Marine Structures 11 (1998) 347 — 371 Experimental response of glass-reinforced plastic cylinders under axial compression A.Y. Elghazouli*, M.K. Chryssanthopoulos, A. Spagnoli Department of Civil Engineering, Imperial College of Science, Technology and Medicine, London SW7 2BU, UK Received 27 July 1998; received in revised form 16 October 1998; accepted 19 October 1998 Abstract This paper presents the results of buckling tests on laminated composite cylinders made from glass fibre reinforced plastic (GFRP). The laminates used are of type ‘DF1400’ consisting of woven glass fibre roving within a polyester resin matrix. In total, six cylinders constructed from two-ply laminates, in which the main variable is the laminate orientation, were tested under axial compression. The specimen details, experimental set-up and loading arrangements are described, and a detailed account of the test results is given. The results include thickness and imperfection mapping, and displacement, load and strain measurements. Use was made of an automated laser scanning system, which was developed for measuring the initial geometric imperfections as well as buckling deformations during various stages of loading. The results of this experimental study demonstrate the influence of laminate orientation on the buckling strength of composite cylinders, and provide detailed information necessary for analytical and design investigations. 1999 Elsevier Science Ltd. All rights reserved. Keywords: Buckling; Composites; Axial compression; Cylinders; GRP structures; Shells 1. Introduction The use of composite materials in the marine and offshore industries has been gaining ground in recent years. However, the limited availability of design criteria for composite structures has generally restricted the efficient use of many forms of composite materials. In particular, the lack of buckling strength design criteria is deemed to be a prohibitive factor in a more widespread use of monolithic laminated composite shells in marine construction. * Corresponding author. 0951—8339/98/$ — see front matter 1999 Elsevier Science Ltd. All rights reserved. PII: S 09 5 1— 8 33 9 ( 98 ) 0 00 1 7— 3 348 A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 One of the possible applications of GRP shells is in pipework. Composite pipes in cargo and ballast systems in tankers were an early application. More recently, pipeline designs in topside modules have been developed using GRP. Their design generally involves several load cases including pressure and axial stress. In this paper the focus is on axial compression and emphasis is placed on local shell buckling, hence the radius-to-thickness ratio examined is in the intermediate range. Due to the complexity of the shell buckling phenomenon, it has attracted a large research effort over many years [1,2]. Early tests were mainly conducted in order to understand the buckling phenomenon, or in order to provide straightforward estimates for the buckling strength using formulae for linear critical loads and empirical test-based ‘knock-down’ factors. More recently, within the last 20 years or so, the objectives of shell buckling tests, whether on metal or on composite specimens, have involved accurate measurement of characteristic input and response parameters prior to and during testing. These measurements are used to provide input for numerical and analytical models, which, subsequent to validation by comparison with test response parameters, may be employed in wider parametric studies. In the case of composite shells, the methodology of integrating a reasonable number of experiments with a complementary computational activity, becomes the only viable approach. The very large number of input parameters (including basic lamina properties, orientations and number of laminae as well as all the geometric and load parameters associated with isotropic homogeneous shells) prohibits a pure experimental approach. To this end, the measurement of relevant properties and response parameters during the testing programme is essential to the development of analytical procedures and design guidelines for buckling strength prediction. As a result, and due to the imperfection sensitivity of shells subjected to axial compression, accurate measurement and mapping techniques form an important part of experimental studies. Tennyson [3] has presented a concise account of early buckling tests on laminated composite cylinders, whereas Simitses et al. [4] have focused on the attempts to correlate tests with theoretical and numerical predictions. More recently, Fuchs et al. [5] have also studied experimental response for cylinders in bending. In most investigations dealing with laminated cylinders, the models are extremely thin walled and made of graphite-epoxy systems, since the intended applications lie in the aeronautics industry. Comparatively, only few glass-fibre composite shells have been tested, and results reported do not enable an analytical or numerical validation study to be undertaken. This paper presents the results of a series of buckling tests on composite cylinders made from laminates of type ‘DF1400’. The laminates are formed from E-glass fibre woven rovings and isophthalic polyester resin. The tests are part of a project carried out at Imperial College involving experimental and analytical investigations into the behaviour of laminated composite shells. An automated laser scanning system, developed for measuring the initial geometric imperfections as well as buckling deformations during various stages of loading, was used. The material properties and specimen details are presented, and a detailed account of the experimental results is given. The results include thickness and imperfection mapping, load and displacement A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 349 measurements, strain gauge readings, deformations before and after buckling as well as salient observations regarding the elastic and buckling behaviour of each model. 2. Experimental set-up The test rig shown schematically in Fig. 1 was used for all the buckling tests. As indicated in the figure, axial loading is applied through a hydraulic actuator of 1000 kN capacity operating in displacement control in order to enable testing in the post-buckling range. A load cell and a displacement transducer are attached to the actuator piston to measure the central load and deflection, respectively. The load from the actuator is transferred to the bottom end of the specimen through a pair of stiff circular platens which are separated by three load cells, each of 500 kN capacity, placed on spherical bearings. The cells are positioned along radii emanating from the centre of the model, each pair forming an angle of 120°. The same Fig. 1. Layout of test-rig. 350 A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 radial arrangement of the three load cells is also used for positioning three displacement transducers which measure the vertical deformation between the ends of the specimen. In order to create well-defined end conditions during the buckling tests, the two ends of the specimen are carefully positioned in heavy, accurately machined steel rings. The gap between the model and the rings is then filled with epoxy resin. In the test rig, the lower ring of the cylindrical specimen is clamped to the circular platen, and the top ring is connected to the top bearing through an intermediate plate. An automated noncontact laser scanning system was used for acquiring the initial imperfections as well as the progressive change in deformations of the inner wall of the specimen during loading. This measurement system has many advantages over conventional transducer-based methods. It provides faster and more reliable data acquisition, and, unlike spring-loaded contact transducers, it does not interfere with the transverse deformation. This effect may be particularly significant when dealing with composite materials of inherently low moduli. Moreover, it should be noted that the external surface of GFRP and other fibre-reinforced shells often tends to be relatively rough and somewhat irregular because of the manufacturing process involved. On the other hand, the internal surface of the composite shells is relatively smooth, owing to an initial layer of resin applied to the mandrel around which the plies are wrapped. As indicated in Fig. 1, the laser scanning system operates inside the specimen. The measurement frame is supported on the lower circular platen, and passes through a central opening in the upper platen. The system allows for full circumferential and axial travel. Vertical travel is performed through a stepper motor/gearbox/lead screw combination, whereas circumferential movement is achieved through a stepper motor/rotary table arrangement. Careful attention was given to the repeatability and accuracy of the results. Further information on the development and verification of the laser system is given elsewhere [6]. In addition to the laser scanning, all loading and data acquisition procedures were fully automated through computer-controlled techniques. 3. Specimen details The nominal dimensions of the cylindrical models are shown in Fig. 2a. All models had an internal diameter of 600 mm and an overall length of 800 mm, which comprised a central 600 mm test length and two end parts each of 100 mm length. The end parts were significantly thicker than the middle part to ensure zero radial displacements along the edges and to minimise the risk of local splitting or delamination at the boundaries. The cylindrical specimens were manufactured by a shipbuilding yard from ‘DF1400’ laminates using a specially built aluminium mandrel and traditional hand lay-up, as typically used in marine composite construction. The fibre material is E-glass woven roving and the resin is isophthalic polyester identified by the reference ‘Synolite 0288-T-1’. The nominal glass fibre volume fraction, » , is 30.8% and the D A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 351 Fig. 2. (a) Specimen geometry. (b) View of both sides of ‘DF1400’ woven mat (vertical: weft, horizontal: warp). matrix volume fraction, » , is about 50.5$0.2%. The fibres have a nominal elastic K modulus of 69 GPa, nominal density of 2.5 g/m and ultimate tensile strength of 2.4 GPa. A close up view of the roving is shown in Fig. 2b. The tex count roving in the warp direction is 1200 (2400/10 mm construction), and 2800 in the weft direction 352 A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 (4340/10 mm construction). The resin has a nominal elastic modulus of 4.0 GPa, nominal density of 1.2 g/m and tensile strength of 73 MPa (ultimate tensile strain of 2.4%). Nominal properties of the ‘DF1400’ ply (1.75 mm nominal thickness) were provided by the manufacturer based on tests carried out on 6-ply 0° laminates [7]. Additional tests were independently carried out at Politecnico di Milano [8] to the relevant ASTM standards using two-ply flat specimens (the same number of plies used in the cylindrical models) and the results are reported in Table 1. The results of the two-ply tests where in agreement with the nominal properties based on 6-ply tests, with maximum variation lower than 10%. In view of the importance of mechanical properties, and the commonly observed variation in their values, further tests were carried out to confirm the material properties of core specimens extracted from the cylindrical models as discussed later in this paper. A total of six two-ply cylinders were tested under concentric axial compression as described in Table 2. Direction 0° indicates that the ply is laid with the weft parallel to the axis of the cylinder. Other ply orientations may be identified through the axis system given in Fig. 2a. As indicated in Table 2, the main variable investigated was the ply orientation. All the cylinders had a nominal radius-to-thickness ratio of about 86. For each laminate construction 0/0, 0/90 and #45/!45, two nominally identical cylinders were tested. The cylinders were manufactured by hand lay-up using a specially prepared mandrel. Fig. 3 shows the details of the overlapping procedure used for the models, in which overlaps of 50 mm nominal width were used in a staggered pattern. For the 0/0 laminates, two diametrically opposite vertical overlaps were used. For the 0/90 Table 1 DF1400 ply properties obtained from two-ply (0°/0°) specimens Property Direction Value (0°) Elastic modulus (GPa) 1-Weft (E ) 2-Warp (E ) l G 1-Weft 2-Warp 16.4$0.1 12.7$0.2 0.20$0.01 3.1$0.1 192.4$12.1 163.2$14.5 Poisson’s Ratio Shear modulus (GPa) Tensile strength (MPa) Table 2 Laminate nominal thickness and ply orientation for test models Number of specimens Specimen reference Lamination Nominal ply thickness (mm) Total nominal thickness (mm) 2 2 2 DF01 and DF02 DF03 and DF04 DF05 and DF06 0/0 0/90 45/!45 1.753 1.753 1.753 3.506 3.506 3.506 A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 353 Fig. 3. Cross-section of cylinders indicating ply construction and relative position of overlaps. laminates, four vertical overlaps were used due to limitations in the roll width combined with the desirable symmetry around two perpendicular axes. In the case of the #45/!45 laminates four overlaps, inclined at 45° were used, for which the cross-section at the cylinder mid-height would be similar to that of the 0/90 laminate. 4. Thickness measurement Mapping of the actual thickness of all cylinders was carried out using a grid of 50 mm;50 mm covering the full circumference and the middle 500 mm of the specimen height. This grid was refined to 25 mm;25 mm at the locations of overlaps, which were nominally of 50 mm width. Measurement of cylinder thickness was carried out using a vernier micrometer mounted on a specially designed bracket. Fig. 4a shows a perspective map of the thickness measurement of model DF01 (0/0) clearly depicting the position of the overlaps. As can be seen, two overlap zones (OL1 and OL2) and two normal zones (N1 and N2) may be identified. Thickness statistics within each zone, together with an overall average value, are given in Table 3. The thickness pattern of the nominally identical model (DF02) is very similar and is therefore not shown here, but the corresponding thickness statistics are also reported in Table 3. Similarly, a typical thickness map for a 0/90 model (DF03) is given in Fig. 4b. The position of the four overlaps may be observed, identifying four normal (N1 to N4) and four overlap (OL1 to OL4) zones. For one of the two-angle-ply (45/!45) models, i.e. DF05, the thickness map is shown in Fig. 4c. As shown, four inclined overlaps were introduced but the distinction between normal and overlap zones becomes somewhat less clear, presumably due to the increased complexity in lay-up. Nevertheless, it is still 354 A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 Fig. 4. Thickness measurement of cylinders. A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 355 Table 3 Measured thickness of test models Model Zone N1 OL1 N2 OL2 N3 OL3 N4 OL4 Overall mean DF01 Mean Cov Mean Cov Mean Cov Mean Cov Mean Cov Mean Cov 3.70 0.07 3.80 0.06 3.94 0.06 4.01 0.10 3.52 0.07 3.58 0.08 4.57 0.10 4.96 0.06 4.92 0.09 4.66 0.06 4.56 0.12 4.37 0.08 3.60 0.07 3.63 0.08 3.90 0.12 4.10 0.10 3.45 0.07 3.70 0.09 4.53 0.10 4.52 0.07 4.96 0.08 4.99 0.11 4.49 0.15 4.66 0.12 — — — — 3.92 0.08 3.93 0.09 3.71 0.08 3.79 0.05 — — — — 5.02 0.15 5.14 0.07 4.51 0.13 4.34 0.11 — — — — 3.99 0.09 3.99 0.07 3.81 0.07 3.81 0.07 — — — — 5.24 0.11 5.05 0.08 4.40 0.10 4.44 0.14 3.65 DF02 DF03 DF04 DF05 DF06 3.72 3.94 4.00 3.62 3.72 Excluding overlaps. Coefficient of variation. possible to classify the model into zones and the results for both models are also summarised in Table 3. It is worth noting that the measured thickness may be up to 15% higher than the nominal values in the normal two-ply zones of some models. Since these values do not include any overlaps, the relative increase must be associated with excess resin which is introduced during the cylinder lay-up process. As evidenced from Fig. 4, the thickness measurement is particularly useful in determining the exact location of overlaps, which would be required for detailed numerical investigations. The thickness mapping may also be used to explain, in conjunction with imperfections and accidental load eccentricities, any asymmetries or irregularities in the observed buckling mode. However, the reported thickness variations should be used carefully in comparative numerical or analytical studies. As mentioned previously, the increase in thickness is mainly due to excess resin which, owing to its relatively low elastic modulus compared to that of the fibres, should be properly accounted for in modifying the overall laminate properties. 5. Initial imperfections Imperfection sensitivity has long been recognised as the main factor for discrepancies between experimental buckling loads and analytical predictions for shell structures in general, and for cylindrical shells subject to axial compression in particular [9,10]. Detailed measurement of initial geometric imperfections was carried out in this testing programme. The automated laser scanning system was first used to obtain the imperfections of the specimen after it was mounted in the test rig and before any load 356 A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 was applied. The internal surface of the specimen, which was painted in white in order to enhance the performance of the laser sensor, was measured in a radial direction at 2232 points. The measuring grid consisted of 31 axial stations (with an interval of 20 mm) and 72 circumferential stations (with an interval of 5° or 26.2 mm). In order to generate a reference surface for the measurements taken on the specimen, the internal surface of an accurately machined steel ring with a diameter of 540 mm was also scanned at 5° intervals. The scan was undertaken at three vertical locations (100, 400 and 700 mm above the bottom platen) by bolting the steel ring on a set of three solid circular columns of corresponding heights. Thus, using these reference measurements, a datum for all imperfection and deflection measurements was created. The ‘raw’ imperfection data were then processed using the so-called ‘best-fit’ cylinder concept [11]. This concept accounts for possible misalignments between the longitudinal axes of the specimen and the measuring frame. Furthermore, it facilitates comparative studies on the effect of the manufacturing process on the magnitude and spatial distribution of initial imperfections. It has been used successfully in previous imperfection measuring studies on composite shells [12]. Following the ‘best fit’ procedure, the resulting imperfections were analysed using two-dimensional harmonic analysis to produce a set of Fourier coefficients. The advantage of this widely used data processing technique is that measured imperfections can be readily fed into analytical and numerical models. Specifically, the following expression was used: K2 L2 mnx w (x, h)" m sin sin(nh# ), KL KL ¸ K L (1) where: 0)x)¸ and 0)h)2n, w (x, h) is the initial imperfection function of the cylinder at any point, m is the number of axial half-waves, n is the number of circumferential waves, and m and are the initial imperfection amplitude and KL KL phase angle associated with mode (m, n), respectively. The imperfection surface was thus described by a set of coefficients, m and , KL KL with m "15 and n "36, these upper limits being determined from the number of 2 2 readings taken axially and circumferentially. Eq. (1) represents a half-range sine expansion in the axial direction, thus, imposing zero imperfection values at the two cylinder ends. Although this is not correct, the error introduced is strictly confined to the end regions, with other parts of the Fourier expansion representing very closely the imperfection surface [6]. It is also useful to plot the distribution of Fourier imperfection coefficients as such a plot may be used to identify dominant features of the imperfection pattern produced by this manufacturing method. Typical imperfection results are given hereafter, with a full account of the measurements given elsewhere [13]. Fig. 5 shows a perspective view of the ‘best-fit’ imperfection scan for model DF01, in which positive/negative values refer to outward/inward directions, respectively. The starting point of the scan (i.e. zero circumferential angle) coincides with the starting point of the thickness measurement. A plot of the Fourier coefficients, as represented by Eq. (1), corresponding to the imperfection measurement A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 357 Fig. 5. Best-fit imperfections of Model DF01. Fig. 6. Fourier coefficients of imperfections of Model DF01. of DF01 is depicted in Fig. 6. A circumferential side view of the imperfection measurement of all models is given in Fig. 7a—f. In general, the results indicate that dominant imperfection wavelengths along both the circumferential and the axial direction are ovalisation (n"2) and barrelling (m"1), with maximum imperfection amplitudes being, on average, between 40 to 358 A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 Fig. 7. Side view of the imperfection surface of all models. 60% of the shell thickness. Ovalisation is often associated with manufacturing involving the use of a mandrel, especially when this is constructed from two semicylindrical parts joined together through bolts. However, it should be noted that A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 359 whereas lower imperfection modes exhibit high amplitudes, higher low-amplitude modes in both the axial and circumferential directions need to be adequately represented in analytical models as these could be more sympathetic to cylinder buckling modes under axial compression. 6. Buckling tests 6.1. Experimental response As mentioned before, the buckling tests were carried out under displacement control. The displacement was increased gradually using the computer-controlled hydraulic actuator. The cylinder wall deformation was captured through the laser system prior to and directly after buckling. Table 4 presents the buckling loads obtained in the tests alongside the measured strains at the point of buckling (i.e. at the peak load). The strains given are the average values obtained from at least three gauges. For the cross-ply models (i.e. DF01—DF04), three groups of gauges, each consisting of one vertical (axial) and one horizontal (circumferential) gauge, were placed at mid-height of the cylinder at equal circumferential distances. In the case of the angle-ply models (i.e. DF05 and DF06), each group consisted of a rosette with vertical, horizontal and diagonal gauges, in addition to independent vertical and horizontal gauges. The compressive axial load versus end-shortening relationships for all six cylinders are given in Figs. 8—10. As illustrated, the behaviour of nominally identical cylinders was very similar, in terms of stiffness, buckling load and post-buckling response. In the case of Models DF01 and DF02, the displacement was increased gradually up to a load of about 200 kN at which point the elastic scan was performed. Upon further loading, buckling occurred suddenly, and audibly, at a load of approximately 285 kN in both models. The load then dropped sharply to less than 100 kN. The deformed shape at this reduced load was associated with fairly localised deformations and some fibre fracture on the crests and troughs of the buckling waves. Under increased displacements in the post-buckling range, the specimens picked up a relatively small amount of load accompanied by significant deformation growth and Table 4 Peak load and corresponding strains for the cylindrical models Model Lamination Buckling load (kN) Axial strain (%) Circumf. strain (%) Diagonal strain (%) DF01 DF02 DF03 DF04 DF05 DF06 0/0 0/0 0/90 0/90 #45/!45 #45/!45 285 285 346 355 235 232 !0.24 !0.25 !0.31 !0.34 !0.44 !0.42 0.045 0.047 0.057 0.061 0.28 0.22 — — — — !0.14 !0.12 360 A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 Fig. 8. Load—displacement relationship for DF01 and DF02 (0/0). Fig. 9. Load-displacement relationship for DF03 and DF04 (0/90). substantial noise indicating matrix cracking and possibly further fibre fracture. The applied displacement was finally reduced incrementally and the specimen was unloaded. In this stage, the specimens had regained their cylindrical shape (as can be inferred from the spring-back nature of the unloading paths) but material damage was clearly evident at positions where large buckling deformations had taken place. A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 361 The pre-buckling (elastic) scans for the models are not presented herein for compactness, but can be found elsewhere [13]. The elastic deformations (difference between pre-buckling and imperfection scans) are predominantly associated with outward barelling, with a maximum amplitude of about 0.5 mm. The post-buckling laser scan for DF01 taken directly after buckling, is shown in Fig. 11a, and a view of Fig. 10. Load—displacement relationship for DF05 and DF06 (#45/!45). Fig. 11. (a) Post-buckling wall deformation scan of Model DF01 (0/0). (b) View of Model DF01 (0/0) after failure. 362 A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 Fig. 11. (Continued.) the cylinder is given in Fig. 11b. The buckling mode extended over about half the circumference, and consisted of three circumferential waves and two axial half-waves, with a maximum inward deformation of about 25 mm. The failure was concentrated in the lower half of the cylinder. Similar behaviour was observed in Model DF02. The same procedure of loading was used in 0/90 cross-ply models (i.e. DF03 and DF04), as shown in Fig. 9. Whereas the stiffness of these two models was about 10% lower than that of models DF01 and DF02, the buckling load was, on average, about 23% higher (346 kN for DF03 and 355 kN for DF04). Buckling failure was brittle with combined radial deformations and more extensive fibre fracture than in the 0/0 models. The shape and amplitude of pre-buckling deformations were similar to those observed in the cross-ply 0/0 models. The post-buckling scan of Model DF04 is depicted in Fig. 12a, and a view of the same model after failure is shown in Fig. 12b. A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 363 The maximum amplitude of the deformation was about 30 mm in an inwards direction. As shown in Fig. 10, the stiffness of the angle-ply cylinders (DF05 and DF06) was significantly lower than the other models (approximately 50% of models DF01 and DF02). The buckling loads were also lower than the other models as shown in Table 4. Pre-buckling deformations measured at a load of about 190 kN indicated more significant outward ‘‘barrelling’’ deformations of the walls compared to other models, with a maximum amplitude of about 1.0 mm. Moreover, the response of the angle-ply models was associated with pronounced cracking noises also in the pre-buckling stages. Although failure was generally similar to the previous models, it occurred less suddenly with a more gradual development of the buckling mode. The post-buckling scan for DF05 is shown in Fig. 13a, and a view of the model at failure is given in Fig. 13b. In both DF05 and DF06, radial deformations were primarily confined between overlaps, with a maximum inward deformation of about 30 mm. 6.2. Axial stiffness As indicated in the load versus end-shortening plots depicted in Figs. 8—10, the axial stiffness of the three cylinder configurations (i.e. 0/0, 0/90 and #45/!45) are significantly different. The experimental elastic stiffness of the cylinders is estimated in Table 5. In order to compare these values with simplified analytical expressions, it is necessary to determine the appropriate equivalent material elastic properties in the direction of the cylinder axes. Based on classical laminate theory and using the material properties given in Table 1, the apparent elastic modulus (E ) in the axial direction (i.e. along the cylinder V Fig. 12. (a) Post-buckling wall deformation scan of Model DF04 (0/90). (b) View of Model DF04 (0/90) after failure. 364 A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 Fig. 12. (Continued.) length) and the two Poisson’s ratios may be determined, as shown in Table 5. These values are in agreement with the results obtained directly from tests carried out on core specimens taken from the cylinders. The results for the latter are shown in Fig. 14 and it was estimated that discrepancies with corresponding values in Table 5 were within $5%. Using the apparent properties, an approximate value for the cylinder axial stiffness may be predicted from Eh V k" , V (1!v v ) VW WV (2) in which k represents the normalised in-plane membrane stiffness for a unit circumV ferential and a unit axial length of the cylinder, and h is the cylinder wall thickness. A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 365 Considering nominal geometry and apparent material properties (E , l , l ) given in V VW WV Table 5, the membrane stiffness (in kN/mm) is estimated and presented in the same table. Whereas the stiffness of the cross-ply 0/0 cylinders appears to be well predicted by the above expression, the stiffness of the 0/90 cylinders is somewhat overestimated possibly due to the membrane/flexural coupling caused by mid-plane section asymmetry. This discrepancy is more pronounced in the angle-ply cylinders where more significant coupling effects are present in addition to notable nonlinearity in the material behaviour. In general, both the experimental results and analytical predictions indicate that the highest axial stiffness is obtained from the 0/0 cylinders, with relatively lower values exhibited by the 0/90 cylinders. This is a direct consequence of the orthotropic elastic properties. Furthermore, it is clearly indicated that considerably lower axial stiffness is provided by the angle-ply cylinders. 6.3. Buckling strength As shown in Table 4 and Figs. 8—10, the experimental load corresponding to buckling of the two cross-ply 0/0 models (DF01 and DF02) was 285 kN compared to an average buckling load of about 350 kN in the 0/90 models (DF03 and DF04). On the other hand, the angle-ply models (DF05 and DF06) exhibited significantly lower buckling loads, of 234 kN on average. Preliminary analytical predictions were carried out in order to determine the upper-bound linear buckling strength of the cylinders. For this purpose, the finite element program ABAQUS [14] was used to estimate the buckling loads using linear Fig. 13. (a) Post-buckling wall deformation scan of Model DF05 (#45/!45). (b) View of Model DF05 (#45/!45) after failure. 366 A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 Fig. 13. (Continued.) eigenvalue analysis. This type of analysis does not account for nonlinearities, and in-particular the effect of initial geometric imperfections is not considered. The cylinder was modelled using 9-noded doubly curved shell elements (type S9R5), with 24 and 72 elements in the axial and circumferential directions, respectively. The material properties given in Table 1 were used in conjunction with nominal uniform wall thickness, thus thickness imperfections were not included. The parameters of the finite element model were determined following a number of benchmark and convergence studies carried out as part of the project [15]. The numerical linear buckling loads obtained for the cylinders are given in Table 6. As shown, the estimated loads are similar for the 0/0 and 0/90 cylinders, with marginally higher loads predicted for the angle-ply #45/!45 models. Further estimations may be carried out using available simple theoretical methods, but these would generally impose some limitations. For example, expressions given by Vinson A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 367 Table 5 Comparison of experimental and analytical axial stiffness Model reference DF01/02 (0/0) DF03/04 (0/90) DF05/06 (#45/!45) Apparent elastic modulus E (GPa) V Poisson’s ratio l VW Poisson’s ratio l WV Analytical membrane stiffness (kN/mm) Experimental stiffness (kN/mm) Ratio of experimental/analytical stiffness 16.4 0.20 0.16 149 148 0.99 14.3 0.18 0.18 139 134 0.96 9.3 0.47 0.47 104 81 0.78 Fig. 14. Stress—strain relationships of specimens cut from the cylinders along the vertical axis. and Sierakowski [16] result in an overestimation of the numerical buckling load by 4% for 0/0 and 0/90 cylinders, and about 14% for the angle-ply models. However, it should be noted that these expressions are based on ideal boundary conditions and special orthotropy rules which do not strictly apply to the tested cylinders, particularly the angle-ply models. The ratio between the experimental buckling strength and the linear buckling loads gives an indication of the ‘knock-down’ factors for these cylinders. Knock-down factors are important for design purposes as they are used to reduce theoretical buckling predictions of nominal shells in order to account for the influence of imperfections. In addition to the significant influence of initial geometric imperfections, other factors such as thickness variation, overlapping and slight load eccentricities would also affect these ratios. 368 A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 Table 6 Comparison of linear numerical buckling loads with experimental results Model reference DF01/02 (0/0) DF03/04 (0/90) DF05/06 (#45/!45) Numerical eigen value (Linear FE) Experimental load (kN) Ratio of experimental/numerical load 463.96 285 0.62 464.20 350 0.75 470.35 234 0.50 Average of the two nominally identical cylinders. Based on initial elastic properties of angle-ply. As shown in Table 6, the ratio of experimental-to-linear buckling strength is estimated as 0.62 for the 0/0 models and about 0.75 for the 0/90 models. The higher experimental buckling strength obtained for the 0/90 cylinders, which is not reflected in the linear eigenvalue analysis using nominal geometry, may be largely attributed to the relatively higher thickness due to excess resin as well as the additional overlaps used in these models. Nevertheless, this requires further investigation using nonlinear numerical analysis with due account of geometric and stiffness imperfections as well as adequate consideration of the influence of excess resin on laminate material properties. On the other hand, a relatively lower ratio of about 0.5 is indicated in Table 5 for the angle-ply cylinders. It should be noted however that the numerical eigenvalue result is based on the initial elastic moduli of the angle-ply laminate. As shown in Fig. 14, the stress—strain relationship of the #45/!45 specimen is essentially nonlinear. Consequently, at the point of buckling significantly reduced moduli, compared to initial values, would be effective. For example, if the elastic moduli are reduced to reflect the nonlinearity in the constitutive relationships corresponding to the level of strain at buckling, the buckling loads would reduce by more than 20% and the ‘knock-down’ ratio would exceed a value of 0.6. Appropriate consideration of this effect in numerical studies would necessitate the use of nonlinear material models. It may also be noteworthy that although, in theory, initial imperfections have a significant effect on buckling strength reduction, this may not be necessarily correlated with the modes found to exhibit a large amplitude in physical models. As indicated in Fig. 7, whereas nominally identical cylinders such as DF05 and DF06 may have different maximum imperfection amplitude, they exhibit similar experimental buckling loads. This suggests a probable significance of imperfection modes with small wavelength and low amplitude, a factor which has to be adequately represented in nonlinear numerical simulations. 7. Conclusions The buckling behaviour under axial compression of laminated woven GFRP cylinders was investigated in this paper. The main experimental aspect examined was A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 369 the influence of ply orientation on the response of the composite cylinders. It was shown that using reliable automated techniques, systematic data acquisition of the salient experimental parameters may be carried out. The experimental results presented provide data for the calibration and verification of analytical models. These are needed for assessing and quantifying the response of cylinders of various geometric and material properties, and for conducting parametric and design studies. Particular observations and conclusions of this experimental study are summarised as follows: 1. Automated laser scanning provided an accurate and reliable non-contact measurement method for initial imperfections and change in wall deformations of the composite shells prior to and after the occurrence of buckling. Integrating this system with computer-controlled loading techniques significantly enhances the precision as well as efficiency of shell buckling tests. 2. The average measured thickness of the cylindrical models was about 5—15% higher than the nominal values. This does not include the effects of overlaps, but is associated with excess resin introduced through the manual lay-up process. The thickness mapping is important in accurately identifying the locations of overlaps, as may be required for numerical modelling. 3. Imperfection scans have revealed that long imperfection wavelengths are dominant with maximum imperfection amplitudes being, on average, between 40 and 60% of the shell thickness. The laser scans provide information on manufacturing imperfections, which with the support of analytical and statistical studies, can find its way into tolerance specification. This is an important objective in shell buckling codes, and controls can be applied on the specific manufacturing conditions to improve product performance. 4. The effect of laminate orientation on the elastic axial stiffness of the cylinder was clearly observed. As expected, the highest axial stiffness was provided by the 0/0 models, with about 10% and 55% lower stiffness for the 0/90 and #45/!45 cylinders, respectively. This was in agreement with analytical predictions based on the apparent properties in the axial direction. 5. In terms of buckling strength, the highest axial resistance was exhibited by the 0/90 cylinders. As expected, the experimental buckling load was significantly lower than the linear buckling strength due to imperfection sensitivity, indicating a knockdown value of about 0.75 in the case of the 0/90 cylinders. 6. Although the numerically estimated linear buckling load, based on uniform nominal properties, indicate similar linear buckling strengths for the 0/0 and 0/90 models, the experimental loads of the 0/0 models were about 18% lower than their 0/90 counterparts. The knock-down factor for the 0/0 models was estimated as 0.62. The relatively higher strength of 0/90 laminates is largely attributed to the extra resin and additional overlaps introduced in these models. This aspect warrants closer analytical examination. 7. The buckling strength of the angle-ply laminates was considerably lower than the cross-ply models. This is in contradiction to the prediction of linear analysis which results in marginally higher buckling loads for the angle-ply cylinders as compared 370 A.Y. Elghazouli et al. / Marine Structures 11 (1998) 347—371 to the cross-ply. However, it was shown that this may be primarily due to the significant nonlinearity of the material when the angle-ply laminate is tested along the cylinder axis. This causes a significant reduction in the buckling strength compared to that obtained from predictions adopting the initial values of material properties. The results presented in this paper form part of a large project dealing with the behaviour of several types of composite cylindrical shells under various loading scenarios. Further numerical and parametric studies are underway, with a view to providing design recommendations. Acknowledgements The work presented in this paper was sponsored by the European Commission under a Brite-Euram programme (Project BE-7550: Design and Validation of Imperfection-Tolerant Shell Structures). Thanks are due to Intermarine-Spa for providing the specimens, to Prof. Poggi of Politecnico di Milano for carrying out material property tests, and to all the other partners for many productive discussions. The authors would also like to express their gratitude to Mr T Boxall and Mr R Millward of the Structures Laboratories at Imperial College for their dedication and professionalism in conducting the tests. References [1] Fung YC, Sechler EE. Thin-shell structures: theory, experiment and design, NJ: Prentice-Hall, 1974. [2] Jullien JF. Buckling of shell structures, on land, in the sea and in the air, London/New York: Elsevier Applied Science, 1991. [3] Tennyson RC. Buckling of laminated composite cylinders: a review. Composites 1975;1:17—24. [4] Simitses GJ, Shaw D, Sheinman I. 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