r r
SW4I
LEnvironmental, Inc.
B|6 1998S
February 13, 1996
File No. 95-0001
Massachusetts Department of Environmental Protection
Bureau of Waste Site Cleanup
20 Riverside Drive
Lakeville, MA 02347
Re:
Immediate Response Action Plan
Augat Inc.
106 Falmouth Road
Mashpee, MA
RTN No.4-11904
To Whom It May Concern:
AWARD Environmental, Inc. (AWARD) has prepared this Immediate Response Action (IRA) Plan
for the above-referenced property (Site) on behalf of Augat Inc. This plan has been prepared in
response to a 72-hour release notification which was made to the Massachusetts Department of
Environmental Protection (DEP) on January 20, 1996 Based on DEP's Notice of Responsibility
letter of January 24, 1996 to Augat Inc., we understand that the following assessment has been
approved. The plan has been prepared in accordance with our verbal notification and 310 CMR
40.0424 - Immediate Response Action Plans.
The information required in 310 CMR 40.0424 is provided below:
Name, address, telephone number and relationship to the Site of the person assuming
responsibility for conducting the IRA
The Site is owned by Augat Inc., which is assuming responsibility for conducting the IRA. The
following person should-be contacted at Augat Inc. regarding this IRA:
William 0. Frigon
Corporate Manager Facility and Environment
Augat Inc.
89 Forbes Boulevard
P.O. Box 448
Mansfield, MA 02048
Phone number: (508) 337-3730
3670 West Shore Road - Warwick, Rhode Island 02886-5051 - Phone: (401) 738-3887 - Fax: (401) 732-1686
DEP
File No. 95-0001
February 13, 1996
Page 2
Release, site conditions and surrounding receptors
The Site is currently utilized by Augat Inc. to manufacture electronic connectors and couplers. The
Site is currently serviced with municipal water and it utilizes an on-Site septic system to dispose of
sanitary wastewaters. On-Site wells were previously utilized to supply potable water to the Site
prior to the availability of municipal water. However, these wells were removed from service in
January 1995.
The area surrounding the Site is a mixture of industrial, commercial and residential land uses. A Site
Plan is provided as Figure 1. Located to the north of the Site, across Falmouth Road, is vacant land
and commercial land uses. Several commercial land uses are located adjacent to and to the east of
the Site. Vacant land, a high tension power line easement and residential properties are located to
the south; and two residences are located adjacent to and to the west of the Site. Municipal sewer
service is not available in the vicinity of the Site and municipal water is only available to the
properties located along Falmouth Road.
On December 27, 1995, AWARD initiated a subsurface exploration program at the Site. This
program included three test borings and the installation of three groundwater monitoring wells (see
Figure 1). During boring advancement, Standard Penetration Tests (SPTs) were performed and
split-spoon soil samples were recovered. Collected soil samples were field screened for total
volatile organic compounds (VOCs) using an HNU Model P-101 Photoionization Detector (PID)
and were classified. No elevated PID readings were detected. The results of field screening are
presented on the boring logs in Appendix A. In addition, three soil samples collected at the
groundwater surface were submitted under chain of custody to Alpha Analytical Laboratories of
Westboro, Massachusetts. These samples were analyzed for VOCs by EPA Method 8260 and for
total petroleum hydrocarbons (TPH) by EPA Method 8100. The results of soil sample analyses are
summarized below:
Table 1
Results of Soil Sample Analysis
-
Location
AW-1
30' - 32'
AW-2
25' - 27'
AW-3
25' - 27'
Volatile Organic Compounds
ND
ND
ND
UTotal Petroleum Hydrocarbons
ND
ND
ND
Parameter
Notes:
Io.
See certificates of analysis for a complete list of parameters, analytical methods and limits of detection.
2.
ND equals not detected.
Certificates of analyses for the soil samples are presented in Appendix B.
I
W
DEP
File No. 95-0001
February 13, 1996
Page 3
The depth to water in each monitoring well was gauged using a stainless steel tape. This included
gauging the wells for the presence of separate-phase petroleum product using the chalk and paste
technique. The relative elevation of each well was surveyed and each well was located from
prominent Site features.
Groundwater was detected at the Site at depths ranging from approximately 22 feet (AW-3) to 28
feet (AW-1). Separate-phase product was not detected in any of the wells. Based on the gauging
and elevation survey, groundwater was determined to be flowing across the Site in a southerly
direction. Groundwater elevation contours and our measured direction of groundwater flow are
presented on Figure 1.
Groundwater samples were obtained using precleaned 1-liter disposable polyethylene bailers. A
separate bailer was used for each well to avoid cross-contamination. Three times the initial volume
of water in each well was purged prior to sampling and the well was allowed to recharge. Samples
were placed in laboratory cleared sample jars and maintained on ice for delivery under chain-ofcustody to Alpha Analytical Laboratories for VOC analyses by EPA Method 8260, TPH analyses
by EPA Method 8100 and polynuclear aromatic hydrocarbon (PAH) analyses by EPA Method 8270.
The results of analyses are summarized below:
Table 2
Results of Groundwater Sample Analyses
Location
Parameter
AT
AW-1
Volatile Organic Compounds
1,1,1-trichloroethane
trichloroethene
ND
Polynuclear Aromatic Hydrocarbons
ND
Total Petroleum Hydrocarbons
ND
Notes:
1.
2.
3.
-
AW-2
AW-3-
RC-GWI
ND
1.3 ug/l
26 ug/l
200 ug/l
5 ug/l
ND
ND
-
ND
ND
---
See certificates of analyses for a complete list of parameters, analytical methods and limits of detection.
ND equals not detected.
RC-GW1 equals the Reportable Concentration for Groundwater Category 1 as presented in 310 CMR 40.1600.
Certificates of analyses for the groundwater samples is provided in Appendix B.
As presented above, the concentration of trichloroethene detected in the groundwater sample
collected from monitoring well AW-3 exceeded its applicable Reportable Concentration as presented
in 310 CMR 40.1600.
MAD1J4
DEP
File No. 95-0001
February 13, 1996
Page 4
On January 16, 1996, AWARD also conducted a soil gas survey beneath the slab of the Site
building. The results of this survey will be included in the IRA report.
Immediate Response Actions undertaken to date
No Immediate Response Actions have been completed at the Site to date.
Why is an IRA required ?
As presented above, trichloroethene was detected in a groundwater sample collected from
monitoring well AW-3 at a concentration of 26 ug/l. This concentration exceeded the applicable
Reportable Concentration of 5 ug/l as presented in 3 10 CMR 40.1600. Monitoring well AW-3 may
be located within 500 feet of a private water supply well. Therefore, in accordance with 310 CMR
40.0313, a 72-hour notification condition potentially exists at the Site. Notification was made to the
DEP on January 20, 1996 in accordance with applicable regulations.
Objective, specific plans and proposed schedulefor the IRA
The objective of the IRA is to evaluate if the trichloroethene detected at the Site has affected nearby
private water supply wells and whether a containment or removal action is necessary. To meet this
objective, this "assessment only" IRA includes reviewing the history of Site use, viewing the Site
for surficial evidences of releases, identifying the location and construction (if available) of nearby
wells, and completing additional subsurface explorations.
This IRA Plan has been prepared based on our current understanding of Site conditions. As more
information concerning the Site becomes evident (following completion of services proposed in the
tasks specified below), additional tasks may be recommended. Therefore, the scope of work
proposed below may require modification as additional information is developed concerning the
Site.
To meet this objective, the following scope of work is proposed:
Task 1: Well Resampling
A second groundwater sample will be collected from monitoring well AW-3 using standard
procedures and protocols (see Task 6). This sample will be placed in a laboratory cleaned sample
jar, maintained on ice, and delivered under chain-of-custody for laboratory analyses. The sample
will be analyzed for VOCs by EPA Method 524.2. Based on the results of this task, the following
tasks may be modified.
JW
N
DEP
File No. 95-0001
February 13, 1996
Page 5
Task 2: Site Sensitivity Review
We will evaluate the Site and nearby areas for the presence of sensitive human and environmental
receptors. This will primarily include identifying and locating private water supply wells within 500
feet of the Site. Our review will include the following:
-
A reconnaissance of the Site and surrounding area (adjacent and nearby properties) for the
presence of wetlands, streams, surface water bodies, visible well heads, etc.
-
Contact with local agencies concerning the potential presence of sensitive receptors,
including the location of private wells in the vicinity of the Site. We will also confirm which
nearby properties are provided with municipal potable water.
-
Review of DEP GIS and topographic maps for the Site vicinity.
Task 3 - Background Information
The following tasks will be completed to develop an understanding of Site history and to identify
potential areas of on-Site and off-Site concern:
Interviews
AWARD will interview knowledgeable facility personnel about the Site to develop an
understanding of Site conditions. Our interview will be conducted by telephone and/or during the
Site visit (Task 4).
Previous Site Investigations
AWARD will review documents detailing previous investigations or studies conducted at
the Site, if such documentation exists.
State and Federal Regulatory Information
AWARD will review state and federal regulatory information concerning the Site and other
nearby properties. Regulatory information will be selected from various regulatory databases which
will be searched by a professional database search firm. In general we anticipate that the following
databases will be searched (as available):
DEP
File No. 95-0001
February 13, 1996
Page 6
National Priorities List sites
CERCLIS list
RCRA TSD list
RCRA generator list
RCRA Administrative Action Tracking System (RAATS)
ERNS list
State hazardous waste sites list
State landfill or solid waste disposal sites
State leaking underground storage tank list
State registered underground storage tank list
I mile
.5 mile
I mile
property and adjoining properties
.5 mile
property only
I mile
.5 mile
.5 mile
property and adjoining property
Task 4 - Site Visit
To evaluate Site conditions, we will visit the Site and local regulatory agencies as follows:
Site Reconnaissance
AWARD will perform a reconnaissance of the Site to observe surficial evidence of releases
of hazardous materials. During our reconnaissance, we will typically make observations for use of
the Site and adjoining properties; hazardous materials use and storage; the presence and locations
of underground and aboveground storage tanks; the location of floor drains, sumps, etc.; and
evidence of spills, releases or discharges of hazardous materials to the soil and groundwater.
Local Agencv Review
AWARD will attempt to contact local regulatory agencies to inquire about environmental
conditions at the Site. We anticipate that these agencies will typically include:
I
Water/Sewer Depts
Fire Department
Tax Assessor's Office
Engineering Department
Building Department
Town Clerk
Contact may be made in person or by telephone interview.
Task 5: Site Setting and Historv Review
AWARD will review historical sources to develop a chain of Site history from undeveloped land
and/or data failure. Historical sources will include the following as available and appropriate for
the Site:
aerial photographs
-
fire insurance maps
city directories
Tax Assessor's records
-
topographic maps
Building Dept. records
Tide Records-if provided
-
street directories
Town Clerk records
AWAAD
DEP
File No. 95-0001
February 13, 1996
Page 7
Task 6 - Subsurface Exploration Program
Subsurface explorations including soil borings, the installation of approximately eight additional
monitoring wells (approximately six shallow wells and two deep wells) and the collection and
analyses of soil and groundwater samples will be completed at the Site. These borings will be
installed at downgradient locations to further define the limits of the trichloroethene detected in AW3. Proposed soil boring/monitoring well locations are presented on Figure 1.
The following subsurface exploration program will be completed at the Site:
Test Borings
Initially, we will perform approximately six shallow test borings at the Site. Soil borings
will be completed using hollow-stem auger drilling techniques. We have assumed that the maximum
depth of the borings will be approximately 20 feet into the field observed water table and that the
total depth of the borings will be approximately 50 feet. During advancement of the borings, soil
samples will be collected by split-spoon sampling techniques at approximately 5-foot intervals, if
conditions allow. Standard Penetration Tests (SPTs) will be performed during sample collection.
In addition, following the initial sampling of these six newly installed "shallow" monitoring wells,
approximately two "deep" monitoring well(s) will be installed adjacent to the shallow wells with the
highest concentration and/or at other selected downgradient locations. These borings will be
installed by casing and wash techniques to a depth of approximately 85 to 100 feet (the actual depth
of these wells will be determined during the shallow borings and Task 2).
Collected soil samples will be field screened for total volatile organic compounds (VOCs)
using a photoionization detector (PID). If indicated by field screening, select soil samples may be
submitted for laboratory analyses.
A monitoring well will be installed in each boring which encounters groundwater.
Monitoring well installation will typically consist of 2-inch diameter PVC well screen and 2-inch
diameter PVC riser pipe. The well screen in the "shallow" wells will be set to scan the watertable
encountered during drilling with approximately 5 feet of screen above and 20 feet of screen below
the watertable, if conditions allow. The "deep" wells will be set with approximately 30-foot screens
above their bases.
Prior to conducting the explorations, we will contact local utilities to request that the on-Site
utilities be located and marked.
Well Gauging and Sampling
The relative elevation of each of the newly installed monitoring wells will be surveyed
(relative to the existing monitoring wells) and the location of the wells will be measured from
prominent Site features. We will also gauge the depth to water in each of the newly installed and
RAO~fl
DEP
File No. 95-0001
February 13, 1996
Page 8
existing monitoring wells at the Site. Each of the wells will also be gauged for the presence of
separate-phase petroleum product.
We will collect groundwater samples from each of the newly installed and existing
monitoring wells using standard procedures and protocols which include using a well dedicated
bailer and purging three well volumes prior to sampling. Each of the groundwater samples will be
submitted for laboratory testing for VOCs by EPA Method 524.2.
Task 7: IRA Completion Statement
An IRA Completion Statement will be prepared in accordance with 310 CMR 40.0427 upon
completion of the above tasks. The statement will include our opinion as to the sensitivity of the
Site, if the trichloroethene detected at the Site has affected nearby private water supply wells and
if any additional assessment and/or remediation is required. The IRA Completion Statement will
also include our opinion to whether or not the TCE detected poses an Imminent Hazard per 310
CMR 40.0320.
The following schedule for the completion of the IRA is proposed:
s
f
Task
1 - Well Resampling
2 through 5 - Sensitivity Review, visit and background
information
(Weeks From Start of IRA
341W31151
6 17
18[9
(10
11 213
DTIE!I
6 - Subsurface Explorations
7 - IRA Completion Statement
Disposition of remediation wastes
We do not currently anticipate that remediation wastes will be generated durin gthis IRA.
Proposed environmental monitoringfor implementation during and/or aftei the IRA
The proposed IRA is for assessment only. No additional monitoring, other than that detailed above,
is proposed.
Required permits
We do not anticipate that any local, state or federal permits are required to con mplete this IRA.
DEP
File No. 95-0001
February 13, 1996
Page 9
Thank you for your time and consideration. Please do not hesitate to call if you have any questions.
Very truly yours,
Principal
i
Thomas J. Dolce, PE, LSP
Principal Engineer
cc:
William 0. Frigon, Augat, Inc.
Attachments: Appendix A
Appendix B
Figure 1
AWORD
Boring Logs
Certificates of Analyses
Site Plan
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APPENDIX A
Boring Logs
nWiiND
f1 YflWEnvironmental Inc.
BORING LOG
Site: Augat Inc.
Boring No.
Page:
File No
3670 West Shore Road
Mashpee, MA
Warwick, RI 02886
Phone: (401) 738-3887, Fax (401) 732-1686
Date: Dec 27 95
Boring Equipment Description: Hollow Stem Auger
AW-1
1of 1
Reported by: Tom Daley
Boring Co: Guild
Foreman: George
Others: Mike
Depth
Sample Information
No.
Penetration/
Blows/
Recovery
6"
I- 2
24/16"
2-2-3-5
Sampler Description: Split Spoon 2" Diameter
Field Testing Equipment: HNV
Sample
Field Test
Data
0
Description:
Equipment Installed
Light Brown Medium and Fine Sand
Protective Casing
5
4-
6
|
24/18"
5-5-10-9
PVC Riser
Pipe
24-0
1
0
Light Brown Medium and Fine Sand
Bentonite
Seal
12-13
10
10-12
24/20"
3-6-9-12
0
Light Brown Medium and Fine Sand
15-17
24/20"
5-9-10-11
0
Light Brown Medium and Fine Sand
26-22
24/20"
6-6-7-9
0
Light Brown Medium and Fine Sand
15
Filter Sand
39-13
20
2" PVC
Well Screen
39-24
25
25-27
24/20"
8-13-16-20
0
30-32
24/18"
6-8-8-8
0
30
Light Brown Medium and Fine Sand
Groundwater at approximately 29 feet
Light Brown and Medium Fine Sand. Wet
35
40
Remarks:
Bottom
of
~
~
~
~ Boring~ 40 feet~
k~ ~ ~
~
~
-I1. Field testing was completed with an HNV Model P-101 I photoionization detector
equipped with a 10.2 EV lamp.
______
____
___
____
____
~
____
~
__
I
~
Total Depth
39
(not to scale)
(o
to____
scale)__________________
BORING LOG
lt~it
I/EnvironmentalInc.
Site: Augat Inc.
3670 West Shore Road
Mashpee, MA
Warwick, RI 02886
Phone: (401) 738-3887, Fax (401) 732-1686
Date: Dec 27 95
Boring Equipment Description: Hollow Stem Auger
Reported by: Tom Daley
Boring Co: Guild
Sampler Description: Split Spoon 2" Diameter
Foreman: George
Field Testing Equipment: HNV
Others: Mike
Sample Information
Depth
Sample
No.
Penetration/
Blows/
Field Test Description:
Recovery
6"
Data
0Dark Brown Fill With Small Rocks
Boring No.
Page:
AW-2
1 of 1
File No
Equipment Installed
Protective Casing
I TPVC Riser
5:
5-10
Light Brown, Fine and Medium Sand and Gravel
with Small Rocks.
Pipe
19-0
Light Brown Medium and Fine Sand
Bentonite
Seal
15-13
10
10-12
6-9-11-18
24-16
0
15
Filter Sand
34-15
20
20-22
6-8-12-13
24-18
0
25
Light Brown Fine and Medium Sand
Groundwater at approximately 24'
25-27
5-5-6-10
24/20
0
2" PVC
Well Screen
34-19
Light Brown Fine and Medium Sand. Wet
30
35
__________
I
40'
Remarks:
_______
________Bottom
of Boring
-
35'
|
Total Depth
34'
(not to scale)
1. Field testing was completed with an HNV Model P-101 photoionization detector
equipped with a 10.2 EV lamp.
BORING LOG
ANItAVEnvironmental Inc.
3670 West Shore Road
Site: Augat Inc.
Mashpee, MA
Boring No.
Page:
Warwick, RI 02886
AW-3
1of 1
File No
Phone: (401) 738-3887, Fax (401) 732-1686
Date: Dec 27 95
Boring Equipment Description: Hollow Stem Auger
Reported by: Tom Daley
Boring Co: Guild
Sampler Description: Split Spoon 2" Diameter
Foreman: George
Field Testing Equipment: HNV
Others: Mike
Depth
No.
0-2
Sample Information
Penetration/
Blows/
Recovery
6"
1
Sample
Field Test
Data
Description:
Equipment Installed
Course Sand Fill
Protective Casing
I T PVC Riser
5
Light Brown, Fine and Medium Sand and Gravel
Pipe
19-0
Bentonite
Seal
15-14
10 10-12
24-20
5-8-11-11
0
Light Brown Medium and Fine Sand
15
Filter Sand
34-15
20 20-22
24/24
7-13-15-18
25 25-27
24/-
0
Light Brown Fine and Medium Sand
8-8-11-14
2" PVC
Well Screen
34-19
Groundwater at approximately 24'
Light Brown Fine and Medium Sand. Wet
30
Bottom of Boring - 35'
35
40
Remarks:
Bottom of Boring - 35'
I
Field testing was completed with an HNV Model P-101 photoionization detector
equipped with a 10.2 EV lamp.
--.
1-
Total Depth
34'
to
(not scale)
APPENDIX B
Certificates of Analyses
AWAO
ALPHA ANALYTICAL
LABORATORIES
Eight Walkup Drive
Westborough, Massachusetts 01581-1019
(508) 898-9220
MA 086
NH 198958-A
CT PH-0574
NY 11148
NC 320
SC 88006
RI A65
CERTIFICATE OF ANALYSIS
Client:
Award Environmental
Address: 3670 West Shore Road
Warwick, RI
Attn:
02886
Alex Rothchild
Invoice Number: 80254
Date Received:
29-DEC-95
Date Reported:
11-JAN-96
Delivery Method: Alpha
Project Number:
Site:
Laboratory Job Number: L9509867
Augat
ALPHA SAMPLE NUMBER
CLIENT IDENTIFICATION
SAMPLE LOCATION
L9509867-01
AW1-30-32'
Mashpee, MA
L9509867-02
AW2-25-27'
Mashpee, MA
L9509867-03
AW3-25-27'
Mashpee, MA
I
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I
I
I
I
U
U
I
01119602:24
Scott McLean - Laboratory Director
Page
1
ALPHA ANALYTICAL LABORATORIES
CERTIFICATE OF ANALYSIS
CT PH-0574
NH 198958-A
MA 086
NY 11148
NC 320
RI A65
Date Collected: 27-DEC-95
Date Received : 29-DEC-95
Date Reported : 11-JAN-96
Laboratory Sample Number: L9509867-01
AW1-30-32'
Sample Matrix:
SOIL
Condition of Sample:
SC 88006
Field Prep:
Satisfactory
None
Number & Type of Containers: 1 Vial
RESULT
PARAMETER
UNITS
RDL
REF
METHOD
ID
DATES
PREP ANALYSIS
Solids, Total
0.10
82.
I
U
I
I
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Xylenes
cis-1,2-Dichloroethene
Dibromomethane
I
I
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
05-Jan ST
2540B
518260
Volatile Organics by-GC/MS
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
3
09-Jan 09-Jan DB
5.0
1.5
1.5
1.0
3.5
1.0
1.5
10.
1.5
3.5
5.0
1.5
1.0
1.0
1.5
1.0
1.0
1.0
1.0
1.5
1.0
10.
2.0
3.5
2.0
1.5
1.5
1.0
10.
10.
10.
10.
1.0
1.0
10.
Comments: Complete list of References and Glossary of Terms found in Addendum I
01119602:24
Page 2
ALPHA ANALYTICAL LABORATORIES
CERTIFICATE OF ANALYSIS
Laboratory Sample Number: L9509867-01
AW1-30-32'
RESULT
PARAMETER
UNITS
RDL
1
Volatile Organics by GC/MS continued
1,4-Dichlorobutane
Iodomethane
1,2,3-Trichloropropane
Styrene
Dichlorodifluoromethane
Acetone
Carbon Disulfide
2-Butanone
Vinyl Acetate
4-Methyl-2-pentanone
2-Hexanone
Ethyl methacrylate
Acrolein
Acrylonitrile
Bromochloromethane
2,2-Dichloropropane
1,2-Dibromoethane
1,3-Dichloropropane
1,1,1,2-Tetrachloroethane
Bromobenzene
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
o-Chlorotoluene
p-Chlorotoluene
1,2-Dibromo-3-chloropropane
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
Naphthalene
n-Propylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
trans-1,4-Dichloro-2-butene
Ethyl ether
REF
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
100.
100.
100.
%
DATES
PREP ANALYSIS
8260
09-Jan 09-Jan DB
10.
10.
10.
1.0
10.
10.
10.
74.
10.
10.
10.
10.
25.
10.
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
25.
SURROGATE RECOVERY
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
Comments: Complete list of References and Glossary of Terms found in Addendum I
01119602:24
Page 3
ID
METHOD
ALPHA ANALYTICAL LABORATORIES
CERTIFICATE OF ANALYSIS
Laboratory Sample Number:
L9509867-01
AW1-30-32'
RESULT
PARAMETER
UNITS
RDL
Hydrocarbon Scan GC 8100 Modified
Mineral Spirits
Gasoline
Fuel Oil #2/Diesel
Fuel Oil #4
Fuel Oil #6
Motor Oil
Kerosene
ND
ND
ND
ND
ND
ND
ND
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
REF
METHOD
ID
DATES
PREP ANALYSIS
1
BlooM
02-Jan 04-Jan DB
100
100
100
100
100
100
100
SURROGATE RECOVERY
80.0
o-Terphenyl
Comments: Complete list of References and Glossary of Terms found in Addendum I
01119602:24
Page 4
ALPHA ANALYTICAL LABORATORIES
CERTIFICATE OF ANALYSIS
I
I
NY 11148
NC 320
a
RI A65
CT PH-0574
Laboratory Sample Number:
Sample Matrix:
L9509867-02
AW2-25-27'
SOIL
Date Collected: 27-DEC-95
Date Received : 29-DEC-95
Date Reported : 11-JAN-96
Condition of Sample:
Satisfactory
Field Prep:
None
Number & Type of Containers: 1 Vial
PARAMETER
RESULT
Solids, Total
83.
UNITS
RDL
0.10
Volatile Organics by GC/MS
I
SC 88006
NH 198958-A
MA 086
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
25.
7.5
7.5
5.0
18.
5.0
7.5
50.
7.5
18.
25.
7.5
5.0
5.0
7.5
cis-1,3-Dichloropropene
ND
ug/kg
5.0
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Xylenes
cis-1,2-Dichloroethene
Dibromomethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
5.0
5.0
5.0
7.5
5.0
50.
10.
18.
10.
7.5
7.5
5.0
50.
50.
50.
50.
5.0
5.0
50.
REF
METHOD
3
2540B
1
8260
DATES
PREP ANALYSIS
05-Jan ST
09-Jan 09-Jan DB
Comments: Complete list of References and Glossary of Terms found in Addendum I
01119602:24
Page 5
ID
ALPHA ANALYTICAL LABORATORIES
CERTIFICATE OF ANALYSIS
3
I
Laboratory Sample Number: L9509867-02
AW2-25-27'
PARAMETER
RESULT
UNITS
RDL
volatile Organics by GC/MS continued
1,4-Dichlorobutane
lodomethane
1,2,3-Trichloropropane
Styrene
Dichlorodifluoromethane
Acetone
Carbon Disulfide
2-Butanone
Vinyl Acetate
4-Methyl-2-pentanone
2-Hexanone
Ethyl methacrylate
Acrolein
Acrylonitrile
Bromochloromethane
2,2-Dichloropropane
1,2-Dibromoethane
1,3-Dichloropropane
1,1,1,2-Tetrachloroethane
Bromobenzene
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
o-Chlorotoluene
p-Chlorotoluene
1,2-Dibromo-3-chloropropane
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
Naphthalene
n-Propylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
trans-1,4-Dichloro-2-butene
Ethyl ether
REF
1
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
100.
98.0
100.
%
METHOD
DATES
PREP ANALYSIS
8260
09-Jan 09-Jan DB
50.
50.
50.
5.0
50.
50.
50.
370
50.
50.
50.
50.
130
50.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
130
SURROGATE RECOVERY
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
Comments: Complete list of References and Glossary of Terms found in Addendum I
01119602:24
Page 6
ID
U
I
I
ALPHA ANALYTICAL LABORATORIES
CERTIFICATE OF ANALYSIS
Laboratory Sample Number: L9509867-02
AW2-25-27'
RESULT
PARAMETER
UNITS
RDL
Hydrocarbon Scan GC 8100 Modified
REF
1
Mineral Spirits
Gasoline
ND
ND
mg/kg
mg/kg
100
100
Fuel Oil #2/Diesel
ND
mg/kg
100
Fuel Oil #4
Fuel Oil #6
Motor Oil
ND
ND
ND
mg/kg
mg/kg
mg/kg
100
100
100
Kerosene
ND
mg/kg
100
METHOD
DATES
ID
PREP ANALYSIS
8100M
02-Jan 04-Jan DB
SURROGATE RECOVERY
o-Terphenyl
82.0
Comments: Complete list of References and Glossary of Terms found in Addendum I
01119602:24
Page 7
ALPHA ANALYTICAL LABORATORIES
CERTIFICATE OF ANALYSIS
CT PH-0574
NH 198958-A
MA 086
NY 11148
SC 88006
NC 320
Date Collected: 27-DEC-95
Date Received : 29-DEC-95
Date Reported : 11-JAN-96
Laboratory Sample Number: L9509867-03
AW3-25-27'
SOIL
Sample Matrix:
Field Prep:
Satisfactory
Condition of Sample:
RI A65
None
Number & Type of Containers: 1 Vial
PARAMETER
RESULT
Solids, Total
83.
Volatile Organics by
UNITS
ug/kg
ug/kg
Chloromethane
ug/kg
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Xylenes
cis-1,2-Dichloroethene
Dibromomethane
ug/kg
Comments: Complete list of References
Page 8
REF
METHOD
0.10
3
2540B
1
8260
CC/MS
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
01119602:24
RDL'
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
DATES
PREP ANALYSIS
ID
05-Jan ST
.09-Jan 09-Jan DB
25.
7.5
7.5
5.0
18.
5.0
7.5
50.
7.5
18.
25.
7.5
5.0
5.0
7.5
5.0
5.0
5.0
5.0
7.5
5.0
50.
10.
18.
10.
7.5
7.5
5.0
50.
50.
so.
50.
5.0
5.0
50.
and Glossary of Terms found in Addendum I
ALPHA ANALYTICAL LABORATORIES
CERTIFICATE OF ANALYSIS
Laboratory Sample Number: L9509867-03
AW3-25-27'
RESULT
PARAMETER
UNITS
RDL
1
volatile Organics by GC/MS continued
3
*
1,4-Dichlorobutane
Iodomethane
1,2,3-Trichloropropane
Styrene
Dichlorodifluoromethane
Acetone
Carbon Disulfide
2-Butanone
Vinyl Acetate
4-Methyl-2-pentanone
2-Hexanone
Ethyl methacrylate
Acrolein
Acrylonitrile
Bromochloromethane
2,2-Dichloropropane
1,2-Dibromoethane
1,3-Dichloropropane
,1,2-Tetrachloroethane
Bromobenzene
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
o-Chlorotoluene
p-Chlorotoluene
1,2-Dibromo-3-chloropropane
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
Naphthalene
n-Propylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
trans-1,4-Dichloro-2-butene
Ethyl ether
I
E
*
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
REF
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
METHOD
ID
DATES
PREP ANALYSIS
8260
09-Jan 09-Jan DE
50.
50.
50.
5.0
50.
370
50.
370
50.
50.
50.
50.
130
50.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
25.
130
SURROGATE RECOVERY
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
102.
100.
102.
i
Comments: Complete list of References and Glossary of Terms found in Addendum I
01119602:24
Page 9
ALPHA ANALYTICAL LABORATORIES
CERTIFICATE OF ANALYSIS
I
Laboratory Sample Number: L9509867-03
AW3-25-27'
PARAMETER
RESULT
UNITS
RDL
Hydrocarbon Scan GC 8100 Modified
Mineral Spirits
Gasoline
Fuel Oil #2/Diesel
Fuel Oil #4
Fuel Oil #6
Motor Oil
Kerosene
ND
ND
ND
ND
ND
ND
ND
REF
1
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
METHOD
DATES
ID
PREP ANALYSIS
BlooM
02-Jan 04-Jan DB
100
100
100
100
100
100
100
SURROGATE RECOVERY
o-Terphenyl
68.0
Comments: Complete list of References and Glossary of Terms found in Addendum I
01119602:24
Page 10
ALPHA ANALYTICAL LABORATORIES
QUALITY ASSURANCE BATCH DUPLICATE ANALYSIS
Laboratory Job Number: L9509867
Value 2
RPD
Parameter
Value 1
Solids, Total
DUPLICATE for sample(s) 01-03
82.
01119602:24
Page 11
81.
1
Units
%
ALPHA ANALYTICAL LABORATORIES
QUALITY ASSURANCE BATCH MS/MSD ANALYSIS
Laboratory Job Number: L9509867
MS %
Parameter
MSD%
RPD
Volatile Organics by GC/MS Spike Recovery MS/MSD for sample(s) 01-03
1,1-Dichloroethene
Trichloroethene
Benzene
112
114
114
114
115
115
2
1
1
Toluene
114
114
0
Chlorobenzene
112
115
3
01119602:24
Page 12
ALPHA ANALYTICAL
ADDENDUM I
LABS
REFERENCES
1.
Test Methods for Evaluating Solid Waste:
846.
1986.
3.
Standard Methods for Examination of Water and Waste Water.
17th Edition. 1989.
Physical/Chemical Methods.
GLOSSARY OF TERMS AND SYMBOLS
IREF
Reference number in which test method may be found.
IMETHOD
was performed.
Method number by which analysis
Initials of the analyst.
ID
01119602:24
Page 13
EPA SW-
APHA-AWWA-WPCF.
00
r
-
Iz
wtL
a-
_-
-C7
.
0
,
.
Dli
C'
(
tJA
M
I
T E t; 2 F' zi
3
~0
AU*s~Idufl I \.f\ kJ)
><
a
ODIJ
gilnos
/ ~qJIg~AJ
-z
wnos /xpe
)
\f)r- 4-
-+-
II
.t-
t-
-
I-
n
Gilt-- --
-
--
-
N
S.,.
0.F'
a
0
I-
2
-
I -1-
t
t-
-
1~1~
C
-j
K
C
a
C
C
C
II
I
----
-
-
I--6-
ALPHA ANALYTICAL LABORATORIES
Eight Walkup Drive
01581-1019
Westborough, Massachusetts
(508) 898-9220
MA 086
NH 198958-A
CT PH-0574
NY 11148
NC 320
SC 88006
RI A65
CERTIFICATE OF ANALYSIS
Client:
Award Environmental
Address: 3670 West Shore Road
Warwick, RI
Attn:
02886
Alex Rothchild
Laboratory Job Number: L9600021
Invoice Number: 80299
Date Received:
02-JAN-96
Date Reported:
15-JAN-96
Delivery Method: Alpha
Project Number:
Site:
ALPHA SAMPLE NUMBER
CLIENT IDENTIFICATION
SAMPLE LOCATION
L9600021-01
AW-1
Mashpee, MA
L9600021-02
AW-2
Mashpee, MA
L9600021-03
AW-3
Mashpee, MA
Authorized by:
Scott McLean - Laboratory Director
01159609:58
Page 1
ALPHA ANALYTICAL LABORATORIES
CERTIFICATE OF ANALYSIS
MA 086
NH 198958-A
CT PH-0574
NY 11148
NC 320
RI A65
Date Collected: 29-DEC-95
Date Received : 02-JAN-96
Date Reported : 15-JAN-96
Laboratory Sample Number: L9600021-01
AW-1
WATER
Sample Matrix:
Condition of Sample:
SC 88006
Field Prep:
Satisfactory
None
Number & Type of Containers: 2 Vial,2 Amber Glass
RESULT
PARAMETER
UNITS
RDL
1
Volatile Organics by GC/MS
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Xylenes
cis-1,2-Dichloroethene
Dibromomethane
1,4-Dichlorobutane
Iodomethane
REF
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
ug/l
ug/l
ug/l
ug/1
ug/1
ug/l
ug/1
ug/l
ug/l
ug/1
ug/l
ug/l
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
METHOD
ID
DATES
PREP ANALYSIS
8260
5.0
1.5
1.5
1.0
3.5
1.0
1.5
10.
1.5
3.5
5.0
1.5
1.0
1.0
1.5
1.0
1.0
1.0
1.0
1.5
1.0
10.
2.0
3.5
2.0
1.5
1.5
1.0
10.
10.
10.
10.
1.0
1.0
10.
10.
10.
Comments: Complete list of References and Glossary of Terms found in Addendum I
01159609:58
Page 2
09-Jan DB
ALPHA ANALYTICAL LABORATORIES
CERTIFICATE OF ANALYSIS
Laboratory Sample Number: L9600021-01
AW-1
RESULT
PARAMETER
UNITS
RDL
1
Volatile Organics by GC/MS continued
1,2,3-Trichloropropane
Styrene
Dichlorodifluoromethane
Acetone
Carbon Disulfide
2-Butanone
Vinyl Acetate
4-Methyl-2-pentanone
2-Hexanone
Ethyl methacrylate
Acrolein
Acrylonitrile
Bromochloromethane
2,2-Dichloropropane
1,2-Dibromoethane
1,3-Dichloropropane
1,1,1,2-Tetrachloroethane
Bromobenzene
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
o-Chlorotoluene
p-Chlorotoluene
1,2-Dibromo-3-chloropropane
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
Naphthalene
n-Propylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
trans-1,4-Dichloro-2-butene
Ethyl ether
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
REF
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
METHOD
ID
DATES
PREP ANALYSIS
8260
10.
1.0
10.
10.
10.
4.5
10.
10.
10.
10.
25.
10.
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
25.
SURROGATE RECOVERY
Toluene-dS
4-Bromofluorobenzene
Dibromofluoromethane
98.0
95.0
105.
%
%
%
Comments: Complete list of References and Glossary of Terms found in Addendum I
01159609:58
Page 3
09-Jan DB
ALPHA ANALYTICAL LABORATORIES
CERTIFICATE OF ANALYSIS
Laboratory Sample Number: L9600021-01
-1
*AW
RESULT
PARAMETER
UNITS
RDL
Polynuclear Aromatics by GC/MS
U
Acenaphthene
2-Chloronaphthalene
Fluoranthene
Naphthalene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Chrysene
Acenaphthylene
Anthracene
Benzo(ghi)perylene
Fluorene
Phenanthrene
Dibenzo(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Pyrene
1-Methylnaphthalene
2-Methylnaphthalene
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
ug/l
ug/l
ug/l
ug/1
ug/l
79.0
62.0
29.0
%
%
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
METHOD
ID
DATES
PREP ANALYSIS
1
8270
03-Jan 06-Jan IG
1
8100M
04-Jan 05-Jan DB
REF
2.41
2.49
2.41
1.83
2.57
3.15
2.91
2.91
2.57
2.16
2.08
4.15
2.24
2.16
4.07
3.90
2.32
5.81
1.49
SURROGATE RECOVERY
Nitrobenzene-dS
2-Fluorobiphenyl
4-Terphenyl-d14
1
Hydrocu bon.Scan ^C 800 Modified
*
Mineral Spirits
Gasoline
Fuel Oil #2/Diesel
Fuel Oil #4
Fuel Oil #6
Motor Oil
ND
ND
ND
ND
ND
ND
mg/l
mg/l
mg/l
mg/i
mg/l
mg/l
1.0
1.0
1.0
1.0
1.0
1.0
Kerosene
ND
mg/l
1.0
108.
%
SURROGATE RECOVERY
o-Terphenyl
Comments: Complete list of References and Glossary of Terms found in Addendum I
01159609:58
Page 4
ALPHA ANALYTICAL LABORATORIES
CERTIFICATE OF ANALYSIS
MA 086
CT PH-0574
NH 198958-A
NY 11148
NC 320
RI A65
Date Collected: 29-DEC-95
Date Received : 02-JAN-96
Date Reported : 15-JAN-96
Laboratory Sample Number: L9600021-02
AW-2
WATER
Sample Matrix:
Condition of Sample:
SC 88006
Field Prep:
Satisfactory
None
Number & Type of Containers: 2 Vial,2 Amber Glass
RESULT
PARAMETER
UNITS
RDL
REF
1
Volatile Organics by GC/MS
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/1
ug/l
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
5.0
1.5
1.5
1.0
3.5
1.0
1.5
10.
1.5
3.5
5.0
1,2-Dichloroethane
ND
ug/l
1.5
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Xylenes
cis-1,2-Dichloroethene
Dibromomethane
1,4-Dichlorobutane
Iodomethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1.0
1.0
1.5
1.0
1.0
1.0
1.0
1.5
1.0
10.
2.0
3.5
2.0
1.5
1.5
1.0
10.
10.
10.
10.
1.0
1.0
10.
10.
10.
METHOD
ID
DATES
PREP ANALYSIS
8260
Comments: Complete list of References and Glossary of Terms found in Addendum I
01159609:58
Page 5
10-Jan DB
ALPHA ANALYTICAL
LABORATORIES
CERTIFICATE OF ANALYSIS
Laboratory Sample Number: L9600021-02
AW-2
RESULT
PARAMETER
UNITS
RDL
1
Volatile Organics by GC/MS continued
1,2,3-Trichloropropane
Styrene
Dichlorodifluoromethane
Acetone
Carbon Disulfide
2-Butanone
Vinyl Acetate
4-Methyl-2-pentanone
2-Hexanone
Ethyl methacrylate
Acrolein
Acrylonitrile
Bromochloromethane
2,2-Dichloropropane
1,2-Dibromoethane
1,3-Dichloropropane
1,1,1,2-Tetrachloroethane
Bromobenzene
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
o-Chlorotoluene
p-Chlorotoluene
1,2-Dibromo-3-chloropropane
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
Naphthalene
n-Propylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
trans-1,4-Dichloro-2-butene
Ethyl ether
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
REF
ug/l
ug/l
ug/l
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
ug/l
ug/1
ug/l
ug/l
ug/l
ug/l
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
ug/l
ug/l
ug/l
ug/l
METHOD
ID
DATES
PREP ANALYSIS
8260
10.
1.0
10.
10.
10.
4.5
10.
10.
10.
10.
25.
10.
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
25.
SURROGATE RECOVERY
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
98.0
100.
105.
1
%
1
Comments: Complete list of References and Glossary of Terms found in Addendum I
01159609:58
Page 6
10-Jan DB
ALPHA ANALYTICAL LABORATORIES
CERTIFICATE OF ANALYSIS
Laboratory Sample Number:
L9600021-02
AW-2
RESULT
PARAMETER
UNITS
RDL
Polynuclear Aromatics by GC/MS
Acenaphthene
2-Chloronaphthalene
Fluoranthene
Naphthalene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Chrysene
Acenaphthylene
Anthracene
Benzo(ghi)perylene
Fluorene
Phenanthrene
Dibenzo(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Pyrene
1-Methylnaphthalene
2-Methylnaphthalene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
METHOD
ID
DATES
PREP ANALYSIS
1
8270
03-Jan 06-Jan IG
1
8100M
REF
2.38
2.46
2.38
1.80
2.54
3.12
2.87
2.87
2.54
2.13
2.05
4.10
2.21
2.13
4.02
3.85
2.30
5.74
1.48
SURROGATE RECOVERY
Nitrobenzene-d5
2-Fluorobiphenyl
4-Terphenyl-d14
71.0
65.0
34.0
Hydrocarbon Scan';GC 8100 Modified
Mineral Spirits
Gasoline
Fuel Oil #2/Diesel
Fuel Oil #4
Fuel Oil #6
Motor Oil
Kerosene
ND
ND
ND
ND
ND
ND
ND
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
103.
%
.04-Jan 05-Jan DB
1.0
1.0
1.0
1.0
1.0
1.0
1.0
SURROGATE RECOVERY
o-Terphenyl
Comments:
01159609:58
Complete list of References and Glossary of Terms found in Addendum I
Page 7
ALPHA ANALYTICAL LABORATORIES
CERTIFICATE OF ANALYSIS
MA 086
NH 198958-A
CT PH-0574
NY 11148
NC 320
RI A65
Date Collected: 29-DEC-95
Date Received : 02-JAN-96
Date Reported : 15-JAN-96
Laboratory Sample Number: L9600021-03
AW-3
WATER
Sample Matrix:
Condition of Sample:
SC 88006
Field Prep:
Satisfactory
None
Number & Type of Containers: 2 Vial,2 Amber Glass
RESULT
PARAMETER
UNITS
RDL
1
Volatile Organics by GC/MS
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Xylenes
cis-1,2-Dichloroethene
Dibromomethane
1,4-Dichlorobutane
Iodomethane
Comments:
01159609:S8
REF
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.3
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
26.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
METHOD
ID
DATES
PREP ANALYSIS
8260
5.0
1.5
1.5
1.0
3.5
1.0
1.5
10.
1.5
3.5
5.0
1.5
1.0
1.0
1.5
1.0
1.0
1.0
1.0
1.5
1.0
10.
2.0
3.5
2.0
1.5
1.5
1.0
10.
10.
10.
10.
1.0
1.0
10.
10.
10.
Complete list of References and Glossary of Terms found in Addendum I
Page 8
10-Jan DB
ALPHA ANALYTICAL LABORATORIES
CERTIFICATE OF ANALYSIS
Laboratory Sample Number:
L9600021-03
AW-3
RESULT
PARAMETER
UNITS
RDL
REF
1
Volatile Organics by GC/MS continued
1,2,3-Trichloropropane
Styrene
Dichlorodifluoromethane
Acetone
Carbon Disulfide
2-Butanone
Vinyl Acetate
4-Methyl-2-pentanone
2-Hexanone
Ethyl methacrylate
Acrolein
Acrylonitrile
Bromochloromethane
2,2-Dichloropropane
1,2-Dibromoethane
1,3-Dichloropropane
1,1,1,2-Tetrachloroethane
Bromobenzene
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
o-Chlorotoluene
p-Chlorotoluene
1,2-Dibromo-3-chloropropane
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
Naphthalene
n-Propylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
trans-1,4-Dichloro-2-butene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/1
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
ug/l
ug/1
ug/l
ug/l
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
10.
1.0
10.
10.
10.
4.5
10.
10.
10.
10.
25.
10.
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
Ethyl ether
ND
ug/1
25.
91.0
95.0
105.
t
%
%
METHOD
ID
DATES
PREP ANALYSIS
8260
SURROGATE RECOVERY
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
Comments: Complete list of References and Glossary of Terms found in Addendum I
01159609:58
Page 9
10-Jan DB
ALPHA ANALYTICAL LABORATORIES
CERTIFICATE OF ANALYSIS
Laboratory Sample Number:
L9600021-03
AW-3
RESULT
PARAMETER
UNITS
RDL
Polynuclear Aromatics by GC/MS
Acenaphthene
2-Chloronaphthalene
Fluoranthene
Naphthalene
Benzo (a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Chrysene
Acenaphthylene
Anthracene
Benzo(ghi)perylene
Fluorene
Phenanthrene
Dibenzo(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Pyrene
l-Methylnaphthalene
2-Methylnaphthalene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
89.0
75.0
38.0
%
METHOD
ID
DATES
PREP ANALYSIS
1
8270
03-Jan 06-Jan IG
1
8100M
REF
2.58
2.67
2.58
1.96
2.76
3.38
3.12
3.12
2.76
2.31
2.23
4.45
2.40
2.31
4.36
4.18
2.49
6.23
1.60
SURROGATE RECOVERY
Nitrobenzene-d5
2-Fluorobiphenyl
4-Terphenyl-d14
%
8100 Modified
Hydrocarbbn Scan GCO
Mineral Spirits
Gasoline
Fuel Oil #2/Diesel
Fuel Oil #4
Fuel Oil #6
Motor Oil
Kerosene
ND
ND
ND
ND
ND
ND
ND
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
96.0
%
.04-Jan 05-Jan DB
1.0
1.0
1.0
1.0
1.0
1.0
1.0
SURROGATE RECOVERY
o-Terphenyl
Comments: Complete list of References and Glossary of Terms found in Addendum I
01159609:58
Page 10
ALPHA ANALYTICAL LABORATORIES
QUALITY ASSURANCE BATCH MS/MSD ANALYSIS
Laboratory Job Number: L9600021
Parameter
MS%
MSD %
RPD
Volatile Organics by GC/MS Spike Recovery MS/MSD for sample(s) 01-03
1,1-Dichloroethene
Trichloroethene
Benzene
Toluene
Chlorobenzene
104
100
102
97
108
101
97
102
95
105
3
3
0
2
3
Semi-volatile Organic by GC/MS MS/MSD for sample(s) 01-03
p-Chloro-m-cresol
2-Chlorophenol
4-Nitrophenol
Pentachlorophenol
Phenol
Acenaphthene
1,2,4-Trichlorobenzene
1,4-Dichlorobenzene
2,4-Dinitrotoluene
N-Nitrosodipropylamine
Pyrene
96
50
29
63
46
88
78
68
128
72
106
110
74
62
84
64
102
96
84
140
86
114
14
39
73
29
33
15
21
21
9
18
7
SURROGATE RECOVERY
2-Fluorophenol
Phenol-dG
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
4-Terphenyl-d14
4
41
78
72
52
96
7
55
88
82
77
104
55
29
12
13
39
8
01159609:58
Page 11
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