ISRO-PAX-304 Issue 2, June 2014 Test Specifications and Requirements for Multilayer Printed Circuit Boards ISRO Reliability Standards Directorate of Systems Reliability and Quality, ISRO Headquarters, Bangalore ¦ÉÉ®úiÉÒªÉ +xiÉÊ®úIÉ +xÉÖºÉÆvÉÉxÉ ºÉÆMÉ`öxÉ Indian Space Research Organisation Department of Space Government of India Antariksh Bhavan New BEL Road, Bangalore - 560 231, India Telephone : +91-80-2341 5241/2217 2333 Fax : +91-80-23415328 e-mail : chairman@isro.gov.in +xiÉÊ®úIÉ Ê´É¦ÉÉMÉ ¦ÉÉ®úiÉ ºÉ®EòÉ® +xiÉÊ®úIÉ ¦É´ÉxÉ xªÉÚ ¤ÉÒ.<Ç.B±É. ®úÉäb÷, ¤ÉåMɱÉÚ®ú-560 231, ¦ÉÉ®úiÉ nÚ®¦ÉɹÉ: +91-80-2341 5241/2217 2333 ¡èòCºÉ: +91-80-23415328 Dr. K. Radhakrishnan Chairman MESSAGE ISRO Reliability Standards, addressing the various disciplines of Engineering, have been in vogue for almost three decades now. These standards are followed across ISRO centres as well as external work centers for design, fabrication, testing, analysis and other processes involved in the realization of Launch Vehicles, Spacecraft, Space Applications, Ground support systems and other launch infrastructure. The need for standardization of processes towards achieving high reliability systems can never be over emphasized, and ISRO Reliability Standards are just an attempt towards explicitly stating this. With the advent of newer techniques and with the evolution of technology itself, over the last 30 years, it has become essential to revisit the existing ISRO Reliability Standards and revise and update the standards wherever essential. Towards this, the Directorate of Systems Reliability and Quality (DSRQ) at ISRO Headquarters has taken an initiative to re-invigorate the reach and visibility of ISRO Reliability standards across all the Centres of ISRO. Specific Inter-centre teams were formed to revise each of these documents and I would like to place on record their commendable efforts in bringing out these documents. There is a pressing need for ensuring uniformity of practices, across various functions of design, fabrication, testing, review mechanisms etc., across the centres and units of ISRO. Towards this goal, the mandatory adoption of ISRO Reliability Standards will ensure standardization in quality processes and products. I am certain that this will go a long way towards ensuring overall system level Quality and Reliability and in achieving the goal of zero defects in the delivery of space systems of ISRO. K Radhakrishnan Chairman, ISRO Directorate of Systems Reliability & Quality ISRO Headquarters Antariksh Bhavan New BEL Road, Bangalore -560231 Ph :080 - 2341 5414 Fax :080 – 2341 2826 Cell:09448397704 Email: sselvaraju@isro.gov.in S Selvaraju Senior Advisor, Systems Reliability and Quality PREFACE ISRO Reliability standards are a result of the need for standardization of processes towards achieving high reliability systems. The transfer of knowledge and techniques from the seniors to their successors is best done with proper documentation and checklists translating the entire know-how into black and white. This document on “Test Specifications and Requirements for Multilayer Printed Circuit Boards” brings out the entire array of tests to be carried out for the acceptance as well as qualification of Printed Circuit Boards for on-board and ground support equipment application of ISRO. A description of the configuration of rigid Multilayer PCBs and the laminates and conductors used is also presented. The most significant element of this document is the thrust on the details of Qualification programme and its implementation comprising of a spectrum of tests like electrical test, mechanical test, solderability test, metal-plating evaluation, pull test and others. The quality assurance aspects in the manufacture of Printed Circuit Boards are of supreme importance and this document lays emphasis on the best practices of record keeping and traceability, incoming inspection of raw materials, calibration, inspection, operator training along with the non-conformance control etc. It is deemed essential that these standards be strictly adhered to, in order to ensure uniformity of practices across ISRO centres and achieve zero defects in the delivery of space systems. I am grateful to Chairman ISRO, for being the source of inspiration in the release of these documents. Thanks are also due to the centre Directors for their encouragement. I am also thankful to the Heads of SR Entities/Groups of various ISRO centres for their relentless support and guidance. I am also indebted to the members of the Integrated Product Assurance Board (IPAB) for the meticulous review of these documents. I also owe gratitude to the task team members and other experts for putting efforts in the realization of these documents. I am glad to carry forward this rich lineage of ISRO reliability standards, championed by Shri R Aravamudan, a revered pioneer in the area of Quality & Reliability in ISRO. S Selvaraju Sr. Advisor (SRQ) LIST OF CONTENTS 1 SCOPE 1 2 APPLICABLE DOCUMENTS 1 2.1 Other Related References 1 GENERAL REQUIREMENTS 2 3.1 2 3 Terms and Definitions 3.2Abbreviations 6 3.3 Process Identification Document (PID) 6 3.4 Test Programme 7 3.5 Qualification Test Pattern/Layout 7 3.6Laminates 3.6.1 Copper Clad Laminate 3.6.2 Base Laminate 3.6.3 Copper Cladding 3.6.4 Laminate Properties 3.6.5 Bonding Sheet (Prepreg) 7 7 7 8 8 8 3.7 MLB Configuration 8 3.8 Production of PCBs 3.8.1 Production Lot 3.8.2Workmanship 8 9 9 3.9Plating 3.9.1 Internal Layers 3.9.2 Thickness (electroless copper) 3.9.3 Thickness (electro-deposited copper) 3.9.4 Surface Finish 3.9.5Workmanship-plating 4 9 9 9 9 9 9 3.10Conductors 3.10.1 Under Cutting 3.10.2Holes 3.10.3 Plated Through Holes (PTH) 3.10.4 Solderable Pads and Terminal Areas 3.10.5 Annular Ring 10 11 11 11 11 11 3.11 Defects in PCBs 3.11.1 Major Defect / Non-conformance (M) 3.11.2 Minor Defect / Non-conformance (m) 12 12 12 EVALUATION 13 4.1 Request for Evaluation 13 4.2 Evaluation of PCBs 13 5 6 4.3 Facility Visit 13 4.4 Qualification Program Flow 14 QUALIFICATION 15 5.1General 15 5.2 Qualification Programme Definition and Approval 15 5.3 Non-conformance Criteria 15 5.4 Qualification Programme Implementation 15 5.5 Qualification PCBs 5.5.1General 5.5.2 Test Pattern A: Electrical Test 5.5.3 Test Pattern B: Mechanical Test 5.5.4 Test Pattern C: Electrical Test 5.5.5 Test Pattern D: Electrical Test and Visual Aspect 5.5.6 Test Pattern E: Electrical Test 5.5.7 Test Pattern F: Metal-Plating Evaluation and Pull Test 5.5.8 Test Pattern G: Surface Solderability Test 5.5.9 Test Pattern H: Electrical Test 5.5.10 Test Pattern J: Solderability Test and Rework Simulation 5.5.11 Test Pattern K: Physical Test 5.5.12 Test Pattern L: Demonstration of Technological Capability 5.5.13 Test Pattern M: CAD/CAM Criteria (Optional) 18 18 18 19 20 20 20 21 21 22 22 23 23 24 5.6 Qualification Approval 25 5.7 Maintenance of Qualification 25 TESTS 26 6.1General 6.1.1Pre-conditioning 6.1.2Cleaning 6.1.3 Bare Board Testing (BBT) 26 26 26 26 6.2 Group 1: Visual Inspection and Non-destructive Test 6.2.1General 6.2.2 Verification of Marking 6.2.3 Visual Aspects 6.2.4 External Dimensions 6.2.5 Warp or Bow 6.2.6Twist 6.2.7 Specific Dimensional Check 6.2.8 Electrical Measurement Methods 6.2.9 Mechanical Test Methods 6.2.10 Microsectioning on Test Pattern F 27 27 27 27 29 30 30 31 31 33 35 6.3 Group 2: Hot, Cold and Vibration Tests 6.3.1 Hot Storage 6.3.2 Cold Storage 6.3.3 Vibration Fatigue 39 39 39 39 7 8 6.4 Group 3: Thermal Stress and Thermal Shock (on PCB) 6.4.1General 6.4.2 Hot Oil Dip Test 6.4.3 Solder Dip Test 6.4.4 Plating Measurements, Pull Test & Microsection on Test Pattern F 40 40 40 41 41 6.5 Group 4: Thermal Cycling (on PCB) 42 6.6 Group 5: Long Term Damp Heat (on PCB) 6.6.1General 6.6.2 Damp Heat 42 42 43 6.7 Group 6: Assembly Compatibility Tests 6.7.1General 6.7.2 Physical Tests on Test Pattern K 43 43 43 QUALITY ASSURANCE FOR MANUFACTURING 45 7.1General 45 7.2 Quality Records 7.2.1 PCB Ordering Information and Data Input 45 45 7.3 Incoming Inspection of Raw Materials 45 7.4Traceability 46 7.5Calibration 46 7.6 46 Workmanship Requirements 7.7Inspection 7.7.1 Microsection Inspection for Major Defects 7.7.2 Visual Inspection for Major Defects 46 46 7.8 Operator and Inspector Training 66 7.9 Quality Test Coupon 7.9.1 Test Coupon Details 7.9.2 Test Coupon Usage 7.9.3 Test Coupon Placement in Panel 66 66 67 67 7.10 Acceptance Tests 7.10.1 Mechanical Inspection Report Format 7.10.2 Microsection and Report Formats 7.10.3 Coupon Test Result Format 7.10.4 Final Inspection Report Format 7.10.5 Data Pack 68 69 70 73 74 76 7.11 Non-conformance Control 76 7.12 Packaging, Storage and Shipment 7.12.1 Storage of the Approved PCBs 7.12.2Precautions 78 79 79 REQUIREMENTS FOR PCBs 80 8.1 80 80 Rigid Multilayer PCBs 8.1.1 Dimensional Characteristics 8.1.2 8.1.3 8.1.4 Electrolytic Coatings Mechanical Characteristics Electrical Characteristics 81 81 82 ANNEXURE-1 : Qualification Test Pattern 83 10 ANNEXURE-2 :Typical Micro Section Defects 101 11 ANNEXURE-3 :Typical Example for Plated Through Hole 102 12 ANNEXURE-4 :Typical Via Types 103 9 LIST OF FIGURES Figure 1: Qualification Test Matrix 16 Figure 2: Example of test pattern for intralayer insulation resistance and dielectric withstanding voltage 19 Figure 3: Example of test pattern for testing peel strength of conductors and pull-off strength of Non-PTH pads 19 Figure 4: Example of test pattern for internal short circuit testing 20 Figure 5: Example of test pattern for etching definition evaluation and continuity testing 20 Figure 6: Example of test pattern for interconnection resistance and current over load testing 21 Figure 7: Example of test pattern for metal plating evaluation & pull test 21 Figure 8: Example of test pattern for plating adhesion testing and analysis of Sn Pb coating composition after reflow 22 Figure 9: Example of test pattern for interlayer insulation resistance and dielectric withstanding voltage testing 22 Figure 10: Example of test pattern for solder wettability and rework simulation testing 23 Figure 11: Example of test pattern for water absorption and outgassing testing 23 Figure 12: Example of test pattern for evaluation of the technological capability 24 Figure 13: Example of test pattern for evaluation of CAD/CAM capability 25 Figure 14: Arbitrary defects on conductors 29 Figure 15: Arbitrary defects on spacing between conductors 29 Figure 16: Warp or Bow 30 Figure 17: Twist 31 Figure 18: Test for internal short circuit 33 Figure 19: Wettability of terminal pads and plated-through holes 35 Figure 20: Dimensional parameters to be measured 36 Figure 21: Microsection of a PTH 37 Figure 22: Undercut for PCBs with fused SnPb finish 37 Figure 23: Microsection of PTH: Possible defects 38 Figure 24: Voids in resin inside buried vias 39 Figure 25 : Horizontal test coupon with drilling details 66 Figure 26 : Vertical test coupon with drilling details 67 Figure 27: Usage details of test coupon 67 Figure 28: Test coupon placement in panel 68 Figure 29: Acceptance test flow 72 Figure 30: Layer 1 83 Figure 31: Layer 2 84 Figure 32: Layer 3 85 Figure 33: Layer 4 86 Figure 34: Layer 5 87 Figure 35: Layer 6 88 Figure 36: Layer 7 89 Figure 37: Layer 8 90 Figure 38: Layer 9 91 Figure 39: Layer 10 92 Figure 40: Layer 11 93 Figure 41: Layer 12 94 Figure 42: Layer 13 95 Figure 43: Layer 14 96 Figure 44: Top solder mask 97 Figure 45: Bottom solder mask 98 Figure 46: Drilling details 99 Figure 47: Zone details 100 Figure 48: Typical microsection defects 101 Figure 49: Typical example of plated through hole 102 Figure 50: Typical via types 103 LIST OF TABLES Table 1: Dimensional and Tolerance Requirements (For finished PCBs) 10 Table 2: Test Specification 16 Table 3: List of PCB Acceptance Tests 68 Table 4: Mechanical Inspection Report Format 69 Table 5: Microsection Report Format-A 70 Table 6: Microsection Report Format-B 71 Table 7: Acceptance Test Report 73 Table 8: PCB Inspection Report Format 74 Table 9: Non-conformance Control Format 77 ISRO-PAX-304 1 SCOPE This document specifies the requirements for qualification and quality conformance (acceptance) testing of Multi Layer Printed Circuit Boards (MLBs) for use in ISRO Projects. PCBs (Printed Circuit Boards) used in all the ISRO projects shall be procured from manufacturers who are qualified to the requirements specified herein. 2 APPLICABLE DOCUMENTS ISRO-PAX-301 Design Requirements for Printed Circuit Board Layouts ISRO-PAS-207 ISRO-PAS-100 Storage, Handling & Transportation Requirements for Electronic Hardware Non Conformance Control Requirements for ISRO Projects ISRO-PAX-300 Workmanship Standards for the Fabrication of Electronic Packages. MIL-PRF-55110 General specification for Printed wiring boards ECSS-Q-ST-70-10C Qualification of printed circuit boards. IPC 4101 Specification for base materials for Rigid and Multilayer PCBs IPC-2221A Generic Standard on Printed Board Design IPC 2222 Sectional Design Standard for Rigid Organic Printed Boards IPC-TM-650 Test Methods Manual 2.1 Other Related References MIL-STD-202 Test methods for electronic and electrical Components parts ECSS-Q-ST-70-02C Thermal vacuum outgassing test for the screening of space materials IPC-SM-840 Qualification and Performance of Permanent Solder Mask 1 ISRO-PAX-304 3 GENERAL REQUIREMENTS 3.1 Terms and Definitions Annular Ring: The portion of conductive material completely surrounding a hole. Assembly: A number of parts or subassemblies or any combination thereof joined together. Associated Test Coupon: Small piece of PCB designated to have a limited specific set of tests performed. Blister: A localized swelling and separation between any of the layers of a laminated base material or between base material and conductive foil. Board Thickness: The thickness of the metal clad base material including conductive layer or layers (May include additional plating and coating depending upon when the measurement is made). Bow/Warp: The deviation from flatness of a board characterized by a roughly cylindrical or spherical curvature such that, if the board is rectangular, its four corners are in the same plane. Cover Layer: (Flexible circuit layer) Insulating material that is applied covering totally or partially over a conductive pattern on the outer surfaces of a PCB. Conductor Spacing: The distance between adjacent edges of isolated conductive patterns in a conductor layer. Conductor Width: The width of a conductor at any point chosen at random on the printed board normally viewed from directly above. Crazing: An internal condition that occurs in reinforced laminate base material whereby glass fibers are separated from the resin at the weave intersections. (This condition manifests itself in the form of connected white spots or crosses that are below the surface of the base material). Delamination: Separation between plies within a base material, between base material and a conductive foil, or any other planar separation within a PCB. Dewetting: Condition that results when molten solder coats a surface and then recedes to leave irregularly‐shaped mounds of solder that are separated by areas that are covered with a thin film of solder and with the base metal not exposed. Etch Back: The controlled removal of non-metallic materials from the sidewalls of holes in order to remove resin smear and to expose additional internal conductor surfaces. 2 ISRO-PAX-304 Etch Factor: The ratio of the depth of etch to the amount of lateral etch, i.e., the ratio of conductor thickness to the amount of undercut. Flexible PCB: PCB either single, double sided or multilayer consisting of a printed circuit or printed wiring using flexible base materials only. Glass Transition Temperature: The temperature at which an amorphous polymer, or the amorphous regions in a partially-crystalline polymer, changes from being in a hard and relatively-brittle condition to being in a viscous or rubbery condition. Haloing: Mechanically induced fracturing or delamination, on or below the surface of a base material, that is usually exhibited by a light area around holes or other machined features. High Frequency PCB: PCB used for high frequency applications, that has specific requirements to the dielectric properties of the base laminates as well as special dimensional requirements to the layout for electrical purposes. Inclusions: Foreign particles, metallic or nonmetallic, that may be entrapped in an insulating material, conductive layer, plating, base material or solder connection. Insulation Resistance: The electrical resistance of an insulating material that is determined under specific conditions between any pair of contacts, conductors or grounding devices in various combinations. Internal Layer: A conductive pattern which is contained entirely within a multilayer printed board. Key Personnel: Personnel with specialist knowledge responsible for defined production or product assurance areas. Laminate: A product made by bonding together two or more layers of material. Layout: Layout is one of the design steps for fabrication of PCB. It is drawn on a inch / mm graph paper or directly using CAD software, identifying the conductor pattern, shape, width, length and spacing with other conductor or component. It also gives the orientation, mounting pads, clearance between components, heat sink mounting requirements photo plotting requirements, MLB layer alignment provisions etc. Measling: Condition that occurs in laminated base material in which internal glass fibres are separated from the resin at the weave intersection. This condition manifests itself in the form of discrete white spots “crosses” that are below the surface of the base material. It is usually related to thermally induced stress. Metal Core PCB: PCB using a metal core base material. 3 ISRO-PAX-304 Microsectioning: The preparation of a specimen of a material or materials, that is to be used in a metallographic examination. (This usually consists of cutting out a cross-section, followed by encapsulation, polishing, etching, staining etc.) Multilayer PCB: PCB that consist of rigid or flexible insulation materials and three or more alternate printed wiring and/or printed circuit layers that have been bonded together and electrically interconnected. Overhang: The sum of outgrowth and undercut. (If undercut does not occur, the overhang is the same as the outgrowth.) Peel Strength: The force per unit width required to peel a conductor or foil from the base material. Pin Holes: A small hole occurring as an imperfection which penetrates entirely through a layer of material. Plated Through Hole: A hole in which electrical connection is made between internal or external conductive patterns or both, by the plating of metal on hole wall. Plating: Metallic deposit on a surface, formed chemically or electrochemically. Prepreg/B-Stage Resin: Sheet of material that has been impregnated with a resin and cured to an intermediate stage. Printed Circuit Board (PCB): A pattern of conductors printed on to the surface of an insulating base to provide interconnection of parts. Registration: The degree of conformity of the position of a pattern (or portion thereof), a hole or other feature to its intended position on a product. Reflow Soldering: A process for joining parts by tinning the mating surfaces, placing them together, heating until the solder fuses and allowing to cool in the joined position. Resin Recession: The presence of voids between the plating of a plated-through hole and the wall of the hole as seen in microsection of plated-through holes that have been exposed to high temperatures. Resin Smear: Base material resin that covers the exposed edge of conductive material in the wall of a drilled hole. (This resin transfer is usually caused by the drilling operation). 4 ISRO-PAX-304 Rigid Double-Sided PCB: Double sided PCB, either printed circuit or printed wiring, using rigid base materials only. Rigid-flex PCB: PCB with both rigid and flexible base materials. Rigid-flex Double-Sided PCB: Double‐sided PCB, either printed circuit or printed wiring, using combinations of rigid and flexible base materials. Rigid-flex Multilayer PCB: Multilayer PCB, either printed circuit or printed wiring, using combinations of rigid multilayer and flexible single and double sided base materials. Rigid PCB: PCB using rigid base materials only. Rigid Single-Sided PCB: Single‐sided PCB, either printed circuit or printed wiring, using rigid base materials only. Rigid Multilayer PCB: Multilayer PCB, either printed circuit or printed wiring, using rigid base materials only . Solder Coat: A layer of solder applied to the printed board conductive path directly from a molten Solder bath. Solderability: The ability of a metal to be wetted by molten solder. Soldering: A process of joining metallic surfaces with solder, without melting the base material. Scratch: Narrow groove in a surface of laminate. Test Board: A printed board suitable for determining acceptability of one board or a batch of boards produced with the same process in order to be representative of the production board. Test Coupon: A portion of the quality conformance test circuitry used for a specific acceptance test or group of related test. Test Point: Special points of access to an electrical circuit, used for electrical testing purposes. Twist: The deformation parallel to a diagonal of a rectangular sheet such that one of the corners is not in the plane containing the other three corners. Test Pattern: Part of the PCB that refers to the copper pattern on and within the PCB laminate for a specific test. Undercut: The distance, measured parallel to the surface of a printed board, from the outer edge of a conductor (excluding over plating and coatings) to the maximum point of the indentation on the same edge of the conductor. (refer overhang image). 5 ISRO-PAX-304 Weave Exposure: A base material surface condition in which unbroken fibers of woven glass cloth are not completely covered by resin. Weave Texture: A surface condition of base material in which a weave pattern of cloth is apparent although the unbroken fibers of woven cloth are completely covered with resin. 3.2 Abbreviations BBTBare Board Test BGA Ball Gridded Array CAD Computer Aided Design CAM Computer Aided Manufacturing CCGA Ceramic Column Grid Array CVCM Collected Volatile Condensable Material DWV Dielectric Withstanding Voltage ICR Interconnection Resistance IR Insulation Resistance m Minor Non-conformance M Major Non-conformance MRB Material Review Board / NCRB NA Not Applicable NCRB Non-Conformance Review Board PCB Printed Circuit Board PID Process Identification Document PTFE Poly Tetra Fluoro Ethylene PTH Plated-Through-Hole r.m.s. Root-Mean-Square SMD Surface Mount Devices TCH Test Coupon Horizontal TCV Test Coupon Vertical TML Total Mass Loss 3.3 Process Identification Document (PID) Before commencements of qualification activity the manufacturer shall submit a draft copy of the process identification document which specifies the process steps and specifications that shall apply to meet the high reliability requirements. 6 ISRO-PAX-304 The PID shall contain the following as a minimum. • Production flow chart • Specification of raw materials and semi-finished products which become a part of the product • Equipment & Machines used in the fabrication process • Process specifications and tolerances • In-process quality control inspection points • Accept/reject criteria for in-process QA/QC • Process traveler formats • Non Conformance management • Functions of all key personnel involved The draft PID shall be reviewed and approved by QA/QC of concerned ISRO centre prior to commencement of the qualification of the process. The stages of ISRO interaction shall be projected in the request for proposal and mutually agreed during the PID review. 3.4 Test Programme The test programme shall consist of Qualification (Certification) tests (as given in para.5) in order to ensure the capability of the manufacturer to meet the quality and reliability requirements. 3.5 Qualification Test Pattern/Layout Layout used for processing the PCBs shall be made in accordance with the guidelines given in ISRO Specification on “Design requirements for PCB layouts” ISRO-PAX-301 issue 3. Only Layouts approved by the QA/QC of ISRO centre concerned shall be used for processing the onboard PCBs. However for process qualification activities ISRO will provide the Gerber file along with relevant data. 3.6 Laminates 3.6.1Copper Clad Laminate The Copper Clad Laminate for individual layers shall be of type FR4 / FR5 and shall meet the requirements of IPC 4101/24 or 4101/29 or equivalent type and copper thickness shall be as specified below. 3.6.2Base Laminate Dielectric thickness of penultimate layers shall be minimum 150 microns. However, in no case dielectric thickness shall be less than 90 microns. Nominal Thickness in mm 0.10 0.15 0.175 Tolerance in mm ± 0.010 (For core only) ± 0.025 ± 0.025 7 ISRO-PAX-304 Nominal Thickness in mm 0.200 0.250 0.300 Tolerance in mm ± 0.038 ± 0.038 ± 0.038 3.6.3Copper Cladding The Copper Cladding shall be as specified in layout and in no case be less than ½ oz with following tolerances. Type ½ oz 1 oz 2 oz Nominal Thickness in microns 18 35 65 Tolerance in microns ±4 ±5 ±5 3.6.4Laminate Properties Specifications and Properties of Laminates, bonding material and resin system shall be in accordance with IPC 4101 (Applicable only for FR-4 high Tg laminates). 3.6.5Bonding Sheet (Prepreg) The bonding interlayer material shall be pre-impregnated (B stage) glass cloth conforming to IPC 4101. 3.7 MLB Configuration The Copper cladding for the individual layers shall be as under: • External signal layers: In general 1 oz Copper (35 ± 5 microns). Special case min ½ oz Copper (18 ± 4 microns) • Internal signal layers: 1 oz Copper (35 ± 5 microns) or 2 oz Copper (65 ± 5 microns) While cutting the prepreg for individual layers it shall be cut in the same direction of the glass cloth so as to avoid internal stresses after pressing. The stack up of the multilayer shall be equally balanced or symmetric. If there is only a single ground/power plane it shall be positioned towards the middle of the assembly. If there are two ground/power planes they shall be positioned symmetrically inside the cross section of the assembly.The component side of the MLB is referred as the top side or layer1.The layer immediately below the component side is layer 2.The layer preceding the soldering side is the (n-1)th layer and the layer corresponding to the soldering side is the nth layer or bottom layer.The 1st and the nth layers are referred as the external layers and all the remaining are internal layers. 3.8 Production of PCBs PCBs shall be manufactured using the Gerber file supplied by the ISRO centre. Dimensional and Tolerance requirements shall be as per Table 1. 8 ISRO-PAX-304 3.8.1Production Lot PCBs manufactured to this specification shall form a part of uniform production lot. All the boards delivered shall be from the same batch and a batch can have multiple panels. All the boards shall be delivered along with the traveler sheet. 3.8.2Workmanship Boards shall be uniform in quality and free from dirt, dust, grease, oil, finger prints, corrosion products, salts, ionic contamination and other defects that affect the quality endurance and serviceability. Boards shall also be free from defects mentioned in para.6.2. 3.9 Plating 3.9.1Internal Layers There shall be no protective plating on the internal layers. Copper plating for the desired levels are allowed for buried via PCBs. 3.9.2Thickness (electroless copper) The electroless copper shall be of sufficient thickness so as to aid further electro deposition for thickness buildup and shall be homogeneous without voids, pores etc. 3.9.3Thickness (electro-deposited copper) • On surface: The electro-deposited copper thickness shall be in the range of 35 ± 10 microns over and above base copper • In holes: The electro-deposited copper thickness inside hole barrels shall be 35 ± 10 microns 3.9.4Surface Finish After Hot air solder leveling, the solder thickness shall be a minimum of 8 microns when measured at the crest. Just coverage (@1µm) is acceptable at the knee and edges of tracks. 3.9.5Workmanship-plating There shall be no surface cracks, scratches exposing copper or residues of metallization. Inside the PTH barrel, the metallization shall not have any interruption which electrically isolates two sides, areas, nor any lack of metallization exposing the base material. There shall be no plating residues inside the holes. There shall be no evidence of any lifting or separation of plating from the surface of the conductor patterns or of the conductors from the base glass epoxy material. Reflowed tin-lead plating shall cover the conductor patterns uniformly and be free from scratches, nicks and voids. There shall be no copper visibility when examined at 10X. There shall be no traces of flux residues or fusing salts. 9 ISRO-PAX-304 Table 1: Dimensional and Tolerance Requirements (For finished PCBs) Conductors and Pads Conductor width (min) Conductor width tolerance Specifications 0.2 mm general; 0.15 mm (special cases) ±10% 0.05 mm minimum. Internal and external layer pad dimensions shall be same in design. 0.130 mm (min.) 0.250 mm (min.) ≤ Total copper thickness 1.20 mm min. 1.00 mm (Special Case vias) Internal Annular ring External Annular ring for PTH External Annular ring for NPTH Undercut Internal /External Pad Dia Spacing Conductor to edge of board Internal layer External layer Layer to layer spacing Coplanar conductor spacing Conductor to free hole spacing Holes Minimum hole dia 1.00 mm min 1.00 mm min 0.09 mm min (Except for penultimate layers) 0.20 mm min; 0.1 mm (special cases) 0.5 mm 0.50 mm finished; 0.4 mm (special cases) +0.05/-0.00 mm upto 1 mm ∅ holes +0.10/-0.00 mm beyond 1mm +0.10/-0.00 mm PTH hole dia tolerance NPTH hole dia tolerance Plating Surface: 25 to 45 microns Holes 25 microns min. Minimum 8 microns at crest and 1 micron at edges Tin-lead thickness & knee Reduction in conductor width due to cuts & nicks 10% or 0.1 mm whichever is less Fabrication allowance (this shall be taken care during fabrication and should not have effect on finished 0.44 mm; 0.34 mm (Special Cases) dimensions) Layer to layer mis-registration 0.25 mm max. For wrap 1.0% max of maximum board dimension Warp and Twist For twist 1.0% max of diagonal board dimension. Composite board thickness ± 10% of nominal or + 0.15 mm Board size tolerance ± 0.2 mm Copper thickness 3.10Conductors Conductors and terminal areas shall be formed as per the Gerber file/master pattern. The edges shall not exceed a maximum roughness of 0.08 mm from peak to valley as measured along any conductor edge over any 10 mm length. 10 ISRO-PAX-304 3.10.1Under Cutting Under cutting at each edge of the conductors shall not exceed total thickness of clad (foil) and plated copper. 3.10.2Holes Holes in the boards both supported (PTH) and unsupported (Non-PTH) shall be free from defects like chipping, torn clad, delamination, burrs, tears, drags, measling, base material exposure around the hole and cracks. A maximum variation of 5 deg and an eccentricity of 0.1 mm shall be accepted. Drilling irregularities shall be less than 0.08 mm. Other feature size / tolerances shall be as per Table 1. 3.10.3Plated Through Holes (PTH) Unless otherwise specified in the gerber file, all the solderable holes shall be plated through. Hole diameters shall be as specified in the gerber file/master pattern. Tolerance of the hole diameter and the hole location shall be as specified inTable 1. Hole diameters specified in gerber file shall be those of completely processed holes including plating, unless otherwise specified. The following requirements shall also apply to plated through holes: 1. When cross sectioned and visually inspected the individual layers of metallization shall be homogeneous and free from defects mentioned in para 3.10.2 2. Internal layers of plated through hole metallization shall not have interruptions which electrically isolate two sides of a board 3. Holes shall be smooth and there shall be no projection of metallization greater than the average wall thickness 4. Holes shall be free from nodules in the hole wall, which reduce the specified hole size 5. Selective plating of hole wall alone shall not be accepted 3.10.4Solderable Pads and Terminal Areas Shape and size of solderable pads and terminal areas shall be as specified in the gerber file. The solderable pads and terminal areas shall not have pin holes or voids extending upto the base material irrespective of their size.The minimum pad size shall be as per Table 1. 3.10.5Annular Ring Annular ring when inspected shall not be less than 0.13 mm for supported holes (PTH) and 0.25 mm for unsupported holes. In case of mechanically fitted parts like turret terminals etc that are to be soldered, the solderable pads shall have a minimum of 0.25 mm of conductor encircling the abutted metal for Non-PTH boards. 11 ISRO-PAX-304 3.11Defects in PCBs Defects in PCBs shall be classified as given below. 3.11.1Major Defect / Non-conformance (M) Major defects shall be those defects which may result in a failure of the board or significant reduction of its functional usability for the intended application. At any stage of the test, unless otherwise specified in the test method, boards shall generally be considered as functionally usable when it meets the requirements specified in this document. The major defects in boards are identified in para. 6 along with accept/reject criteria. 3.11.2Minor Defect / Non-conformance (m) Minor defects shall be those defects which are unlikely to reduce significantly the functional usability of a board for its intended application or those which are only minor deviations from the specified requirements and are not likely to jeopardize the performance of a board during its intended use.10 minor defects shall be treated as one major defect. The minor defects in boards are identified in para.6 along with accept/reject criteria. 12 ISRO-PAX-304 4 EVALUATION The PCB manufacturer/vendor shall request for evaluation of the boards prior to actual process qualification activity. They shall supply 3 nos. of evaluation PCBs. If the result is satisfactory, then the qualification programme for each of the technologies that have been evaluated can be taken up.The evaluation tests shall be an appropriate subset of the tests performed within the qualification programme. 4.1 Request for Evaluation The PCB manufacturer’s request for evaluation shall contain: • A description of the technology for which the PCB manufacturer wishes to be evaluated • A description of the manufacturing line • Experience 4.2 Evaluation of PCBs The PCB manufacturer shall produce three evaluation PCBs with the materials, processes and equipment that are intended for use in subsequent production. The evaluation PCBs shall be representative in terms of technology for which the PCB manufacturer applies for qualification. • Dimensions of the boards, vias, pads and tracks • Number of layers • Pattern design The PCB manufacturer shall perform the evaluation test and document, it in conformance with para 7.10. The evaluation PCBs shall be provided with associated test coupons and traveler sheet. • Evaluation tests like, initial visual inspection, solder dip followed by microsection and rework simulation tests on the samples submitted shall be carried out. If samples fail the evaluation tests, PCB manufacturer shall resupply samples along with close out note with data analysis and root cause of the problem noticed, if consequently three such iterations are failed qualification exercise shall be terminated 4.3 Facility Visit Before or After evaluation PCBs are accepted, QA/QC /Audit team of ISRO Centres/Task team shall audit the manufacturing line when PCB production is in progress. During the audit, the PCB manufacturer shall make the following documents available to the audit team: 1. Names and functions of all key personnel involved 2. Identification of the parameters of the technologies 3. List of materials and equipment (including types and names of companies) used for production of PCBs 13 ISRO-PAX-304 4. Incoming material inspection, certificate of compliance monitoring, in-process inspection plans 5. List of process and control specifications with number, issue number and date of issue 6. Production flowchart, including quality assurance inspection point and relevant process specification 7. Route card/Traveler card/In-process log sheet of the PCBs under investigation or audit 8. Details of facility like metallographic examination, chemical analysis, failure analysis, mechanical and electrical test including functional testing of PCBs and acceptance test plans 4.4 Qualification Program Flow 1. Vendor’s request for the process qualification submitting brochures regarding process types, equipments, capacity, capability and list of important certifications obtained 2. Documentation review by QA/QC of ISRO centre concerned 3. Communication to the manufacturer regarding submission of PID by the manufacturer to QA/QC of ISRO centre concerned 4. Preliminary review of the PID by QA/QC of ISRO centre concerned 5. If PID review results are satisfactory, ISRO centre concerned shall supply test pattern design/gerber file to the PCB manufacturer in the format listed in ISRO-PAX-301 along with the test coupon gerber files. 6. Input data verification, panelization and attachment of test coupons to the test pattern PCB and submission of panel gerber file to QA/QC of ISRO centre concerned for review and approval. This is to carry out the panelization process and test coupon attachment process correctness 7. Review of panel design and clearance by QA/QC of ISRO centre concerned 8. Fabrication of PCBs strictly as per PID and submission of 9 MLBs to QA/QC of ISRO centre concerned after conduct of acceptance tests on one set of coupons by the manufacturer. Acceptance tests shall be conducted as per para. 7.10 by manufacturer 9. Conduct of acceptance tests on the remaining two coupons by the ISRO centre concerned 10. On completion of successful acceptance tests, qualification tests as per this document shall be conducted 11. Review results of qualification tests and issue of certificate if found satisfactory. If samples fails in test, non-conformance control listed in para 7.11 shall be exercised and resubmit the samples for qualification. If three such iterations are unsuccessful qualification exercise shall be terminated 14 ISRO-PAX-304 5 QUALIFICATION 5.1 General A qualification programme shall be initiated in the following cases: 1. Initial qualification 2. When previous qualification is more than two years old and maintenance of qualification was not assured 3. Interruption of the manufacturing of the PCBs for more than two years 4. Use of new technology or materials 5. Change in the manufacturing line for example, any changes in material, chemical products, mechanical processing parameters,equipments and key personnel 6. The manufacturing line is moved to another location 5.2 Qualification Programme Definition and Approval • After successful evaluation, qualification programme shall be initiated • The qualification programme shall identify: 1. The test houses/Labs 2. The test procedure and test sequence 3. The proposed schedule of testing 5.3 Non-conformance Criteria The non-conformances shall be dispositioned in conformance with ISRO-PAS-100 :: Issue 3 • Major non-conformances (M) shall be disposed off at a non-conformance review board (NCRB) /Task Team established by the appropriate ISRO authority having a representative from the PCB manufacturer • Minor non-conformances (m) shall be: 1. Impact analysis by QA/QC of the ISRO centre concerned 2. Processed through an internal NCRB to determine the causes and consequences 3. Reported in the qualification test report 5.4 Qualification Programme Implementation • The qualification programme shall be performed by qualification team of the ISRO centre concerned • The qualification programme shall be performed in conformance with the test sequence specified in Figure 1 and the group tests are listed in Table 2. Specification and test procedures are detailed in para.6 • A qualification test report shall be prepared after completion of tests listed in para.6 • If the PCBs are used for manned space programmes, PCB base material is tested for the following items 1. Base material is to be tested for flammability and toxicity (odour) in addition to outgassing 15 ISRO-PAX-304 9 PCBs with two sets of coupons (H & V) BBT tested Group 1: (7 PCBs with one set of coupon) On PCB: Preconditioning, Cleaning, Visual examination, Warp and Twist, Continuity test, ICR test, IR inter and intra layer, DWV test Inter & Intra layer On Coupons: Peel strength, Bond strength, Solderability, initial micro section, ICR, Rework simulation, Solder dip Group 2 (1 PCB) • Hot storage. o Warp & Twist o Visual Inspn • Cold storage. o Warp & Twist o Visual Inspn • Vibration fatigue. o Warp & Twist o Visual Inspn oContinuity oMicrosection Group 3 (2 PCBs) Group 4 (2 PCBs) Group 5 (2 PCBs) • High. Temp. dip. Test (Hot oil dip). o Warp & Twist o Visual inspection o Peel strength o Bond strength oContinuity oInterconnection resistance oMicrosection • Thermal cycling o Visual inspection o Peel strength oContinuity oInterconnection resistance o IR & DWV oMicrosection • current over load • Long term damp heat. o Visual inspection o Peel strength oContinuity oSolderability ICR o IR & DWV oMicrosection 1 PCB as reference Group 6(1 PCB with one set of coupon) On PCB • Cleaning. • Preconditioning • Visual examination. • Plating adhesion On Coupon • Initial microsection • Solderability. • ICR, Solder dip & post dip ICR. • ICR Rework simulation & post rework ICR • Water absorption • TML & CVCM of laminate & solder mask On PCB • Compatibility to fabrication line tests. This includes cleaning, baking, swaging, soldering, reworking, potting, ecco bonding and conformal coating etc. Figure 1: Qualification Test Matrix Table 2:Test Specification Group Group Tests Visual inspection tests on boards Preconditioning Cleaning Verification of marking Visual aspects External dimensions of boards Warp Twist Specific dimensional check Electrical measurements on boards Intra layer insulation resistance (Zone A) Group 1 Inter layer insulation resistance (Zone H) Interlayer dielectric withstanding voltage (Zone H) Intralayer dielectric withstanding voltage (Zone A) Continuity (Zone D) Interconnection resistance (Zone E) On one set of coupons Peel strength, bond strength(TCH8, TCH5) Solderability(TCH11) Initial microsection(TCH2) 3 times solder dip (with pre and post ICR & microsection) :: (TCH4) Plating measurements, Pull test & microsection :: (TCH2 / TCH5) 16 Para. 6.2 6.1.1 6.1.2 6.2.2 6.2.3 6.2.4 6.2.5 6.2.6 6.2.7 6.2.8 6.2.8.1 6.2.8.2 6.2.8.3 6.2.8.3 6.2.8.4 6.2.8.5 6.2.9.1 & 6.2.9.2 6.2.9.3 6.2.10 6.4.3 6.4.4 No of PCBs 7 PCBs ISRO-PAX-304 Group Group Tests Hot Storage Monitoring tests Warp & Twist Defects in base material Defects in pattern Defects in protective plating Plated through hole requirements Cold Storage Monitoring tests Warp & Twist Group 2 Defects in base material Defects in pattern Defects in protective plating Plated through hole requirements Vibration Fatigue Monitoring tests Visual inspection Electrical continuity (If feasible, throughout vibration is preferred ) Warp & Twist Microsection Hot Oil Dip Monitoring tests Warp & Twist Visual inspection (Measling / De-lamination) Group 3 Peel strength Bond strength Continuity Interconnection resistance Microsection Thermal Cycling Test Monitoring tests Visual inspection Peel strength Continuity Interconnection resistance Group 4 Intralayer insulation resistance Interlayer insulation resistance Intralayer dielectric withstanding voltage Interlayer dielectric withstanding voltage Microsection 17 Para. 6.3.1 No of PCBs 6.2.5 & 6.2.6 6.2.3 6.2.3 6.2.3 6.2.3 6.3.2 6.2.5 & 6.2.6 6.2.3 6.2.3 6.2.3 6.2.3 6.3.3 1 PCB 6.2.3 6.2.5 & 6.2.6 6.2.10 6.4.2 6.2.5 & 6.2.6 6.2.3 6.2.9.1 6.2.9.2 6.2.8.4 6.2.8.5 6.2.10 6.5 6.2.3 6.2.9.1 6.2.8.4 6.2.8.5 6.2.8.1 6.2.8.2 6.2.8.3 6.2.8.3 6.2.10 2 PCBs 2 PCBs ISRO-PAX-304 Group Group Tests Long Term Damp Heat Test Monitoring tests Visual inspection (Evidence of corrosion) Peel strength Intralayer insulation resistance Interlayer insulation resistance Group 5 Intralayer dielectric withstanding voltage Interlayer dielectric withstanding voltage Inter connection resistance (ICR) Solderability Current over load (Zone E) Microsection Assembly Compatibility Test Preconditioning Cleaning Visual inspection Initial microsection :: Coupon Solder dip :: Pre, post ICR & microsection :: Coupon Plating measurements, Pull test & microsection Group 6 Solderability :: Coupon Water absorption : Board-cut coupon TML & CVCM of laminate & solder mask :: Coupon Para. 6.6 6.2.3 6.2.9.1 6.2.8.1 6.2.8.2 6.2.8.3 6.2.8.3 6.2.8.5 6.2.9.3 6.2.8.6 6.2.10 6.7 6.1.1 6.1.2 6.2.3 6.2.10 6.4.3 6.4.4 6.2.9.3 6.7.2.1 6.7.2.2 No of PCBs 2 PCBs 1 PCB Fabrication compatibility like; Cleaning, baking, swaging, soldering, reworking, potting, ecco bonding and conformal coating etc. Followed 6.7 by thermal vacuum cycling 5.5 Qualification PCBs 5.5.1General • The qualification PCBs shall have test patterns as given in the ISRO approved gerber file which includes patterns for evaluation of the specific characteristics, summarized in Table 2 and details are described in para. 6 • The qualification PCB shall consist of a test pattern demonstrating the technological capability (Annexure 1) together with the other test patterns • The test pattern layout and design shall be in conformance with the design shown in this document or shall comply with ISRO-PAX-301, Issue 3 • Qualification test pattern designs are shown in para 9 and it shall be agreed between PCB manufacturer and QA/QC of ISRO centres concerned /qualification authority 5.5.2Test Pattern A: Electrical Test • The following measurements shall be performed on test pattern A (Figure 2) 1. Intralayer insulation resistance 2. Dielectric withstanding voltage 18 ISRO-PAX-304 • The conductor width and spacing within each layer shall represent the minimum dimensions to be qualified Figure 2: Example of test pattern for intralayer insulation resistance and dielectric withstanding voltage 5.5.3Test Pattern B: Mechanical Test • The following measurements shall be performed on test pattern B 1. Peel strength of copper track on laminate 2.Pull‐off strength of Non-PTH pads Figure 3: Example of test pattern for testing peel strength of conductors and pull-off strength of Non-PTH pads 19 ISRO-PAX-304 5.5.4Test Pattern C: Electrical Test • The internal short circuit shall be measured on test pattern C 1. This consists of verifying the insulation between plated-through holes in daisy chain through all layers and ground plane 2. Bottom set is a (penultimate) layer daisy chain to be used for rework simulation Figure 4: Example of test pattern for internal short circuit testing 5.5.5Test Pattern D: Electrical Test and Visual Aspect • The following measurements shall be performed on test pattern D: 1.Marking 2. Etching definition 3. Continuity between plated‐through holes in daisy chain through all layers 4. Visual aspects Figure 5: Example of test pattern for etching definition evaluation and continuity testing 5.5.6Test Pattern E: Electrical Test • The following measurements shall be performed on test pattern E: 1. Interconnection resistance between plated-through holes in daisy chain through all layers before and after thermal cycling and thermal stress 20 ISRO-PAX-304 2. Current overload between plated-through holes in daisy chain through all layers for short and long duration Figure 6: Example of test pattern for interconnection resistance and current over load testing 5.5.7Test Pattern F: Metal-Plating Evaluation and Pull Test • The following measurements shall be performed on test pattern F: 1. Microsectioning to measure metal plating thickness. Microsectioning after thermal cycling, thermal stress and damp heat (optional). 2. PTH Pull test Figure 7: Example of test pattern for metal plating evaluation & pull test 5.5.8Test Pattern G: Surface Solderability Test • The following measurements shall be performed on test pattern G: 1. Surface Solderability 2. Plating adhesion 3. Solder mask adhesion test (As per IPC-TM-650 Test method 2.4.28.1) 21 ISRO-PAX-304 Figure 8: Example of test pattern for plating adhesion testing and analysis of Sn Pb coating composition after reflow 5.5.9Test Pattern H: Electrical Test • The following measurements shall be performed on test pattern H 1. Interlayer insulation resistance and dielectric withstanding voltage before and after thermal cycling and optionally after damp heat 2. Interlayer insulation resistance and dielectric withstanding voltage measured between plated-through holes and a central ground plane Figure 9: Example of test pattern for interlayer insulation resistance and dielectric withstanding voltage testing 5.5.10Test Pattern J: Solderability Test and Rework Simulation • The following measurements shall be performed on test pattern J 1. Solder wettability of pads and plated-through holes 2. Rework simulation on plated-through holes 22 ISRO-PAX-304 Figure 10: Example of test pattern for solder wettability and rework simulation testing 5.5.11Test Pattern K: Physical Test • The following measurements shall be performed on test pattern K 1. Water absorption 2. Out gassing test on base laminate material as per ISRO procedure Figure 11: Example of test pattern for water absorption and outgassing testing 5.5.12Test Pattern L: Demonstration of Technological Capability • The following measurements shall be performed on test pattern L 1. Minimum conductor width 2. Minimum spacing 3. Minimum hole diameter 4. Other features that characterize the level of technological capability of the PCB design in terms of dimensional outline, build-up and non-standard use of materials 23 ISRO-PAX-304 Figure 12: Example of test pattern for evaluation of the technological capability 5.5.13Test Pattern M: CAD/CAM Criteria (Optional) • The CAD/CAM capability of the PCB manufacturer shall be evaluated on test pattern M by visual inspection • For this purpose the layout of the test pattern shall 1. Be divided into 3 zones with identical surfaces 2. Have various pads in each zone (circular, oblong, square, rectangular) 3. Have a thermal shunt for internal layers 24 ISRO-PAX-304 Figure 13: Example of test pattern for evaluation of CAD/CAM capability 5.6 Qualification Approval 1. After successful qualification of all the tests mentioned in this document, manufacturing process of the PCBs will be declared as qualified for the manufacture of PCBs for onboard use 2. Process Identification Document shall be prepared by the manufacturer and submit for review to the QA/QC of ISRO centres concerned 3. During qualification exercise, in each group tests one major defect is allowed provided total qualification program shall not have more than two major defects. Also, major defect observed during qualification program shall be addressed and closed through the regular non-conformance management process 4. The qualification approval shall be valid for a period of two years and final corrected PID shall be submitted to QA/QC of ISRO centres concerned before actual production 5.7 Maintenance of Qualification Maintenance of certification shall be carried out in the following manner 1. Periodic (Once in 6 months) facility audit at manufacturer’s site by the ISRO centre concerned 2. Verification of Qualification shall be carried out once in every two years or if the manufacturer has not supplied flight grade PCBs for past six months Incremental or Re-qualification shall be carried out, if; • Consistency in the quality is not maintained & assured • Changes made in the process, materials, PID, devices, laminates, key personnel or changing of equipment layout (Plant layout) 25 ISRO-PAX-304 6 TESTS 6.1 General 6.1.1Pre-conditioning Unless otherwise specified, all tests shall be carried out under the conditions specified below • Room temperature: (22 ± 3) °C • Relative humidity: (55 ± 10)% • Normal Atmospheric pressure • Before testing is started, the PCBs shall be subjected for 48 h to ambient conditions • The PCBs to be tested shall not be covered with a protective varnish • During the testing period, the following precautions shall be taken: - Keep the boards flat against a plane surface - Protect boards used for electrical tests from any contamination and hold them only by their edges during the tests • Before environmental exposure, soldering operation, electrical and mechanical testing, clean the boards in conformance with para 6.1.2 6.1.2Cleaning Prior to the test programme all the boards shall be ultrasonically cleaned for 5 minutes using approved solvents. Purity of the cleaning solvent shall be such that any residue does not exceed 5 micro gram/cc of solvent. After cleaning the boards shall be dried at ambient temperature for five minutes. 6.1.3Bare Board Testing (BBT) Bare board Testing shall be performed in accordance with IPC-9252 (Guidelines and Requirements for Electrical Testing of Unpopulated Printed Boards). In case of controlled impedance boards, testing shall be performed to assure the impedance requirements as specified in PCB ordering sheet. Spool/gerber file data used for PCB manufacturing shall be used for extracting the BBT net list. Testing shall be performed for both continuity and isolation after the hot air leveling of the PCB. If inner layer net open failure is detected after hot air leveling of PCBs, it shall be reported and all the PCBs from this panel shall be subjected for non-conformance review. If only one card is available per panel and if the board fails in BBT at open mode after Hot Air Leveling, then the card has to be rejected after establishing the root cause of failure. Net continuity shall be tested using 100 mA current with 5 ohms or less threshold. Isolation shall be tested with a minimum of 100 mil proximity rule at 250V with a minimum of 6 mega ohms threshold. All the power/ ground/split planes shall be tested for isolation with all other nets in the PCB. Bare board test report shall be preserved along with other test reports by the manufacturer. 26 ISRO-PAX-304 A BBT OK sticker shall be affixed on the board which passes the test. BBT test report shall be provided along with PCBs. BBT sticker shall not leave residues that affect the quality of bare PCBs. 6.2 Group 1:Visual Inspection and Non-destructive Test 6.2.1General All qualification PCBs shall undergo visual and dimensional checks. Unless otherwise specified the requirement criteria are as per Table 1 &Table 8. 6.2.2Verification of Marking • Each board shall be inspected with the naked eye for correct marking • The marking shall be legible and resistant to test stresses. The non-conformance criteria shall be as follows: 1. Identification impossible M 2. Marking not conforming to the specification M 3. Defects not affecting identifications m 6.2.3Visual Aspects • Each board shall be inspected by magnification ≥ 10X with suitable lighting conditions to verify that construction and workmanship meet the requirements • In case of any irregularity, the area shall be examined at higher magnification • The non-conformance criteria for the general cleanliness and contamination shall be as follows: 1. Contamination visible to the naked eye and not removable by cleaning according to para 6.1.2 2. Contamination visible to the naked eye and removable by cleaning according to para 6.1.2 6.2.3.1Laminate Defects 1. Scratches, cutting glass fibre or leaving marks in the dielectric laminate 2. Superficial Scratches on the surface of the laminate 3. Dents, crazing and haloing • Visible with naked eye m M m M 4. • Only visible with magnification aids (10X) Non-homogeneity regarding coloring and opacity 5. Discoloured copper oxide layer on internal layer is acceptable; 6. Inclusion of foreign material,blistering or air bubbles: • M Visible with naked eye m m/M M • Only visible with magnification aids (10X or more) 7.Delamination m M 8.Measling • General measling spread over the whole PCB 27 M ISRO-PAX-304 • Total measling area > 2% of board surface area M • Local measling that causes reduction of insulation distance in the outer layer to below the requirement M Continuous measling size > 10 sq. mm M • • 9. Local measling that does not cause reduction of insulation distance in outer layer to below the requirement Fungus growth m M 6.2.3.2Non Plated Through Hole Defects The non-conformance criteria for non‐plated‐through holes shall be as follows: 1. Holes plated unintentionally 2. Incompletely drilled holes, missing or additional holes M M 6.2.3.3Routing Defects The non-conformance criteria for the routing shall be as follows: 1. Incomplete routing of board, such that dimensional or mechanical requirements are not met 2. Arbitrary cutting defects that remain acceptable within the dimensional requirements M m 6.2.3.4Surface Metallization Defects The non-conformance criteria for the surface metallization shall be as follows 1. Conductors or pads not conforming to given specification M 2. Terminal pads or conductors partially or completely missing M 3. Terminal pads or conductors that are cut M 4. Terminal pads or conductors forming a short circuit M 5. Lifting/delamination of conductive pattern from laminate M 6. Scratches in the SnPb metallization exposing the underlying copper plating M 7. Copper or nickel visible on top/sides surface plated areas M 8. Large number of superficial scratches not attributed to a manufacturing process evidencing bad workmanship M Dewetting of fused tin lead finish on solder pads M 9. 10. Granular surface structure of fused tin lead finish on solder pads 11. Corrosion of exposed copper m/M M 6.2.3.5Plated Through Hole Defects The non-conformance criteria for plated‐through holes shall be as follows: 1. Incompletely drilled, additional or missing holes M 2. Partially or completely missing metallization 3. Component holes ≥ 0.6 mm filled or partially filled with solder resulting in a diameter smaller than the requirement m 28 M ISRO-PAX-304 6.2.3.6 Conductor Defects The non-conformance criteria for arbitrary defects of conductors and terminal pads shall be as follows (Refer Figure 14 and Figure 15). 1. a ≤ 20% of x and minimum conductor width > requirement m 2. a > 20% of x M 3. Minimum conductor width < requirement M 4. b ≤ x m 5. b > x M 6. Opposite peaks: if z < 80% of y M 7. Isolated peaks or valleys: h > 20% of x and z < requirement M 8. Conducting island: a + h > 20% of y and the isolation spacing < requirement M 9. Minimum remaining spacing y-a < requirement M 10. b > y M X: normal conductor widh Figure 14: Arbitrary defects on conductors Y: Nominal spacing between conductors Figure 15: Arbitrary defects on spacing between conductors 6.2.4External Dimensions • Each board shall be measured by means of suitable standard measuring equipment to verify that the physical dimensions, including board thickness and external dimensions meet this specification/ supplied design data • The non-conformance criteria for the thickness of base laminate (average of 4 measurements on the board) shall be as follows: o Thickness not conforming to tolerance limits of the specification (+10% or 0.15 mm and whichever is less) M • The non-conformance criteria for the length and width of board (average of 4 measurements on the board) 29 ISRO-PAX-304 shall be as follows: o Length or width not conforming to tolerance limits (+ 0.2 mm) of specification M 6.2.5Warp or Bow • The PCBs shall be placed unrestrained on a plane horizontal surface with the convex side upward • The warp shall be expressed in percentage terms • The maximum warp between the plane horizontal surface and the PCB Shall be measured as defined in Figure 16 • The length of the PCB shall be measured • The warp percentage shall be calculated as per following equation Warp or bow % = Max.bow in mm Length of the PCB in mm *100 • The non-conformance criteria shall be as follows: o Warp >1% (for CCGA > 0.75%) M Figure 16: Warp or Bow 6.2.6Twist • The PCB shall be placed on a plane horizontal surface so that it rests on three corners • The twist shall be expressed in percentage terms • The distance between the plane horizontal surface and the fourth corner of the PCB shall be measured as defined in Figure 17 • The length of the diagonal shall be measured • The twist percentage shall be calculated as per following equation Twist % = Max.twist in mm Length of the diagonal in mm 30 *100 ISRO-PAX-304 • The non-conformance criteria shall be as follows: o Twist >1% (for CCGA > 0.75%) M A, B and C are touching base Figure 17:Twist 6.2.7Specific Dimensional Check Two PCBs shall be used for the tests. • Minimum and maximum plated-through hole and soldering pad diameter • Minimum and maximum conductor width • Minimum and maximum distance between conductors • The measurement of dimensional parameters relating to metal plating shall be taken at the copper/board base interface (Figure 20). Examples for dimensional parameters relating to metal plating are width of conductor, spacing between conductors, minimum annular ring diameter. Hole diameter can be measured with gauges / microscope • The non-conformance criteria shall be as follows 1. Dimensions not conforming to the circuit definition document and acceptable tolerance limits of the given specification M NOTE: Example of such dimensions are diameter of holes, width of conductors and diameter of terminal pads. 2. Diameter of non-soldering holes not conforming to tolerance limits of given specification m 6.2.8Electrical Measurement Methods 6.2.8.1Intralayer Insulation Resistance on Test Pattern A • A direct voltage of (500 ± 50) V shall be applied between the two closest conductors that are not electrically connected • The insulation resistance (R) shall be measured 1 minute after the voltage has been applied • The non-conformance criteria shall be as follows: R < 1x1010 Ω Before environmental tests R < 1x109 Ω After environmental tests 31 M M ISRO-PAX-304 6.2.8.2Interlayer Insulation Resistance on Test Pattern H • The test shall be carried out as per para.6.2.8.1 and 6.2.8.2 • The voltage shall be applied between two ground planes or between one ground plane and one conductor that are superimposed, i.e. on two separate adjacent layers • The non-conformance criteria shall be as follows R <1x1011 Ω Before environmental tests R <1x1010 Ω After environmental tests M M 6.2.8.3Dielectric Withstanding Voltage Intralayer on Test Pattern A and Interlayer on Test Pattern H • For interlayer measurements the test voltage shall be applied between two super imposed conductors (i.e. between layers). For intra layer measurements the test voltage shall be applied between two adjoining, but not electrically connected conductors within the same layer • The AC voltage at 50 Hz shall be gradually applied progressing from 200 V r.m.s. per second per mm of spacing between two conductors up to 1500 V r.m.s. • This voltage shall be kept steady for 30 seconds • The leakage current shall be limited to 100 μA • The final evaluation shall be visual aspect and measurements of the continuity • The non-conformance criteria shall be as follows 1. Evidence of breakdown, flashover or sparking M 6.2.8.4Continuity on Test Pattern D • Conductor continuity shall be tested by measuring the interconnection resistance on test pattern D • The measurement shall ensure an error less than 5% (four wire method) • The current shall be limited to 0.1 A • The measuring voltage shall not exceed 5 V • The post-test measurements taken on each sample shall be compared with pre-test measurements • The non-conformance criteria shall be as follows 1.Discontinuity 2. M ICR >10% from the initial conductor resistance M 6.2.8.5Interconnection Resistance on Test Pattern E • The test conditions shall be the same as for continuity testing • The non-conformance criteria shall be as follows 1.Discontinuity 2. M ICR > 10% from the initial conductor resistance M 6.2.8.6Current Overload on Test Pattern E 6.2.8.6.1 Short-time Overload • The test shall be carried out on a pattern including holes (50 holes minimum) connected in series by conductors • Two connecting wires shall be soldered to both ends of the circuit being tested • Interconnection resistance between two ends shall be measured and recorded • Voltage shall be applied between ends in such a way that current flow into the circuit is 32 ISRO-PAX-304 1. 7 A for 35 μm thick basic copper 2. 14 A for 70 μm thick basic copper • This current shall be maintained for (4 ± 1) s • After ambient reconditioning for 2 hrs, circuit continuity shall be checked by measuring the interconnection resistance • The non-conformance criteria shall be as follows 1. Electrical discontinuity M 2. Blistering visible to the naked eye M 3. Interconnection resistance increased by more than 10% M 6.2.8.6.2 Long-time Overload • Same initial conditions as in para.6.2.8.6.1with application of a voltage to the circuit terminals such that the current varies by successive steps 1. lo = 2 A for 3 min 2. li = 4 A for 3 min 3. Further increments of 2 A every 3 min until destruction (open circuit) or for I = 18 A • The non-conformance criteria shall be as follows: 1. Destructive current < 7 A for 35 μm basic copper, 14 A for 70 μm basic copper M 6.2.8.7Internal Short Circuit on Test Pattern C • The test shall be carried out in an insulation area in conformance with Figure 18 • A polarized voltage of 100 V DC shall be applied between the ground plane connected to earth and the plated through hole passing through the access opening for 1 min (see Figure 18) • The insulation resistance shall be measured • The non-conformance criteria shall be as follows 1. Insulation resistance < 1x1011 Ω for inter layer, 1x1010 Ω for intra layer Figure 18:Test for internal short circuit 6.2.9 Mechanical Test Methods 6.2.9.1 Peel Strength on Test Pattern B • The conductor selected shall be peeled back at one end for a length of about 10 mm • The detached end of the conductor shall be firmly gripped over its whole width 33 M ISRO-PAX-304 • Traction shall be applied in a direction perpendicular to the plane of the PCB until the copper starts to peel away. The rate of traction shall be kept constant at 50 mm/min • The traction direction shall be kept perpendicular to the plane of the PCB • Machine inertia shall not have effect on the measurement • The conductor width to be taken into account shall be the actual width over which the conductor is adhered to the laminate • The non-conformance criteria for the peel strength shall be as follows 1. Peel strength < Requirements listed in para 8.1.3 Sl. No 2 M 6.2.9.2 Pull-off Strength on Test Pattern B • Temperature of iron shall be (270 ± 10) °C • The solder shall be tin-lead 63/37 alloy with non-corrosive resin core as specified in ISRO-PAX-300 Para 5.2 • A tinned copper wire with a diameter of 0.3 mm less than the hole diameter and with a length of approximately 150 mm shall be soldered onto the pad • Soldering shall be between 2 second and 3 second • After 5 min ambient reconditioning the soldering operations shall be repeated (second soldering) • The ambient reconditioning time before final measurement shall be more than 10 min • For the measurement of pull-off strength the following steps shall be carried out 1. Force is applied on the wire by using a traction machine 2. This force increases with a constant rate of between 5 N/s and 50 N/s until the terminal pad separates from the board base material NOTE: The preferred rate is 10 N/s. • The non-conformance criteria for the pull-off strength for terminal pads shall be as follows 1. Pull-off strength which do not meet requirements listed in para 8.1.3 Sl No. 3 M 6.2.9.3 Solderability, Wettability and Via Fill-unfill Simulation Test Pattern J • Flux used shall conform to the requirements of ISRO-PAX-300 Issue-5 para 5.3 • The solder shall be Sn 63/37 and conform to ISRO-PAX-300 Issue para 5.2 • The test machine shall be a rotary dip tester or similar equipment • The specimens shall be fluxed by immersion • Surplus flux shall be allowed to flow off the specimen by keeping it upright for 5 min • The specimen shall be arranged on the soldering machine and brought into contact with the surface of the solder bath that is kept at the temperature of (235 ±5) °C for the below specified period: 1. For evaluation of wetting: 3 second 2. For evaluation of de-wetting: 10 second • A visual inspection shall be made with a 10X or higher magnification • If the coupon is used for via fill/unfill simulation o Via shall be filled and unfilled 4 times and fill during the fifth time followed by microsection to assess the inner layer connection integrity o Initial and final ICR to be noted down o Minimum 5 vias in the chain shall undergo via fill / unfill operations 34 ISRO-PAX-304 • Microsection to be performed and visual inspection at 100x or higher magnification • The non-conformance criteria shall be as follows: 1. Poor wettability of solder pads and plated-through holes: see Figure 19 M 2. Microsectioning: broken metallization M 3. Pad lift M Good wettability Poor wettability Figure 19: Wettability of terminal pads and plated-through holes 6.2.10Microsectioning on Test Pattern F 6.2.10.1 General • For high frequency conductors, the circuit designer shall specify height of the conductor, where the width shall be measured NOTE: Microsection with typical defects in PTH is shown in para 10. 35 ISRO-PAX-304 W - Width of conductor te - minimum annular ring on external layer ti - minimum annular ring on internal layer td - finished diameter of plated through hole h - Total conductor thickness Figure 20: Dimensional parameters to be measured 6.2.10.2 Thickness of Metal-plating • The measurement shall be carried out on a microsectioned sample • Observations shall be made with magnification greater than or equal to 250X • The non-conformance criteria for the thickness of copper plating on external layers shall be as follows 1. Basic copper M 2. o Thickness not conforming to this specification/ supplied design data Basic copper plus electrolytic copper on non-soldering areas M 3. o Thickness < Specification as per PCB ordering data sheet Basic copper plus electrolytic copper soldering pads (see Figure 21 number 2) o M Thickness < Specification as per PCB ordering data sheet • The non-conformance criteria for the thickness of copper in plated-through holes that are component holes shall be as follows 1. Average thickness based on 3 measurements taken on the hole walls (see Figure 21number 1): o Thickness < 25 microns M • The non-conformance criteria for the thickness of copper layer on internal layers shall be as follows 1. Thickness not conforming to this specification / supplied design data M • The non-conformance criteria for the thickness of copper in plated-through holes that are vias, buried vias shall be as follows 1. Thickness < 25 microns M • The non-conformance criteria for the thickness of tin-lead alloy on surface, measured along the conductor longitudinal axis, shall be as follows 1. thickness < 8 microns M 2. thickness > 30 microns M 36 ISRO-PAX-304 • The non-conformance criteria for the thickness of tin-lead alloy in holes shall be as follows: 1. In highest part of half of the hole wall height (see Figure 21number 3): thickness < 8 μm 2. On angle of hole corner (See Figure 21number 4): thickness < 1 μm M M • The non-conformance criteria for the etch undercut on external and internal layers for fused SnPb (see Figure 22) shall be as follows: 1. Undercut (u) > total copper thickness (h) M 1 = Cu in PTH 2 = Cu at surface pattern 3 = SnPb in hole 4 = SnPb in angle area Internal bulging b < a Figure 21: Microsection of a PTH Figure 22: Undercut for PCBs with fused SnPb finish 6.2.10.3 Plated-Through Hole Aspects • Sections of plated-through holes shall be observed with magnification greater than or equal to 100X • Layer misregistration compared to the minimum annular ring on pads • The non-conformance criteria for the layer misregistration on the external layer (see Figure 20) shall be as follows 1. te < 130 microns M • The non-conformance criteria for the layer misregistration on the internal layers (see Figure 20) shall be as follows 1. ti < 50 microns M 37 ISRO-PAX-304 2. Minimum insulation between layers < as per layer stack diagram (minimum 90 microns) 3. The non-conformance criteria for irregular drilling (see figure 23) shall be as follows 4. Infiltration of copper into base laminate (Wicking) o 40 μm < infiltration < 80 μm M m o Infiltration > 80 μm Presence of adhesive on basic copper not leading to rupture during fusing process or thermal shock M 6. Adhesion defects between metal-plating and basic copper M 7. Adhesion defects between metal-plating and inner layers M 8. Resin smear on the interface between internal conductor and plated copper M 9. Void in laminate greater than 50% of dielectric thickness M 5. m The non-conformance criteria for voids in PCB base laminate and resin recession in holes shall be as follows: 1. Voids in the PCB base laminate M 2. o Void size > 80 μm Resin recession in hole after test o M If resin recession > 40% of height of hole Figure 23: Microsection of PTH: Possible defects • The non-conformance criteria for the copper plating inside buried, blind, via and component holes shall be as follows: 1. Void in copper plating in holes M • The non-conformance criteria for the resin inside buried vias shall be in conformance with following figure. 38 ISRO-PAX-304 Not Acceptable Acceptable Figure 24: Voids in resin inside buried vias 6.3 Group 2: Hot, Cold and Vibration Tests 6.3.1Hot Storage The board shall be subjected to a temperature of +85 0C, at atmospheric pressure, for an un-interrupted period of 336 hours in a temperature chamber. Direct heat from heating element to the board shall be minimized. Upon completion of the specified storage period, the boards shall be cooled without forced air circulation for a period of not less than two hours. After hot storage test the boards shall meet the requirements of: • Warp and twist • Defects in base material • General defects in pattern • Defects in protective plating • Plated through holes requirements 6.3.2Cold Storage The boards shall be subjected to a temperature of -65 0C, at atmosphere pressure, for an un-interrupted period of 24 hours in a temperature chamber. Boards shall not be subjected to direct cooling but the whole chamber shall be subjected to uniform cooling. Boards shall be brought to room temperature naturally. Necessary precaution shall be taken to avoid condensation of moisture on the boards. After cold storage tests the boards shall meet the requirements specified in para 6.3.1. 6.3.3Vibration Fatigue After completion of hot & cold storage tests board shall be stabilized for a period of atleast 2 hours.The board shall be (in the direction of its length) mounted by drilling minimum 4 free holes at the card corners which are located at 1.5 times of the drill diameter inside the card edge on a rigid structure attached to the shaker, in order to facilitate the establishment of resonance perpendicular to the plane of the board. The resonance frequency (fo) shall first be searched at an input vibration level of 1G by sweeping frequency 20 Hz to 2000 Hz (sine wave), with the control accelerometer approximately positioned at the center of the board. 39 ISRO-PAX-304 The board shall then be subjected to the following fatigue test: Duration : 30 min Frequency : f0 Level : 200 G output (at the center of the board), measurements to be performed after testing • Visual inspection of PCB • Electrical continuity check of pattern including atleast four holes • Warp & twist. • Microsection Accept/reject criteria 1. Discontinuity in the circuit M 2.Delamination M 6.4 Group 3: Thermal Stress and Thermal Shock (on PCB) 6.4.1General Two PCBs shall be subjected for these tests. 6.4.2Hot Oil Dip Test Prior to testing, the sample shall be pre-conditioned for one hour at 125 ± 2 ºC in an air-circulating oven and allowed to cool down until its temperature is less than 85 ºC. Also ICR values of the ICR coupon shall be measured and noted down. A bath of well-stirred silicone oil, kept at 260 ± 5 ºC throughout the test, shall be used. This fluid shall have a self-ignition temperature above 450 ºC and a decomposition temperature above 280 ºC (like silicone compound Si 710). Any other bath, such as a fluidized sand bath may be used, provided the heat capacity is such that the temperature of the bath cannot be altered by the immersion of the specimen under test. The sample, held in a vertical position, shall be totally immersed in the fluid for 20 seconds. Final measurements after recovery of more than one hour. Boards shall be subjected for Visual inspection, warp and twist test, Peel strength, Bond strength, continuity, interconnection resistance and Microsectioning Accept/reject criteria 1. Warp & twist failure M 2.Measling • Generalized M 3. • Localized Broken metallization M M 4. Peel strength less than requirement value M 5.Microsectioning Epoxy smearing on basic copper at hole corner with no evidence of crack in plated copper 40 M ISRO-PAX-304 6. Bond strength less than requirement value M 7. Continuity failure M 8. Increase in ICR beyond 10% M 6.4.3Solder Dip Test • Measure inter connection resistance between the daisy chain pads and record the values • Precondition/bake the samples at 125 oC, 6 h in an air circulating oven • Cut, isolate the specimen and coarse grind the edges • Clean the sample with IPA and dry it by forced cold air • Make sure that no moisture is present on the sample. Caution : If moisture is present on the sample, it is hazardous to dip in solderability tester • Make the test setup and switch on the solderability tester and set the temperature to 288 + 5 oC, dip height to 5 mm minimum, immersion speed to 25 mm per second and immersion time to 10 seconds • After the required temperature is attained in the bath apply the flux and clamp the sample to the sample holder • Operate the machine to dip the sample for 10 seconds • Repeat the dip for two more cycles with 120 seconds break between the dips (Total six dips : High Tg it shall be 6 times) • Allow the sample to cool down and clean the sample with IPA • Conduct visual inspection on the surface for defects as described in specification. (No blisters, charring, discoloration, separation of plating or conductor, epoxy starvation, measling, delamination, lifted land shall not be more than the copper thickness subject to no corner crack) • Measure the ICR again between the daisy chain pads and record. The change in resistance shall not be more than 10% of the ICR values measured prior to solder dip test After the solder dip test, samples shall be subjected for microsectioning. The microsectioned sample shall not show thick demarcation lines, severe Z axis expansion which causes corner copper crack or barrel copper crack, resin recession which is more than 20% of dielectric thickness between adjacent layers, discontinuities between barrel and inner layer copper etc. A micrograph of the solder dipped sample (microsection) shall be preserved in electronic format for reference 6.4.4Plating Measurements, Pull Test & Microsection on Test Pattern F • A thermal shock shall be applied to the test pattern F by soldering and unsoldering a wire five times • Copper wires shall be of diameter 1. 0.7 mm for PTH holes ∅ = 0.8 mm (∅ of land = 1.5 mm) PTH • A sufficient wire length to fit the gripping mechanism of the tensile tester shall be prepared for each hole • The wire shall be inserted in the holes and soldered to the terminal areas using a conventional soldering iron, operating at a tip temperature of (270 ± 10) °C • The wires shall not be clinched on the other side of the PCB • They shall be soldered and then de-soldered and removed from the hole • This cycle shall be repeated four times, using a new wire for each soldering operation 41 ISRO-PAX-304 • During the soldering/unsoldering cycles, the soldering iron shall be applied to the wire and not to the terminal pads • After the fifth cycle, the wires shall be soldered into the holes and the PCB shall be left to cool for 30 min. minimum • Pull test shall be carried out as per para 6.2.9.2 and requirement values are mentioned in Table 7. It should be ensured that, this test should be carried out on a separate sample • A microsection shall be performed on the soldered holes to evaluate possible cracking of the copper of the throughhole plating • The non-conformance criteria shall be as follows 1. Cracked copper M 6.5 Group 4: Thermal Cycling (on PCB) Two PCBs shall be used for the tests. • The test is performed on an entire PCB • Lower temperature = -65 oC • Higher temperature = +125 oC • The number of cycles shall be 200 • The temperature change rate shall be approximately 10 °C/min. • The conditioning time at the extreme temperatures within a cycle shall be15 min • After ambient reconditioning for at least 2 h the following final measurements shall be performed 1. Laminate visual aspect 2. Peel strength on test pattern B 3. Continuity on test pattern D and interconnection resistance on test pattern E 4.Intra and interlayer insulation resistance on test pattern A and H 5. Dielectric withstanding voltage on test patterns A and H 6. Microsectioning on test pattern F • The non-conformance criteria shall be as follows: 1. Peel strength <1.2 kg/cm M 2. Increase in resistance > 10% M 3. Intralayer insulation resistance < 1x109 Ω M 4. Interlayer insulation resistance < 1x1010 Ω M 5. Evidence of flashover, breakdown, sparking M 6. Microsectioning: broken metallization M 7. Technological and functional defects M 6.6 Group 5: Long Term Damp Heat (on PCB) 6.6.1General Two PCBs shall be used for the tests. 42 ISRO-PAX-304 6.6.2Damp Heat • The test conditions shall be: 1. Temperature: (40 ± 2) °C 3. Relative humidity: 93% (+2%, ‐3%) 4. Active test for IR measurement 2. Duration of test: 21 days • The sample shall be reconditioned to normal atmospheric conditions from a period of at least 1 h and not more than 2 h after which the following final measurements shall be taken: 1. Peel strength on test pattern B 2. Intra and interlayer insulation resistance on test patterns A and H 3. Dielectric Withstanding voltage on test patterns A and H 4. Micro sectioning (if necessary) on test pattern F 5. Corrosion of circuits for electrolytic Au finish • The non-conformance criteria shall be as follows 1. Peel strength <1.2 kg/cm M 2. Intralayer insulation resistance < 1x109 Ω M 3. Interlayer insulation resistance < 1x10 Ω M 4. Evidence of flashover, breakdown, sparking M 5. Microsectioning (if required): broken metallization M 6. Evidence of corrosion M 10 6.7 Group 6: Assembly Compatibility Tests 6.7.1General • One PCB shall be used for the tests. Assembly compatibility tests like cleaning, baking, turret swaging, component mounting, soldering, reworking, conformal coating, RTV potting, ecco bonding and jumper wiring are carried out as per ISRO-PAX-300 on this PCB. 1. Not compatible with standard fabrication procedures M 6.7.2Physical Tests on Test Pattern K 6.7.2.1 Water Absorption (optional) • The specimen, completely devoid of copper, shall be dried in an oven for (24 ± 1) h at a temperature between 50 °C and 55 °C • It shall be cooled in a container with a siccative until the temperature is (23 ± 1) °C • At this stage it shall be weighed to the nearest milligram • It shall be placed in a de-ionized water bath maintained at (23 ± 0.5) °C • It shall be placed on the edge, remain completely submerged and not in contact with the edges of the bath • After (24 ± 1) h it shall be withdrawn from the water and dried with a dry fluff-free cloth or filter paper • It shall be weighed to the nearest milligram within a minute, following its removal from the water 43 ISRO-PAX-304 • The non-conformance criteria for the percentage of absorbed water (Δm) in various types of laminates shall be as follows 1. Glass fibre‐epoxy base laminate: Δm > 0.2% M 6.7.2.2 Outgassing • The test shall be carried out in conformance with ECSS-Q-ST-70-02C. • The test shall be carried out on a specimen entirely devoid of copper in order to determine the volume of included gas constituents, which threaten to contaminate a space environment. • The outgassing shall be determined after measurement of the difference in weight of the specimen before and after the test. • The non-conformance criteria shall be as follows: 1. TML or RML > 1% and CVCM > 0.1% M 6.7.2.3 PCB Wiring PCB assembly subjected for assembly compatibility test shall be visually inspected for compliance to ISRO-PAX-300 requirements. Conformal coated assembly shall be subjected for thermal vacuum cycling. Limits are +85 oC, -55 oC, 10-5 torr pressure 24 h hot and 24 h cold (single cycle). Assembly shall be visually inspected for compliance to ISRO-PAX-300 requirements. 44 ISRO-PAX-304 7 QUALITY ASSURANCE FOR MANUFACTURING 7.1 General • The quality assurance requirements defined in this standard shall apply 7.2 Quality Records • The quality records shall be composed of the following 1. Documentation of the final inspection of manufactured PCBs 2. Non-conformance reports and corrective actions in conformance with ISRO-PAS-100 Issue 3 3. Copy of the acceptance test results 7.2.1PCB Ordering Information and Data Input PCB ordering information is as below. 1. 2. 3. 4. Parameter Laminate material Protective plating material type Solder mask required Number of layers 5. Layer stack 6. Requirement As per IPC 4101 Hot Air Leveled Solder Required / Not Required 2, 4, 6, 8, 10, 12, 14 As agreed by standing instructions or as supplied along with input data pack. As mentioned in the layer stack or PCB ordering data sheet Eg:1.6 + 0.15 mm 2.2 + 0.15 mm 35 / 70 microns. As specified in mechanical drawing and input gerber file Card thickness 7. Inner layer copper thickness 8. Card size Data input pattern related - scale - gerber format - Drill details 9. - Rout file - Mechanical drawing 1:1 RS 274X Both Excellon format and colour copy in GIF/ JPG/ Post script format/PDF. Excellon format GIF/JPG/PDF format - Communication Through E-mail 7.3 Incoming Inspection of Raw Materials • Raw materials and semi-finished products shall be selected, inspected and tested (eg. chemical and physical tests) in conformance with the production flow chart of PCB manufacturer and records shall be maintained • The PCB manufacturer shall separate and prevent the use of raw materials and semi-finished products that are awaiting for completion of test results 45 ISRO-PAX-304 7.4 Traceability • The PCB manufacturer’s control system shall make it possible to determine, in respect of any lot of PCBs, the history of all raw materials (Batch code, Batch acceptance test results or Certificate of compliance) and semi-finished products listed in the production flow chart and the individual process steps mentioned herein and to verify that the items originate from one production lot • In case of materials with limited shelf-life, the PCB manufacturer’s control system shall provide means to verify the validity of the relevant material for use • In case of materials (like pre-pregs) which requires specific environmental conditions for the storage shall be kept in appropriate storage conditions. Log books pertaining to the storage conditions shall be maintained by the manufacturer 7.5 Calibration • The PCB manufacturer shall calibrate all related electrical and mechanical manufacturing equipment to traceable reference standards • The PCB manufacturer shall record any suspected or actual equipment failure as a non-conformance report according to ISRO-PAS-100 Issue 3 NOTE: This is to ensure that previous manufacturing results are examined to ascertain whether or not a reinspection or re-testing is necessary 7.6 Workmanship Requirements • Visual standards consisting of photos or drawings of microsections or other visual aids are given in following paragraph.These illustrate the quality characteristics 7.7 Inspection • During all stages of the manufacturing, the inspection shall be carried out as per Process Identification Document 7.7.1Microsection Inspection for Major Defects Sl No Micrograph of major defects Description Pad lift is visible after rework simulation. 1. 46 ISRO-PAX-304 Sl No Micrograph of major defects 2. Description Glass fiber protrusion Irregular barrel and zero annular ring. 3. Inner layer annular ring less than 50 microns 47 ISRO-PAX-304 Sl No Micrograph of major defects Description 4. zero annular ring 5. Zero annular ring, less annular ring and discontinuity 48 ISRO-PAX-304 Sl No Micrograph of major defects Description 6. Irregular barrel 7. Tapered barrel 49 ISRO-PAX-304 Sl No Micrograph of major defects Description 8. Crack in inner layer copper 9. Plating crack 50 ISRO-PAX-304 Sl No Micrograph of major defects Description 10. Plating crack 11. Crack in copper at PTH Knee 12. Knee crack 51 ISRO-PAX-304 Sl No Micrograph of major defects Description 13. Barrel discontinuity 14. Barrel discontinuity 52 ISRO-PAX-304 Sl No Micrograph of major defects Description 15. Insufficient inner layer copper thickness 16. Plating nodule which is more than 80 microns 17. Plating nodule which is more than 80 microns 53 ISRO-PAX-304 Sl No Micrograph of major defects Description 18. Nodules and zero annular ring. 19. Insufficient plating thickness in barrel less than 25 microns 20. Wicking. Spoke length more than 80 microns. 54 ISRO-PAX-304 Sl No Micrograph of major defects Description 21. Barrel copper to Inner layer copper separation 22. Barrel copper to Inner layer copper separation. 23. Thick demarcation line between inner layer copper and barrel copper after solder dip. 55 ISRO-PAX-304 Sl No Micrograph of major defects Description 24. Resin recession 25. Barrel pull away 56 ISRO-PAX-304 Sl No Micrograph of major defects Description 26. Barrel copper to Inner layer copper separation in horizontal sectioning 27. Nail heading. Negative etch back 28. 57 ISRO-PAX-304 Sl No Micrograph of major defects Description Delamination & Copper nodules in barrel blocking solder flow, leading to copper visibility 29. 58 ISRO-PAX-304 7.7.2Visual Inspection for Major Defects Sl No Major visual defects Description 1. Burrs at edges 2. Haloing at edges 3. Weave texture 59 ISRO-PAX-304 Sl No Major visual defects Description 4. Exposed fibers 5. Pits on laminate 6. Measling 7. Crazing 60 ISRO-PAX-304 Sl No Major visual defects Description 8. De-lamination 9. Foreign material intrusion 10. Non wetting 11. De-wetting 61 ISRO-PAX-304 Sl No Major visual defects Description 12. Nodules in the barrel 13. Pinking red 14. Void in barrel 15. Lifted land 62 ISRO-PAX-304 Sl No Major visual defects Description 16. Haloing 17. Solder mask skip 18. Solder mask mis-registration 19. Soldermask cover the lands 63 ISRO-PAX-304 Sl No Major visual defects Description 20. Blister 21. Flaked soldermask 22. Solder mask wrinkles Soda strawing 23. 64 ISRO-PAX-304 Sl No Major visual defects Description 24. Reduced conductor width 25. Poor edge resolution for conductors 26. Reduced conductor spacing 27. Reduced annular ring i.e. less than 50 microns in inner layer or less than 130 microns in external layer. 65 ISRO-PAX-304 Sl No Major visual defects Description Zero annular ring 28. 7.8 Operator and Inspector Training • All operators and inspectors shall be suitably trained for their task and for the understanding of the necessary quality assurance requirements 7.9 Quality Test Coupon • The PCB manufacturer shall produce with each panel quality test specimens for in-house quality control purposes and one set to be supplied to the qualification authority 7.9.1Test Coupon Details Test coupon drilling details and usage of test coupon areas for various tests are described as below. Gerber file of the test coupon shall be supplied by QA of the ISRO centre concerned. Figure 25 : Horizontal test coupon with drilling details TCH : Test coupon which is placed horizontally in the panel 66 ISRO-PAX-304 Figure 26 : Vertical test coupon with drilling details TCV : Test coupon which is placed vertically in the panel Note : Generic feature size of microsection pads are 0.8 mm hole on 1.5 mm pad. If smaller pad diameter and drill diameter is used, these shall be replaced with smallest most drill size and respective pad diameters. 7.9.2Test Coupon Usage Figure 27: Usage details of test coupon 7.9.3Test Coupon Placement in Panel Test coupons shall be placed in the panel as below. Coupons marked for vendor shall be utilized by the PCB manufacturer, to conduct the acceptance tests listed in in para 7.10 of this document. Report of the tests shall be supplied as data pack for each panel. 67 ISRO-PAX-304 BOARD/s TO ISRO TEST COUPON TO ISRO VERTICAL TEST COUPON FOR VENDOR’s TESTING VERTICAL TEST COUPON FOR VENDOR’s TESTING; HORIZONTAL TEST COUPON TO ISRO; HORIZONTAL Note: 1.Test coupon placement can be changed by the manufacturer but, shall have prior approval on the spool file before proceeding with further processes like photoploting. Figure 28:Test coupon placement in panel 7.10Acceptance Tests The PCB manufacturer shall have an in‐house procedure for final inspection of PCBs; this shall include the following tests; Table 3: List of PCB Acceptance Tests Sl No. 1 2 3 4 5 6 7 8 9 10 11 12 13 Test Name Bare board testing Mechanical inspection Visual inspection Peel strength Bond strength Rework simulation Solder dip Solderability Inter connection resistance Insulation resistance intra layer Insulation resistance inter layer Dielectric withstanding voltage intra layer Dielectric withstanding voltage inter layer 68 Test on Actual board Actual board Actual board Coupon Coupon Coupon Coupon Coupon Coupon Coupon Coupon Coupon Coupon ISRO-PAX-304 Sl No. 14 15 16 Test Name Microsectioning of initial sample Microsectioning of solder dip tested samples. Microsectioning of rework simulated samples. Test on Coupon Coupon Coupon The quality test specimen are representative of the PCB and produced on the same panel shall be subjected to continuity, solderability and thermal stress tests. • Microsectioning of holes as received and after thermal stress tests (rework simulation) shall be performed • The PCBs shall be cleaned and dried before packing • Acceptance test flow is depicted in Figure 29 • Report format requirements are listed in para 7.10.5 7.10.1Mechanical Inspection Report Format Table 4 : Mechanical Inspection Report Format REPORT NO: PROJECT: DATE: MODEL: SL NO. CARD NUMBER DISPOSITION SPECIFIED DIMENSIONS Card size, pitch, thickness, free hole dimensions MEASURED DIMENSIONS, Box matching / WARP AND TWIST trial suiting Card size, pitch, thickness, free hole dimensions REMARKS ACCEPTED REWORK REJECTED CLARIFICATION INSPECTED BY Note: Unless otherwise specified in drawing, the acceptable values for the listed parameters are : card size ± 0.2 mm, pitch ± 0.1 mm, thickness ± 0.15 mm for <2.4 mm PCB thickness, ± 10% for > 2.4 mm PCB thickness, Free holes dia +0.1 / -0.0 mm, warp maximum 1.0% of length and twist maximum 1.0% of diagonal length. 69 ISRO-PAX-304 7.10.2Microsection and Report Formats • Microsection report format is as below (Table 5 and Table 6 ) Table 5 : Microsection Report Format-A Card No: No of Layers SL. NO PARAMETER Batch No: Qty/Panel Panel No: QA/QC Code OBSERVATIONS (VALUE IN MICRONS) HOLE NO. SIDE 1 SIDE 2 HOLE NO. SIDE 1 SIDE 2 1. LAND REGION (TOP) 01 Total Copper Thickness 02 Basic Copper thickness 03 Deposited Copper thickness 04 Protective plating thickness a. At center max. (for tin lead) b. On side max. (for tin lead ) c. At knee 05 Conductor under cut 06 Solder mask thickness II. HOLE WALL 01 Copper thickness 02 Protective Plating thickness (for tin lead ). 03 Copper thickness at knee 04 Resin recession Unless otherwise specified in the ordering sheet the default values are as below 52.5/70/105 +10 microns 18 + 4/35/65 +5 microns 35 + 10 microns 8 to 30 microns 8 to 30microns minimum 1 μm / just coverage < Cu thickness. 17 to 25 microns 35 + 10 microns 8 to 30 microns 35 + 10 microns Less than 20% III. LAND REGION (BOTTOM) 01 Total Copper Thickness 02 Basic copper thickness 03 Deposited copper thickness 04 Protective plating thickness a. At center max. (for tin lead) b. On side max(for tin lead) c. At knee 05 Conductor under cut 06 Solder mask thickness 01 Homogenity Drilling/barrel irregularity Protective plating uniformity Registration error Other defects, if any. 52.5/70/105 +10 microns 18 + 4/35/65 +5 microns 35 + 10 microns 8 to 30 microns 8 to 30 microns minimum 1 μm / just coverage < Cu thickness. 17 to 25 microns. Max. 80 microns 8 to 30 microns Max. 250 microns provided annular ring requirements are met. • If protective plating is gold then thickness is 2.5 to 3 microns. • If protective plating is gold over nickel then 3 to 5 microns of nickel and 1 to 3 microns of gold is required. 70 ISRO-PAX-304 Table 6 : Microsection Report Format-B HOLE NO: Layer no Copper thickness 01 02 03 04 05 06 07 08 09 10 11 12 13 14 HOLE NO: Layer no Copper thickness 01 02 03 04 05 06 07 08 09 10 11 12 13 14 Etch back Etch back SIDE NO: Dielectric separation 1-2: 2-3: 3-4: 4-5: 5-6: 6-7: 7-8: 8-9: 9-10: 10-11: 11-12: 12-13: 13-14: SIDE NO: Dielectric separation 1-2: 2-3: 3-4: 4-5: 5-6: 6-7: 7-8: 8-9: 9-10: 10-11: 11-12: 12-13: 13-14: Annular ring Annular ring Layer No 01 02 03 04 05 06 07 08 09 10 11 12 13 14 Layer No 01 02 03 04 05 06 07 08 09 10 11 12 13 14 HOLE NO: Copper thickness Etch back HOLE NO: Copper thickness Etch back SIDE NO: Dielectric Annular separation ring 1-2: 2-3: 3-4: 4-5: 5-6: 6-7: 7-8: 8-9: 9-10: 10-11: 11-12: 12-13: 13-14: SIDE NO: Dielectric Annular separation ring 1-2: 2-3: 3-4: 4-5: 5-6: 6-7: 7-8: 8-9: 9-10: 10-11: 11-12: 12-13: 13-14: Remarks Remarks Unless otherwise specified the default values of inner layer Cu thickness is 65 ± 5 microns and it shall not be less than 30 microns (for 12 or 14 layer MLBs). Preferred etch back 5 to 13 microns (100% de-smear mandatory), minimum annular ring of 50 microns for inner layer and annular ring of 130 microns for outer layer. For half ounce basic copper thickness, total copper thickness shall be between 52.5 ± 10 microns. Minimum dielectric thickness shall be generally 150 microns. Unless otherwise supported by requirement specifications dielectric thickness less than 100 microns shall be referred to appropriate forum for disposition. However in no case it shall be less than 90 microns. Negative etchback beyond 5 microns shall not be accepted. 71 ISRO-PAX-304 Figure 29 : Acceptance test flow HASL : Hot Air Solder Levelled OLQC : Online QC HAL : Hot Air Levelling NC : Non-conformance 72 ISRO-PAX-304 7.10.3Coupon Test Result Format Table 7: Acceptance Test Report Card No: Batch No: Layers Qty/Panel INSULATION RESISTANCE (INTRA LAYER) SPEC.: >1 x 1010 ohms Panel No: INSULATION RESISTANCE (INTER LAYER) SPEC.: >1 x 10 11 ohms INTER CONNECTION RESISTANCE SPEC.: < 3 mΩ per layer for 2 ounce; < 6 mΩ per layer for 1 ounce 1-1 1 1-2 1-2 2-2 1 2-3 2-3 3-3 1 3-4 3-4 4-4 1 4-5 4-5 5-5 1 5-6 5-6 6-6 1 6-7 6-7 7-7 1 7-8 7-8 8-8 8-9 8-9 9-9 1 9-10 9-10 10-10 1 10-11 10-11 11-11 1 11-12 11-12 12-12 1 12-13 12-13 13-13 1 13-14 13-14 1 14-14 1 PLATED THROUGH HOLE BOND STRENGTH AFTER 5 TIMES REWORK SIMULATION at 300 o C soldering temperature SPEC.; >7.12 Kg/mm 2 ( 9kg pull force ) TRACK PEEL STRENGTH SOLDERABILITY SPEC.; minimum 1.2 kg/cm SPEC.: >95% Wetting on conductor surface OBSERVATIONS OBSERVATIONS OBSERVATIONS VALUES TO BE RECORDED VALUES TO BE RECORDED VALUES TO BE RECORDED SOLDER DIP TEST ICR BEFORE AND AFTER SOLDER DIP at 288 oC, 2 Cycles with 120 seconds break between dips. (3 dips for Tg>180 oC) SPEC .:ICR shall not increase > 10% w.r.t. initial reference value. M/S AFTER SDT PTH WALL & INNER LAYER INTERFACE WITH WALL INTEGRITY AFTER SOLDER DIP SPEC.: Microsectioned samples shall not have barrel separation, cracks, thick demarcation line between plated copper and inner layer copper presence of crack, smear, discontinuity are not allowed. DIELECTRIC WITHSTANDING VOLTAGE SPEC.: With 350V - AC for 30 seconds Leakage current < 100 µA OBSERVATIONS VALUES TO BE RECORDED OBSERVATIONS VALUES TO BE RECORDED OBSERVATIONS VALUES TO BE RECORDED REWORK SIMULATION ICR MEASUREMENT PRIOR TO REWORK SIMULATION AND ICR MEASUREMENT AFTER REWORK SIMULATION SPEC .:ICR shall not increase > 10% w.r.t. initial reference value. M/S AFTER R/W SIMULATION Microsectioned samples shall not have barrel separation, cracks, thick demarcation line between plated copper and inner layer copper presence of crack, smear, pad lift, discontinuity not allowed. HIGH TEMPERATURE ICR OBSERVATIONS VALUES TO BE RECORDED OBSERVATIONS VALUES TO BE RECORDED ICR Measurement shall be done at Tg + 10 oC and % increase from ambient shall be less than +90% (<1.9 times) of initial value. (Optional Test: when any one of the board fails inopen mode BBT after hot air leveling) OBSERVATIONS VALUES TO BE RECORDED NON CONFORMANCE REPORTS /DETAILS, IF ANY: ACCEPTED / REJECTED Signature of the Inspector Date : M/S : Microsection SDT : Solder Dip Test 73 ISRO-PAX-304 7.10.4Final Inspection Report Format Every card inspected shall be accompanied by a visual inspection report. The report format is enclosed. Table 8 : PCB Inspection Report Format Card No: Layers Centre S.No 1.0 1.1 1.2 1.3 1.4 1.5 Week-Year Qty/Panel ISAC/VSSC/IISU /SAC 1.6 1.7 PARAMETER BOARD QUALITY Material Board dimension Stacking hole pitch Stacking hole diameter Board Thickness (metal- to- metal) Board Warpage Edge trimming 1.8 Visual cleanliness of PCB 1.9 Laminate materials defects 1.10 Laminate materials defects Measling PAD / HOLE Location & dia PTH & NPTH drilling PTH Hole diameter 2.0 2.1 2.2 2.3 2.4 2.5 2.6 2.7 3.0 3.1 Annular ring a. PTH b. NPTH PTH defect PTH in place of NPTH and vice versa PTH hole block CONDUCTOR Width Project Panel No: Weight in g To be filled by PCB Batch No: project allocating agency QA code: SPECIFICATION/Ref.Para. IPC4101 complied LxW as specified in Layout ± 0.2 mm As specified in layout ± 0.1 mm As specified in layout ± 0.1 mm 1.6 mm to 2.2 mm+ 0.15 mm <1% of the length Smooth finish, haloing/ chipping <0.25 mm Presence of dirt, grease, finger prints, oils, chemicals, solvent residues not allowed. Crack / Chipping / Discolorations / Epoxy Starvation / Crazing / Blistering / Weave Exposure / Delamination/ Measling / foreign materials / Weave texture not allowed. < 10 Sq mm continuous, should not bridge > 25% between pad & conductor As per Master pattern Extra PTH / NPTH not allowed. + 0.05 / -0.00 mm up to 1 mm ∅ holes + 0.10 / -0.00 mm beyond 1 mm External layers > 0.13 mm > 0.25 mm Chipping / Torn cladding /Burrs/ voids> 80 microns/ Nodules / de-lamination, Laminate exposure around the hole - Not to be present Not allowed Allowed for thermal vias and not allowed for regular vias. As per Master pattern 0.2 mm (minimum) 0.15 mm (minimum) for fine pitch SMD/ CCGA/BGA. Or as specified in layout; +0.00 mm: -0.03 mm for ½ oz Copper +0.00 mm: -0.05 mm for 1 oz Copper +0.00 mm: -0.10 mm for 2 oz Copper 74 OBSERVATION ISRO-PAX-304 3.2 3.3 3.4 4.0 Spacing 0.2 mm [0.1 mm special cases] or as specified in layout + 10% Defects in conductor pinhole/ Defects shall not reduce the width by more than 10% in pits/ void/cut/scratch/ any combination dent/line definitions Copper visibility Nil under 10X PROTECTIVE COATING/ Solder Nickel-Gold or Gold PLATING Fused Not fused 4.1 Plating Defects 4.2 4.3 Microsectioning [test coupon result] Solder Masking Defects 4.5 4.6 5.0 5.1 5.2 5.3 5.4 5.5 5.6 5.7 5.8 5.9 Solder Mask thickness BBT Results ACCEPTANCE TESTS Peel strength Rework simulation [5 times] PTH bond strength Interconnection resistance Insulation resistance Dielectric withstanding voltage Solderability Solder dip test High temperature ICR Porosity/Blisters/Wrinkles/granular surface/ dewetting not to be present As per given format Solder mask overlapping on pads/ scratches, peel offs, contamination, non-uniform colour, tackiness, ragged edges not allowed 17-25 microns. Refer Microsection data. Ensure BBT is conducted and BBT OK tag is enclosed As per para 7.10.3 REMARKS IF ANY : ACCEPTED/ REJECTED/ ACCEPTED BY appropriate forum Signature of the Inspector Name:&Date: Auditor/Reviewer comments: Auditor/Reviewer signature 75 PASS/FAIL PASS/FAIL PASS/FAIL ISRO-PAX-304 7.10.5Data Pack The following data pack shall be supplied along with the PCB/Panel. • IPC Compliance certificate of the laminate and pre-preg material used • Traveller card of the PCB panel • Bare board test label on the PCB • Mechanical inspection report (As per format in para 7.10.1) • Microsection report (As per format in para 7.10.2) • Coupon testing report (As per format in para 7.10.3) • Final inspection report (As per format in para 7.10.4) • Non-conformance and close out report if any (As per ISRO-PAS-100 Issue 3) 7.11Non-conformance Control If non-conformances are observed at manufacturer side, during the process of acceptance/qualification testing of PCBs, QA/QC shall note all the deviations and discuss by approved forum. Data pack of the PCBs shall contain the dispositions made. If non-conformances are observed at ISRO side, during the process of acceptance/qualification testing of PCBs, QA/QC (qualification team) of ISRO centre concerned shall note all the deviations and submit to the concerned authority for clearance. 76 ISRO-PAX-304 Table 9: Non-conformance Control Format NON-CONFORMANCE REPORT PROJECT NCR No. DATE: DRAWING No. ORIGINATOR ITEM NOMENCLATURE SUBSYSTEM MODEL NON-CONFORMANCE DESCRIPTION PROBABLE CAUSE DESIGN PARTS MATERIALS MANUFACTURING HANDLING TEST EQUIPMENT SOFTWARE OTHERS REPERCUSSION CLASSIFICATION AFFECTS ASSEMBLY MINOR MAJOR AFFECTS FUNCTION AFFECTS RELIABILITY AFFECTS INTERCHANGEABILITY AFFECTS WEIGHT AFFECTS SAFETY OTHERS (SPECIFY) REFERRED TO MRB ON: DISPOSITION ON: *MRB No. ACTION COMPLETED ON: * MRB or any appropriate non-conformance review boards 77 ISRO-PAX-304 7.12Packaging, Storage and Shipment • There is a slow decline in wettability with an indication of a plateau after 8 to 9 months in Tin / Lead finishes. This degradation is independent of packaging material and even between packaging and not packaging. The root cause of Solderability loss is growth and oxidation of Cu6 Sn5 and Cu3 Sn intermetallic phases. When these intermetallic compounds (IMCs) reach the surface and oxidize, Solderability is lost. Thinnest areas (knees of PTH’s for HASL finishes) lose solderability faster (6 months to a year typical). Remaining surfaces typically remain solderable for 1-2 years depending on SnPb thickness • Packaging materials, Bags and other packaging are available in a variety of materials and forms of construction. The selection of packaging material and construction directly influence the longevity and preservation of printed boards with regard to moisture absorption, especially those destined for exposure to the higher temperatures and longer dwell times associated with lead-free processing • The Water Vapor Transmission Rate (WVTR) is the rate that water vapor passes through a specific area of barrier material, measured in grams of water vapor per 100 Sq. inch of barrier material, for a 24 hour period (gm/100 Sq. inch /24 h). The WVTR for dry packaging of printed boards should meet the requirements of IPC-J-STD-033, which specifies a WVTR of < 0.002 g /100 Sq. inch. Bags with lower WVTR values may be considered, to increase shelf life of the printed board package or reduce the amount of desiccant required • Packaging Material Types a) Nylon/Foil/Poly– A commonly available Moisture Barrier Bag (MBB) construction that incorporates an outer layer of static dissipative nylon, aluminum foil middle layer, and an inner layer of polyethylene. This structure provides very good moisture barrier characteristics with typical WVTR values of < 0.0005 gm/100 sq. inch) b) Clear Plastics/Polymers (non-metallic) - Plastics that do not incorporate a metallic layer in the construction provide limited moisture barrier performance, and should not be used for dry-packaging of printed boards, especially those destined for Hi-Rel assembly • The quantity and quality of the desiccant material selected should be such that it keeps PCBs moisture free. It should be placed along the edges of printed boards inside the MBB. This will avoid stress that can warp the printed boards if packages are stacked within the shipping carton and will prevent desiccant from interacting with the printed board final finish • Prior to packaging, the printed boards should be clean. Moisture Barrier Bag should be heat sealed to keep out moisture. Full air evacuation is not needed or recommended; light air evacuation will reduce the packaging bulk and facilitate carton packing. Excessive evacuation may impede desiccant performance and lead to MBB punctures • Empty space in the box should be filled with appropriate packing material so that the product cannot shift within the packaging and will be protected during shipment. When necessary, especially for large printed boards, corner protectors should be used. Materials used should be free of contaminants. Use of anti-static or static dissipative materials provided for transportation are to be opened within an ESD Protected Area (EPA) for assembly • Before opening, dry packed packages should be inspected to verify that there are no tears punctures or openings of any kind that expose the contents. If openings are found, the dry environment of the bag has been compromised, then the printed boards should be visually inspected for any changes to the final finish that may indicate that Solderability has been degraded • During physical inspection, intact bags may be opened for inspection by cutting at the top of the bag near the seal. Time of exposure to ambient conditions should be controlled to minimize moisture uptake • During assembly operations printed boards should be protected from moisture uptake, contamination and extremes of temperature (Temperature, Humidity and Cleanliness) and it shall be in accordance with ISROPAX- 300 guidelines 78 ISRO-PAX-304 7.12.1Storage of the Approved PCBs All the PCBs after successful inspection and approval shall be stored in dry Nitrogen storage cabinet or controlled environment desiccators. In case of non-availability of dry Nitrogen cabinets, polythene bags purged with dry Nitrogen may be used. Long duration stored boards shall undergo rescreening/retesting as follows PCBs stored in the Bonded Stores shall be categorized as follows: Category-1: PCBs w/o dry N2 purged bags and Category-2: PCBs Stored with dry N2 purged bags. PCB storage Period Category-1 PCBs w/o dry N2 purged bags Category-2 PCBs Stored with dry N2 purged bags/ cabinet More than six months but less Visual Inspection of actual cards than one year Use as is More than one year but less than •Visual inspection of actual card 2 years. •Solderability test on one card Only visual inspection More than 2 years Not recommended for space use • Visual inspection on actual card. • Solderability test on one card. More than 5 years Not recommended for space use Not recommended for space use. • PCBs stored more than 5 years shall not be used for onboard • The batch of PCB left with one card balance shall not be taken for re-screening. Moreover, these shall not be allowed for space use 7.12.2Precautions Following precautions shall be taken during packing and handling of PCBs. • PCBs shall not be dropped while handling • PCBs shall not be abraded against any hard surface • Stapler pins shall not be used for sealing the polythene bags o Vacuum sealing or nitrogen purged packing is preferred for PCBs for storage and transportation • Handling after the cleaning operation shall be done with protective gloves • PCBs shall be packed along with a sachet of silica gel, which shall retain blue color throughout storage period • PCBs shall not be allowed to come in contact with any paper containing sulphur traces • PCBs shall be stored in moisture free environment 79 ISRO-PAX-304 8 REQUIREMENTS FOR PCBs 8.1 Rigid Multilayer PCBs The base materials shall be in conformance with IPC-4101/24 or /29 and shall be one of the following 1. Woven-glass-reinforced epoxy resin 2. Woven-glass-reinforced polyimide resin 3. Woven-glass-reinforced bismaleimide/trazine modified epoxy (High Tg) resin 8.1.1Dimensional Characteristics 1. External dimension tolerance ± 0.2 mm 2. Thickness tolerance: ± 10% or ± 0.15 mm as per ordering data 3. Maximum active board size: As per given gerber data 4. Maximum board thickness:2.4 mm (2.25 + 0.15 mm) 5. Positioning between registration mark and edge of circuit: ± 0.2 mm 6. Conductor width: o Internal: 0.2 mm minimum o 7. External: 0.2 mm minimum (for fine pitch 0.15 mm width if less than 5 mm from component pad/ 0.125 mm line width for CCGA/BGA); Conductor spacing: o Internal / External: 0.2 mm minimum / 0.1 mm for CCGA/BGA 8. Conductor tolerance (minimum/maximum): ± 10% subject to spacing requirements are met 9. Tolerance on diameter of terminal pads: ± 10% subject to spacing requirements are met 10. Minimum drilled hole diameter o Component hole: in conformance with ISRO-PAX-301 o Via hole: 0.4 mm minimum and maximum aspect ratio t/d = 6 for standard cards; for CCGA/BGA cards aspect ratio shall be limited to be (2.4/0.25) 9.6 11. Tolerance on diameter of plated-through holes o Nominal +0.05 / -0.00 mm up to 1 mm ∅ holes o Nominal +0.10 / -0.00 mm beyond 1 mm 12. Tolerance on diameter of non-plated-through holes: +0.10 mm -0.00 mm 13. Positioning of holes with respect to reference mark: ± 0.1 mm 14. Relative misregistration pad/hole: ≤ 0.15 mm 15. Misalignment determined by measuring minimum annular ring o External layers: solder side: 0.13 mm o External layers: component side : 0.10 mm o External layers: NPTH hole: 0.25 mm o Internal layers: 0.05 mm 16. Layer to layer registration: ± 0.25 mm 17. Number of layers: 14 maximum 80 ISRO-PAX-304 8.1.2Electrolytic Coatings 1. 2. 3. 4. Electrolytic copper plating o Minimum purity: 99.5% o Thickness of surface pattern: ≥ 25 μm o Thickness of plated-through holes: ≥ 25 μm o Thickness of via holes: ≥ 20 μm Tin lead plating after reflow o Tin content of alloy: (63 ± 8)% o Thickness on surface: ≥ 8 μm in highest part o Thickness in plated-through holes: ≥ 8 μm in highest part (minimum half height of hole wall) o On corner angle: ≥ 1μm Electrolytic gold plating o Minimum purity: 99.8% o Not containing more than 0.2% silver o Thickness on nickel: (4 ± 3) μm o Thickness on copper: (3± 2) μm Electrolytic nickel plating o 5. 6. Thickness: 2 μm to 10 μm NOTE: It is optional under gold Insulation between layers: 90 μm minimum Insulation between last but one layers / penultimate layers 150 microns 8.1.3Mechanical Characteristics 1. 2. 3. Warp and twist o Warp ≤ 1.0% (≤ 0.75% for CCGAs) of warp measured side length o Twist ≤ 1.0% (≤ 0.75% for CCGAs) of diagonal length o Co-planarity in the CCGA zone shall be less than 100 micron Conductor adhesion/peel strength: o On epoxy with Tg < 180 °C: ≥1.42 kg/cm o On epoxy with Tg > 180 °C: ≥1.2 kg/cm o On polyimide: ≥ 1.2 kg/cm o On bismaleimide/trazine modified epoxy HTg: ≥1.2 kg/cm Bond strength/pull strength for NPTH only: o For terminal pads 4 mm Ø on epoxy Tg < 180 °C: ≥ 140 N o For terminal pads 4 mm Ø on epoxy Tg > 180 °C: ≥ 80 N o For terminal pads 4 mm Ø on polyimide: ≥ 80 N o For terminal pads 4 mm Ø on bismaleimide/trazine modified epoxy HTg: ≥ 60 N o For terminal pads 2 mm Ø on epoxy Tg < 160 °C: ≥ 35 N o For terminal pads 2 mm Ø on epoxy Tg > 180 °C: ≥ 20 N o For terminal pads 2 mm Ø on polyimide: ≥ 20 N o For terminal pads 2 mm Ø on bismaleimide/trazinemodified epoxy HTg: ≥ 12 N 81 ISRO-PAX-304 8.1.4Electrical Characteristics 1. 2. Insulation resistance o Intralayer: > 1x 1010 Ω o Interlayer: > 1x 1011 Ω Dielectric withstanding voltage per mm spacing between conductors: o 3. 4. 5. Intralayer and interlayer: 1500 V/mm or 350 r.m.s when spacing is 0.25 mm. Short time overload: o 35 μm copper thickness: 7 A for 4 s o 70 μm copper thickness: 14 A for 4 s Long time overload, destructive current: o 35 μm copper thickness: I ≥ 8 A o 70 μm copper thickness: I ≥ 16 A Internal short circuit: o Insulation resistance: ≥ 1 x 109 Ω 82 ISRO-PAX-304 9ANNEXURE-1 : Qualification Test Pattern Figure 30: Layer 1 83 ISRO-PAX-304 Figure 31: Layer 2 84 ISRO-PAX-304 Figure 32: Layer 3 85 ISRO-PAX-304 Figure 33: Layer 4 86 ISRO-PAX-304 Figure 34: Layer 5 87 ISRO-PAX-304 Figure 35: Layer 6 88 ISRO-PAX-304 Figure 36: Layer 7 89 ISRO-PAX-304 Figure 37: Layer 8 90 ISRO-PAX-304 Figure 38: Layer 9 91 ISRO-PAX-304 Figure 39: Layer 10 92 ISRO-PAX-304 Figure 40: Layer 11 93 ISRO-PAX-304 Figure 41: Layer 12 94 ISRO-PAX-304 Figure 42: Layer 13 95 ISRO-PAX-304 Figure 43: Layer 14 96 ISRO-PAX-304 Figure 44:Top solder mask 97 ISRO-PAX-304 Figure 45: Bottom solder mask 98 ISRO-PAX-304 Figure 46: Drilling details 99 ISRO-PAX-304 Figure 47: Zone details 100 ISRO-PAX-304 10 ANNEXURE-2 :Typical Micro Section Defects Figure 48:Typical microsection defects • A Undercut 13.Glass Bundle Void 29.Resin Smear • B Outgrowth 14.Severe Etchback 30.Copper & Over Plate Void • C Overhang 15.Nail Heading 31.Burned Plating 1.(Resin) Blistering 16.Drill Wall Tear / Wicking 32.Copper Foil Contamination 2.Laminate Void 17.Negative etch back 33.Lifter Land 3.(Resin) De-lamination 18. Hole Wall Pull Away 34.Resin Crack De-lamination 4.Pad Cratering 19. Corner Crack 35.Crazing 5.Lifted Land Crack 20. (Copper) Blistering 36.Foreign Inclusion 6.Burr 21.Glass Fiber Protrusion 37.Prepreg Void 7.Bond Enhancement Removed – 22.Innerlayer (Post) Separation 38.Copper Clad Laminate Void “Pink Ring” 23.Wicking 39.Measling 8.Negative Etchback 24.Over Plating Resist Void 40.Resin Recession 9.Foil Crack 25. Positive Etchback 41.Glass-Weave Texture 10.Hole Plating Void 26.Barrel Crack 42.Glass – Weave Exposure 11.Wedge Void 27.Shadowing 12.Glass Fiber Void 28.Nodule 101 ISRO-PAX-304 11 ANNEXURE-3 :Typical Example for Plated Through Hole Figure 49 :Typical example of plated through hole 1. Plating void 11. Lifted land 21. Negative etchback 2. Pin hole 12. Pull away 22. Nail heading 3. Plating crack 13. Wicking (Copper) 23. Weave Exposure (fibers visible) 4. Basic copper crack 14. Glass fiber protrusion 24. Weave Texture(Glass cloth 5. De-lamination 15. Rough drilling and wicking 6. De-lamination 25. Tin lead thickness less than 1 (Copper) μm at an angle 7. Measling 16. Burr 8. Laminate void (out of thermal 17. Plating nodule zone) shape visible) 18. Smearing 9. Resin recession inner layer 19. Adhesion defect 10. Resin crack 20. Positive etchback (inner layer copper imbedded in plated copper) 102 ISRO-PAX-304 12 ANNEXURE-4 :Typical Via Types Figure 50:Typical via types 103 Contributors Task Team: M.M.Vachhani, SAC M.P.James, ISAC G. Jayaprasad, IISU V.V. Janardanan,VSSC (Retd.) Thomas John,VSSC (Retd.) Co-opted: Rangalakshmi, ISAC Mukesh Kumar Patel, SAC