Physical Structure of Matter Radioactivity Law of distance and absorption of gamma or beta rays 5.2.41-01/11 What you can learn about … Radioactive radiation Beta-decay Conservation of parity Antineutrino Gamma quanta Half-value thickness Absorption coefficient Term diagram Pair formation Compton effect Photoelectric effect Conservation of angular momentum Forbidden transition Weak interaction Dead time Principle: The inverse square law of distance is demonstrated with the gamma radiation from a 60Co preparation, the half-value thickness and absorption Set-up of experiment P2524111 with Cobra3 What you need: µ cm Experiment P2524111 with Cobra3 Experiment P2524101 with GM Counter Unit-construction plate for radioactivity 09200.00 1 1 Counter tube, magnet held 09201.00 1 1 Source holder, magnet held 09202.00 1 1 Plate holder for demo. board with magnet 09204.00 1 1 Counter tube, type A 09025.11 1 1 Screened cable, BNC, l = 750 mm 07542.11 1 1 Vernier caliper 03010.00 1 1 Radioactive sources, set 09047.50 1 1 Absorption plates for b-radiation 09024.00 1 1 Absorption material, lead 09029.01 1 1 Absorption material, iron 09029.02 1 1 Absorption material, aluminium 09029.03 1 1 Absorption material, Plexiglas® 09029.04 1 1 Absorption material, concrete 09029.05 1 1 Geiger-Müller Counter 13606.99 1 RS232 data cable 14602.00 1 Cobra3 Basic Unit 12150.00 1 Power supply, 12 V- 12151.99 1 Counter tube module 12106.00 1 Cobra3 Radioactivity Software 14506.61 1 PC, Windows® 95 or higher Complete Equipment Set, Manual on CD-ROM included Law of distance and absorption of gamma or beta rays P25241 01/11 PHYWE Systeme GmbH & Co. KG · D - 37070 Göttingen g cm Attenuation coefficient of different materials as a function of the material density (from left to right: Plexiglas®, concrete, aluminium, iron, lead). coefficient of various materials determined with the narrow beam system and the corresponding mass attenuation coefficient calculated. Tasks: 1. To measure the impulse counting rate as a function of the distance between the source and the counter tube. 2. To determine the half-value thickness d1/2 and the absorption coefficient of a number of materials by measuring the impulse count- ing rate as a function of the thickness of the irradiated material. Lead, iron, aluminium, concrete and Plexiglas are used as absorbers. 3. To calculate the mass attenuation coefficient from the measured values. Laboratory Experiments Physics 225 LEP 5.2.41 -01 Law of distance and absorption of gamma or beta rays Related topics Radioactive radiation, beta-decay, conservation of parity, antineutrino, gamma quanta, half-value thickness, absorption coefficient, term diagram, pair formation, Compton effect, photoelectric effect, conservation of angular momentum, forbidden transition, weak interaction, dead time. Principle The inverse square law of distance is demonstrated with the gamma radiation from a 60CO preparation, the half-value thickness and absorption coefficient of various materials determined with the narrow beam system and the corresponding mass attenuation coefficient calculated. Equipment Radioactive sources, set Absorption plates for b-radiation Unit-construction plate for radioactivity Counter holder, magnet held Source holder, magnet held Plate holder for demonstration board with magnet Vernier caliper Screened cable, BNC, l = 750 mm Counter tube, type A, BNC 09047.50 09024.00 09200.00 09202.00 09201.00 1 1 1 1 1 09204.00 03010.00 07542.10 09025.11 1 1 1 1 Geiger-Müller Counter Absorption material, lead Absorption material, Plexiglas Absorption material, iron Absorption material, concrete Absorption material, aluminium 13606.99 09029.01 09029.04 09029.02 09029.05 09029.03 1 1 1 1 1 1 Tasks 1. To measure the impulse counting rate as a function of the distance between the source and the counter tube. 2. To determine the half-value thickness d1/2 and the absorption coefficient m of a number of materials by measuring the impulse counting rate as a function of the thickness of the irradiated material. Lead, iron, aluminium, concrete and Plexiglas are used as absorbers. 3. To calculate the mass attenuation coefficient from the measured values. Set-up According to Fig. 1. The distance between the front edge of the source rod and the counting tube window is approximately 4 cm; consequently, the absorption plates can be easily inserted into the radiation path. Fig. 1: Experimental set-up for measuring the half-value thickness of different materials. PHYWE series of publications • Laboratory Experiments • Physics • © PHYWE SYSTEME GMBH & Co. KG • D-37070 Göttingen 25241-01 1 LEP 5.2.41 -01 Law of distance and absorption of gamma or beta rays Theory and evalution The cobalt isotope 60 27 Co has a half-life of 5.26 years; it undergoes beta-decay to yield the stable nickel isotope 60 28 Ni– see Fig. 2. Fig. 3: Law of distance relating to rays which are propagated in a straight line from a point source. From the regression lines from the measured values in Fig. 4, applying the exponential expression . N ( r) = a · rb, we obtain the value b = – 2.07 ± 0.01 for the exponent. This thus proves the applicability of the inverse square law. Fig. 2: Term diagram of 60 27 Co. As with most beta emitters, disintegration leads at first to daughter nuclei in an excited state, which change to the ground state with the emission of gamma quanta. Whereas the energy levels of the beta electrons can assume any value up to the maximum because of the antineutrinos involved, the gamma quanta which participate in the same transition process have uniform energy, with the result that the gamma spectrum consists of two discrete, sharp lines (Fig. 2). . The impulse counting rate N ( r) per area A around a pointsource decreases in inverse proportion to the square of the distance provided the gamma quanta can spread out in straight lines and are not deflected from their track by interactions. r2 2 r1 A2 4 · A1 a r2 2 b · A1 r1 The reason for this is that, as shown by Fig. 3, the area of a sphere round the source through with a beam of rays passes, increases as the square of the distance r. In vacuum (in air), therefore N 1r2 N 1o2 1 2 · r A A 4p . If we plot the counting rate N( r) versus the distance r on a loglog scale, we obtain a straight line of slope – 2. 2 25241-01 Fig. 4: Counting rate plotted against distance (log-log plot). The attenuation of the gamma rays when they pass through an absorber of thickness d is expressed by the exponential law . . N (d) = N (o) · e–Nd, . where N (d) is the. impulse counting rate after absorption in the absorber, and N (o) is the impulse counting rate when no PHYWE series of publications • Laboratory Experiments • Physics • © PHYWE SYSTEME GMBH & Co. KG • D-37070 Göttingen LEP 5.2.41 -01 Law of distance and absorption of gamma or beta rays absorption takes place: N is the absorption coefficient of the absorber material and depends on the energy of the gamma quantum. The absorption of the gamma rays is brought about by three independent effects – the Compton effect, the photelectric effect and pairformation. The relative contributions of these three effects to total absorption depends primarily on the energy of the quanta and on the atomic number of the absorber (Fig. 5). . Fig. 6: Impulse counting rate N as a function of the thickness d of the absorber. The half-value thickness d1/2 of a material is defined as the thickness at which the impulse counting rate is reduced by half, and can be calculated from the absorption coefficient in accordance with d1/2 = ln 2 . m Fig. 5: Absorption of gamma rays by leads as a function of the energy (NCo = fraction due to Compton effect, NPh = fraction due to photoelectric effect, NPa = fraction due to pair formation). The total absorption coefficient (attenuation coefficient) is N = NCo + NPH + NPa From the regression lines from the measured values in Fig. 6 we obtain the following values for N = b and for d1/2 and N/S, with the relevant standard errors, using the exponential expression . N = aebd. We can see from the N/E curves in Fig. 6 that lead is particularly suitable as an absorber of gamma rays of low or high energy. Lead: (S = 11.34 gcm-3) N = 0.62 cm-1, d1/2 = 1.12 cm, m = 0.055 cm2g-1; The attenuation of gamma rays therefore takes place predominantly in the electron shell of the absorber atoms. The absorption coefficient N should therefore be proportional to the number of electrons in the shell per unit volume, or approximately proportional to the density S of the material. The mass attenuation coefficient N/S is therefore roughly the same for the different materials. r sN = 0.009 cm-1 sd1/2 = 0.02 cm sN/S = 0.001 cm2g-1 Aluminium: (S = 2.69 gcm-3) N = 0.15 cm-1, sN = 0.01 cm-1 d1/2 = 4.6 cm, sd1/2 = 0.3 cm m = 0.056 cm2g-1; sN/S = 0.004 cm2g-1 r PHYWE series of publications • Laboratory Experiments • Physics • © PHYWE SYSTEME GMBH & Co. KG • D-37070 Göttingen 25241-01 3 LEP 5.2.41 -01 Law of distance and absorption of gamma or beta rays Iron: (S = 7.86 gcm-3) N = 0.394 cm-1, d1/2 = 1.76 cm, m r = 0.050 cm2g-1; Plexiglas: (S = 1.119 gcm-3) sN = 0.006 cm-1 sd1/2 = 0.03 cm sN/S = 0.001 cm2g-1 Concrete: (S = 2.35 gcm-3) N = 0.124 cm-1, sN = 0.009 cm-1 d1/2 = 5.6 cm, sd1/2 = 0.4 cm m r 4 = 0.053 cm2g-1; 25241-01 sN/S = 0.004 cm2g-1 N = 0.078 cm-1, d1/2 = 8.9 cm, m r = 0.066 cm2g-1; sN = 0.004 cm-1 sd1/2 = 0.5 cm sN/S = 0.003 cm2g-1 Comment The procedure and evaluation are shown here in an exemplary experiment for g-quanta; however, they can also be performed in an analogous manner for electrons. In the latter case, the Sr-90 source rod from the radioactive sources set (09047.50) and the absorption plate set for b-radiation (09024.00) must be used. PHYWE series of publications • Laboratory Experiments • Physics • © PHYWE SYSTEME GMBH & Co. KG • D-37070 Göttingen LEP 5.2.41 -11 Law of distance and absorption of gamma or beta rays with Cobra3 Related topics Radioactive radiation, beta-decay, conservation of parity, antineutrino, gamma quanta, half-value thickness, absorption coefficient, term diagram, pair formation, Compton effect, photoelectric effect, conservation of angular momentum, forbidden transition, weak interaction, dead time. Principle The inverse square law of distance is demonstrated with the gamma radiation from a 60Co preparation, the half-value thickness and absorption coefficient of various materials determined with the narrow beam system and the corresponding mass attenuation coefficient calculated. Equipment Cobra3 BASIC-UNIT Cobra3 Power supply RS232 data cable Cobra3 Radioactivity Software Counter tube module Unit-construction plate for radioactivity Counter tube, magnet held Source holder, magnet held Plate holder for demonstration board with magnet Counter tube, type A Screened cable, BNC, l = 300 mm 12150.00 12151.99 14602.00 14506.61 12106.00 09200.00 09201.00 09202.00 1 1 1 1 1 1 1 1 09204.00 09025.11 07542.10 1 1 1 Vernier caliper Radioactive sources, set Absorption plates for b-radiation Absorption material, lead Absorption material, iron Absorption material, aluminium Absorption material, Plexiglas® Absorption material, concrete PC, Windows® 95 or higher 03010.00 09047.50 09024.00 09029.01 09029.02 09029.03 09029.04 09029.05 1 1 1 1 1 1 1 1 Tasks 1. To measure the impulse counting rate as a function of the distance between the source and the counter tube. 2. To determine the half-value thickness d1/2 and the absorption coefficient N of a number of materials by measuring the impulse counting rate as a function of the thickness of the irradiated material. Lead, iron, aluminium, concrete and Plexiglas are used as absorbers. 3. To calculate the mass attenuation coefficient from the measured values. Set-up According to Fig. 1. The distance between the front edge of the source rod and the counting tube window is approximately 4 cm; consequently, the absorption plates can be easily inserted into the radiation path. Fig. 1: Experimental set-up. PHYWE series of publications • Laboratory Experiments • Physics • © PHYWE SYSTEME GMBH & Co. KG • D-37070 Göttingen 25241-11 1 LEP 5.2.41 -11 Law of distance and absorption of gamma or beta rays with Cobra3 Procedure — Activate the ”Radioactivity” program module, and start the measurement stand-by phase (cf. Fig. 2). — Measure the background radiation without the radiation source. To do this, it is advisable to use a gate time of more than 500 s. The measured background rate remains in the Cobra3’s memory until it is overwritten by a new background measurement. Fig. 2. Measuring parameters. — Diagram settings: y axis: 0 to 15 x axis: 0 to 30 mm — Activate measurement by clicking on <Continue>. — During the measurement the distance between the counting tube and the source (Co-60) must not be changed. Initially, enter ”0” in the input field for the absorber layer (cf. Fig. 3) and click on <Measure>. Remarks Immediately after <Continue> has been clicked on in the Parameter field (Fig. 2), the measurement process begins, i.e. one must wait until a gate time period has elapsed before a measuring result appears in the display. — After each measurement increase the layer thickness of the lead absorber by 5 mm, enter the new thickness value of the absorber layer in the appropriate field and click on <Measure>. Continue in the same manner until the maximum thickness of 30 mm has been reached. After the last measurement has been made, click on the <Close> button. — Perform absorption measurements in the same manner with the following absorber materials: Iron, aluminium, Plexiglas®, concrete. Results — Figure 3 shows the counting rate as a function of the absorber layer thickness. The data (measured) points confirm the approximately exponential decrease in the counting rate as a function the layer thickness. — The g-quanta emitted by the source (Co-60) are absorbed in the lead layer to differing degrees depending on the layer thickness d. Accordingly, the quantum flux I is attenuated by the absorption layer compared to quantum flux I0 in the air. The attenuation of the quantum flux occurs in accordance with the absorption law; the quantum flux I decreases approximately exponentially with increasing layer thickness d. I I0 · e md Fig. 3. Typical display structure during the measurement; counting rate (Co-60) as a function of the absorber layer thickness (Pb plates). 2 25241-11 Fig. 4. Half-value thickness and the attenuation for lead absorber plates. PHYWE series of publications • Laboratory Experiments • Physics • © PHYWE SYSTEME GMBH & Co. KG • D-37070 Göttingen Law of distance and absorption of gamma or beta rays with Cobra3 where m is the attenuation coefficient characteristic for the material (and the energy of the g-radiation). For a very specific layer thickness dH the initial quantum flux is reduced to half of its original value. 1 I I0 · e mdH 2 0 From this it follows that the half-value thickness dH is determined by the attenuation coefficient m. dH ln 2 m or m ln 2 dH . LEP 5.2.41 -11 — In the second part of the experiment layers of material exhibiting differing thickness d and different densities r are positioned in the radiation field between the g-source Co60 and the counter tube. In a manner analogous to the evaluation described above, determine the half-value thicknesses for iron, aluminium, Plexiglas® and concrete, and calculate their attenuation coefficient: Material Density g/cm3 Half-value (layer) thickness dH in cm Attenuation coefficient m in cm-1 Lead 11.11 1.41(1) 0.50 Iron 7.68 2.3(4) 0.30 Aluminium 2.70 7(3) 0.09 Concrete 1.87 6(3) 0.12 Plexiglas® 1.19 35(82) 0.02 The attenuation coefficient m characterises the absorption behaviour of the material with respect to g-quanta. — Determination of the half-value thickness and the attenuation coefficient m. Both parameters are displayed if the exponential measurement curve in the active image can be seen and then the evaluation functions <Analysis>, <Half-value time /-layer thickness> are selected. Naturally, these parameters can also be manually determined by initially calculating the natural logarithm of the measured values with <Channel modification> and by subsequently fitting a straight line through the thus manipulated measured values. The following is then true for the halfvalue layer thickness dH: ln 2 dH , m The attenuation coefficient m increases approximately proportionally to the density r of the absorption material. m mm · r The proportionality factor, the mass attenuation coefficient mm for lead is obtained from the attenuation coefficient m according to the following equation: mm m cm2 0.045 . r g The mass attenuation coefficient mm is approximately the same for all materials (if the energy of the g-quanta is fixed). Consequently, the attenuation law is also pragmatically written in the following form: where m is the slope of the straight line. In this exemplary measurement the half-value thickness of lead is dH = 1.416 ± 0.009 cm and the attenuation coefficient is m = 0.5 ± 0.1 cm-1. Fig. 5. Attenuation coefficient m of different materials as a function of the material density r (from left to right: Plexiglas®, concrete, aluminium, iron, lead). I I0 · e mmm'' with m'' r · d . The mass coverage m” states which mass an absorption layer has per unit surface. The mass coverage m” is a decisive parameter for the attenuation of a g-flux. Remarks — The counting rates measured depend on the source used and on the age of the specimen. — The attenuation coefficients m are also a function of the energy of the emitted g-quanta, which is relatively high for Co-60 (hard g-radiation). At lower energies (soft g-radiation) the attenuation coefficients exhibit different values. — When using radioactive substances, conform absolutely to the stipulations of the respective applicable radiation protection regulations. Radioactive substances can be hazardous to your health! Always reduce the time spent handling radioactive substances to a minimum. Do not eat or drink in the presence of radioactive substances and always wash you hands after contact with radioactive substances! PHYWE series of publications • Laboratory Experiments • Physics • © PHYWE SYSTEME GMBH & Co. KG • D-37070 Göttingen 25241-11 3 LEP 5.2.41 -11 4 Law of distance and absorption of gamma or beta rays with Cobra3 25241-11 PHYWE series of publications • Laboratory Experiments • Physics • © PHYWE SYSTEME GMBH & Co. KG • D-37070 Göttingen