VTT TECHNICAL RESEARCH CENTRE OF FINLAND LTD CV [J] Uper shelf "Ductile" Sub-sized CVN specimen conversion methodology Transition region Lower shelf "Brittle" 0 T [ C] ASTM A01-13 meeting Tampa 2015 Kim Wallin 1 ASTM A370 Table 9 60 50 Table 9 is based on a simple thickness-ratio correction. KV10 [J] 40 30 ASTM A370 Table 9 20 3/4 2/3 1/2 1/3 1/4 10 0 0 21/10/2015 5 10 15 20 25 KVB [J] 30 35 40 45 2 Subsized specimens Sub-size specimens yield higher absolute energies 100 80 1/2 2/3 1/1 A simple ratio-correction KV5x10 [J] is not sufficient for the 60 adjustment of sub-size Charpy-V specimen energies. 40 20 0 0 50 100 150 200 KV10x10 [J] Sub-size specimens yield lower proportional energies 3 Effect of thickness on transition curve 140 2 KV/(Bb) [J/cm ] 120 McNicol 1965 100 80 1.25 2.5 5 10 15 60 40 20 0 -100 -50 0 50 100 150 o T [ C] McNicol, R. (1965, September). Correlation of Charpy Test Results for Standard and Nonstandard Size Specimens. Welding Research Supplement, pp. 385-393. 21/10/2015 4 Subsized specimens 20 0.25 TCV28J = TCV35J/cm - 51.4 ln{2 (B/10) 2 95 % -1} Similar to a statistical size effect related to cleavage initiation. See e.g. ASTM E1921. 0 o TCV35J/cm - TCV28J [ C] Sub-size specimens yield lower transition temperature 0 T 5 C 5% -20 2 .2 84 UG ME s S er A w To -40 -60 THICKNESS CORRECTION FOR CVN TRANSITION TEMPERATURE -80 -100 0 2 4 6 8 10 Included in BS7910-13 12 B [mm] Wallin K. Methodology for selecting Charpy toughness criteria for thin high strength steels - Part 1: Determining the fracture toughness: D733. Jernkontorets Forskning, 1994. 5 Subsized specimens 20 Similar to a statistical size effect related to cleavage initiation. See e.g. ASTM E1921. 95 % o TCV35J/cm - TCV28J [ C] Sub-size specimens yield lower transition temperature 0 -20 .2 5% 2 ME S A 4 -8 G U TCV28J = TCV35J/cm - 51.4 ln{2 (B/10) -40 2 we o T -60 rs -1} 0 T 5 C THICKNESS CORRECTION FOR CVN TRANSITION TEMPERATURE -80 -100 0.25 0 2 4 6 8 10 12 14 16 18 20 Included in BS7910-13 22 B [mm] Wallin K. Methodology for selecting Charpy toughness criteria for thin high strength steels - Part 1: Determining the fracture toughness: D733. Jernkontorets Forskning, 1994. 6 Subsized specimens Sub-size specimens yield lower proportional upper shelf energies 350 20 mm 8 mm 7 mm 6 mm 4 mm 3.3 mm 2.5 mm 2 CVB-US/(Bb) [J/cm ] 300 250 9 mm 7.5 mm 6.7 mm 5 mm 3.6 mm 3 mm s dcg s Some shear and some flat fracture. 200 s All shear fracture. 150 Due to a competition between shear and flat fracture. 100 50 0 0 50 100 150 200 250 300 350 2 CV10-US/0.8 [J/cm ] Wallin K Upper shelf energy normalisation for sub-sized Charpy-V specimens. Int J of Pressure Vessels and Piping, 78, 2001, pp 463-470. 7 Subsized specimens Sub-size specimens yield lower proportional upper shelf energies 1.3 (CVB-USx10)/(CV10-USxB) 1.2 1.1 1.0 1.0 All shear 0.9 0.8 0.7 1 0.6 0.5 0.5 0.4 0 20 40 60 80 100 120 CV10-US/B [kN] Wallin K Upper shelf energy normalisation for sub-sized Charpy-V specimens. Int J of Pressure Vessels and Piping, 78, 2001, pp 463-470. 8 Subsized specimens Sub-size specimens yield lower proportional upper shelf energies Normalisation is insensitive to strength but sensitive to modulus of elasticity . Austenitic stainless slightly different than structural steel. Wallin K Upper shelf energy normalisation for sub-sized Charpy-V specimens. Int J of Pressure Vessels and Piping, 78, 2001, pp 463-470. 9 Subsized specimens Sub-size specimens yield lower proportional upper shelf energies THICKNESS CORRECTION FOR UPPER SHELF 500 B = 7.5 mm B = 5 mm B = 3.3 mm B = 2.5 mm 2 KV10/0.8 [J/cm ] 400 300 200 100 Mean predictions 0 0 50 100 150 200 250 300 350 2 KVB/(0.8xB) [J/cm ] Wallin K Upper shelf energy normalisation for sub-sized Charpy-V specimens. Int J of Pressure Vessels and Piping, 78, 2001, pp 463-470. 10 Temperature adjustment Energy conversion 11 • The conversion accounts for the lower energy required to fracture shear lips. • CV10-US corresponds basically to a value without shear lips. • For high CVN energies the measured full size specimen energy becomes therefore less than indicated by the equation. • Begins to effect when CV10 > 100 J. 12 Energy conversion 300 Estimated measured energy. KV10 [J] 200 KV3/4 KV2/3 100 KV1/2 KV1/3 KV1/4 0 0 50 100 150 200 KVB [J] 13 160 2 KV10est/(Bb) [J/cm ] 140 McNicol 1965 120 100 80 1.25 2.5 5 10 15 60 40 20 0 -20 0 20 40 60 80 100 120 140 160 o Tadjusted [ C] McNicol, R. (1965, September). Correlation of Charpy Test Results for Standard and Nonstandard Size Specimens. Welding Research Supplement, pp. 385-393. 14 50 45 4340 low toughness 40 10 7.5 5 2.5 KV10est [J] 35 30 25 20 15 10 y 1480 MPa 5 0 -200 -100 0 100 200 300 400 o Tadjusted [ C] Enrico Lucon, C. N. (2015). Impact Characterization of 4340 and T200 Steels by Means of Standard, Sub-Size and Miniaturized Charpy Specimens. NIST Technical Note 1858. 15 140 120 4340 high toughness 10 7.5 5 2.5 KV10est [J] 100 80 60 40 y 952 MPa 20 0 -200 -150 -100 -50 0 50 100 o Tadjusted [ C] Enrico Lucon, C. N. (2015). Impact Characterization of 4340 and T200 Steels by Means of Standard, Sub-Size and Miniaturized Charpy Specimens. NIST Technical Note 1858. 16 300 KV10est [J] 250 T200 200 10 7.5 5 2.5 150 100 50 y 1134 MPa 0 -200 -150 -100 -50 0 50 100 150 o Tadjusted [ C] Enrico Lucon, C. N. (2015). Impact Characterization of 4340 and T200 Steels by Means of Standard, Sub-Size and Miniaturized Charpy Specimens. NIST Technical Note 1858. 17 80 X52 70 KV10est [J] 60 10 6.67 5 50 40 30 20 y 325 MPa 10 0 -100 -50 0 50 100 150 200 250 o Tadjusted [ C] E. Lucon, C. N. McCowan, and R. L. Santoyo, (2015). Impact Characterization of Line Pipe Steels by Means of Standard, Sub-Size and Miniaturized Charpy Specimens. NIST Technical Note 1865. 18 500 X65 KV10est [J] 400 10 6.67 5 300 200 100 y 514 MPa 0 -150 -100 -50 0 50 100 150 o Tadjusted [ C] E. Lucon, C. N. McCowan, and R. L. Santoyo, (2015). Impact Characterization of Line Pipe Steels by Means of Standard, Sub-Size and Miniaturized Charpy Specimens. NIST Technical Note 1865. 19 500 X70 KV10est [J] 400 300 10 6.67 5 200 100 y 0 -160 -140 -120 -100 -80 -60 -40 503 MPa -20 0 20 40 o Tadjusted [ C] E. Lucon, C. N. McCowan, and R. L. Santoyo, (2015). Impact Characterization of Line Pipe Steels by Means of Standard, Sub-Size and Miniaturized Charpy Specimens. NIST Technical Note 1865. 20 300 X100 KV10est [J] 250 y 817 MPa 200 150 100 10 6.67 5 50 0 -150 -100 -50 0 50 100 150 o Tadjusted [ C] E. Lucon, C. N. McCowan, and R. L. Santoyo, (2015). Impact Characterization of Line Pipe Steels by Means of Standard, Sub-Size and Miniaturized Charpy Specimens. NIST Technical Note 1865. 21 Upper shelf behaviour (KVBx10)/(KV10xB) 1.2 4340L 4340H T200 X52 X65 X70 X100 1.0 KV10 > 400 J 0.8 0.6 0.4 0 20 40 60 80 100 120 KV10/B [kN] 22 400 U 350 <450MPa =500-550MPa U 300 = =600-700MPa ISO/DIN U 80 U >800MPa 250 U 30° Pa Pa M 0 = 45 200 CVISO J r = 2 mm CVASTM J 0 0 50 100 150 200 250 30° 50 r = 8 mm 100 300 C J 12 VASTM U MPa 350 400 2 The ASTM hammer show for high toughness higher energies than the ISO hammer 4 150 ASTM CV [J] ISO U 0 M 450 500 CV [J] ASTM E23 23 energy conversion Full size [J] 10 14 16 18 20 22 27 34 41 48 54 60 68 76 86 100 3/4 [J] 7 10 12 13 15 16 20 25 31 36 40 45 51 57 65 75 2/3 [J] 7 9 11 12 13 15 18 23 27 32 36 40 45 51 57 66 1/2 [J] 5 7 8 9 10 11 13 17 20 24 27 30 34 38 43 49 1/3 [J] 3 5 5 6 7 7 9 11 14 16 18 20 22 25 27 31 1/4 [J] 2 3 4 4 5 5 7 8 10 12 13 14 16 18 19 20 temperature adjustment Thickness Full size 3/4 2/3 1/2 1/3 1/4 Adjustment [°C] 0 8 11 20 34 45 24 TECHNOLOGY FOR BUSINESS 25