocarbons and moisture. Removes hydrocarbons, moisture, and oxygen. 3 As n-butane. 1 2 22020 21982 base plate Restek Super-Clean Gas Filter Kits and Replacements Description Carrier Gas Cleaning Kit Includes: mounting base plate, 1/8" inlet/outlet fittings, and oxygen/moisture/hydrocarbon triple gas filter Fuel Gas Purification Kit Includes: mounting base plate, 1/8" inlet/outlet fittings, and hydrocarbon/moisture fuel gas filter Ultra-High Capacity Hydrocarbon Filter Ultra-High Capacity Moisture Filter Ultra-High Capacity Oxygen Filter Replacement Triple Gas Filter (removes oxygen, moisture, and hydrocarbons) Replacement Fuel Gas Filter (removes moisture and hydrocarbons) Helium-Specific Carrier Gas Cleaning Kit Includes: mounting base plate, 1/8" inlet/outlet fittings, and oxygen/moisture/hydrocarbon helium-specific filter Replacement Helium-Specific Gas Filter (removes oxygen, moisture, and hydrocarbons) Gas Filter Bundle Kit Includes: one triple gas filter (cat.# 22020) and two fuel gas filters (cat.# 22022) qty. cat.# kit 22019 kit 22021 ea. ea. ea. ea. ea. 22030 22028 22029 22020 22022 kit 21983 ea. 21982 kit 22031 tech tip Oxygen and Moisture Traps Restek highly recommends oxygen and moisture traps for make-up gas when operating sensitive detectors such as electron capture detectors (ECD). The hydrogen reaction gas for sensitive electrolytic conductivity detectors (ELCD) also requires a hydrocarbon trap to remove trace impurities. 14 www.restek.com 1-800-356-1688 or 1-814-353-1300 Scoring Wafer with Handle Septum Puller • Ceramic wafer is straightedged for cutting fused silica tubing cleanly. • Unique, ergonomic handle is made of soft, comfortable rubber. • Use hooked end for removing septa and O-rings; pointed end works well for removing stuck ferrules or debris. • Keep several on hand in your laboratory—can be used in many different ways. 23015 Remove a septum without damaging an expensive weldment. Hold tubing firmly in one hand, allowing about two inches to extend freely. Hold the scoring wafer at a 45° angle to the tubing. Exert just enough pressure to put a slight arc in the tubing. Pull perpendicularly across the tubing. The tubing should fall off on its own, or it should easily break at the score with a slight tap of the wafer. Description Scoring Wafer with Handle Check the cut against the white of the scoring wafer. Look for a clean, square cut. Make Life Easier! qty. 2-pk. Dislodge a stuck ferrule quickly and easily—without scoring the fitting. Description Septum Puller MLE 20117 Tools qty. ea. cat.# 20117 save money! Save money on column installation tools by purchasing the MLE Capillary Tool Kit. See page 16. cat.# 23015 27194 Ceramic Scoring Wafer • Four straight scoring edges for cutting fused silica tubing and four serrated edges for cutting MXT® metal capillary columns. GC-MS Cleaning Kit 20116 The Restek GC-MS Cleaning Kit (cat.#s 27194, 27195) includes: • lint-free nylon gloves (small-2 pair) • lint-free nylon gloves (large-2 pair) • lint-free cotton cloth, 9 x 9 (10-pk.) • micro mesh 4 x 6 sheet (4-pk.) • aluminum oxide (1-kg jar) • cotton tip applicators • tweezers, large • tweezers, small • septum puller • Dremel® tool, battery-operated (optional, 27194) • tool kit bag Reorder Kit (cat.# 27196) includes: • lint-free nylon gloves (small-2 pair) • lint-free nylon gloves (large-2 pair) Exert just enough pressure to put a slight arc in the tubing. Pull perpendicularly across the tubing. The tubing should fall off or break with a slight tap of the wafer. Description Ceramic Scoring Wafers 1-800-356-1688 or 1-814-353-1300 Check the cut against the white of the scoring wafer. Look for a clean, square cut. qty. 5-pk. cat.# 20116 • lint-free cotton cloth, 9 x 9 (10-pk.) • micro mesh 4 x 6 sheet (4-pk.) Poor sensitivity, loss of sensitivity at high masses, or high multiplier gain during an auto tune are all indicators that your mass spectrometer source may need to be cleaned. Restek has assembled all of the necessary components for cleaning and polishing your ion source. Description Mass Spec Cleaning Kit with Dremel Tool Mass Spec Cleaning Kit without Dremel Tool Mass Spec Cleaning Kit Replacement Parts Kit Includes: cloths, micro mesh sheets, small and large gloves qty. kit kit cat.# 27194 27195 kit 27196 www.restek.com 15 Tools 21159 MLE Make Life Easier! Injector Wrench for Shimadzu 17A, 2010, and 2014 GCs • Designed specifically for removing Shimadzu injection ports. • High-quality stainless steel construction. Description Injector Wrench for Shimadzu 17A, 2010, and 2014 GCs Similar to Shimadzu part # qty. cat.# 221-46977-00 ea. 21159 22182 Everything you need in one complete kit! Make Life Easier (MLE) Capillary Tool Kit for Shimadzu GCs 22333 Capillary Installation Gauge for Shimadzu 17A, 2010, and 2014 GCs • Seats ferrule* onto column for consistent installations. • Prevents crushed column ends. • Made from high-quality stainless steel. Description Capillary Installation Gauge for Shimadzu 17A, 2010, and 2014 GCs qty. cat.# ea. 22333 *For use with graphite ferrules only. Includes: • capillary installation gauge for Shimadzu GCs • injector wrench for Shimadzu GCs • 1/8", 3/16", and 1/4" nylon brushes • 1/4", 3/8", and 3/16" stainless steel wire tube brushes • stainless steel surface brush • 6 stainless steel jet reamers (0.25–0.65 mm OD) • 1/4" x 5/16" open end wrench • 3/8" x 7/16" open end wrench • 6 mm x 7 mm open end wrench • 8 mm x 10 mm open end wrench • 16 mm x 17 mm open end wrench • rubber-tipped slide-lock tweezers Description MLE Capillary Tool Kit for Shimadzu GCs • • • • • • • • • • • • scoring wafers inlet liner removal tool septum puller mini wool puller/inserter tool 4-inch tapered needle file swivel head flashlight mini hand drill set 15 cm compact steel ruler pocket magnifier high-temperature string (1 meter) pipe cleaner (12 inch) cotton tip swabs (pk. of 25) qty. kit cat.# 22182 also available Shimadzu FID Jets Please contact Customer Service or your Restek representative for details. 22334 Open-End Wrench Set for use with Shimadzu 17A, 2010, and 2014 Capillary Installation Gauge Description 1/4" x 5/16" and 10 mm x 11 mm Open-End Wrench Set for use with Shimadzu 17A, 2010, and 2014 Capillary Installation Gauge 16 www.restek.com qty. cat.# ea. 22334 1-800-356-1688 or 1-814-353-1300 Ferrules Vespel® Ferrules • 100% high-temperature polyimide. • Stable to 350 °C. • Durable, leak-tight. tech tip Graphite Ferrules • • • • • Vespel® ferrules Preconditioned to eliminate out-gassing. High-purity, high-density graphite. Smoother surface and cleaner edges than conventional graphite ferrules. Contain no binders that can off-gas or adsorb analytes. Stable to 450 °C. Vespel®/Graphite Ferrules • 60%/40% Vespel®/graphite blend offers the best combination of sealing and ease of workability. • Seal with minimal torque, reusable, and preferred for vacuum and high-pressure uses. • Stable to 400 °C. • Recommended for mass spec transfer lines. Choosing the Right Ferrule Graphite ferrules are soft, easy to seal, stable to 450 °C, and contain no binders that might off-gas. Vespel®/graphite ferrules work better for vacuum and high-pressure applications (e.g., GC-MS) because they will not fragment or allow oxygen to permeate into the system, whereas graphite ferrules will. Because Vespel® and graphite ferrules are made from a harder material, they might require retightening after several temperature cycles. Alumaseal® ferrules are ideal for GC-MS. They will not crack or fragment and require no retightening after temperature cycles. Capillary Ferrules for 1/16-Inch Compression-Type Fittings Available in Vespel®, graphite, or Vespel®/graphite material. Ferrule ID 0.3 mm 0.4 mm 0.4 mm 0.5 mm 0.5 mm 0.6 mm 0.8 mm 0.8 mm 1.0 mm 1.2 mm 1.6 mm Fits Column ID 0.10/0.15/0.18/0.25/0.28 mm 0.10/0.15/0.18/0.25/0.28 mm 0.32 mm 0.32 mm 0.28 mm** 0.45/0.53 mm 0.45/0.53 mm 0.75 mm* 0.75 mm* 1.00 mm* qty. 10-pk. 10-pk. 50-pk. 10-pk. 50-pk. 10-pk. 10-pk. 50-pk. 10-pk. 10-pk. 10-pk. Vespel 22213 22214 — 22215 — — 22216 — 22217 22218 — Graphite 20233 20200 20227 20201 20228 — 20202 20224 21058 — 21060 Vespel/Graphite 20275 20211 20229 20212 20231 20232 20213 20230 24912 — — graphite ferrules *For micropacked columns. **For 0.28 mm MXT columns. Encapsulated Ferrules for 1/16-Inch Compression Fittings • Reusable—will not deform and stick in fittings. • Less torque needed to seal ferrule. • Restek’s unique blend of graphite minimizes fragmentation and out-gassing. Ferrule ID 0.4 mm 0.5 mm 0.8 mm Fits Column ID 0.25 mm 0.32 mm 0.53 mm qty. 10-pk. 10-pk. 10-pk. cat.# 21036 21037 21038 graphite ferrules Standard Ferrules for 1/16-, 1/8-, and 1/4-Inch Fittings Available in Vespel®, graphite, or Vespel®/graphite material. Fitting Size 1/4" 1/16" 1/8" 1/8" 1/4" 1/4" 1/4" Ferrule ID 3/16" 1/16" 1/8" reduce to 1/16" 1/4" reduce to 1/8" reduce to 1/16" 1-800-356-1688 or 1-814-353-1300 qty. 5-pk. 10-pk. 10-pk. 10-pk. 10-pk. 10-pk. 10-pk. Vespel — 22210 22211 — 22212 22219 — Graphite — 20207 20208 20209 20210 20225 20226 Vespel/Graphite 20258 20218 20219 20220 20221 20222 20223 graphite ferrules www.restek.com 17 Ferrules Two-Hole Ferrules for 1/8-Inch and 1/16-Inch Compression-Type Fittings Fitting Size 1/16" 1/16" 1/8" Ferrule ID 0.4 mm 0.5 mm 0.8 mm Fits Column ID 0.25/0.28 mm 0.32 mm 0.45/0.53 mm qty. 5-pk. 5-pk. 5-pk. Vespel/Graphite 24848 24849 20246 Graphite 20205 20205 20206 20203 20203 20204 Vespel/Graphite 20254 20255 20215 — 20257 20217 Reducing Ferrules Available in graphite or Vespel®/graphite material. Fitting Size 1/8" 1/8" 1/8" 1/4" 1/4" 1/4" Ferrule ID 0.4 mm 0.5 mm 0.8 mm 0.4 mm 0.5 mm 0.8 mm Fits Column ID 0.25 mm 0.32 mm 0.53 mm 0.25 mm 0.32 mm 0.45/0.53 mm qty. 5-pk. 5-pk. 5-pk. 5-pk. 5-pk. 5-pk. Blank Ferrules for 1/16-Inch Fittings Fitting Size 1/16" Ferrule ID no hole qty. 10-pk. Vespel/Graphite 20240 Alumaseal® Ferrules restek innovation! Alumaseal® Ferrules • Will not crack or fragment. • Excellent for GC-MS. 18 www.restek.com • • • • Aluminum construction—will not crack or fragment. No retightening required after temperature cycles—excellent for GC-MS. Eliminate out-gassing and make leak-tight seals for less detector noise. Unique two-piece design permanently locks on fused silica tubing without causing breakage. • Will not stick in fittings, unlike Vespel® or graphite ferrules. • Stable to 550 °C. • Use with any 1/16" compression-type fitting. Ferrule ID 0.4 mm 0.5 mm 0.8 mm Fits Column ID 0.25 mm 0.32 mm 0.53 mm qty. 10-pk. 10-pk. 10-pk. cat.# 21472 21473 21474 1-800-356-1688 or 1-814-353-1300 Ferrules PTFE Ferrules • Upper temperature limit 250 °C. • 100% PTFE; completely inert. • One-piece design requires no back ferrule. Fitting Size 1/16" 1/16" 1/16" 1/16" 1/8" 3/16" 1/4" Ferrule ID 1/16" 0.4 mm 0.5 mm 0.8 mm 1/8" 3/16" 1/4" qty. 10-pk. 10-pk. 10-pk. 10-pk. 10-pk. 10-pk. 10-pk. cat.# 21122 21123 21124 21125 21126 21127 21128 qty. 10-pk. cat.# 21121 qty. cat.# 10-pk. 10-pk. 10-pk. 24827 24828 24829 5 mm Ferrules for Shimadzu 17A GCs • For use with packed columns. • Graphite construction. Description 5 mm Ferrules for Shimadzu 17A GCs Graphite Ferrules for Shimadzu 17A, 2010, and 2014 GCs • Graphite 2-piece construction. • Available in 0.4, 0.5, and 0.8 mm sizes. • Packaged on mandrel for easy handling. Ferrule ID Fits Column ID 0.4 mm 0.5 mm 0.8 mm 0.25 mm and less 0.32 mm 0.53 mm Similar to Shimadzu part # 220-90765-00 221-32126-05 221-32126-08 also available Restek now carries Swagelok® fittings in brass & stainless steel. See pages 32–33. 1-800-356-1688 or 1-814-353-1300 www.restek.com 19 Connectors Vu2 Union® Connectors Fit both Restek cage designs. • Connect a guard column to an analytical column. • Connect a column to a transfer line. • Connect two columns in series. • Repair a broken column. • Fit both Restek cage designs. Restek’s Vu2 Union® connector combines the simplicity of a Press-Tight® union with the strength of a metal union. A guard column connected to an analytical column by a Vu2 Union® connector. injector detector Vu2 Union® connector analytical column guard column How does a Vu2 Union® connector work? A Press-Tight® union in the Vu2 Union® connector joins the fused silica tubing ends together; the ferrule and knurled nut at each end of the connector hold the tubing in place via a secondary seal between the ferrule and the Press-Tight® union. Each knurled nut applies independent pressure to each ferrule to make leak-tight seals with the column ends. These ultra-strong connections will not unexpectedly disconnect under temperature changes, vibrations, or other stresses normally encountered in GC analyses. The open design allows visual confirmation of the seal between the column and the Press-Tight® union to ensure confidence in the connection. Hang the connector from the column cage to minimize stress on the connections. Secure, reliable column-to-column connections! Who will benefit from using Vu2 Union® connectors? Any analyst using guard columns, transfer lines, or restrictor tubing; performing a dual-column analysis with columns connected in series; or seeking to repair a broken column will find Vu2 Union® connectors the simple, reliable, easy-to-use solution to their connection needs. The Vu2 Union® connector's open design allows visual confirmation of the seal; secondary seals ensure leak-tight connections. NOTE: This product is not recommended for GC columnto-MS connections—use the Vacuum Vu-Union® union for this type of connection. knurled nut fused silica column, guard column, or transfer line hanger body ferrule Press-Tight® connector Kits include: Vu2 Union® body, 2 knurled nuts, 2 Press-Tight® unions, and 4 ferrules Description Vu2 Union Connector Kit Vu2 Union Connector Kit Vu2 Union Connector Kit Vu2 Union Connector Kit Knurled nut 20480 20400 Ferrules Fit Column ID 0.10–0.15 mm 0.18–0.28 mm 0.32 mm 0.45–0.53 mm qty. kit kit kit kit 2-pk. cat.# 22220 21105 21106 21107 21108 25-pk. 20401 20430 20449 100-pk.e 20402 Graphite 2-pk./ 22221 20280 20282 20284 Graphite 10-pk./ 22222 20281 20283 20285 Universal Press-Tight® Connectors Description Universal Press-Tight Connectors Universal Press-Tight Connectors, Deactivated Universal Press-Tight Connectors, Siltek Deactivated 5-pk. 20400 20429 20480 Graphite Ferrules for Vu2 Union® Connectors • • • • High-purity, high-density graphite. Stable to 450 °C. No binders that can off-gas or adsorb analytes. Smooth surface and clean edges. Ferrule ID 0.3 mm 0.4 mm 0.5 mm 0.8 mm 20 www.restek.com Fits Column ID 0.10–0.15 mm 0.18–0.28 mm 0.32 mm 0.45–0.53 mm 1-800-356-1688 or 1-814-353-1300 Connectors SeCure® “Y” Connector Kits • Connect two analytical columns to a transfer line or guard column. • Use standard “Y” Press-Tight® connectors and 1/16" graphite ferrules. • Reliable seal integrity—will not unexpectedly disconnect during temperatureprogrammed analyses. • Open design allows visual confirmation of the seal for added confidence in the connection. • Fit both Restek cage designs. Combine the simplicity of a “Y” Press-Tight® connector with the strength of a metal union. The ferrules and knurled nuts hold the fused silica tubing in place, which prevents the tubing from unexpectedly disconnecting, even at temperatures as high as 400 °C. The SeCure® “Y” connector's open design allows visual confirmation of the seal. fused silica column, guard column, or transfer line knurled nut hanger Fit both Restek cage designs. Dual-column confirmational analysis with a single injection—one of the SeCure® “Y” connector's many uses. detectors injector analytical columns ferrule body guard column Press-Tight® connector SeCure® “Y” connector Secure, reliable column-to-column connections! Kits include: SeCure® “Y” connector body, 3 knurled nuts, “Y” Universal Press-Tight® union, 3 ferrules. Description SeCure “Y” Connector Kit SeCure “Y” Connector Kit SeCure “Y” Connector Kit Knurled nut Ferrules Fit Column ID 0.18/0.25/0.28 mm 0.32 mm 0.45/0.53 mm qty. kit kit kit 3-pk. cat.# 20276 20277 20278 20279 Universal “Y” Press-Tight® Connectors An alternative method of performing dual-column confirmational analyses! • Split sample flow onto two columns—perform confirmation analysis with a single injection. • Split a single column flow to two detectors. Description Universal “Y” Press-Tight Connector Universal “Y” Press-Tight Connector, Deactivated Universal “Y” Press-Tight Connector, Siltek Deactivated ea. 20405 20405-261 20485 3-pk. 20406 20406-261 20486 Graphite 10-pk./ 20200 20201 20202 Graphite 50-pk./ 20227 20228 20224 20485 20405 Graphite Ferrules for SeCure® “Y” Connectors • • • • • Preconditioned to minimize out-gassing. High-purity, high-density graphite. Stable to 450 °C. No binders that can off-gas or adsorb analytes. Smooth surface and clean edges. Ferrule ID 0.4 mm 0.5 mm 0.8 mm Fits Column ID 0.10/0.15/0.18/0.25/0.28 mm 0.32 mm 0.45/0.53 mm 1-800-356-1688 or 1-814-353-1300 www.restek.com 21 Connectors Press-Tight® Connectors • Deactivated Press-Tight® connectors maintain complete inertness for the GC flow path. • Siltek®-deactivated connectors are ideal for organochlorine pesticides analysis. • Fit 0.33–0.74 mm OD columns (Restek 0.1–0.53 mm ID). Universal Press-Tight® Connectors 20480 • Connect a guard column to an analytical column. • Repair a broken column. • Connect a column outlet to a transfer line. Description Universal Press-Tight Connectors Universal Press-Tight Connectors, Deactivated Universal Press-Tight Connectors, Siltek Deactivated 20400 5-pk./ 20400 20429 20480 25-pk. 20401 20430 20449 100-pk. 20402 Universal “Y” Press-Tight® Connectors An alternative method of performing dual-column confirmational analyses! 20485 • Split sample flow onto two columns—perform confirmation analysis with a single injection. • Split a single column flow to two detectors. Description Universal “Y” Press-Tight Connector Universal “Y” Press-Tight Connector, Deactivated Universal “Y” Press-Tight Connector, Siltek Deactivated 20405 ea. 20405 20405-261 20485 3-pk. 20406 20406-261 20486 Universal Angled “Y” Press-Tight® Connectors 20487 • Perform confirmation analysis with a single injection. • Inlet and outlet ends conform to the column curvature—alleviates column-end connection strain. Description Universal Angled “Y” Press-Tight Connector Universal Angled “Y” Press-Tight Connector, Deactivated Universal Angled “Y” Press-Tight Connector, Siltek Deactivated 20403 ea. 20403 20403-261 20487 3-pk. 20404 20404-261 20469 Polyimide Resin Securely connects a Press-Tight® connector to a fused silica column. Description Polyimide Resin Max. Temp. 350 °C qty. 5 grams cat.# 20445 20445 22 www.restek.com 1-800-356-1688 or 1-814-353-1300 Connectors MXT®-Union Connector Kits for Fused Silica Columns • • • • Low-dead-volume, leak-tight connection. Reusable. Siltek® treatment ensures maximum inertness. Ideal for connecting a guard column or transfer line to an analytical column. • Use to oven temperatures of 360 °C. • Available in union and “Y” configurations. • Can also be used for connecting fused silica to metal. These MXT® connectors can be used with fused silica tubing because of a Valcon polyimide, 1/32-inch, one-piece fused silica adaptor. This unique graphite-reinforced composite allows a capillary column to slide into the adaptor and be locked in place simply by loosening and tightening the fitting. 20140 20141 20389 Valco® Connectors—One-Piece Valcon Polyimide Adaptor Ferrule for Fused Silica Fused silica adaptor ferrules are made from Valcon polyimide, a unique, graphite-reinforced composite specially prepared to maximize mechanical stability at temperatures up to 350 °C. The determining factor for selecting adaptor ferrule size is the fused silica tubing OD. 1/32-Inch Valco® Adaptor Ferrules (Valcon Polyimide) Tubing OD 0.25–0.40 mm 0.40–0.50 mm 0.50–0.80 mm Tubing ID 0.25 mm 0.32 mm 0.53 mm 1/32" Replacement Nut Valco # FS.4-5 FS.5-5 ZF.5V-5 qty. 5-pk. 5-pk. 5-pk. 5-pk. cat.# 20137 20140 20141 20389 21386 MXT®-Union Connector Kits for Fused Silica Columns Each kit contains the MXT® union; two 1/32-inch nuts; and two, one-piece, fused silica adaptors. Description For 0.25 mm ID Fused Silica Columns For 0.32 mm ID Fused Silica Columns For 0.53 mm ID Fused Silica Columns qty. kit kit kit cat.# 21386 21385 21384 20146 Ferrule Removal Kit MXT® “Y”-Union Connector Kits The tapered tools in this kit have teeth designed to grip and remove fused silica adaptor ferrules that have become stuck in the fitting detail. Each kit has two tools: one for removing 1/32-inch adaptor ferrules and one for removing 1/16-inch adaptor ferrules. for Fused Silica Columns Each kit contains the MXT® union; three 1/32-inch nuts; and three, one-piece, fused silica adaptors. Description Ferrule Removal Kit 21389 Description For 0.25 mm ID Fused Silica Columns For 0.32 mm ID Fused Silica Columns For 0.53 mm ID Fused Silica Columns qty. kit kit kit 1-800-356-1688 or 1-814-353-1300 qty. kit cat.# 20146 cat.# 21389 21388 21387 20389 1/32-Inch Replacement Nut Description 1/32" Replacement Nut Valco # FRK1 qty. 5-pk. cat.# 20389 www.restek.com 23 Vial Accessories Electronic Rechargeable Crimpers and Decappers NEW! 22358 Universal plug set for battery charger included in all kits. NEW! • • • • • • • Easy to use; comfortable grip. Hundreds of operations from one charge. Adjustable crimping force. Large battery allows for faster charge cycle. All kits include a universal plug set for the battery charger. For 11 mm and 20 mm caps. One-year warranty. These electronic crimpers and decappers have a rechargeable 6.4-volt battery installed. The large battery allows for quick, powerful operation and a faster charge cycle, minimizing downtime. Charging the battery takes thirty minutes to two hours. The universal plug set includes U.S., European, UK, and Australian plug clips. Description Electronic Crimper Electronic Crimper Electronic Decapper Electronic Decapper Replacement Battery for Electronic Crimpers and Decappers Size 11 mm 20 mm 11 mm 20 mm qty. kit kit kit kit ea. cat.# 22358 22359 22360 22361 22362 Easy Grip Manual Crimpers and Decappers Crimper Decapper Our new Easy Grip Crimpers and Decappers feature tough, light, glass-filled plastic bodies with curved handles that improve hand comfort during use. The bottom-pull handle allows for a steadier hold than top-push handles. An easily viewed adjustment knob is located at the head of the product. The clearly shown + and – symbols, along with directional arrows, simplify adjusting the intensity of the crimp/decap needed. The knob is also designed to indicate when the crimp setting has been reached, when it fully contacts the body of the product. Description Crimper Crimper Decapper Decapper Size 11 mm 20 mm 11 mm 20 mm qty. ea. ea. ea. ea. cat.# 23396 23398 23397 23399 Safer than removing caps with pliers, knives, or screwdriver blades! 24 www.restek.com 1-800-356-1688 or 1-814-353-1300 Vials 2.0 mL Crimp-Top Vials, 12 x 32 mm, 11 mm Choose with or without white graduated marking spots. Description Vial w/White Graduated Marking Spot Vial w/White Graduated Marking Spot Vial without Graduated Marking Spot Color Clear Amber Clear Material Glass Glass Glass 100-pk. 24383 24385 21152 1,000-pk. 24384 24386 21153 500-pk. — — — — — 21724 — — — — — 21725 — 1,000-pk. 21175 24352 24354 24356 24358 — 24360 24362 24364 24366 24368 — 24370 2.0 mL, 11 mm Aluminum Crimp Seals With Septa Seal Color Silver Blue Green Red Yellow Mixed Silver Blue Green Red Yellow Mixed Silver Septa Material PTFE/Natural Rubber PTFE/Red Rubber PTFE/Red Rubber PTFE/Red Rubber PTFE/Red Rubber PTFE/Rubber PTFE/Silicone PTFE/Silicone PTFE/Silicone PTFE/Silicone PTFE/Silicone PTFE/Silicone PTFE/Silicone/PTFE 100-pk. 21174 24351 24353 24355 24357 — 24359 24361 24363 24365 24367 — 24369 24385 24383 21724 2.0 mL, 11 mm crimp-top vials are compatible with Shimadzu SIL-10A, 10Ai, 10Axl, and AOC 20i instruments. 2.0 mL Crimp Vial Convenience Kits (Vials, Caps & Septa) Vials packaged in a clear-lid tray. Caps with septa packaged in a plastic bag. Description Clear 2.0 mL Vial, Deactivated, Silver Seal, PTFE/Natural Rubber Septa Amber 2.0 mL Vial, Deactivated, Silver Seal, PTFE/Natural Rubber Septa Clear 2.0 mL Vial, Untreated, Silver Seal, PTFE/Natural Rubber Septa Amber 2.0 mL Vial, Untreated, Silver Seal, PTFE/Natural Rubber Septa Clear 2.0 mL Vial, Untreated, Silver Seal, PTFE/Silicone Septa Amber 2.0 mL Vial, Untreated, Silver Seal, PTFE/Silicone Septa 100-pk. 24671 24673 21196 21198 24646 24648 1,000-pk. 24672 24674 21197 21199 24647 24649 24671 Inserts for 2.0 mL, 11 mm Crimp-Top & 2.0 mL, 9 mm Short-Cap, Screw-Thread Vials Description Big Mouth Insert w/Bottom Spring Big Mouth Insert w/Bottom Spring Big Mouth Insert w/Glass Flange (Step Design)* Insert, Flat Bottom Insert, Flat Bottom w/ID Ring Big Mouth Insert w/Bottom Spring Big Mouth Insert w/Bottom Spring & Graduated Markings Big Mouth Insert, Top Flange Big Mouth Insert, No Spring Volume 50 μL 250 μL 250 μL 350 μL 350 μL 250 μL Material Glass Glass Glass Glass Glass Polypropylene 100-pk. 24513 21776 24516 21780 24692 24518 1,000-pk. 21782 21777 21779 24517 24693 — 250 μL Polypropylene 24518A — 250 μL 250 μL Polypropylene Polypropylene 24519 24520 — — 100-pk. 24651 24653 1,000-pk. 24652 — 21776 24692 24518A *Big Mouth insert w/glass flange (step design) not to be used with 9 mm screw-thread vials. 2.0 mL Crimp-Top Vial With 100 μL Insert • Plastic vial. • Choice of glass or polypropylene insert. Description Clear Plastic Vial Clear Plastic Vial w/100 μL Polypropylene Insert w/100 μL Glass Insert 24651 1-800-356-1688 or 1-814-353-1300 www.restek.com 25 Vials 2.0 mL, 11 mm Poly Crimp Seal Caps: Snap-On or Crimp The Poly Crimp seal is versatile, working as either a snap-on or crimp-top cap. Simply use a standard crimping tool to secure the Poly Crimp seal onto any crimp-top vial. It’s that easy! Seal Color Clear Clear Blue Clear Blue Mixed Liner Material PTFE/Butyl Rubber PTFE/Silicone PTFE/Silicone PTFE/Silicone/PTFE PTFE/Silicone/PTFE PTFE/Silicone/PTFE 100-pk. 24433 24443 24445 24453 24455 — 400-pk. — — — — — 21728 1,000-pk. 24434 24444 24446 24454 24456 — 100-pk. 21729 21731 21733 1,000-pk. 21730 21732 21734 *Based on continual use for 3–4 days. 2.0 mL, 11 mm GC Snap Ring Cap With Septum • Snaps on any crimp-style vial. • Save money! Use this snap cap when you don’t need to crimp. 21731 Description Polypropylene Snap Ring Cap w/Liner Polypropylene Snap Ring Cap w/Septum Polypropylene Snap Ring Cap w/Septum Liner/Septa Material PTFE, 10 mil PTFE/Butyl Rubber PTFE/Silicone Certified Autosampler Vial Kits Certified Vials, 2.0 mL Screw-Thread Vials • Certificates enclosed with each kit. • Vials of clear or amber borosilicate glass with ID marking spots. • Closures with pre-inserted septa. • Each kit sealed for integrity. 22788 Certification Parameters Include: Vial Dimensions: height, diameter, bottom thickness, neck length, thread profile, and annealing Cap/Septum: diameter, height, thread integrity, center flash, septa insertion, sealing/resealing test, residue by headspace GC, and extractables Chemical Test: HPLC Test: nonvolatile residue GC Test: volatile residue Description Assembled Clear 2.0 mL Vial w/Marking Spot, Cap, Bonded PTFE/Silicone Slit Septa Assembled Amber 2.0 mL Vial w/Marking Spot, Cap, Bonded PTFE/Silicone Slit Septa Unassembled Clear 2.0 mL Vial w/Marking Spot, Cap, Bonded PTFE/Silicone Septa Unassembled Amber 2.0 mL Vial w/Marking Spot, Cap, Bonded PTFE/Silicone Septa Unassembled Clear 2.0 mL High-Recovery Vial w/Marking Spot, Cap, Bonded PTFE/Silicone Slit Septa Unassembled Amber 2.0 mL Vial w/Marking Spot, Cap, Bonded PTFE/Silicone Slit Septa 100-pk. 22789 22788 22792 22790 22793 22791 22792 26 www.restek.com 1-800-356-1688 or 1-814-353-1300 Vials 2.0 mL, 9 mm Short-Cap, Screw-Thread Vials, 12 x 32 mm • Fit all 2.0 mL, 12 x 32 mm, crimp-top vial–based autosamplers. 2.0 mL, 9 mm Short-Cap, Screw-Thread Vials (vial only) Description Short-Cap Vial w/White Graduated Marking Spot Short-Cap Vial w/White Graduated Marking Spot Short-Cap Vial without Graduated Marking Spot Color Clear Amber Clear 100-pk. 21140 21142 21154 1,000-pk. 21141 21143 21155 21140 2.0 mL, 9 mm Short-Cap, Screw-Vial Closures (Polypropylene, preassembled) Cap Color Blue Mixed Blue Green Yellow Mixed Blue Black Natural Red Yellow Mixed Liner Material PTFE/Red Rubber PTFE/Red Rubber PTFE/Silicone PTFE/Silicone PTFE/Silicone PTFE/Silicone PTFE/Silicone/PTFE PTFE/Silicone/PTFE PTFE/Silicone/PTFE PTFE/Silicone/PTFE PTFE/Silicone/PTFE PTFE/Silicone/PTFE 100-pk. 24473 — 24485 24487 24493 — 24497 24495 24501 24503 24505 — 500-pk. — 24668 — — — 24669 — — — — — 24670 1,000-pk. 24474 — 24486 24488 24494 — 24498 24496 24502 24504 24506 — 24668 2.0 mL, 9 mm short-cap, screw-thread vials are compatible with Shimadzu SIL-10A, 10Ai, and 10Axl instruments. 2.0 mL Sample Vial Racks • Racks feature alphanumeric indexing for easier vial identification. • Racks can be stacked for efficient storage. • Fits most 2.0 mL, 12 x 32 mm vials (vials sold separately). Description Polypropylene Storage Rack for 12 x 32 mm Vials Capacity qty. cat.# qty. cat.# 50 vials, 5 x 10 ea. 22856 5-pk. 22857 22856 1-800-356-1688 or 1-814-353-1300 www.restek.com 27 Vials 2.0 mL Screw-Thread Vials, 12 x 32 mm, 8 mm/425 Thread • Fit all 2.0 mL, 12 x 32 mm, screw-thread 8 mm/425 vial-based autosamplers. 2.0 mL, 8 mm Screw-Thread Vials (vial only) Description Vial w/White Graduated Marking Spot Vial w/White Graduated Marking Spot 24619 All vials undeactivated unless otherwise noted. 2.0 mL, 8 mm screw-thread vials are compatible with Shimadzu AOC-8B/9, SIL-6A, AOC14/1400, AOC-17, SIL-6B, -9A, -8A, SIL-10A, 10Ai, and 10Axl instruments. Volume 2.0 mL 2.0 mL Color Clear Amber 100-pk. 24619 24621 1,000-pk. 24620 24622 100-pk. 21149 21721 1,000-pk. 21720 21722 100-pk. 21176 21178 21795 1,000-pk. 21177 21179 21147 2.0 mL, 8 mm Caps and Septa (preassembled) Cap Color Black Black Top Hat Septa Material Red PTFE/Silicone, 0.065" PTFE/Silicone Caps & Septa for 2.0 mL, 8 mm Screw-Thread Vials Description Black Polypropylene, Open-Hole Caps Septa, 8 mm x 0.045" Septa, 8 mm x 0.065" Septa Material Red PTFE/Silicone Red PTFE/White Silicone 2.0 mL Autosampler Vial Convenience Kits • Vials packaged in a clear-lid tray. Preassembled caps with septa packaged separately in a plastic bag. • Black polypropylene open-hole caps and 8 mm red PTFE/silicone septa, 0.065". Description Clear 2.0 mL Vial, Silcote CL7-Deactivated, Black Cap, Red PTFE/Silicone Septa, 0.065" Amber 2.0 mL Vial, Silcote CL7-Deactivated, Black Cap, Red PTFE/Silicone Septa, 0.065" Clear 2.0 mL Vial, Untreated, Black Cap, Red PTFE/Silicone Septa, 0.065" Amber 2.0 mL Vial, Untreated, Black Cap, Red PTFE/Silicone Septa, 0.065" 100-pk. 1,000-pk. 24638 24639 24640 24641 21192 21194 21193 21195 100-pk. 24630 24632 1,000-pk. 24631 24633 2.0 mL Preassembled Vial Kits 8 mm/425 Screw-Thread, Unmarked Vials, Septa, and Caps Caps attached to vials. Description Clear 2.0 mL Vial, Black Cap, Red PTFE/Silicone Septa, 0.045" Amber 2.0 mL Vial, Black Cap, Red PTFE/Silicone Septa, 0.045" 4.0 mL WISP 48 Crimp-Top 13 mm Vials, 15 x 45 mm, Snap Seal 4.0 mL WISP 48 Crimp-Top Vial (vial only) Description WISP 48 Snap Seal Vial w/White Graduated Marking Spot Volume 4.0 mL Color Clear 100-pk. 24658 1,000-pk. 24659 100-pk. 21753 21755 1,000-pk. 21754 21756 Aluminum Seals w/Septa for 4.0 mL WISP Crimp-Top Vials 24658 4.0 mL WISP 48 style vials are compatible with Shimadzu AOC-14/1400, AOC-17, and SIL-2AS instruments. Seal Color Silver Silver instrument reference For 4.0 mL WISP 48–Style Vials The following instruments are compatible with 4.0 mL WISP 48–style vials. For more information or questions, please contact your Restek sales representative or technical service. Manufacturer Bruker Hitachi Phillips Shimadzu 28 www.restek.com Septa Material PTFE/Natural Rubber PTFE/Silicone Instrument/Model # LC 51 L-7200, L7250 LC-XP AOC-14/1400, AOC-17, SIL-2AS Manufacturer TosoHaas Unicam Waters Instrument/Model # TSK-6080, AS-8010, AS-8020 LC-XP 48-pos. M700, 710, 717+ 1-800-356-1688 or 1-814-353-1300 Syringes Autosampler Syringes for Shimadzu GCs • Hamilton and SGE syringes are designed and tested to meet critical autosampler performance needs. • Needle point styles are designed to withstand multiple, rapid injections through a septum. Hamilton for Shimadzu AOC 9 GCs Volume 5 μL 5 μL 10 μL Needle Term. RN N RN Needle Gauge 26s 26s 26s Needle Length 2"/51 mm 2"/51 mm 2"/51 mm Point Style 2 2 2 Hamilton Model 75RN 75N 701RN cat.# 87930 87900 80330 qty. ea. ea. ea. Restek cat.# 24617 24938 24530 cat.# 000445 000440 001988 001987 002898 002902 002897 006682 qty. ea. ea. ea. ea. ea. ea. ea. ea. Restek cat.# 24841 24840 24843 24842 24845 24846 24844 24847 SGE for Shimadzu AOC 14, 17, 20, and 20i GCs Volume 0.5 μL 0.5 μL 5 μL 5 μL 10 μL 10 μL* 10 μL 250 μL* Needle Term. R R F F R R R F Needle Gauge 23 26 23 26 23 23 26 23 Needle Length 42 mm 42 mm 42 mm 42 mm 42 mm 42 mm 42 mm 42 mm Point Style Cone Cone Cone Cone Cone Cone Cone Cone SGE Model 0.5BR-S-0.63 0.5BR-S-0.47 5F-S-0.63 5F-S-0.47 10R-S-0.63 10R-S-GT-0.63 10R-S-0.47 250F-S-GT-0.63 *Gas-tight syringe. 24530 24843 Replacement Needles for Shimadzu Autosampler Syringes SGE Syringe Volume 0.5 μL 0.5 μL 10 μL 10 μL Needle Gauge 23 26 23 26 Needle Length 42 mm 42 mm 42 mm 42 mm Point Style Cone Cone Cone Cone SGE cat.# 033745 033738 037747 037745 qty. ea. ea. 2-pk. 2-pk. Restek cat.# 24747 24746 24749 24748 24749 Guide to Needle Termination Codes Hamilton: (N) Cemented Needle (RN) Removable Needle SGE: (F) Fixed Needle (R) Removable Needle 1-800-356-1688 or 1-814-353-1300 www.restek.com 29 Gas Regulators & Accessories Overview of Restek Ultra-High Purity (UHP) Gas Regulators • • • • Regulators feature metal-to-metal seals throughout for long-term leak-tightness. Metal diaphragm outlet valve ensures gas purity. Each regulator is helium leak-test-certifiable to 1x10-8 scc/sec. Temperature range: -40 °C to 60 °C. Ultra-High Purity (UHP) Brass Body Gas Regulators UHP brass regulators are the best choice when using ultra-high purity carrier gas for sensitive GC applications using MS, PID, or ECD detection methods. They feature reduced internal dead-volume relative to stainless steel bodies. The metal valve diaphragm ensures leak-free shutoff. Oxidation-resistant chrome plating maintains a likenew appearance. Dual-Stage Ultra-High Purity Chrome-Plated Brass Gas Regulators • • • • • Inlet gauge: Outlet assembly: 0 to 4,000 psig (0–27,579 kPa) diaphragm valve, 1/4" tube fitting Oxidation-resistant, chrome-plated. Most stable outlet pressure control. Secondary pressure regulation not needed. Most widely used regulator. Less internal volume than stainless steel gas regulators. Fitting CGA 580 (N2 He, Ar) CGA 350 (H2, P5) CGA 590 (Air) DIN 477 #1 (H2) DIN 477 #6 (He, Ar) DIN 477 #9 (Air) DIN 477 #10 (N2) Outlet Pressure 0 to 100 psig (0–689 kPa) 0 to 100 psig (0–689 kPa) 0 to 100 psig (0–689 kPa) 0 to 7 bar (0–100 psig) 0 to 7 bar (0–100 psig) 0 to 7 bar (0–100 psig) 0 to 7 bar (0–100 psig) Outlet Gauge 30" – 0 to 200 psig (0–1,379 kPa) 30" – 0 to 200 psig (0–1,379 kPa) 30" – 0 to 200 psig (0–1,379 kPa) 30" – 0 to 14 bar (0–200 psig) 30" – 0 to 14 bar (0–200 psig) 30" – 0 to 14 bar (0–200 psig) 30" – 0 to 14 bar (0–200 psig) qty. ea. ea. ea. ea. ea. ea. ea. cat.# 21667 21668 21669 22369 22368 22370 22371 NOTE: CGA fittings are for U.S. use; DIN fittings are for European use. Single-Stage Ultra-High Purity Chrome-Plated Brass Gas Regulators • Oxidation-resistant, chrome-plated. • Use when there is secondary pressure regulation downstream. • Identical gas purity protection as with dual-stage gas regulators. Inlet gauge: Outlet assembly: 0 to 4,000 psig (0–27,579 kPa) diaphragm valve, 1/4" tube fitting Fitting CGA 580 (N2, He, Ar) CGA 350 (H2, P5) CGA 590 (Air) DIN 477 #1 (H2) DIN 477 #6 (He, Ar) DIN 477 #9 (Air) DIN 477 #10 (N2) Outlet Pressure 0 to 100 psig (0–689 kPa) 0 to 100 psig (0–689 kPa) 0 to 100 psig (0–689 kPa) 0 to 7 bar (0–100 psig) 0 to 7 bar (0–100 psig) 0 to 7 bar (0–100 psig) 0 to 7 bar (0–100 psig) Outlet Gauge 30" – 0 to 200 psig (0–1,379 kPa) 30" – 0 to 200 psig (0–1,379 kPa) 30" – 0 to 200 psig (0–1,379 kPa) 30" – 0 to 14 bar (0–200 psig) 30" – 0 to 14 bar (0–200 psig) 30" – 0 to 14 bar (0–200 psig) 30" – 0 to 14 bar (0–200 psig) qty. ea. ea. ea. ea. ea. ea. ea. cat.# 20646 20647 20648 22373 22372 22374 22375 NOTE: CGA fittings are for U.S. use; DIN fittings are for European use. Ultra-High Purity Chrome-Plated Brass Line Gas Regulator • Oxidation-resistant, chrome-plated. • Use where you need to reduce the line pressure by 20 psig (138 kPa) or more. • Same purity protection as high-pressure cylinder regulators. Fitting 1/4" female NPT ports* 1/4" female NPT ports* Inlet connections: 1/4" FPT Outlet assembly: 1/4" FPT port Outlet Pressure 0-50 psig (0-345 kPa) 0-100 psig (0-689 kPa) Outlet Gauge 30" - 0 to 100 psig (0-689 kPa) 30" - 0 to 200 psig (0-1,379 kPa) qty. ea. ea. cat.# 21666 22452 *Order appropriate male connector, pipe-to-tube fittings. Swagelok® Male Connector, Pipe-to-Tube Fittings Fitting Type 23134 30 www.restek.com 23179 Male Connector Male Connector Tube End Reducer Size (inches) 1/4" to 1/4" NPT 1/8" to 1/4" NPT 1/4" to 1/8" Similar to Swagelok 400-1-4 200-1-4 200-R-4 Brass qty. 10-pk. 10-pk. 5-pk. cat.# 23134 23136 23129 Stainless Steel qty. cat.# 2-pk. 23184 2-pk. 23186 2-pk. 23179 1-800-356-1688 or 1-814-353-1300 Gas Regulators & Accessories Ultra-High Purity (UHP) Stainless Steel Body Gas Regulators UHP stainless steel regulators are the standard for ultra-high-purity and corrosionresistant pressure regulation. They are more easily purged of atmospheric components compared to brass gas regulators, making them ideal for the most demanding applications. Stainless steel is especially useful in atmospheres of dry corrosive gases such as hydrogen. Dual-Stage Ultra-High Purity Stainless Steel Gas Regulators • Most stable outlet pressure control. • Secondary pressure regulation not needed. Fitting CGA 580 (N2, He, Ar) CGA 350 (H2, P5) CGA 590 (Air) DIN 477 #1 (H2) DIN 477 #6 (He, Ar) DIN 477 #9 (Air) DIN 477 #10 (N2) Outlet Pressure 0 to 100 psig (0–689 kPa) 0 to 100 psig (0–689 kPa) 0 to 100 psig (0–689 kPa) 0 to 7 bar (0–100 psig) 0 to 7 bar (0–100 psig) 0 to 7 bar (0–100 psig) 0 to 7 bar (0–100 psig) Outlet Gauge 30" – 0 to 200 psig (0–1,379 kPa) 30" – 0 to 200 psig (0–1,379 kPa) 30" – 0 to 200 psig (0–1,379 kPa) 30" – 0 to 14 bar (0–200 psig) 30" – 0 to 14 bar (0–200 psig) 30" – 0 to 14 bar (0–200 psig) 30" – 0 to 14 bar (0–200 psig) qty. ea. ea. ea. ea. ea. ea. ea. cat.# 20662 20663 20664 22377 22376 22378 22379 Inlet gauge: Outlet assembly: 0 to 4,000 psig (0–27,579 kPa) diaphragm valve, 1/4" tube fitting Inlet gauge: Outlet assembly: 0 to 4,000 psig (0–27,579 kPa) diaphragm valve, 1/4" tube fitting NOTE: CGA fittings are for U.S. use; DIN fittings are for European use. Single-Stage Ultra-High Purity Stainless Steel Gas Regulators • Use when there is secondary pressure regulation downstream. • Identical gas purity protection as with dual-stage gas regulators. Fitting CGA 580 (N2, He, Ar) CGA 350 (H2, P5) CGA 590 (Air) DIN 477 #1 (H2) DIN 477 #6 (He, Ar) DIN 477 #9 (Air) DIN 477 #10 (N2) Outlet Pressure 0 to 100 psig (0–689 kPa) 0 to 100 psig (0–689 kPa) 0 to 100 psig (0–689 kPa) 0 to 7 bar (0–100 psig) 0 to 7 bar (0–100 psig) 0 to 7 bar (0–100 psig) 0 to 7 bar (0–100 psig) Outlet Gauge 30" – 0 to 200 psig (0–1,379 kPa) 30" – 0 to 200 psig (0–1,379 kPa) 30" – 0 to 200 psig (0–1,379 kPa) 30" – 0 to 14 bar (0–200 psig) 30" – 0 to 14 bar (0–200 psig) 30" – 0 to 14 bar (0–200 psig) 30" – 0 to 14 bar (0–200 psig) qty. ea. ea. ea. ea. ea. ea. ea. cat.# 20665 20666 20667 22380 22445 22446 22447 qty. ea. ea. cat. # 21339 21340 NOTE: CGA fittings are for U.S. use; DIN fittings are for European use. Flexible Stainless Steel Hoses Description Flexible Stainless Steel Hose Flexible Stainless Steel Hose Length 36" 18" Fittings 1/4" Female NPT 1/4" Female NPT Flammable Gas Flash Arrestor—Factory Mutual Approved* • Gas flow shuts off in the event of a flashback. • Flame extinguished—flame front prevented from reaching the gas supply. • No gas flow restriction under normal operating conditions. Description Flammable Gas Flash Arrestor, Brass Body Fittings 1/4" NPTF qty. ea. cat.# 21334 21334 *Approved for brass body servicing hydrogen, acetylene, propane, or natural gas only. CGA Fittings CGA-specified nuts and nipples with internal frit, 1/4-inch NPT nickel-plated brass. Description CGA 580 Fitting, (N2, He, Ar) CGA 350 Fitting, (H2, P5) CGA 590 Fitting, (Air) qty. ea. ea. ea. cat.# 21336 21337 21338 21336 ordering note International Fittings All gas regulators are available with the following BS (British Standard) and DIN (German Industrial Standards Organization) connections. Please contact your local Restek representative for more information. BS 341 #01 BS 341 #02 BS 341 #03 BS 341 #04 BS 341 #08 BS 341 #10 BS 341 #13 BS 341 #14 BS 341 #15 DIN 477 #01 DIN 477 #03 DIN 477 #05 1-800-356-1688 or 1-814-353-1300 DIN 477 #06 DIN 477 #07 DIN 477 #08 DIN 477 #09 DIN 477 #10 DIN 477 #11 DIN 477 #12 DIN 477 #13 DIN 477 #14 DIN 477 #15 www.restek.com 31 Fittings Swagelok® Fittings (Brass & Stainless Steel) Restek is pleased to offer one of the premier lines of fittings available for chromatographers in the market today. We can supply the entire line of Swagelok® fittings. If you don't see the exact product you're looking for, please call us or contact your Restek representative for a quote. Brass Fitting Type Nut nut front ferrule Front Ferrule Back Ferrule Nut & Ferrule Set back ferrule Plug nut & ferrule set Union Reducing Union plug union Tee Cross reducing union tee Tube End Reducer Port Connector tube end reducer Male Connector cross port connector Female Connector male connector Male & Female Quick Couplings male quick coupling female connector Size 1/16" 1/8" 1/4" 1/16" 1/8" 1/4" 1/16" 1/8" 1/4" 1/16" 1/8" 1/4" 1/16" 1/8" 1/4" 1/16" 1/8" 1/4" 1/8" to 1/16" 1/4" to 1/16" 1/4" to 1/8" 1/16" 1/8" 1/4" 1/8" 1/4" 1/8" to 1/16" 1/4" to 1/16" 1/8" to 1/4" 1/4" to 1/8" 1/8" 1/4" 1/8" to 1/4" 1/8" to 1/8" NPT 1/4" to 1/4" NPT 1/16" to 1/8" NPT 1/8" to 1/4" NPT 1/4" to 1/8" NPT 1/8" to 1/8" NPT 1/4" to 1/4" NPT 1/4" to 1/8" NPT 1/8" male* 1/8" male 1/8" female* 1/4" male* 1/4" male 1/4" female* Swagelok # 102-1 202-1 402-1 103-1 203-1 403-1 104-1 204-1 404-1 100-P 200-P 400-P 100-6 200-6 400-6 200-6-1 400-6-1 400-6-2 100-3 200-3 400-3 200-4 400-4 100-R-2 100-R-4 400-R-2 200-R-4 201-PC 401-PC 401-PC-2 200-1-2 400-1-4 100-1-2 200-1-4 400-1-2 200-7-2 400-7-4 400-7-2 QC4D-200 QC4S-200 QC4B-200 QC4D-400 QC4S-400 QC4B-400 qty. 20-pk. 40-pk. 40-pk. 20-pk. 40-pk. 40-pk. 20-pk. 40-pk. 40-pk. 10-pk. 20-pk. 20-pk. 5-pk. 10-pk. 10-pk. 3-pk. 5-pk. 5-pk. 5-pk. 5-pk. 5-pk. 2-pk. 2-pk. 2-pk. 2-pk. 2-pk. 5-pk. 5-pk. 5-pk. 5-pk. 5-pk. 10-pk. 5-pk. 10-pk. 10-pk. 5-pk. 10-pk. 10-pk. 5-pk. 5-pk. 5-pk. — — — — — — cat.# 23100 23101 23102 23103 23104 23105 23106 23107 23108 23109 23110 23111 23112 23113 23114 23115 23116 23117 23118 23119 23120 23121 23122 23123 23124 23125 23126 23127 23128 23129 23130 23131 23132 23133 23134 23135 23136 23137 23138 23139 23140 — — — — — — 316 Grade Stainless Steel qty. cat.# 5-pk. 23150 10-pk. 23151 10-pk. 23152 10-pk. 23153 20-pk. 23154 20-pk. 23155 10-pk. 23156 20-pk. 23157 20-pk. 23158 2-pk. 23159 5-pk. 23160 5-pk. 23161 2-pk. 23162 4-pk. 23163 4-pk. 23164 ea. 23165 2-pk. 23166 2-pk. 23167 ea. 23168 2-pk. 23169 2-pk. 23170 ea. 23171 ea. 23172 ea. 23173 ea. 23174 ea. 23175 2-pk. 23176 2-pk. 23177 2-pk. 23178 2-pk. 23179 2-pk. 23180 2-pk. 23181 2-pk. 23182 2-pk. 23183 2-pk. 23184 2-pk. 23185 2-pk. 23186 2-pk. 23187 2-pk. 23188 2-pk. 23189 2-pk. 23190 ea. 23191 ea. 23192 ea. 23193 ea. 23194 ea. 23195 ea. 23196 *Includes self-sealing shutoff valve. female quick coupling 32 www.restek.com 1-800-356-1688 or 1-814-353-1300 Fittings Swagelok® Fittings (Siltek®/Sulfinert® & Silcosteel®-CR Treated) • Full line of treated 1/16", 1/8", and 1/4" fittings. • Silcosteel®-CR treatment enhances corrosion resistance by 10x or more. • For custom treatment on any Swagelok® fitting or other system parts not listed here, call us or contact your Restek representative. Fitting Type Union Tee Reducing Union Elbow Plug Cross Tube End Reducer Port Connector Male Connector Female Connector Bulkhead Union Size 1/16" 1/8" 1/4" 3/8" 1/16" 1/8" 1/4" 3/8" 1/8" to 1/16" 1/4" to 1/16" 1/4" to 1/8" 3/8" to 1/4" 1/8" 1/4" 1/8" 1/4" 1/8" 1/4" 1/8" tube to 1/16" 1/4" tube to 1/16" 1/8" tube to 1/4" 1/4" tube to 1/8" 1/8" 1/4" 1/8" tube to 1/4" 1/8" to 1/8" NPT 1/4" to 1/4" NPT 1/16" to 1/8" NPT 1/8" to 1/4" NPT 1/4" to 1/8" NPT 3/8" to 3/8" NPT 1/8" to 1/8" NPT 1/4" to 1/4" NPT 1/4" to 1/8" NPT 1/8" to 1/4" NPT 1/8" 1/4" Siltek/Sulfinert Treated qty. cat.# ea. 22540 ea. 22541 ea. 22542 ea. 22909 ea. 22543 ea. 22544 ea. 22545 ea. 22910 ea. 22546 ea. 22547 ea. 22548 ea. 22911 ea. 22549 ea. 22550 ea. 22573 ea. 22574 ea. 22551 ea. 22552 ea. 22553 ea. 22554 ea. 22555 ea. 22556 ea. 22557 ea. 22558 ea. 22559 ea. 22561 ea. 22562 ea. 22563 ea. 22564 ea. 22565 ea. 22912 ea. 22566 ea. 22567 ea. 22568 ea. 22569 ea. 22570 ea. 22571 Swagelok # SS-100-6 SS-200-6 SS-400-6 SS-600-6 SS-100-3 SS-200-3 SS-400-3 SS-600-3 SS-200-6-1 SS-400-6-1 SS-400-6-2 SS-600-6-4 SS-200-9 SS-400-9 SS-200-P SS-400-P SS-200-4 SS-400-4 SS-100-R-2 SS-100-R-4 SS-400-R-2 SS-200-R-4 SS-201-PC SS-401-PC SS-401-PC-2 SS-200-1-2 SS-400-1-4 SS-100-1-2 SS-200-1-4 SS-400-1-2 SS-600-1-6 SS-200-7-2 SS-400-7-4 SS-400-7-2 SS-200-7-4 SS-200-61 SS-400-61 Silcosteel-CR Treated qty. cat.# ea. 22575 ea. 22576 ea. 22577 ea. 22904 ea. 22578 ea. 22579 ea. 22580 ea. 22905 ea. 22581 ea. 22582 ea. 22583 ea. 22906 ea. 22584 ea. 22585 ea. 22620 ea. 22597 ea. 22586 ea. 22587 ea. 22588 ea. 22589 ea. 22590 ea. 22591 ea. 22592 ea. 22593 ea. 22594 ea. 22595 ea. 22596 ea. 22610 ea. 22611 ea. 22612 ea. 22907 ea. 22613 ea. 22614 ea. 22615 ea. 22616 ea. 22617 ea. 22618 union tee reducing union elbow plug cross port connector tube end reducer male connector female connector bulkhead union Swagelok® Fitting Kits Save more than 40% by purchasing a Restek Swagelok® fittings kit compared to paying full price for the individual parts! • Includes the most common assortment of 1/8" and 1/4" brass or stainless steel fittings. • Parts list makes reordering easy. • Parts come in sturdy toolbox for easy and convenient storage. 40% savings Description Swagelok Fitting Kit, Brass qty. kit 1-800-356-1688 or 1-814-353-1300 cat.# 23141 Description Swagelok Fitting Kit, Stainless Steel qty. kit cat.# 23197 www.restek.com 33 More Parts & Accessories for More GC Systems Agilent Bruker/Varian PerkinElmer Shimadzu Thermo Scientific and more! www.restek.com/GCacc Also look to Restek for: GC Columns & Accessories | LC Columns & Accessories Sample Preparation | Certified Reference Materials (CRMs) | Expert Support PATENTS & TRADEMARKS Restek® patents and trademarks are the property of Restek Corporation. (See www.restek.com/Patents-Trademarks for full list.) Other trademarks appearing in Restek® literature or on its website are the property of their respective owners. The Restek® registered trademarks used here are registered in the United States and may also be registered in other countries. Lit. Cat.# GNMC1160-UNV © 2012 Restek Corporation. All rights reserved. Printed in the U.S.A. U.S. • 110 Benner Circle • Bellefonte, PA 16823 • 1-814-353-1300 • 1-800-356-1688 • fax: 1-814-353-1309 • www.restek.com China • phone: +86-10-5629-6620 • fax: +86-10-5814-3980 • cn.restek.com France • phone: +33 (0)1 60 78 32 10 • fax: +33 (0)1 60 78 70 90 • www.restek.fr Germany • phone: +49 (0)6172 2797 0 • fax: +49 (0)6172 2797 77 • www.restekgmbh.de Italy • phone: +39-02-7610037 • fax: +39-02-70100100 • www.superchrom.it Japan • phone: +81 (3)6459 0025 • fax: +81 (3)6459 0025 • e-mail: restekjapan@restek.com UK • phone: +44 (0)1494 563377 • fax: +44 (0)1494 564990 • www.thamesrestek.co.uk