AN ABSTRACT OF THE DISSERTATION OF Jimmy Klick for the degree of Doctor of Philosophy in Horticulture presented on November 14, 2014. Title: Marking, Movement, and Management of Drosophila suzukii in Oregon Berry Crops Abstract approved: ______________________________________________________ Wei Q. Yang Denny J. Bruck Drosophila suzukii Matsumura (Diptera: Drosophilidae) are small invasive flies that in the past five years (2009-2014) invaded berry and stone fruit production regions in Europe and the Americas. Evolutionary adaptations, biological traits, and anthropogenic factors have contributed to its current status as a global pest. Females oviposit eggs into ripe fruit. Eggs develop into larvae that feed on fruit interiors, rendering fruit unmarketable. Growers currently prevent infestation by targeting adult D. suzukii with broad-spectrum insecticides multiple times during the harvest season. Aside from environmental and non-target impacts of this intensive management strategy, growers are faced with other challenges, such as fruit knockdown from sprayers, abiding by insecticide restricted entry and preharvest intervals, disrupting current integrated pest management (Southwood and Way 1970) programs, and increased input costs. Pest activity levels and movement were tested in a field mark-capture study with previously evaluated and inexpensive protein markers. Results confirmed high adult D. suzukii activity and movement from surrounding non-FURSKRVWVVXFKDVµ+LPDOD\D¶ blackberry into nearby susceptible raspberry. Systemic markers are another method to test pest ecology hypotheses that protein markers cannot help answer. Albeit more expensive than protein marking, markers such as the trace element, rubidium, and stable isotope, 15N, are readily absorbed by plants. In a greenhouse study, both markers were detected in adults, from larvae that fed on enriched strawberry fruits; however, 15N was highly persistent in adults after 14 days compared to the rapidly decaying rubidium. Given D. suzukii¶Vhighly mobile nature and propensity to use non-crop areas surrounding susceptible crop as overwintering sites or refugia, reduced insecticide application strategies were tested from 2011±2013. Only the border of crop areas was treated with insecticides while leaving the center untreated. Multiple border sprays during two blueberry harvest VHDVRQVZHUHPDGHWRFUHDWHDµZDOORILQVHFWLFLGHV¶ and prevent invasion of D. suzukii from surrounding non-crop areas. In addition, alternate row (middle) sprays was tested, where one side of two rows was treated with each sprayer pass. The untreated side of each row is thought to provide a refuge for natural enemies. Subsequent sprays were applied on the previously untreated rows. Multiple raspberry sites were treated with this method during three harvest seasons. These reduced insecticide application methods managed D. suzukii adults and larvae as well as complete field applications (border sprays in a low pressure situation), mitigated grower insecticide application challenges (e.g., application time, fruit knockdown in border sprays depending on grower practice), conserved post-harvest natural enemy populations, and reduced input costs. These methods could be easily integrated into a pest management program if associated risks (e.g., pest pressure) are accounted for. ©Copyright by Jimmy Klick November 14, 2014 All Rights Reserved Marking, Movement, and Management of Drosophila suzukii in Oregon Berry Crops by Jimmy Klick A DISSERTATION submitted to Oregon State University in partial fulfillment of the requirements for the degree of Doctor of Philosophy Presented November 14, 2014 Commencement June 2015 Doctor of Philosophy dissertation of Jimmy Klick presented on November 14, 2014. APPROVED: Co-Major Professor, representing Horticulture Co-Major Professor, representing Horticulture Head of the Department of Horticulture Dean of the Graduate School I understand that my dissertation will become part of the permanent collection of Oregon State University libraries. My signature below authorizes release of my dissertation to any reader upon request. Jimmy Klick, Author ACKNOWLEDGEMENTS I must start by thanking my co-advisor, Denny Bruck, whose eloquent thinking, ceaseless idioms, and serene personality inspired me to study insects. He is the creator and fearless leader of the infamous J-Team (Joe Kleiber and myself), who battled the evil menace Drosophila suzukii. The strong bond among the three of us and the entomology laboratories at the USDA-ARS-HCRU (Molly Albrecht, Adam Cave, Austin Cuenca, Hannah Curry, Evan Dishion, Kelly Donahue, Dave Edwards, Christina Fieland, Amanda Lake, Jana Lee, Jesse Mindolovich, Danielle Selleck, Scott Shane, Bev Thomas, Amelia Thornhill, Jeff Wong) created an aura of passion for research. At the inception of my PhD, Wei Yang, Jana Lee, Amy Dreves, and Vaughn Walton graciously joined the force as my committee members. I credit my co-advisor, Wei Yang, with financing much of my work and salary and with expanding my skills in presentations and extension by providing ample opportunities for me to share my research findings. I idolize Amy 'UHYHV¶SDVVLRQDQGHQWKXVLDVPLQH[WHQVLRQDQGVFLHQFHDQGWKDQNKHUIRUDOOKHU patience and time in sculpting my thoughts towards an integrated pest management (IPM) approach. Jana Lee was instrumental in instilling confidence in my statistics and writing skills. 9DXJKQ:DOWRQ¶VFRQVWDQWZRUGVRIVXSSRUWDQGDGYLFHprovided much relief and strength in my academic pursuit. I must also thank Jay Pscheidt, who facilitated my preliminary and final exams as a graduate student representative. Many thanks to Scott Machtley and James Hagler at the USDA-ARS-ALARC in Maricopa, AZ for training and protein analysis; and James for exceptional writing and review contributions towards manuscripts. I greatly appreciate 6XMD\D5DR¶VGLOLJHQWZRUNGHYHORSLQJWKH2UHJRQ State University Entomology Program, with the following members contributing their thoughts and expertise to my projects: Leonard Coop, Danny Dalton, Joe DeFrancesco, Chris Hedstrom, George Hoffman, Louisa Hooven, Gail Langellotto-Rhodaback, Peter McEvoy, Betsey Miller, Jeffrey Miller, Stephanie Parreira, Robin Rosetta, Peter Shearer, Sam Tochen, Nik Wiman, and Megan Woltz. A special thank you to Paul Jepson, whose incredible words and numerous publications shaped my perspective on IPM and whose research advice stuck with me. I will never forget feeling inspired and enlightened after our meetings. Much of my research would not have been possible without the patience, support, and humor from the raspberry growers (Jeff Kreder, Willard & Wendell Kreder, Jason Laube, Gabriel, Charley & Nathan Goodman), blueberry growers (Doug Kramer, Mac Stewart, Don Hatai), and Jacto Inc. I am grateful to berry consultant, Tom Peerbolt, and berry professor, Bernadine Strik, for inviting me to give talks to growers and for helpful discussions. I greatly benefited from the outgoing and kind people at the USDA-ARSHCRU, such as Andy Albrecht, Pauly Charron, Man-Yeon Choi, Chad Finn, Amanda Howland, Karen Keller, Ted Mackey, Walt Mahaffee, Bob Martin, Jesse Mitchell, Tara Neill, Suean Ott, Amy Peetz, Mary Peterson, Carolyn Scagel, Paul Schreiner, Lindsey Thiessen, Inga Zasada, and the late and great Pete Moppin. No acknowledgement is complete without thanking the current and former administrative staff of the Department of Horticulture and USDA-ARS-HCRU (Lee Ann Julson, Nancy Bremner, Caroline Charlton, Gina Hashagen, Ruth Hamlyn, Maryann Resendes, Stefani Morgan) for making things easy in the spur of the moment. I acknowledge the current and former Horticulture Department Heads, Bill Braunworth and Anita Azarenko, respectively, and the Graduate Student Program Coordinator, John Lambrinos, for their kindness and support. Aside from being great friends, Danielle Lightle, Laura Sims, and Hannah Tavalire are queens of the statistics world and helped me overcome obstacles in data analysis. Joe Kleiber, the heart and soul of the J-Team, provided fruitful discussions, taught me about HIILFLHQF\WUDQVODWHG'HQQ\¶VLGLRPV expanded my vocabulary, and made me enjoy life to the fullest. Other friends that deserve mention and have given me much relief and joy during the hours not devoted to rigorous research were Jan & Toni Egli, Rheadawn Gomez, Matt Johnson, Kojun Kanda, Dabao Lu, Lorena Rangel, Jessie Reimer, Tim Skalland, Emily Smith, Brandon Vig, Emily Weiss, Derek Wells, and Joy Yang. Lastly and most importantly, I thank my mom, dad, brotherlove, and his amazing wife, with pets Ruedi, Fritz, and Lola. They have fueled my thirst for a PhD with their love and delicious treats from afar. Denny, you really hit the nail on the head when you said these would be the best days of my life! CONTRIBUTION OF AUTHORS Drs. Denny Bruck, Amy Dreves, Jana Lee, and Wei Yang oversaw the planning, design, and funding of projects. Dr. James Hagler analyzed all protein marking samples (Chapters 2 and 3). Dr. Vaughn Walton and Danny Dalton assisted with spatial statistics (Chapter 3). All co-authors provided invaluable reviews to manuscripts they were associated with. TABLE OF CONTENTS Page CHAPTER 1. Introduction..............................................................................................1 History.................................................................................................................2 Biology................................................................................................................2 Identification .......................................................................................................3 Monitoring ..........................................................................................................5 Hosts ...................................................................................................................5 Movement ...........................................................................................................6 Marking ...............................................................................................................7 Management ........................................................................................................8 CHAPTER 2. Evaluating Drosophila suzukii immunomarking for mark-capture research .........................................................................................................................15 Abstract .............................................................................................................16 Introduction .......................................................................................................16 Materials and methods ......................................................................................19 Results ...............................................................................................................21 Discussion .........................................................................................................24 Acknowledgements ...........................................................................................27 CHAPTER 3. Distribution and activity of Drosophila suzukii in cultivated raspberry and surrounding vegetation ...........................................................................39 Abstract .............................................................................................................40 Introduction .......................................................................................................40 Materials and methods ......................................................................................42 Results ...............................................................................................................45 Discussion .........................................................................................................46 Acknowledgements ...........................................................................................49 CHAPTER 4. Reduced spray programs for Drosophila suzukii management in berry crops ....................................................................................................................56 TABLE OF CONTENTS (Continued) Page Abstract .............................................................................................................57 Introduction .......................................................................................................57 Materials and methods ......................................................................................59 Results ...............................................................................................................65 Discussion .........................................................................................................67 Acknowledgements ...........................................................................................71 CHAPTER 5. Marking Drosophila suzukii with rubidium or 15N................................81 Abstract .............................................................................................................82 Introduction .......................................................................................................82 Materials and methods ......................................................................................83 Results ...............................................................................................................86 Discussion .........................................................................................................86 Acknowledgements ...........................................................................................87 CHAPTER 6. Conclusion .............................................................................................91 Bibliography .................................................................................................................95 LIST OF FIGURES Figure Page 2.1 Effect of the number of days on mean (+ SE) ELISA optical density (OD) readings and % laboratory-marked Drosophila suzukii adult males (M) and females (F) treated topically with (A) egg albumin, (B) milk casein, and (C) soy trypsin proteins ......30 2.2 Effect of the number of days on mean (+ SE) ELISA optical density (OD) readings and % marked cultivated blackberry leaves treated in field in (A±C) April, (D±F) May, and (G±I) June with (A, D, G) egg albumin, (B, E, H) milk casein, and (C, F, I) soy trypsin protein...................................................................................................31 2.3 Effect of the number of days on mean (+ SE) ELISA optical density (OD) readings and % marked adult male (M) and female (F) Drosophila suzukii exposed to egg albumin protein-treated cultivated blackberry leaves for (A, D, G) 1 min, (B, E, H) 10 min, and (C, F, I) 60 min in (A±C) April, (D±F) May, and (G±I) June..................33 2.4 Effect of the number of days on mean (+ SE) ELISA optical density (OD) readings and % marked adult male (M) and female (F) Drosophila suzukii exposed to milk casein protein-treated cultivated blackberry leaves for (A, D, G) 1 min, (B, E, H) 10 min, and (C, F, I) 60 min in (A±C) April, (D±F) May, and (G±I) June..................35 2.5 Effect of the number of days on mean (+ SE) ELISA optical density (OD) readings and % marked adult male (M) and female (F) Drosophila suzukii exposed to soy trypsin protein-treated cultivated blackberry leaves for (A±G) 1 min, (B±H) 10 min, and (C±I) 60 min in (A±C) April, (D±F) May, and (G±I) June ..............................37 3.1 Monitoring traps for D. suzukii WUDSFDSWXUHVZHUHDPRGLILHGµFOHDU¶WUDS(Lee et al., 2012) made of a bottomless 946 ml clear plastic deli container (DM32R, Solo Cup Company, Lake Forest, IL) with ten 3.5-mm holes near the top, and nested over a plastic cup (D32, Solo, Urbana, IL) containing ~100 ml apple cider vinegar (ACV) (5% acidity, Fred Meyer Apple Cider Vinegar, Kroger Co., Cincinnati, OH) .......52 3.2 Mean D. suzukii (+SE) captured per plot (n=3) in Early Susceptible (ES) and Late Susceptible (LS) 2011 and 2012 in (A) HB (Himalaya blackberry) and NH (non-host) field margins and (B) crop by HB and NH .............................................................53 3.3 SADIE (Spatial Analysis with Distance IndicEs) contour maps created in Surfer® overlaid with traps (small dots) of 3 plots near HB in the south and 3 plots near NH in the north and the crop boundaries denoted in a dotted line in Early Susceptible (ES) 2011 (A), Late Susceptible (LS) 2011 (B), Early Susceptible 2012 (C), and Late Susceptible 2012 (D)...............................................................................................54 LIST OF TABLES Table Page 2.1 Mean (± SE) precipitation, air temperature, relative humidity, and leaf wetness during 2-week experiments performed in April, May, and June collected from iMetos Ag weather station within 4 km from the trial site .......................................................29 3.1 Number of protein-marked (nm), assayed (na), the percentage (%) of marked D. suzukii, and yearly marked ratio (i.e. the total marked flies between HB and NH in ILHOGPDUJLQRUFURSLQDQGLQµ+LPDOD\D¶EODFNEHUU\+%DQGQRQ-host (NH) field margins (area treated with egg marker) and in the crop near HB and NH field margins during Early Susceptible (ES) and Late Susceptible (LS) in 2011/2012 ...............................................................................................................50 3.2 SADIE (Spatial Analysis with Distance IndicEs) summary statistics of Early Susceptible (ES) and Late Susceptible (LS) in 2011/2012 .....................................51 4.1 Insecticide applications in the alternate row trials (Farms A±D) of raspberry and border spray trials (Farm E) of blueberry during pre-harvest (p) and harvest (h) seasons ....................................................................................................................73 4.2 Economic costs associated with alternate row and border spraying compared to the complete spray method on 4.05 ha .........................................................................75 4.3 Comparison of mean (±SE) D. suzukii adults and larvae in alternate row and complete spray plots throughout the harvest season and during the After Spray period (3±12 d after treatment application) in 2011, 2012, and 2013 in raspberry .........................76 4.4 Comparison of mean (±SE) natural enemies in alternate row and complete spray plots 7 d post-harvest in 2011, 2012, and 2013 in raspberry ...........................................77 4.5 Comparison of mean (±SE) common pests found in alternate row and complete spray plots 7 d post-harvest in 2011, 2012, and 2013 in raspberry ..................................78 4.6 Comparison of mean (±SE) D. suzukii adults throughout the harvest season and natural enemies and common pests 7 d post-harvest in 2012 and 2013 in border and FRPSOHWHVSUD\SORWVLQµ/LEHUW\¶EOXHEHUU\............................................................79 4.7 Comparison of mean (±SE) D. suzukii adults throughout the harvest season and natural enemies 7 d post-harvest in 2012 and 2013 collected from border (~5 m into the field) and interior (40 ± 60 m into the field) trap positions of border and complete spray plots in µ/LEHUW\¶EOXHEHUU\ ...........................................................................80 LIST OF TABLES (Continued) Table Page 5.1 Mean ȝJ5EJD. suzukii (Rb marking) and 15N atom% D. suzukii (15N marking) (± SD), ratio of marked: non-marked, and percent marked (%) in female and male D. suzukii 1, 7, and 14 d after emergence from fruits of strawberry plants enriched with Rb or 15N .................................................................................................................89 5.2 Output of statistical comparisons for Rb marker content and ratio of marked: nonmarked 1, 7, and 14 d after emergence from fruits of strawberry plants enriched with Rb ............................................................................................................................90 Dedicated to mom and dad CHAPTER 1 Introduction Jimmy Klick 2 History Drosophila suzukii Matsumura (Diptera: Drosophilidae) seem to inhabit coastal to high elevations (up to 2,000 m) of subtropic, Mediterranean, and temperate mountainous areas (Kaneshiro, 1983; Mitsui et al., 2010; Cini et al., 2012; Ometto et al., 2013; Deprá et al., 2014). The native range of D. suzukii is thought to be Pakistan, northern India, Indochina, North and South Korea, Taiwan, China, and Far East Russia (Lin et al., 1977; Sidorenko, 1992; Hauser et al., 2009; Ometto et al., 2013). Flies were first described and reported as a pest of cherries in 1916 in a µhills region at the base of mountains¶ in Japan (Kanzawa, 1935). Drosophila taxonomists recognized its presence in Hawaii in 1980 at about 1,200 m elevation (Kaneshiro, 1983). In September 2008, a specimen suspected of causing damage in healthy raspberry fruit in California was identified to Drosophila. No alarm was raised because members of this genus are typically not considered pests and infest overripe or damaged fruit. In spring 2009, larval specimens from healthy California cherry fruit were initially falsely identified, but subsequently correctly identified to D. suzukii (Hauser, 2011). Specimens collected in Spain and Italy in October 2008 were confirmed as D. suzukii (Calabria et al., 2012; Cini et al., 2012). By 2009, D. suzukii was also reported in Oregon, Washington, British Colombia, Florida, and France with first reports of economic damage (Hauser, 2011; Cini et al., 2012). The fly continued to spread across Europe, North America and most recently into South America, where it was found for the first time in the coastal subtropical areas of Southern Brazil (Deprá et al., 2014). Given the delay in recognizing this invasion, understanding its large host range, and the effect of global trade on fresh fruits, D. suzukii was able to arrive, establish, and spread across the globe at a rapid pace (Liebhold & Tobin, 2008). Biology Drosophilids, also known as vinegar or pomace flies, are typically associated with infestation of damaged or overripe fruit or known as a laboratory workhorse (Borror & 'H/RQJ0DUNRZ2¶*UDG\. D. suzukii has evolved a unique trait to fit an ecological niche and reduce competition with most other drosophilids: females have a serrated and sclerotized ovipositor used to cut through the skin of undamaged and ripe fruit for egg deposition (Lee et al., 2011a; Atallah et al., 2014). Eggs develop into larvae, 3 which molt three times (i.e., 3 instars) before turning into pupae that eclose into adults. The entire life cycle can occur relatively rapidly (8±30 d) and can result in 3±15 generations per year (Kanzawa, 1935; Coop & Dreves, 2014), dependent on humidity and temperature (Dalton et al., 2011; Tochen et al., 2014a,b). The optimal conditions for D. suzukii development are 28 °C and 79% RH (Tochen et al., 2014b). In Corvallis, Oregon three to seven generations per year were estimated based on a 20-year average of weather data (Tochen et al., 2014b; Coop & Dreves, 2014). Adults mature after 1±2 d (Kanzawa, 1935) and use visual (i.e., wing spot), chemical (i.e., pheromones), and sound (i.e., wing song) at close range for mating (Fuyama, 1978; Atallah et al., 2014). Adult females are believed to primarily overwinter in a reproductive diapause state in litter, bark, and buildings (Kanzawa, 1939; Dalton et al., 2011; Ometto et al., 2013). However, some have found adults in the protection of tree bark, lichens and nooks of branches (A. J. Dreves, unpublished). Adults and larvae can feed on yeasts and bacteria rich in carbohydrates (Shorrocks, 1972; Hamby et al., 2012). Identification It is vital to correctly identify a pest for the purpose of monitoring, which is one of the essential steps in any IPM program (Stern et al., 1959). Key identifying features of drosophilids are: 2±4 mm body length; tan body color with red eyes; two small gaps in the costal vein known as humeral and costal breaks; plumose arista; and convergent postvertical bristles. Furthermore, Drosophila can be distinguished by the following characters: dense short hairs on the eyes; well developed post-vertical bristles crossing over each other and three orbital bristles on the head; and two pairs of dorso-central bristles on the thorax (Shorrocks, 1972). D. suzukii are polymorphic. Adult males have a smaller body mass (~0.32 mg), a dark gray dot that appears 1±2 d after eclosion near the apex of each wing and centered on the first major wing vein, and two sex combs that run parallel on each foreleg. Females have a larger body mass (~0.46 mg), spotless wings, and a dark and slightly curved serrated ovipositor tucked into the posterior end of the abdomen (ovipositor typically exposed when in liquid) (Hauser et al., 2009). Both genders have unbroken bands across the abdomen, no markings on the side of the thorax, and clearly defined wing veins. Examples of Drosophila characteristics that might be 4 mistaken for D. suzukii in Oregon are: a smaller spot at the very apex of each wing, 1±2 µeyelash-like¶ sex combs that run perpendicular to male forelegs, broken bands on the abdomen, µsmoky¶ wing veins, and a weak ovipositor with finer and lighter serrations (A.J. Dreves, unpublished). Eggs are small and creamy white with two filamentous breathing tubes, visible on fruit surface after egg deposition into fruit. There are three instars: 1st instar is 1±2 mm, 2nd instar is 2±3.5 mm, and 3rd instar is 3.5±5 mm in size. Larvae are slightly curved without legs or a visible head capsule, creamy white to pale yellow with black visible mouth hooks anteriorly, and anterior and posterior spiracles (Ashburner et al., 2011). Male larvae have gonads about three times the size of females, making them relatively easy to distinguish (Hartenstein, 1993). The following examples may appear similar to D. suzukii larvae collected from Oregon blueberry and caneberry fields: seeds and floral parts, fruit pulp, thrips, aphids, aphid exoskeleton, and the larvae of fruitworm, leafrollers, sap beetle, syrphid, lacewing and other drosophilids (Dreves et al., 2014). The larvae of D. suzukii are difficult to distinguish from other drosophilids, but are generally considered to be D. suzukii if fruit collected was intact and ripe. Furthermore, larvae can be reared to adulthood to confirm identification using adult morphological features. The D. suzukii genome was recently sequenced (Ometto et al., 2013; Chiu et al., 2013), making the identification of adults and larvae using polymerase chain reaction now possible (Dhami & Kumarasinghe, 2014; Kim et al., 2014). At least two other drosophilids have similar capabilities of infesting undamaged and ripe fruit: D. subpulchrella (Atallah et al., 2014) and Zaprionus indianus (Markow et al., 2014). At this time, species overlap is not thought to occur in Oregon. D. subpulchrella is a warm temperature species that is currently found only in Japan and China, where its pest status is unknown (Takamori et al., 2006; Mitsui et al., 2010). Morphological features are very similar to D. suzukii. Males have nearly identical spots and females have a large serrated ovipositor, however, differences are evident in male sex combs and female spermatheca and can further be distinguished using DNA barcoding (Hauser, 2011; Cini et al., 2012). Z. indianus, also known as the African fig fly, is a new pest capable of developing on 70 species of fruit (Markow et al., 2014) and is morphologically 5 distinct from D. suzukii. To date, it has been reported in the Southwestern USA, Florida and Virginia (Markow et al., 2014), and appears to be spreading rapidly. Monitoring Monitoring is essential to any IPM program because it infers pest densities and facilitates decision-making (Southwood & Henderson, 2000; Pedigo, 2002; Kleiber et al., 2014). It is also useful in developing model forecasts for pests, such as the validated degree-day model for D. suzukii activity (Coop & Dreves, 2014). Initially, the most commonly used monitoring tools for D. suzukii adults are wet lure attractants of fermented products, such DVDSSOHFLGHUYLQHJDUDVXJDUEDNHU¶V\HDVWor wine, inside a clear cup trap with ten 3±4 mm holes 2 cm below the lid (Lee et al., 2012). Attractants and trap designs are still being improved with the goal of developing a dry lure and trap design for a more specific (i.e., fewer non-targets), persistent, and attractive adult monitoring tool. Larval counts in fruit can be estimated using a boil method (Van Timmeren & Isaacs, 2013), salt, or sugar solutions (Dreves et al., 2014). In the boil method berries are boiled for 1 min in water, placed on a wire strainer with 0.64 cm mesh, lightly mashed, and rinsed into a tray (Van Timmeren and Isaacs 2013). Larvae are washed through the strainer while most of the fruit pulp remains. In the salt and brown sugar methods, solutions of 350 g (1 cup) salt or 650 g (2.5 cups) brown sugar, respectively, per 3.79 liter of water at 10 brix are added to lightly mashed fruit, poured into a tray, and larvae recorded up to 15 min (Dreves et al., 2014). The sugar solution is relatively messy, but has the advantage of keeping larvae alive to confirm identification using morphological features. Hosts A variety of cultivated and non-cultivated plant species serve as D. suzukii hosts (Lee et al., 2011b; Lee et al., 2014) ripening over an extended period of time (April-October), facilitating persistence and increasing densities of D. suzukii throughout the growing season. The host range of D. suzukii includes commercial berries (e.g., strawberry, blueberry, caneberries) and stone fruits (e.g., cherry, apricots, peaches) as well as noncrop hosts (wild and ornamental) (Lee et al., 2014). D. suzukii are opportunistic and when food is scarce may be found mainly feeding and sometimes ovipositing on overripe, split, or damaged apples, persimmon, figs, and tomatoes (Hauser et al., 2009; Lee et al., 2014). 6 Early season non-crop hosts such as wild cherries, Lonicera sp. (MI), and ornamental Sarcoccoca may substantially contribute to population influxes threatening nearby susceptible commercial crops. µ+LPDOD\D¶EODFNEHUU\Rubus armeniacus, is a ubiquitous late season non-crop host in Oregon suspected of supporting fall populations and providing refugia (Lee et al., 2014; Klick et al., 2014a). Understanding non-crop host presence, contribution, and quality (i.e., preference, fruit maturity, and suitability) in a large and small spatial and temporal scale are important in assessing risk to cultivated crops and determining their ecological role relative to D. suzukii ecology (i.e., refuge, overwinter, sink-source relationship). The benefits of these non-crop areas must be determined before management strategies can be recommended as they may also harbor important resources for natural enemies, pollinators, and wildlife. Movement Agroecosystems are less diverse in insect and animal life than natural ecosystems. They are composed of monocultures of typically 1±4 crops (Metcalf & Luckmann, 1994) interconnected by natural corridors, such as hedgerows and riparian areas; and can provide resources for insect pests and natural enemies, impact insect movement, and can affect insect dispersal (Barrett, 2000). Pest dispersal occurs between and within these crop and non-crop areas. According to Southwood & Way (1970) insect populations are affected by on 1) surrounding and within-crop vegetation, 2) permanence of the crop in space and time, 3) intensity of management (e.g., disruption by pesticides), and 4) isolation from surrounding unmanaged vegetation. Most drosophilids distribute in patches influenced by moisture and light and are found at the edge of forests with peak activities at dusk and dawn (Shorrocks, 1972; Hamby et al., 2013). Vertical distribution of drosophilids was favored at 10±15 m in oaks and conifers (Shorrocks, 1972). Although there are no oviposition sites in oaks and conifers, flies seem to be attracted to microorganisms in tree sap (Shorrocks, 1972). Drosophila spp. are avid fliers known to disperse over long distances. D. suzukii were believed to migrate from unfavorable (i.e., resource poor) habitat at low elevation to more favorable (i.e., resource rich) habitat at high elevation during the summer (Mitsui et al., 2010). D. pseudoobscura dispersed from several meters in favorable habitats to several km per day in unfavorable habitats (Iliadi 7 et al., 2002). Other Drosophila have been shown to disperse 150±200 m per day (McInnis et al., 1982; Taylor et al., 1984). Marking Insect marking can be used to track movement, determine trophic interactions, and understand physiological mechanisms of insects. Movement and dispersal of insects in the field can be studied using mark-release recapture and mark-capture. In mark-releaserecapture a known number of reared or wild-caught insects are marked in the laboratory, released at a focal point, and recaptured in traps at a priori distances. In mark-capture, resident insects are self-marked through direct or residual contact with a marked target area (e.g., suspected refuge or overwintering habitat) and collected at a priori distances. Successful movement studies require (an) effective marker(s) and highly attractive traps for collecting marked individuals, as (re)capture rate is often relatively low (Hagler & Jackson, 2001). An ideal marker should not affect insect behavior and biology; withstand environmental degradation and persist in or on the insect; be nontoxic to humans and the environment; be inexpensive and easy to apply over vast areas; and be easy to detect and clearly identifiable (Southwood & Henderson, 2000; Hagler & Jackson, 2001). The most appropriate marker may be species dependent. Protein marking has been shown to be cost effective, easy to apply, and easy to detect via enzyme-linked immunosorbent assays. Protein markers do not appear to have any adverse side effects on insects (Hagler, 1997; Slosky et al., 2012). The first-generation protein markers were based on vertebrate protein such as chicken or rabbit immunoglobulin G, but are non-economical for large-scale marking studies (Hagler et al., 1992). The second-generation markers of food proteins such as chicken egg white (egg albumin protein), cow milk (milk casein protein), and soy milk (soy trypsin inhibitor protein) are low-cost markers. These have been used successfully in the field to study movement and dispersal of pests between managed and unmanaged areas of citrus (Boina et al., 2009; Krugner et al., 2012), orchards (Jones et al., 2006; Horton et al., 2009; Basoalto et al., 2010), and vineyards (Lessio et al., 2014). Fluorescent dust (Prasifka et al., 1999; Hagler et al., 2011) and dye (Schellhorn et al., 2004) markers have been used for mark-capture research but are difficult to apply over vast areas. Elemental markers 8 (e.g., trace elements, stable isotopes) (Prasifka et al., 2001; Qureshi et al., 2004) also have been used in mark-capture type research; nonetheless, high costs in both marker types and potential for negative behavioral and developmental effects in trace elements (Hagler and Jackson 2001) limit the application of these markers at large scales. However, these markers are systemic in plants and permit a unique application in markcapture research. The markers above are extrinsic markers, or markers that are added to an organism. Conversely, intrinsic markers use information that is already in or on the insect (Bayes et al., 2014). For example, isotope ratios vary in nature and can be used in ecological studies of migration, trophic interactions, and feeding preferences. Large-scale migration of monarch butterflies was determined with natural abundance of isotopic signatures (Hobson et al., 1999). Smaller scale insect movement studies using natural abundance of a unique 13C to 12C ratio between C3 and C4 plants are also possible (Gould et al., 2002). Management Insecticides are easily applied at low costs for rapid pest control; however, several environmental and ecological problems arise when insecticides are depended on exclusively in pest management (Stern et al., 1959; Carson, 1962). Sub-lethal and lethal effects of chemicals on non-target natural enemies can lead to secondary pest outbreaks (Croft, 1990) because the µgeneral equilibrium position¶ (i.e., density in the absence of change) of pest and its natural enemy is disrupted (Gray et al., 2009). Furthermore, overuse of an insecticide on a target pest may result in insecticide resistance. An IPM program uses multiple tools to manage a pest and uses insecticides only when densities reach the economic (action) threshold to prevent economic injury (Stern et al., 1959; Gray et al., 2009). The economic injury level is driven by variation in management costs, market values, pest activities, host response to injury, and efficient management tactics. Currently, no threshold and injury level exist for D. suzukii partly because of limited pest knowledge and a near zero pest tolerance. The aforementioned factors make it challenging to develop a sound IPM program that uses tools other than insecticides. Parasitoids in the Figitidae, Pteromalidae, Diapriidae, and Braconidae families have successfully developed in or on D. suzukii larvae and pupae 9 (Cini et al., 2012; Chabert et al., 2012), however, their role in limiting D. suzukii populations is largely unknown or thought to be minor. Recently, a previously undescribed braconid parasitoid from Japan apparently specializes on D. suzukii and will be further tested as a possible biological control agent (Nomano et al., 2014). Explorations in South Korea in search of native and specialist D. suzukii parasitoids are currently being undertaken (J.C. Miller et al., unpublished). Commercially available predators, entomopathogenic fungi, and nematodes did not produce satisfactory control in the laboratory (Woltz et al., 2014). Effectiveness of natural enemies in the field is currently being explored (J.M. Woltz, unpublished). Cultural control methods include sanitation, physical barriers (i.e., mesh netting), and altering the host environment (e.g., canopy or floor management, irrigation method). Other control methods currently being studied are mass trapping (Hampton et al., 2014), area-wide management, and sterile-insect technique (Cini et al., 2012). A post-harvest strategy, such as cold storage, has resulted in 70±90% early instar mortality in infested fruit when placed in cold at 0.5° C or less for a period of 96 hours or more (A.J. Dreves, unpublished). To prevent D. suzukii infestations and meet near zero tolerance infestation levels set by packing plants, growers currently apply broad-spectrum insecticides from the pyrethroid, organophosphate, carbamate, neonicotinoid, and spinosyn chemical classes 1± 10 times during a typical 4±6 wk harvest season (Beers et al., 2011; Bruck et al., 2011; Van Timmeren & Isaacs, 2013; Wise et al., 2014). Pyrethroids have been reported to have the longest residual activity ranging from 7±14 d, followed by organophosphates and carbamates at 7±10 d, and spinosyn at 3±5 d (Bruck et al., 2011). Neonicotinoids were not effective on adults in direct or residual (i.e., exposure to treated leaves) trials, but have shown efficacy against adult and immature stages in semi-field and field trials (Beers et al., 2011; Van Timmeren & Isaacs, 2013) and curatively for infested fruit (Wise et al., 2014). Organically certified biological insecticide formulations of pyrethroid and spinosyn chemical classes known as pyrethrum and spinosad, respectively, are less effective than synthetic insecticides and not as persistent (i.e., residual activity) (Cox, 2002). Pyrethrum and spinosad have zero to low (3±5 d) residual activity, respectively 10 (Bruck et al., 2011). Pyrethrum is derived from chrysanthemum flower extract (Cox, 2002) and spinosad is derived from fermentation of the actinomycete bacteria, Saccharopolyspora spp. (Dripps et al., 2011). A semi-synthetic second-generation derivative, spinetoram, is the form used in conventional pest management. Both forms have short residence times in the environment, low impact on non-target organisms (i.e., natural enemies, pollinators, vertebrates), and greater effectiveness on pests than beneficial organisms, thus providing an excellent tool for facilitating integration of chemicals with biological control programs (Dripps et al., 2011). Rotating chemical classes with different modes of action is an important strategy for reducing insecticide resistance development. The mode of action of carbamates and organophosphates is through inhibition of the acetylcholinestirase enzyme (Tomlin, 2003), however, in carbamates the enzyme is not blocked for as long as in organophosphates (Thacker, 2002). Most organophosphates (e.g., malathion) and carbamates (e.g., carbaryl) are non-systemic in plants; however, some, such as diamethoate (organophosphate) and pirimicarb (carbamate) are systemic (Thacker 2002). All pyrethroids are non-systemic and are contact or feeding poisons. They are also neurotoxic and interfere with axonal transmission of nerve impulses and movement of the sodium ions and characterized by quick pest knockdown (i.e., paralysis) (Thacker 2002). Neonicotinoids are a relatively new insecticide class (1984) of contact and systemic poisons. They bind to postsynaptic nicotinic acetylcholine receptors (Nauen & Jeschke, 2011). Spinosyns are an even newer class and have a similar mode of action as neonicotinoids, but are highly specific of certain receptor subtypes, reducing the risk of cross-resistance between chemical classes (Dripps et al., 2011). Most organophosphates, carbamates, and pyrethroids have high vertebrate, mammalian, and non-target toxicities. The neonicotinoids are less toxic to mammals, however, they are coming under increased scrutiny for their non-target impact (Van der Sluijs et al., 2014). A recently registered product in the US, from the anthranilic diamides (e.g., cyantraniliprole) chemical class, is having acceptable levels of mortality on D. suzukii (Beers et al., 2011). This class has a novel mode of action acting on ryanodine receptor modulators. The receptor is partially propped open, causing uncontrolled release of calcium ions, which can lead to muscle 11 paralysis and rapid feeding cessation (Lahm et al., 2005). Despite the potential as an additional chemical tool, several countries have not yet established maximum residue levels (MRLs) for this class, limiting export of treated fruit. Acceptable pesticide MRLs vary by country. Growers must use caution to avoid exceeding these MRLs or suffer fines and possible industry-wide consequences. These broad-spectrum insecticides applied to entire fields multiple times during the harvest season have disrupted current IPM programs adopted by growers. In Washington and Oregon cherries, for example, an organic attract-and-kill product (GF-120) containing sugar, plant proteins, and extract as bait and spinosad as toxicant, was applied at a low active ingredient per hectare rate to prevent infestations of Rhagoletis indifferens, the western cherry fruit fly, with minimal impact to non-target organisms (Beers et al., 2011). This program is now obsolete in cherries because insecticides used against D. suzukii are also effective against R. indifferens. Until the arrival of D. suzukii, blueberry and raspberry growers in the Willamette Valley of Oregon have had the fortune of relatively few pest problems. In blueberry, aphids were occasionally treated for contamination problems (D. Kramer, personal communication) because honeydew from aphids is known to reduce fruit quality (Oatman & Platner, 1972; Blackman & Eastop, 1984); or as vectors of blueberry scorch virus (T. Peerbolt, personal communication). Scales and winter moth (Operophtera brumata) are typically managed off-season (T. Peerbolt, personal communication). In raspberries, 1±3 pre-harvest µFOHDQ-XS¶sprays targeting orange tortix (Argyrotaenia franciscana) and oblique-banded leafroller (Choristoneura rosaceana) as contamination problem are typically applied (Knight & Croft, 1987). Soil drenches with insecticides are commonly used for raspberry crown borer (Pennisetia marginata) management (T. Peerbolt, personal communication). Also, late-season problems of spider mites can be common (Shanks Jr. et al., 1992). Since the arrival of D. suzukii growers have significantly increased spray applications, which may also control these pests or result in secondary pest outbreaks. Pesticide sprays are highly inefficient at reaching the target pest. Only 0.03±6% of insecticide active ingredient entering a system was estimated to reach the target organism (Hull & Beers, 1985; Metcalf & Luckmann, 1994; Pimentel, 1995; Jepson, 2009). Proper 12 insecticide delivery to the target pest is critical to reduce costs, improve efficacy, and mitigate non-target impacts. Insecticides have been delivered onto the fruiting crop plants in various ways. A common application method in tree fruits and caneberries is by airblast sprayer, which uses air to propel the insecticide solution into dense canopies. In caneberry and blueberry, a boom sprayer mounted to the rear of a tractor with a highcapacity pump is often used. Both methods use high-volume and pressure for adequate penetration and coverage (Matthews, 2000). The electrostatic sprayer uses less volume and pressure. Very fine droplets are charged as they emerge from nozzles, reducing drift and improving coverage. However, deposition is affected by various factors and use is limited by commercial development (Matthews, 2000). Aerial sprays are an expensive but quick way to cover a fruiting crop, however, large droplet size, drift, and poor canopy penetration limit the efficacy of this method. Level of insecticide residual activity varies between production regions and may be influenced by weather. For example, western Oregon likely has longer insecticide residual activity (Bruck et al., 2011) than North Carolina because of lower humidity and less rainfall in the summer (Burrack et al., 2013). Other factors possibly impacting insecticide efficacy include the method of irrigation, ultraviolet light breakdown, and inactive ingredients such as adjuvants, stickers, and spreaders (Van Timmeren & Isaacs, 2013). Overhead irrigation is suspected of reducing spray residuals and creating a more favorable habitat of higher humidity and moisture for D. suzukii (Tochen et al., 2014a), thus increasing crop risk. Even with insecticides, growers are faced with challenges, such as knocking mature fruit off of plants from machinery traveling down row alleys, managing insecticide preharvest and restricted entry intervals (PHI and REI), impacting natural enemies, risking possible secondary pest outbreaks, and increasing production costs. Reduced insecticide application strategies are tools that require fewer chemicals, conserve natural enemies, and lower management costs, while providing adequate pest control. Examples of these strategies include attract-and-kill, spatially targeted sprays, alternate row middle sprays, and border sprays (Hull & Beers, 1985; Metcalf & Luckmann, 1994). Attract-and-kill involves a semiochemical that draws the target pest towards a toxicant. Spatially targeted 13 sprays require knowledge of high-density and concentrated pest areas that are treated. Alternate row middle sprays skip an alley so that only one side of two plant rows is treated at the first application and the other sides treated at the next application. Border sprays treat only the crop plants on the border of a plot, leaving the crop plants in the center of the plot untreated. These strategies can be effective on pests that are mobile or with a predictably favorable habitat (i.e., high-density areas), mitigating the impact on the environment and natural enemies and reducing input costs such as fuel, labor, tractor wear, and amount of insecticides. The concept of alternate row and border sprays is not new. DeBach et al. (1955) and Ripper (1956) reported in the early 1950s that spraying every third row of orange trees and alternate 12 m strips of sugar beets, respectively, provided sufficient pest control and conserved natural enemies that moved from untreated to treated areas. The term alternate row middle first appeared in 1964 as a method to reduce application time when an apple scab period was forecast in orchards (Lewis & Hickey, 1964). By the 1970s it was widely used by Pennsylvania apple orchards to control an array of arthropod pests (Hull et al., 1983). This method was also shown to be compatible with biological control agents of pest mites (Asquith & Colburn, 1971) and scales (DeBach et al., 1955; Ripper, 1956). The treatment of border areas was tested as early as 1949. Nishida and Bess (1950) reported that treating the surrounding vegetation with DDT using a mist blower successfully reduced melon fly infestation in tomato fruit from 65% in untreated to 3% in treated sites. More recently, the crop is treated with a border spray application to prevent pests from migrating into the field (Lafleur & Hill, 1987; Reardon & Spurgeon, 2003; Ferguson et al., 2003), rather than treating the surrounding vegetation, which is a biologically important area to the agroecosystem (Van Driesche & Bellows, 1996; Barrett, 2000). In summary, the minimal biological control, large monocultures, high production standards, global trade of fruits, delayed identification, expansive host range, and unique pest biology and ecology created the perfect storm for D. suzukii to establish as a global pest. Insecticides are the primary management tool used today for protecting susceptible fruit from infestation at a relatively low cost and high efficacy. However, environmental 14 and non-target concerns, insecticide resistance development, and lack of a sound IPM program are driving research towards developing sustainable management tools. 15 CHAPTER 2 Evaluating Drosophila suzukii immunomarking for mark-capture research Jimmy Klick, Jana C. Lee, James R. Hagler, Denny J. Bruck, Wei Q. Yang Entomologia Experimentalis et Applicata Wiley-Blackwell Publishing 101 George Street Edinburgh, Scotland, EH2 3ES United Kingdom 152(1): 31±41 (2014) 16 Abstract Drosophila suzukii 0DWVXPXUD'LSWHUD'URVRSKLOLGDHXWLOL]HVµ+LPDOD\D¶EODFNEHUU\ Rubus armeniacus Focke (Rosaceae), as a host and may invade berry and stone fruit crops from field margins containing this invasive weed. Laboratory and semi-field studies were conducted to determine (1) the persistence of protein marks including 10% chicken egg whites (egg albumin protein), 20% bovine milk (milk casein protein), and 20% soy milk (soy trypsin inhibitor protein) on topically sprayed D. suzukii, (2) protein retention on blackberry leaves, and (3) D. suzukii acquisition of protein after exposure to marked blackberry leaves for up to 14 d after application. All flies and leaves were assayed for the presence of the protein marks using protein-specific enzyme-linked immunosorbent assays. Egg albumin, milk casein, and soy trypsin proteins persisted on 94, 49, and 25% of the topically marked D. suzukii, respectively, throughout the 14-day study period. Egg albumin was retained on 100% of treated leaves for 14 d, regardless of environmental conditions. At least 50% of flies exposed residually to egg albumin-treated leaves were marked for 3 d, regardless of exposure time and environmental conditions. However, increasing fly exposure time to treated leaves in April and June appeared to improve protein mark acquisition. Acquisition of protein by flies from treated leaves for milk casein was inconsistent, and poor for soy trypsin, despite detectable levels on treated leaves. Egg albumin had the longest and most consistent persistence on flies, leaves, and flies exposed to leaves in laboratory and semi-field studies, under a variety of environmental conditions and exposure times. Keywords: Spotted wing drosophila, Rubus armeniacus, ELISA, insect dispersal, protein marking, Diptera, Drosophilidae Introduction Spotted wing drosophila, Drosophila suzukii Matsumura (Diptera: Drosophilidae), is an invasive pest that is capable of causing major economic loss in berry and stone fruit crops. Drosophila suzukii is native to Southeast Asia and was first discovered in mainland USA, in California, in 2008 (Hauser et al., 2009; Walsh et al., 2011). Drosophila suzukii is now widely established across North America and Europe (Hauser, 2011; Calabria et al., 2012). In 2009, reports of yield losses in all susceptible crops 17 ranged from negligible to 80% in Pacific coast states (Bolda et al., 2010). Adult flies oviposit in ripening fruit (Lee et al., 2011b). Fly larvae feed on the fruit interior, making the fruit unmarketable. Growers heavily rely on protective insecticide applications to manage this pest. A number of insecticides currently labeled for use in susceptible crops are efficacious against D. suzukii (Beers et al., 2011; Bruck et al., 2011); however, their increased use threatens existing integrated pest management programs and has high potential for insecticide resistance. Increased pesticide use also elevates the cost of production, but these expenditures are small in comparison to yield losses in the absence of management (Goodhue et al., 2011). A variety of cultivated and non-cultivated plant species serve as hosts ripening over an extended period of time (April ± October) and may facilitate persistence and increased densities of D. suzukii throughout the Pacific states (Lee et al., 2011b, 2014). The most abundant invasive and noxious weed commonly found along field margins and riparian areas of commercial fruits throughout the Pacific Northwest of the USA is µ+LPDOD\D¶EODFNEHUU\+%Rubus armeniacus Focke (Rosaceae) (Ringold et al., 2008). The effects of HB on D. suzukii population dynamics, presence, and movement between field margins and cultivated crops are unknown. Unpublished field observations from 2010 through 2013 suggest that D. suzukii populations increase in field margins containing HB and other non-cultivated hosts initially and subsequently colonize interiors of cultivated crops when fruit begins to ripen. Landscape ecology and overwintering studies from 2009 to 2013 also indicate that HB and diverse riparian habitat provide ideal refuge for D. suzukii adults (A.J. Dreves, unpublished). These observations suggest that the presence of HB in field margins is a key factor in annual D. suzukii infestations in neighboring crops. An understanding of D. suzukii dispersal will aid in the timing of and need for pest treatments and may allow for implementation of alternative management VWUDWHJLHVVXFKDVFURSµERUGHU-VSUD\V¶PDVVWUDSSLQJDQGSRVVLEOHIXWXUHEDLWVSUD\VWR mitigate D. suzukii invasion, significantly reducing insecticide usage, potential negative environmental impacts, and grower expense. However, we currently lack definitive data on the timing and extent of D. suzukii dispersal from non-cultivated hosts neighboring cultivated plantings. 18 Insect mark-capture type dispersal research often requires (a) marker(s) to tag the resident insect population of interest. Ideal markers should not affect insect behavior (e.g., flight, growth, life span), withstand environmental degradation, be inexpensive and easy to apply over vast areas, and be easy to detect (Hagler & Jackson, 2001). Furthermore, the most appropriate marker may be species dependent. Therefore, studies are necessary to determine the most suitable mark for the mobile D. suzukii prior to conducting an extensive mark-capture study. Dust (Prasifka et al., 1999; Hagler et al., 2011) and dye (Schellhorn et al., 2004) markers have been used for mark-capture research, but they are difficult to apply over vast areas. Elemental markers (Prasifka et al., 2001; Qureshi et al., 2004) also have been used in mark-capture type research; however, high costs and potential for negative behavioral and developmental effects (Hagler & Jackson, 2001) likely limit the application of these markers in large-scale mark-capture studies for the small (2±3 mm) D. suzukii. Protein marks have been shown to be cost effective, easy to apply, and easy to detect via enzyme-linked immunosorbent assays (ELISA) (Jones et al., 2006). Additionally, protein marks do not appear to have any adverse side effects on insects (Hagler, 1997; Slosky et al., 2012). Proteins have been used successfully in the field to study movement and dispersal of pests between managed and unmanaged areas of citrus (Boina et al., 2009; Krugner et al., 2012) and orchards (Jones et al., 2006; Horton et al., 2009; Basoalto et al., 2010). Currently, the efficacy of marking D. suzukii with proteins has not been determined. Also, little is known on the effect of environmental conditions (e.g., rain, temperature, humidity) on protein mark persistence. The objective of this study was to identify the most compatible protein marker, which included egg albumin in chicken egg whites, milk casein in bovine milk, and soy trypsin inhibitor (hereafter referred to as soy trypsin) in soy milk, for future use in mark-capture dispersal studies of D. suzukii. The attributes of each mark type were determined by analyzing (1) protein persistence on topically-sprayed D. suzukii, (2) retention on blackberry leaves under varying environmental conditions, and (3) residual acquisition of protein by flies exposed to marked blackberry leaves up to 14 d after contact. Suitable protein marks identified here will be used to study D. suzukii movement in 19 agroecosystems. Materials and methods Laboratory colony. Drosophila suzukii originated from adults collected from infested fruit from grower fields in the Willamette Valley of Oregon in 2009. Male and female D. suzukii adults were placed in 75-ml plastic culture vials filled with ca. 9.4 cm3 Drosophila cornmeal diet (San Diego Drosophila Stock Center, San Diego, CA, USA) ZLWKDOLJKWVSULQNOLQJRI)OHLVFKPDQQ¶VDFWLYHGU\\HDVW$&+)RRG&RPSDQLHV Memphis, TN, USA) and capped with foam plugs. Cultures were maintained in climate chambers held at 22 ± 1 °C, 35 ± 5% RH, and L16:D8 photoperiod. Field-collected D. suzukii were introduced into the colony on multiple occasions in 2010 and 2011 to ensure that the genetic make-up was representative of the field population. Adult flies, ranging from 3±15 d old, were used in the experiments. Direct contact topical exposure. A laboratory study was conducted to evaluate the persistence of three protein marks that were topically applied to adult flies. The experiment was performed in a completely randomized block design with the date of protein application used as the blocking factor. Each protein treatment was replicated 3× on three application dates (4 May, 3 and 21 June 2011). An experimental unit of 50 D. suzukii adults of each sex was randomly chosen from the colony and immobilized with a portable CO2 dispenser (Genesee Scientific, San Diego, CA, USA) for 3±5 s, placed on a 100 × 15-mm Petri plate (VWR International, Randor, PA, USA), and treated with 2 ml of 10% chicken egg whites (vol/vol) (All Whites; Papetti Foods, Elizabeth, NJ, USA), 20% bovine milk (vol/vol) (Hy-Top 2% reduced fat milk; Federated Group, Arlington Heights, IL, USA), 20% soy milk (vol/vol) (WestSoy organic unsweetened soya milk; The Hain Celestial Group, Melville, NY, USA), or water (untreated control) using a Precision Potter Spray Tower (Burkard Scientific, Uxbridge, UK). Application treatments were randomly assigned to flies. Within an hour after treatment, treated flies were moved into respective transparent cages (22 × 22 × 27 cm) designated by treatment and replicate to avoid cross contamination, and maintained in climate chambers as previously described. The cages contained a Petri dish of the diet (as previously described) and a watering system (water container with sponge wick). To determine marker durability, 20 five randomly selected D. suzukii of each sex were removed from each cage 1, 3, 7, 10, and 14 d after treatment, killed by freezing, individually placed into 1.5-ml microcentrifuge tubes, and stored at -80 oC until they were assayed for the presence of the protein mark by ELISA, as described below. Indirect contact residual exposure. 5HVLGXDOH[SRVXUHZDVGHILQHGDVDQXQPDUNHGIO\¶V direct contact with a protein-PDUNHGOHDILHDIO\¶VDFTXLVLWLRQRIDJLYHQSURWHLQDIWHU walking over a protein-treated leaf surface. Protein mark acquisition and subsequent persistence was evaluated by exposing flies to treated blackberry leaf surfaces for 1, 10, or 60 min. Mark acquisition was performed as a semi-field experiment in a completely randomized block design with date of application (April, May, and June) as the blocking factor. Four mature cultivated blackberry plants were systematically selected from a stand of eight outdoor plants (buffer plant between each experimental treatment to avoid cross contamination) located at the USDA-ARS Horticultural Crops Research Unit (Corvallis, Oregon, USA). Plants were sprayed with fine droplets of chicken egg white, bovine milk, and soy milk, or water (control) using a hand-held spray bottle on 17 April, 4 May, and 21 June 2011 at the same concentrations as used above. Each plant was sprayed with a 500-ml solution of each treatment to ensure full coverage of all leaf surfaces at a time when no precipitation was forecasted for at least 24 h. Nine leaves were randomly selected throughout each plant canopy 1, 3, 7, 10, and 14 d after treatment, with measures to avoid contamination. Each leaf was trimmed to a 50-mm-diameter disc and placed into a 50 × 11-mm Petri dish, randomly assigned to 1, 10, or 60 min of exposure, and replicated 3×. Five D. suzukii adults of each sex were anesthetized with CO2 for 3±5 s and placed into the Petri dish containing the treated leaf. After the exposure time elapsed, flies were killed by freezing, leaf samples were taken by pressing the end of a plastic drinking straw firmly into the surface and cutting a small section (fresh straws were used between samples to avoid cross contamination), and fly and leaf samples individually placed into 1.5 ml microcentrifuge tubes and stored at -80 °C until they were assayed for the presence of protein by ELISA. ELISA analysis. Flies and leaves were analyzed using protein-specific ELISAs (Jones et al., 2006). In brief, each sample was soaked in 750 Pl Tris buffered saline (pH 7.4) at 27 21 °C for 1 h at 100 r.p.m. on an orbital shaker and then assayed for the presence of protein using the anti-chicken egg albumin, anti-milk casein, or anti-soy trypsin inhibitor ELISA. Fly and leaf samples were scored positive for the presence of the protein mark if the ELISA optical density (OD) reading was three standard deviations greater than the mean negative control result (Hagler & Jones, 2010). Weather station. Weather data were collected from iMETOS Ag weather stations (Pessl Instruments, Styria, Austria) with temperature/RH and leaf wetness sensors at a location within 4 km from the trial site (Table 2.1). Statistical analysis. Proteins on leaves and topically- and residually-treated flies were statistically analyzed using Proc GLIMMIX (SAS Ver. 9.3; SAS Institute, Cary, NC, USA), with ELISA OD as the continuous response variable and assuming Gaussian, exponential, or lognormal data distribution, where appropriate. Separate analyses were done for each protein (egg albumin, milk casein, or soy trypsin) from each study (leaf, WRSLFDORUUHVLGXDOFRQWDFW7KHSUHGLFWRUYDULDEOHVIRUµOHDI¶ZHUHGD\VDQGPRQWKVIRU µGLUHFWFRQWDFW¶H[SRVXUHWLPHVH[DQGGD\VDQGIRUµUHVLGXDOFRQWDFW¶H[SRVXUHWLPH sex, days, and month. Interaction terms were included as predictor variables, but only the highest-order interaction terms were analyzed as non-significant interactions were sequentially removed from the model. The model included month of application (April, May, and June) as a random factor in analysis of topically treated flies, but as a fixed effect in residual experiments because we were interested in the effect of month (i.e., environmental conditions). To detect ELISA OD differences across days, LSMeans comparison tests were applied. To simplify, the LSMeans only compared means from each sex when the effect of sex was significant. Due to the variation by month, separate LSMeans tests were done for each month for the leaf and residual studies. To investigate the interaction between exposure time and day, the 15 combinations of exposure time and day (i.e., 1 min and 1 day) were compared altogether by LSMeans for each month of the residual study. Results Direct contact topical exposure. The egg albumin persisted on all D. suzukii for 7 d after the application and declined only slightly (<15%) after 10 and 14 d. The ELISA OD 22 readings significantly declined over time and were higher for females than males (day effect: F4,438 = 36.59, P-value<0.0001; sex effect: F1,438 = 7.40, P-value = 0.0068; Figure 2.1A). Milk casein was detected on only 65% of the flies the day after the application and then decreased to 50% after 3 d, after which it remained relatively constant. The mean ELISA OD readings yielded by the milk casein-marked flies was almost 3× less than that of the egg albumin-marked flies (sex*day interaction: F4,438 = 4.46, P-value = 0.0015; Figure 2.1B). The persistence of soy trypsin on the flies sharply declined after the 1st day to less than 10% by day 14. ELISA OD readings for soy trypsin-marked D. suzukii were similar to the milk casein-marked individuals and gradually decreased over time. The females had significantly higher ELISA OD readings than males (day effect: F4,435 = 36.46, P-value <0.0001; sex effect: F1,435 = 5.65, P-value = 0.018). Indirect contact residual exposure. Egg albumin was detected on 100% of the field-aged cultivated blackberry leaves over the course (14 d) of the study (Figure 2.2A,D,G) despite exposure to a variety of environmental conditions (e.g., precipitation, temperature, relative humidity, and leaf wetness) during the three trial periods (Table 2.1: April, May, and June). Mean ELISA OD readings for leaves treated with chicken egg white in April, May, and June were high and showed very little variation over time (day effect, April: F4,30 = 8.41, P-value <0.0001; May: F4,30 = 1.64, P-value = 0.19; June: F4,24 = 1.48, Pvalue = 0.24; Figure 2.2A,D,G). Milk casein ZDVGHWHFWHGRQRIDOOOHDYHVRYHUWKH 2-wk study in April and May. However, in June the protein was not retained well on leaf surfaces. The percentage of leaves marked with bovine milk fluctuated for 10 d between 80 and 100% and then sharply declined to 30% by day 14. The milk casein ELISA OD readings were consistently lower than egg albumin and gradually declined over time (day effect, April: F4,30 = 2.92, P-value = 0.038; May: F4,30 = 3.25, P-value = 0.025; June: F4,30 = 5.11, P-value = 0.0029; Figure 2.2B,E,H). Milk casein retention on leaves was lowest in June. The leaves treated with soy milk yielded similar ELISA OD values as the milk casein mark; that is, they were lower than egg albumin and lowest in June. In addition, ELISA OD readings for soy milk-treated leaves decreased over time (day effect, April: F4,30 = 14.34, P-value<0.0001; May: F4,30 = 6.27, P-value = 0.0009; June: F4,30 = 7.65, Pvalue = 0.0002; Figure 2.2C,F,I). The total percentage of leaf samples containing soy 23 trypsin was 100% in April; however, the retention of the mark on the leaves decreased to 60% after 2 wk in May and June. Exposure time*day interaction was significant for those flies exposed to the egg albumin treated leaves in all three trial periods (April: F8,420 = 4.64, P-value<0.0001, Figure 2.3A±C; May: F8,420 = 15.14, P-value<0.0001, Figure 2.3D±F; June: F8,420 = 2.95, P-value = 0.0032, Figure 2.3G±I). In June, female flies yielded significantly higher readings than males (F1,420 = 5.60, P-value = 0.018; Figure 2.3G,H,I). Overall, at least 50% of the flies acquired and retained the egg albumin mark for 3 d after a 1, 10, or 60 min exposure period to the treated leaves (Figure 2.3). In April, the percentage of marked flies subjected to the 1 and 10 min exposure treatments sharply declined to less than 40% after 3 d (Figure 2.3A,B). However, 60% of the female flies subjected to the 60-min treatment acquired and retained the egg albumin for up to 10 d (Figure 2.3C). In May, RIWKHIOLHVwas marked over the duratLRQRIWKHVWXG\DQGIRUXSWRd after residual exposure to the leaves (Figure 2.3D±),Q-XQHRIWKHIOLHVZHUH marked 7 d after exposure (Figure 2.3G±I). Increasing exposure time from 1 to 10 or 60 min resulted in more marked flies 10 and 14 d after contact exposure of the flies to the protein treated leaves. 7KHUHZHUHQRVLJQLILFDQWGLIIHUHQFHVLQWKHIO\¶VDFTXLVLWLRQIURPPLONFDVHLQ-treated leaves with regard to exposure time and day in the April and May experiments. However, in June, there was a significant exposure time*day interaction (F8,420 = 11.58, Pvalue<0.0001; Figure 2.4G±I) with males having significantly higher ELISA OD readings than females (F1,420 = 11.74, P-value = 0.0007). In April and May, less than 50% of the flies were marked throughout the 2-wk study. In June, no flies were marked on day 1, regardless of exposure time (Figure 2.4G±I). Surprisingly, as the milk casein residue RQWKHOHDIDJHGWKHSHUFHQWDJHRIPDUNHGIOLHVLQFUHDVHGWRDIWHUd. High concentrations on the milk casein-treated leaves (e.g., high ELISA OD values) resulted in low ELISA OD readings and percentages of marked flies exposed to those leaves. Conversely, low ELISA OD readings on milk casein-treated leaves resulted in higher readings and percentages of marked flies. This discrepancy is discussed below. No differences were found in flies exposed to soy trypsin-treated leaves. However, in 24 May and June, there were significant exposure time*day interactions (May: F8,417 = 3.63, P-value = 0.0004, Figure 2.5D±F; June: F8,419 = 2.47, P-value = 0.013, Figure 2.5G±I) and females had higher ELISA OD readings than males (May: F1,417 = 6.24, Pvalue = 0.013; June: F1,419 = 11.12, P-value = 0.0009). The percentage of flies marked containing soy trypsin was never greater than 20% in all trials. Discussion Throughout the 14-day laboratory trials, the vast majority (94%) of flies topically marked with egg albumin retained the mark, whereas only 49 and 25% of the milk casein and soy trypsin marked flies were positive for the mark, respectively. Female flies retained more egg albumin and soy trypsin than males. An interaction effect in milk casein did not permit analysis of sex alone. Females may have acquired more protein because of physiological (e.g., larger body size) (Hauser, 2011) or behavioral (e.g., feeding, grooming) differences. Regardless, quantifying female movement in the field is more important than male movement because females cause the direct damage to the fruit. Soy trypsin was readily detectable on the leaves, but not on flies exposed to those leaves. Specifically, the retention of soy trypsin on flies sharply declined after only 1 day. Similar findings have been reported by Jones et al. (2006). They suggested that the soy trypsin on leaves might flake off or dry, thus making the protein less available to the target insect. Despite thorough coverage of egg albumin on leaf surfaces in April, May, and June, it appears that flies did not acquire the egg albumin mark as well in the wettest (April) and driest (June) months of the study. Specifically, mark acquisition declined after 3 d in short exposure (1 and 10 min) and 7 d in longer exposure (60 min) treatments (except for a spike on day 10 in April); whereas in May, egg albumin mark acquisition only slightly declined after 10 d, regardless of the exposure time treatment. ELISA OD readings yielded by the flies exposed to egg albumin marked leaf tissue were similar for each exposure time treatment. Further research is needed to determine whether continuous light rain that occurred in May improved the acquisition of egg albumin from the plant tissue to the flies and to determine the effect of other weather conditions (i.e., heavy rain, dry periods) on fly marking. 25 Overall, the leaves treated with milk casein in June yielded poor ELISA results, but those flies exposed to the leaves yielded strong positive results (except flies exposed to day 1 leaves). This seems counterintuitive, as one might expect day 1 to have the highest percent flies marked. Instead, none of the flies were marked, suggesting that a protein PDUNLQWHUIHUHQFHZLWKWKH(/,6$LHWKHVDPSOHVPD\KDYHKDGµWRRPXFK¶PLONFDVHLQ on them) might have occurred (Hagler et al., 2011). If so, this phenomenon, known as µVWHULFLQKLELWLRQ¶&URZWKHUGRHVQRWDOORZWKHWDUJHW-specific antibody to bind to the antigen (protein), because the overcrowding of marker molecules interferes with DQWLERG\DWWDFKPHQW7KHUHIRUHLWLVSRVVLEOHWKDWDPRUHµRSWLPDO¶DPRXQWRIPLONFDVHLQ was present on the leaves in June (compared to April and May) and improved as the protein degraded over time. This increasing trend in milk casein acquisition over time has been shown in previous research (Hagler & Jones, 2010; Irvin et al., 2012). For instance, milk casein-marked Gonatocerus ashmeadi Girault increased 12% from day 1 to day 11 (Irvin et al., 2012). None of these papers specifically address this increasing trend in percent marked, perhaps this was due to the fact that it was a more subtle trend than that REVHUYHGLQRXUVWXG\)XUWKHUUHVHDUFKLVQHHGHGWRGHWHUPLQHWKHµRSWLPDO¶DPRXQWRI milk casein needed for effective acquisition. Milk casein may still be appropriate for large-scale field studies because applications will likely result in variable coverage (with VRPHµRSWLPDO¶SURWHLQDPRXQWRQOHDYHVIRUVXFcessful acquisition by flies (J.R. Hagler, unpublished). Many factors potentially influence the retention of proteins in field settings. For instance, abiotic factors such as rain, temperature, relative humidity, and dew point might influence protein retention on surfaces and protein acquisition by insects in the field. Jones et al. (2006) simulated rain events by washing treated leaf surfaces for various amounts of time. They found that milk casein had a greater rain-fastness than egg albumin or soy trypsin. However, a 1.5-mm rainfall event 12 d after application, in that same study, caused an increased immunoresponse to egg albumin and a decreased response to milk casein and soy trypsin to protein-treated leaf samples. Boina et al. (2009) showed that simulated rainfall to field-marked leaves decreased egg albumin, milk casein, and soy trypsin detection. Similarly, all proteins on field-aged leaves decreased in 26 activity due to three rainfall events. Contrary to these previous studies, our data suggest that a 2-wk mean of 4 (0±21.5) and 2 (0±8.2) mm rainfall per day in April and May, respectively, did not reduce protein detection on leaves. Furthermore, milk casein detection on leaves was poorest during the driest month, June (mean rainfall of 0.2 mm per day, ranging from 0 to 2 mm). The effect of temperature on proteins has also been investigated. Boina et al. (2009) showed that there was no significant difference in protein acquisition to insects exposed to treated leaves (residual acquisition) when held in 25 or 35 °C growth chambers. They concluded that temperature did not have an effect on protein retention. Our study shows that perhaps a combination of factors (e.g., rainfall, temperature) may influence protein detection. For example, the highest number of flies retained their mark with egg albumin after exposure to field-aged leaves during May (i.e., light steady rain and a mean temperature of 11 °C) compared to April (i.e., occasional heavy rain and cool weather) and June (i.e., dry and warm weather). Biotic factors related to insects and plants may also influence protein acquisition and retention. These factors include insect body size, body type (e.g., hairy, smooth, scaly), and behavior (e.g., feeding, grooming). Hagler & Jones (2010) showed that Hippodamia convergens GuérinMéneville and Lygus hesperus Knight obtained an egg albumin mark after only 5 min of contact exposure to protein-treated cotton leaf tissue; however, acquisition of the protein by Trichoplusia ni (Hübner) took between 20 and 240 min. Various additives incorporated into protein solutions may also influence protein detection; however, their effects remain uncertain (Jones et al., 2006; Williams et al., 2013). The water softener, EDTA, when added to protein solutions resulted in a positive effect (Jones et al., 2006) or no effect (Boina et al., 2009). These differences may have been influenced by abiotic (e.g., UV light, RH) and/or biotic (e.g., phenotypic traits of plants and insects) factors that contribute to the dissipation of protein-marked leaf surfaces and residually marked flies. For example, protein persistence on pubescent (apple leaves used in Jones et al., 2006) vs. glossy (citrus leaves used in Boina et al., 2009) leaf surfaces has not been tested. The biological solvent, dimethyl sulfoxide, when added to the protein solutions enhanced rabbit and chicken IgG protein retention for marking a beetle and its predator, but may have had a deterrent effect on beetles (Williams et al., 2013). Future studies are 27 needed to test the effect of these factors on protein mark persistence and insect behavior in the environment. We hypothesized that longer exposure time would improve protein mark acquisition by flies exposed to protein marked leaves. Increasing the exposure time of D. suzukii to treated leaf surfaces appeared to improve protein mark acquisition. We tested 1, 10, and 60-min exposure periods of insects to marked leaf tissue to mimic short, medium, and long field exposure situations. However, at present, it is unknown how much time D. suzukii VSHQGVLQILHOGPDUJLQVFRQWDLQLQJµ+LPDOD\D¶EODFNEHUU\$QRWKHUGLIIHUHQFH between these laboratory/semi-field studies and field-scale studies is the application method. Herein we used a hand-held sprayer, whereas conventional spray equipment (e.g., airblast, boom, backpack, aerial spray) has been used to apply these proteins in the field (Krugner et al., 2012; Sivakoff et al., 2012; Swezey et al., 2013). Coverage will likely depend on the method of application. In conclusion, the egg albumin protein appears to be the most effective mark for tagging D. suzukii. It was well retained on flies and leaves and is rapidly and readily acquired by flies exposed to protein-marked plant tissue. Rainfall did not appear to adversely affect egg albumin retention on the leaves; however, a steady amount of rain throughout the trial appeared to improve the acquisition of the protein by residual contact with protein-treated plants. Based on the results from this study, we have selected the egg albumin mark to tag the resident D. suzukii population for future mark-capture field studies. Acknowledgments We are grateful for the technical support of Amelia Thornhill, Scott Shane, Bev Thomas, Kelly Donahue, Adam Cave, Amanda Lake, and Scott Machtley. Thanks to Dr. Walter Mahaffee for sharing weather data. We also would like to acknowledge Bruce Mackey and Danielle Lightle for assistance with statistical analysis. We appreciate manuscript reviews by Vaughn Walton and Amy Dreves. Thanks to Vaughn Walton for travel funds to Arizona and California for laboratory procedure training and a visual design workshop, respectively. Funding was provided by Oregon State University Agricultural Research Foundation, USDA SCRI Grant 2010-51181-21167, and USDA CRIS 5358-22000-032- 28 00D. Mention of proprietary or brand names are necessary to report factually on available data; however, the USDA neither guarantees nor warrants the standard of the product, and the use of the name by USDA implies no approval to the exclusion of others that also may be suitable. This article is in the public domain and not copyrightable. It may be freely reprinted with customary crediting of source. 29 Table 2.1 Mean (± SE) precipitation, air temperature, relative humidity, and leaf wetness during 2-wk experiments performed in April, May, and June collected from iMetos Ag weather station within 4 km from the trial site. Month April May June Precipitation (mm) 4 ± 1.5 2 ± 0.7 0 ± 0.1 Temperature (°C) Mean Min 8 ± 0.3 2 ± 0.7 11 ± 0.3 6 ± 0.7 17 ± 0.4 10 ± 0.6 RH (%) Max 13 ± 0.6 16 ± 0.7 24 ± 0.8 76 ± 2.1 76 ± 1.6 71 ± 1.4 Leaf wetness (min) 212 ± 68.1 121 ± 37.8 114 ± 45.1 Leaf wetness is the mean period when top and bottom leaf surfaces were wet 30 0.3 OD F % egg F b c OD M % egg M d 0.2 e 0.1 3 0.4 Mean optical density (OD) 40 0 1 7 Days after mark applied 10 14 100 OD F % milk F 0.3 OD M % milk M 80 60 0.2 40 0.1 bc ab dc dc 1 3 a de de e de de 0 C! 20 0 0.4 Mean optical density (OD) 60 20 0 B! 80 7 Days after mark applied 10 14 100 OD F % soy F 0.3 OD M % soy M 80 60 0.2 % D. suzukii marked 100 a % D. suzukii marked 0.4 a 40 b 0.1 c d 7 Days after mark applied 10 c 20 0 % D. suzukii marked Mean optical density (OD) A! 0 1 3 14 Figure 2.1 Effect of the number of days on mean (+ SE) ELISA optical density (OD) readings and % laboratory-marked Drosophila suzukii adult males (M) and females (F) treated topically with (A) egg albumin, (B) milk casein, and (C) soy trypsin proteins. Fly samples were scored positive for the presence of the protein mark if the OD reading was three standard deviations greater than the mean negative control result. Mean ODs within a panel (and in panel B within sex) capped with different letters are significantly different (LSMeans comparisons of transformed data: P-value<0.05). LSMeans estimates of soy trypsin-treated D. suzukii (C) were 2.50, 2.69, 2.78, 2.92, 2.82 for 1, 3, 7, 10, 14 d after treatment, respectively. 31 Figure 2.2 Effect of the number of days on mean (+ SE) ELISA optical density (OD) readings and % marked cultivated blackberry leaves treated in field in (A±C) April, (D± F) May, and (G±I) June with (A, D, G) egg albumin, (B, E, H) milk casein, and (C, F, I) soy trypsin protein. Leaf samples were scored positive for the presence of the protein mark if the OD reading was three standard deviations greater than the mean negative control result. Mean ODs within a panel capped with different letters are significantly different (LSMeans comparisons of transformed data: P-value<0.05). 32 b 1 60 40 0.5 20 0 0 1 3 7 10 14 Days OD after application % egg ab a b 1 ab ab 80 60 40 0.5 20 0 0 1 G 3 7 10 14 % egg Days OD after application 1.5 1 80 a a a ab b 0.5 1.5 a b ab ab 1 80 60 40 0.5 20 0 0 1 3 7 10 14 Days after application 60 40 0 20 1 E 3 7 10 14 OD % milk Days after application %% soy marked with soy 100 1.5 1 80 a 60 a b b 0.5 b 1.5 1 80 a ab bc 0.5 60 ab c 0 40 20 1 H 3 7 10 14 % milk Days OD after application 0 0 1 F 3 7 10 14 OD % soy Days after application 100 1.5 1 80 a ab 60 ab c 0.5 bc 0 0 1 I 80 1 0.5 60 a 0 1 ab b bc 40 c 3 7 10 14 Days after application 20 40 20 3 7 10 14 OD application % soy Days after 100 100 1.5 40 20 100 100 ab OD 100 100 1.5 C % leaves marked with soy a %% milk marked with milk 1.5 80 1 60 a 0.5 40 b b bc c 0 20 0 1 3 7 10 14 Days after application % leaves marked with soy a OD Mean leaf optical density (OD) % leaves marked with milk a B Mean leaf optical density (OD) Mean leaf optical density (OD) % leaves marked with milk % leaves marked with milk 80 a Mean optical density %leaf leaves marked with(OD) egg 1.5 D JUNE MAY Mean leaf optical density (OD) Mean leaf optical density (OD) marked with egg %% egg 100 OD Mean optical density leaf optical density % leaf leaves marked with(OD) egg Mean % leaves marked with (OD) egg APRIL Mean leaf optical density (OD) A % leaves marked with soy Figure 2.2 33 Figure 2.3 Effect of the number of days on mean (+ SE) ELISA optical density (OD) readings and % marked adult male (M) and female (F) Drosophila suzukii exposed to egg albumin protein-treated cultivated blackberry leaves for (A, D, G) 1 min, (B, E, H) 10 min, and (C, F, I) 60 min in (A±C) April, (D±F) May, and (G±I) June. Fly samples were scored positive for the presence of the protein mark if the ELISA OD reading was three standard deviations greater than the mean negative control result. Mean ODs within a month (i.e., group of three panels) capped with different letters are significantly different (LSMeans comparisons of transformed data: P-value<0.05). 34 Figure 2.3 0.4 Mean OD % marked MAY Mean optical density (OD) % marked Mean OD D hi i 1 Days 3 after7application 10 14 OD F % egg F 0 0 E 0.4 600.3 bc bc 0.2 de de de 0.1 0 OD F % egg F a 0.4 d 0.2 e 0.1 fg g 10 14 0 OD F % egg F 3 7 H Days after application 0.2 0 d cd ef 0 OD M % egg M F 100 0.6 80 0.5 a ab 20 0.1 1 40 ghi Days 3 after 7 application 10 14 OD F % egg F b 40 de e e a 0 1 Days3 after 7application 10 14 80 OD F % egg F OD M % egg M 80 0.5 0.4 60 0.3 40 0.2 20 0.1 bc ef efg 0 0 1 3 7 10 Days after application 14 cd 40 de de 0 80 0.5 0.4 60 0.3 40 0.2 20 0.1 cd b 0.1 1000.6 cd 60 0.3 I 0 100 0.2 20 20 OD M % egg M 60 0.4 1000.6 0 1 hi 0 OD M % egg M 0.6 0.3 ghi 1 Days 3 after7application 10 14 400.2 1 Days3 after 7application 10 14 0.5 fgh 200.1 0 G 40 bc 0.6 100 0.5 800.4 0.5 60 0.3 200.1 OD M % egg M 0.6 0.3 60 cd % marked Mean OD 0.1 0 JUNE Mean optical density (OD) de Mean OD % marked 0.2 efg 100 80 0.4 20 0 1 Days3 after 7application 10 14 OD F % egg F OD M % egg M 100 80 ab % marked Mean OD a 0.3 OD M % egg M % D. suzukii marked 80 0.5 OD F % egg F % D. suzukii marked 800.5 0.4 60 0.3 40 0.2 60 min C OD M % egg M 1000.6 OD F % egg F 0.5 Mean OD % marked APRIL Mean optical density (OD) 0.6 10 min B OD M % egg100 M0.6 OD F % egg F cd 60 d 40 ef ef 0 20 0 1 3 7 10 Days after application 14 % D. suzukii marked 1 min A 35 Figure 2.4 Effect of the number of days on mean (+ SE) ELISA optical density (OD) readings and % marked adult male (M) and female (F) Drosophila suzukii exposed to milk casein protein-treated cultivated blackberry leaves for (A, D, G) 1 min, (B, E, H) 10 min, and (C, F, I) 60 min in (A±C) April, (D±F) May, and (G±I) June. Fly samples were scored positive for the presence of the protein mark if the ELISA OD reading was three standard deviations greater than the mean negative control result. Mean ODs within a month (i.e., group of three panels) capped with different letters are significantly different (LSMeans comparisons of transformed data: P-value<0.05). 36 Figure 2.4 20 0.1 0.6 0 0 E 14 OD M 100 % milk M0.6 0.5 0.2 0.4 60 0.3 40 0.2 0.1 20 0.1 0.3 1 3 7 10 OD F % milk F 0.6 0.5 14 H OD M % milk 100 M 0.6 80 0.5 0.4 0 0 F 3 after7application 10 14 Days OD F OD M % milk F % milk M1000.6 80 h h cd bc de 0 3 7 10 Days after application 14 3 after7application 10 14 Days OD F OD M % milk F % milk M 0.5 100 80 60 20 0.1 20 60 0.3 40 0 1 3 after7application 10 Days OD F % milk F 14 OD M % milk M 40 0.2 0 I 0 1 3 after7application 10 Days OD F % milk F 1000.6 14 OD M % milk M 80 0.5 0.4 60 0.3 40 0.2 h g a ab f 0 0 1 0 1 20 0.1 0 1 3 7 10 Days after application 14 100 80 Mean OD 0.2 0.3 40 0.2 20 0.1 20 0.4 0.4 60 0.3 0.1 1 0 0 0 40 0.2 20 0.1 0.5 80 0.4 G JUNE Mean optical density (OD) 3 after7application 10 Days OD F % milk F 40 % marked MAY Mean optical density (OD) 1 Mean OD 0 D 60 0.3 % D. suzukii marked 0.1 0.4 % D. suzukii marked 0.2 0.3 60 80 60 40 h ef f cd ef 0 20 0 1 3 7 10 Days after application 14 % D. suzukii marked 0.4 60 0.3 40 0.2 OD M % milk M 100 Mean OD % marked 0.4 OD F % milk F 80 0.5 Mean OD 0.5 80 Mean OD % marked 0.5 60 min C OD M % milk M 1000.6 OD F % milk F Mean OD % marked APRIL Mean optical density (OD) 0.6 10 min B OD M % milk 100 M0.6 OD F % milk F % marked 1 min A 37 Figure 2.5 Effect of the number of days on mean (+ SE) ELISA optical density (OD) readings and % marked adult male (M) and female (F) Drosophila suzukii exposed to soy trypsin protein-treated cultivated blackberry leaves for (A±G) 1 min, (B±H) 10 min, and (C±I) 60 min in (A±C) April, (D±F) May, and (G±I) June. Fly samples were scored positive for the presence of the protein mark if the ELISA OD reading was three standard deviations greater than the mean negative control result. Mean ODs within a month (i.e., group of three panels) capped with different letters are significantly different (LSMeans comparisons of transformed data: P-value<0.05). 38 Figure 2.5 OD M % soy M 100 0.6 0.4 0.4 60 0.3 40 0.2 20 0.1 0.3 0.2 0.1 gh 0.6 defg defg 0.5 80 0.4 60 0.3 40 0.2 Mean OD JUNE 80 0.4 0.3 0.2 abc cd cde cde bcd 0 20 0.1 60 3 7 10 Days after application 14 100 80 0.4 60 0.3 40 ab fgh de efg efg 40 0.2 20 0.1 bc def cd h defg 60 20 0 1 Days 3 after 7application 10 14 OD F OD M % soy F % soy M 80 0.5 100 80 0.4 60 0.3 40 abc cd bc cd de 0 0 1 0 1 Days 3 after 7application 10 14 OD F OD M % soy F % soy M 0.5 0 0 0 0 3 after 7application 10 14 1 Days 3 after 7application 10 14 I H 1 Days OD F OD M OD F OD M 0.6 100 % soy F % soy M0.6 % soy F % soy100 M 0.5 0.1 20 0.1 20 20 0.1 Mean OD % marked 0 fg 40 0.2 Mean OD % marked Mean OD a 0.1 G 40 0.4 60 0.3 40 0.2 0.3 60 0.3 0.5 80 0.4 100 80 0.4 0 0 0 0 1 Days 3 after 7application 10 14 3 after 7application 10 14 F E 1 Days OD F OD M OD F OD M % soy F % soy100 M % soy F % soy M0.6 0.6 100 0.5 0.2 60 % marked MAY Mean optical density (OD) 0.6 OD M % soy M 80 0.5 % marked 0 D OD F % soy F OD M % soy M0.6 100 Mean OD % marked 0.5 80 OD F % soy F 60 min C % marked 0.5 Mean OD APRIL 0.6 10 min B OD F % soy F 20 0.1 0 1 3 7 10 Days after application 14 40 0.2 a cde ab e e 20 0 0 1 3 7 10 Days after application 14 % D. suzukii marked 1 min A 39 CHAPTER 3 Distribution and activity of Drosophila suzukii in cultivated raspberry and surrounding vegetation Jimmy Klick, Wei Q. Yang, Vaughn M. Walton, Daniel T. Dalton, James R. Hagler, Amy J. Dreves, Jana C. Lee, Denny J. Bruck Journal of Applied Entomology John Wiley & Sons Inc. 350 Main Street Malden, MA 02148 USA Manuscript accepted and currently in revision 40 Abstract Spotted wing drosophila, Drosophila suzukii Matsumura (Diptera: Drosophilidae), UHDGLO\XWLOL]HVZLOGµ+LPDOD\D¶EODFNEHUU\+%Rubus armeniacus Focke, as a refuge, among other non-crop plants, and possibly exploits adjacent field margins before colonizing cultivated fruiting crops. Studies were conducted to determine the role of field margins containing HB and their effect on D. suzukii activity, density, and distribution in an adjacent commercial red raspberry crop. One-ha plots adjacent to field margins containing HB or non-hosts (NH) (winter wheat in 2011; tall fescue in 2012) were established and replicated three times. Each plot contained two transects with monitoring traps for D. suzukii in the field margin (0 m) and spaced approximately 10 (crop boundary), 40, 70 and 100 m into the adjacent crop (n=10 traps/plot). Field margin vegetation was treated weekly from pre-harvest until the end of harvest with a 10% chicken egg white mark solution using a cannon sprayer. Adult D. suzukii were collected from traps weekly and analyzed for the presence of the egg white mark using an egg white-specific enzyme-linked immunosorbent assay (ELISA). During both years, significantly more marked flies were collected in HB field margins and virtually no marked flies were found where adjacent vegetation contained no known alternate host. Spatial Analysis by Distance IndicEs (SADIE) and mean D. suzukii trap captures additionally displayed elevated fly densities in the raspberry field near HB. These results indicate that HB may contribute to elevated D. suzukii populations and pest pressure in comparison to field margins containing no known alternate D. suzukii host vegetation. Other non-crop plants may also contribute towards a favorable field margin for D. suzukii and this work indicates the importance of surrounding vegetation when considering pest management options. Keywords: Spotted wing drosophila, Rubus armeniacus, immunomarking, insect dispersal, non-crop host, spatial statistics, Drosophilidae Introduction Drosophila suzukii Matsumura (Diptera: Drosophilidae) is a pest of small and stone fruits in all major production regions throughout North America and Europe (Walsh et al., 2011; Cini et al., 2012). Biological attributes that favored its population growth and 41 widespread establishment include: mobility (Mitsui et al., 2010), high reproductive capacity (Tochen et al., 2014b), a lack of natural enemies (Cini et al., 2012; Chabert et al., 2012), and an ability to utilize a wide range of ripe and intact fruit (Walsh et al., 2011; Burrack et al., 2013), including non-crop hosts (Atallah et al., 2014; Lee et al., 2014). The globalization of fruit markets and recent expansion of susceptible fruit production likely resulted in the rapid spread and contributed to the rise in economic importance of D. suzukii (Bolda et al., 2010; Goodhue et al., 2011; Cini et al., 2012). In 2009, up to 80% annual crop loss ($421.5 million) of cherry, blueberry, caneberry, and strawberry was estimated in the absence of control as worst-case scenario in western US production regions (Bolda et al., 2010). Host plants adjacent to cultivated commercial crops may exacerbate the economic impact of pests (Lafleur & Hill, 1987; Boina et al., 2009; Basoalto et al., 2010). Nearby µ+LPDOD\D¶EODFNEHUU\+%Rubus armeniacus Focke (formerly R. discolor and R. procerus) and seedling cherry, Prunus spp., habitats (Poyet et al., 2014), may be a possible refuge and source of D. suzukii invasion when residual toxicity of field applied insecticides decreases (Schneider, 1989; Longley et al., 1997; Bruck et al., 2011). Movement of D. suzukii from field margins to commercial crops is, however, largely unknown. Major cultivated D. suzukii host crops tested in a laboratory include, in order of host potential rating: raspberry, strawberry, blackberry, cherry, peach, blueberry, and grape (Bellamy et al., 2013). Wild hosts in the same genera include R. armeniacus, HB (Caplan & Yeakley, 2006; Fierke & Kauffman, 2006), Prunus avium Linnaeus (sweet cherry) and P. cerasus Linnaeus (sour cherry) (Thilenius 1968; Poyet et al., 2014), all of which can be found in unmanaged field margins of the Pacific Northwest and could serve as refuge and overwintering site. Drosophila species are highly mobile and opportunistic in order to optimize seasonal survival (Taylor et al., 1984; Coyne & Milstead, 1987; Bell, 1990; Iliadi et al., 2002). Provided unfavorable conditions, D. pseudoobscura (Frolova and Astaurov) can disperse from a few meters to several kilometers per day to exploit more favorable conditions (Iliadi et al., 2002). Drosophila suzukii is known to have high dispersal capabilities, which may have contributed to its rapid spread to virtually all suitable production regions 42 in North America and Europe within a relatively short period (Hauser, 2011). When resources decline or population densities exceed optimal levels, D. suzukii are believed to migrate to more favorable habitats (Mitsui et al., 2010). Given these potential dispersal capabilities and the close proximity of wild hosts preferentially utilized by D. suzukii to commercially cultivated hosts suggest that the impact of adjacent crop surroundings on D. suzukii crop invasion needs to be determined (Becher et al., 2010). A better understanding of seasonal activity and distribution of D. suzukii between non-crop areas and proximate crops will aid to formulate future integrated pest management strategies (Lee et al., 2011a; Cini et al., 2012). Various protein mark-capture methods have been used to study insect movement (Jones et al., 2006; Boina et al., 2009; Horton et al., 2009; Basoalto et al., 2010; Krugner et al., 2012; Swezey et al., 2013, 2014; Lessio et al., 2014). In mark-capture studies, as opposed to mark-release-recapture studies, resident populations self-mark. This technique provides several advantages for D. suzukii within a crop. Protein mark-capture techniques are inexpensive, easily applied, environmentally benign, persistent, and clearly identifiable (Jones et al., 2006; Hagler & Jones, 2010; Hagler et al., 2011; Sivakoff et al., 2012; Klick et al., 2014b). The overall goal of this work was to conduct mark-capture studies to determine the activity levels of D. suzukii within non-crop host field margins and cultivated raspberry crop fields. Our specific objectives were to determine: 1) if D. suzukii utilize HBcontaining field margins as a refuge, 2) if crops adjacent to HB-containing field margins have higher population densities compared to crops near non-host (NH) field margins, 3) the role of the field margins on D. suzukii activity in comparison with cultivated raspberries, and 4) the distribution pattern of D. suzukii in cultivated raspberries adjacent to field margins containing HB in comparison to NH field margins. Materials and methods Study site and design. A 33.4-ha cultivated red raspberry (R. idaeus Linnaeus) study site with field margins containing either HB or NH was located near Jefferson, Oregon ¶´1¶´:7KH1+DUHDLQZDVSODQWHGZLWKDVRIW-white winter wheat (Triticum aestivum /LQQDHXVµ0DGVHQ¶PRQRFXOWXUHDQGWKHVDPH1+DUHDLQ 2012 was planted with tall fescue (Lolium arundinaceum Darbyshire ex. Schreb.) for turf 43 seed production. The commercial raspberry crop was grown using conventional management practices. One-ha plots were systematically selected near the two field margin classifications and replicated three times. Each plot contained two transects with D. suzukii traps in the field margin (0 m) and spaced approximately 10 (crop boundary), 40, 70 and 100 m into the adjacent crop (n=10 traps/plot). The plots with HB in the field margin were spaced 70±180 m from each other. The plots with NH in the field margin were spaced approximately 50 m from each other. The two plot types (HB vs. NH in field margin) were spaced 350±500 m from each other. Monitoring traps for D. suzukii were a modified clear 10-hole trap (Lee et al., 2012) made of a bottomless 946-ml clear plastic deli container (DM32R, Solo Cup Company, Lake Forest, IL) with ten 3.5-mm holes near the top, and nested over a plastic cup (D32, Solo, Urbana, IL) containing ~150 ml apple cider vinegar (ACV) (5% acidity, Fred Meyer Apple Cider Vinegar, Kroger Co., Cincinnati, OH) (Figure 3.1). A 6.5 × 9 cm double-sided yellow sticky card (ASTO103, Alpha Scents Inc., West Linn, Oregon) was placed on top of the mesh that was positioned between the two cups. This trapping method attracted flies into the cup with bait and onto yellow sticky cards, while preventing flies from drowning and potentially washing off the protein mark. The trap in Figure 3.1, mounted on a trestle pole and shielded from machine harvesters by two pieces of plywood, is located at the edge of the red raspberry field approximately 10 m from the field margin containing HB (seen in the background). Insect marking. The field margins were treated weekly with 10% liquid chicken egg white (All Whites; Papetti Foods, Elizabeth, NJ) (Klick et al., 2014b) using a cannon sprayer (AJ-401, Jacto Inc., Pompea, Brazil) at 282 L ha-1 from pre-harvest (27 June 2011 and 14 June 2012) through harvest (12 August 2011 and 15 August 2012). The cannon sprayer treated a field margin width of approximately 15 m. The monitoring traps were removed from the field margins prior to protein application and returned to their designated locations within 0.5 h after application in order to limit contamination. On each insect collection date, sticky cards containing adult D. suzukii were removed from the traps, covered with wax paper, and placed in a cooler. Traps were refreshed weekly at each location by adding ACV and a clean sticky card. Collected sticky cards were returned to the laboratory and frozen at -80 °C. Sticky cards were removed from the 44 freezer and each D. suzukii adult was carefully removed with a disposable toothpick and individually placed into a 1.5-ml microcentrifuge tube along with the tip of the toothpick to prevent cross-contamination. Trap location and number of D. suzukii captured per trap were recorded. All fly samples were returned to -80 °C freezer until adults were removed and analyzed for the presence of egg albumin by enzyme-linked immunosorbent assay (ELISA). Egg albumin ELISA. Fly samples were thawed and 1.0 ml of tris buffered saline (pH 7.4) was added to each sample. The samples were placed on an orbital shaker at 100 rpm for ca. 1 h. After an hour, a 100 µl aliquot from each sample was added to an individual well of a 96-well ELISA plate. All samples were then assayed by the egg albumin ELISA described in detail by Hagler & Jones (2010). Drosophila suzukii samples were scored positive for the presence of the mark using the positive ELISA reaction threshold criteria defined by Sivakoff et al. (2011). Data analysis. Data collected from the field margins and crop areas were divided into two distinct time periods to address the changes in fly abundance and host plant SKHQRORJ\µ(DUO\6XVFHSWLEOH¶DQGµ/DWH6XVFHSWLEOH¶6HDVRQDOSKHQRORJ\RIWKHFURS and D. suzukii counts were considered when determining the two selected time periods. 7KHµ(DUO\6XVFHSWLEOH¶SHULRGZDVIURPWKHDSSHDUDQFHRIWKHILUVWULSHEHUU\WRMXVW before the first substantial D. suzukii SRSXODWLRQLQFUHDVHZKLFKFRLQFLGHGZLWKWKHµILUVW generation peak egg-OD\LQJ¶DVGHILQHGDQGYDOLGDWHGE\DGHJUHH-day model for D. suzukii activity (Coop, 2014)7KHµ/DWH6XVFHSWLEOH¶SHULRGZDVGHILQHGIURPILUVW generation peak egg-OD\LQJWRWKHHQGRIKDUYHVW,QWKHµ(DUO\6XVFHSWLEOH¶SHULRG ZDV-XQHWR-XO\DQGµ/DWH6XVFHSWLEOH¶SHULRGZDV-XO\WR$XJXVW,Q WKHµ(DUO\6XVFHSWLEOH¶SHULRGZDV-XQHWR-XO\DQGµ/DWH6XVFHSWLEOH¶SHULRGZDV July to 15 August. All statistical analyses were made in R v3.0.3 (R Core Team 2013) using RStudio v0.97.306 (RStudio, 2012) with D = 0.05. All D. suzukii captured in the HB or NH field margin and adjacent crop regardless of marked/unmarked status were averaged across collecting dates and traps within each time period, log10 (x + 1)-transformed in the instance that model assumptions were not met, and statistically compared using linear 45 mixed-effects model with field margin type as fixed effect and plot as random effect (Crawley, 2013). Averages, instead of totals or repeated measures, were used to account for variability in harvest period and differences in field management between plots. 0DUNHGIOLHVDUHSUHVHQWHGDVPDUNHGWRWDODVVD\HGDQGSHUFHQWDJHPDUNHGIOLHV7KHȤ2 goodness-of-fit test was used to determine the significant level of marked ratio, i.e. the total marked flies between HB and NH in field margin or crop in 2011 and 2012. Non-parametric spatial analysis was conducted in order to describe general spatial trends. SADIE (Spatial Analysis with Distance IndicEs; Perry, 1995) was used to determine the overall index of aggregation of D. suzukii total trap captures for each time period. The index of aggregation, Ia, quantified aggregation patterns found in plots during the Early Susceptible and Late Susceptible periods of each year. The observed counts have spatially random arrangement when Ia is near to unity (i.e. between -1.5 and 1.5), aggregated arrangement when values are larger than unity, and regular arrangement when values are smaller than unity (Perry, 1996; Maestre & Cortina, 2002; De Villiers 2006). Another index, v, is a dimensionless index of clustering. This index was used to measure the degree of clustering in areas with above-average density i.e., patches (high counts near each other) or areas with below-average density i.e., gaps (low counts near each other) (Winder et al., 2001, 2012; Maestre & Cortina, 2002; De Villiers 2006). Values of vi between -1.5 and 1.5 indicate randomness (Winder et al., 2001; Perry & Dixon, 2002; De Villiers 2006). To test for non-randomness, the mean values of the clustering indices, ݒi and ݒj were used. Significant clustering in patches, random association, and gaps were illustrated using Surfer® v12 (Golden Software, Inc., Golden, CO). Interpolation between data points created by SADIE cluster analysis was calculated using the inverse distance weighted method in order to illustrate spatial distribution patterns. Results Mean captured flies in the HB field margin were numerically higher than NH during Early Susceptible 2011 (t = -1.00, d.f. = 2, P-value = 0.42), Late Susceptible 2011 (t = 1.39, d.f. = 2, P-value = 0.30), Early Susceptible 2012 (t = -1.00, d.f. = 2, P-value = 0.42), and Late Susceptible 2012 (t = -1.99, d.f. = 2, P-value = 0.19) (Figure 3.2A). Mean captured flies in the crop near HB were numerically higher than near NH during Late 46 Susceptible 2011 (t = -1.31, d.f. = 2, P-value = 0.32) and Late Susceptible 2012 (t = 0.58, d.f. = 2, P-value = 0.62) and statistically higher in Early Susceptible 2012 (t = 22.52, d.f. = 2, P-value = 0.002), but not in Early Susceptible 2011 (t = 0.68, d.f. = 2, Pvalue = 0.68) (Figure 3.2B). In 2011, field margins treated with egg protein resulted in 22 marked flies in HB and zero in NH (Table 3.1). In the adjacent crop, five flies were marked near HB and four near NH (Table 3.1). In 2012, field margins treated with egg resulted in 66 marked flies in HB and one in NH. In the adjacent crop, 21 flies were marked near HB and 16 near NH. Although there were numerically more marked flies in HB and the adjacent crop, the PDUNHGUDWLRZDVRQO\VLJQLILFDQWLQWKHILHOGPDUJLQȤ2 = 22.00, d.f. = 1, PvalueȤ2 = 63.06, d.f. = 1, P-value<0.0001) but not in the adjacent crop Ȥ2 = 0.11, d.f. = 1, P-value Ȥ2 = 0.68, d.f. = 1, P-value = 0.41). Spatial analysis (Table 3.2, Figure 3.3) indicated significant D. suzukii aggregation (Ia) and clustering in all time periods except Early Susceptible 2011. Contour maps overlaid with locations of monitoring traps show patches in three HB regions in the south and gaps near three NH regions in the north (Figure 3.3). In Late Susceptible 2012, a small patch is visible near NH in the north. Discussion Understanding landscape complexity and pest activity are key elements of developing a pest management strategy (Schneider, 1989; Holland & Fahrig, 2000; Carriere et al., 2006; Blackshaw & Vernon, 2006). This study is the first to demonstrate that D. suzukii utilize nearby habitat containing HB as a refuge and from there may migrate and colonize within the crop. Several arthropods are known to seasonally colonize nearby non-crop areas and cultivated crops (Duelli, 1990; Pedigo 2002) including Cydia pomonella Linnaeus (Lepidoptera: Torticidae) (Basoalto et al., 2010), Sitobion avenae Fabricius (Hemiptera: Aphididae) (Longley et al., 1997), Scaphoideus titanus Ball (Hemiptera: Cicadellidae) (Lessio et al., 2014), and Diaphorina citri Kuwayama (Hemiptera: Psyllidae) (Boina et al., 2009). Focusing on field margins, management tools proven for other pests such as bait sprays (Vargas et al., 2001; Prokopy et al., 2003), mass trapping (Cohen & Yuval, 2000), and non-crop host removal (i.e., ecological management) may 47 significantly reduce D. suzukii populations, especially if implemented in area-wide programs. However, field margins may play an important ecological role by providing food and habitat for pollinators and natural enemies (Holland & Fahrig, 2000; Marshall & Moonen, 2002). Furthermore, field margins could provide a refuge to reduce D. suzukii insecticide resistance development as it may house pesticide resistant alleles (Tabashnik & Croft, 1985). We demonstrated that elevated D. suzukii populations within the cultivated crops are often associated with high activity levels in the field margin, which may contain HB and possible other host plants. We propose three hypotheses as to why a similar number of marked flies were caught in the crop near both field margin types: 1) the greater influx of flies from HB field margins made it more difficult to detect marked flies, essentially diluting the proportion of marked flies near HB, whereas marked flies near NH were not so strongly affected by these influxes due to presence of fewer flies overall; 2) the total adult fly population is most likely underestimated and marked flies from HB in the southern plots moved toward NH in the northern plots. Drosophila obscura Pomini (Diptera: Drosophiliade) and D. subobscura Collin dispersed up to 100 and 200 m per day, respectively (Taylor et al., 1984). A preliminary mark-release-recapture study using fluorescent dusts found that D. suzukii moved approximately 67±87 m in 36 h (J.C. Lee, unpublished), and; 3) inefficient trap design, bait attraction, or placement inaccurately assessed population density (Knight & Croft, 1987; Cha et al., 2014; Kleiber et al., 2014). All NH plots and one HB plot had field margin traps exposed to full sun which seems to be less preferred habitat for D. suzukii (Tochen et al., 2014a). These traps had low counts throughout the two-year study, which may have been a reason for not detecting a statistical difference between captures in HB and NH field margins. Evaluating the impact of vegetation containing early ripening hosts of D. suzukii populations adjacent to a commercial fruit crop needs further investigation. Prunus avium (Thilenius 1968), which provides important resources to D. suzukii (Poyet et al., 2014), was present in an HB field margin that had consistently high trap counts. The fruitripening period of P. avium around the end of June to early July can provide an early ovipositional habitat for D. suzukii. Peak egg-laying by first generation females predicted 48 by degree-day model in mid July (Coop, 2014) coincided with the presence of susceptible cherry fruit and designates a key shift from low to high populations. By the time HB ripens in the Pacific Northwest of the USA, the raspberry crop is near the end of harvest (typically early August). In 2012, the crop adjacent to the field margin containing P. avium and HB had substantial dieback, which reduced fruit and canopy load (i.e., unfavorable canopy architecture) and likely reduced humidity. Early Susceptible 2012 flies may have traveled further in search of the ideal crop area (Coyne & Milstead, 1987; Iliadi et al., 2002). This could explain why a similar number of marked flies were found near HB and NH field margins (i.e., flies from HB flew further to the crop near NH). Spraying the NH field margin with a different protein marker, such as milk, may have explained the importance of this factor more clearly; however, the logistics of the project and uncertainties of the milk marker made this an unfeasible option (Klick et al., 2014b). In summary, mark-capture using egg white protein has documented the movement of self-marked resident D. suzukii from field margins into the adjacent cultivated crop. Field margins containing possible host plants as highlighted may have contributed to D. suzukii population buildup and resultant emigration to the cultivated crop. These conclusions were reached based on statistically and numerically higher marked D. suzukii trap counts in field margins containing HB. Higher levels of D. suzukii activity were found in crop areas, illustrated by significant patching in close proximity to HB. Finally, our marking data indicated movement of D. suzukii into the crop. These findings illustrate the potential risks associated with surrounding vegetation on pest pressure exerted by D. suzukii to crops. Limited information is available on the relative importance of differing landscape types adjacent to cultivated crops, host plant usage, and the impact of distance of non-crop hosts on pest pressure from D. suzukii into the crop. Overall, the activity of D. suzukii in non-crop host areas may be dependent on plant architecture, age, competition, multiple hosts, water source, and seasonal fruit selection. A landscape with a combination of diverse and abundant overstory and understory plants that provide D. suzukii with a spring-fall food source, overwintering refuge, and satisfactory environmental conditions could increase potential risks by D. suzukii. The benefits of surrounding vegetation, such as D. suzukii resistance 49 management, potential as D. suzukii trap crop, alternate resources for pollinators, and possible enhancement of biological control need to be determined before management strategies can be recommended. Acknowledgements We acknowledge Adam Cave, Kelly Donahue, Joe Kleiber, Amanda Lake, Scott Machtley, Scott Shane, Bev Thomas, and Amelia Thornhill for their diligent technical support and the cooperating raspberry grower for his collaboration and patience during the busy field season. Thanks to Oregon State University Statistics Student Consulting Service and Laura Sims for statistical assistance. Funding was provided by Oregon State University Agricultural Research Foundation, USDA SCRI Grant 2010-51181-21167 and USDA CRIS 5358-22000-032-00D. Mention of proprietary or brand names are necessary to report factually on available data; however, the USDA neither guarantees nor warrants the standard of the product, and the use of the name by USDA implies no approval to the exclusion of others that also may be suitable. This article is in the public domain and not copyrightable. It may be freely reprinted with customary crediting of source. 50 Table 3.1 Number of protein-marked (nm), assayed (na), the percentage (%) of marked D. suzukii, and yearly marked ratio (i.e. the total marked flies between HB and NH in ILHOGPDUJLQRUFURSLQDQGLQµ+LPDOD\D¶EODFNEHUU\+%DQGQRQ-host (NH) field margins (area treated with egg marker) and in the crop near HB and NH field margins during Early Susceptible (ES) and Late Susceptible (LS) in 2011/2012. ES 2011 Location nm/na % Field margin: HB 2/16 12.5 Field margin: NH 0 0 Marked ratiob by year nm/na % 20/134 14.9 0 0 22:0 (P-value<0.0001)a ES 2012 nm/na % 3/53 5.7 0/1 0 LS 2012 nm/na % 63/312 20.2 1/7 14.3 66:1 (P-value<0.0001) Crop: near HB 0/9 0 5/53 9.4 1/29 3.5 20/283 7.1 Crop: near NH 2/9 22.2 2/21 9.5 1/14 7.1 15/254 5.9 Marked ratio by year a LS 2011 5:4 (P-value = 0.74) 21:16 (P-value = 0.41) P-YDOXHVEDVHGRQȤ2 goodness-of-fit test (d.f. = 1) b Ratio of total marked flies between HB and NH in field margin or crop in 2011 and 2012 51 Table 3.2 SADIE (Spatial Analysis with Distance IndicEs) summary statistics of Early Susceptible (ES) and Late Susceptible (LS) in 2011/2012. Ia = index of aggregation; ݒj = mean index of gap clustering; ݒi = mean index of patch clustering; P = probabilities associated with indices. Time Iaa Pba ݒjc Pj ݒid Pi ES 2011 1.118 0.325 -1.057 0.327 1.142 0.259 LS 2011 3.141 <0.001 -3.988 <0.001 2.928 0.003 ES 2012 2.216 0.008 -2.114 0.018 2.174 0.015 LS 2012 1.866 0.034 -1.866 0.042 1.504 0.021 a Spatially random arrangement when the index of aggregation (Ia) is near to unity (i.e. between -1.5 and 1.5), aggregated arrangement when values are larger than unity, and regular arrangement when values are smaller than unity b Probabilities associated with indices c Mean index of gap clustering (i.e., clustering gap, vj<-1.5, or a low density of counts near each other) d Mean index of patch clustering (i.e., clustering patch, vi>1.5, or high density of counts near each other) 52 Figure 3.1 Monitoring traps for D. suzukii WUDSFDSWXUHVZHUHDPRGLILHGµFOHDU¶WUDS(Lee et al., 2012) made of a bottomless 946 ml clear plastic deli container (DM32R, Solo Cup Company, Lake Forest, IL) with ten 3.5-mm holes near the top, and nested over a plastic cup (D32, Solo, Urbana, IL) containing ~100 ml apple cider vinegar (ACV) (5% acidity, Fred Meyer Apple Cider Vinegar, Kroger Co., Cincinnati, OH). A 6.5 × 9 cm doublesided yellow sticky card (ASTO103, Alpha Scents Inc., West Linn, Oregon) was placed on top of the mesh that was positioned between the two cups. 53 Figure 3.2 Mean D. suzukii (+SE) captured per plot (n=3) in Early Susceptible (ES) and Late Susceptible (LS) 2011 and 2012 in (A) HB (Himalaya blackberry) and NH (nonhost) field margins and (B) crop by HB and NH. Significant differences are denoted with DQDVWHULVNĮ above the bars. 54 Figure 3.3 SADIE (Spatial Analysis with Distance IndicEs) contour maps created in Surfer® overlaid with traps (small dots) of 3 plots near HB in the south and 3 plots near NH in the north and the crop boundaries denoted in a dotted line in Early Susceptible (ES) 2011 (A), Late Susceptible (LS) 2011 (B), Early Susceptible 2012 (C), and Late Susceptible 2012 (D). The dark areas denote a clustering patch (vi>1.5) or high density of counts near each other. The light gray areas denote a clustering gap (vj<-1.5) or low density of counts near each other. The white areas denote a random distribution pattern (vi<1.5 and vj>-1.5). 55 Figure 3.3 56 CHAPTER 4 Reduced spray programs for Drosophila suzukii management in berry crops Jimmy Klick, Wei Q. Yang, Jana C. Lee, Denny J. Bruck Pest Management Science John Wiley & Sons Inc. 350 Main Street Malden, MA 02148 USA Manuscript currently in review 57 Abstract Since the arrival of Drosophila suzukii (Matsumura) (Diptera: Drosophilidae), field applications of broad-spectrum insecticides have significantly increased to protect susceptible fruit from infestation in berry crop production. Field studies were conducted from 2011 to 2013 to determine whether alternate row middle or border treatment reduced spray programs could manage D. suzukii as well as complete sprays and have less of an impact on non-target arthropods. Four raspberry sites and one blueberry site were alternate row middle and border sprayed, respectively. Captures of D. suzukii were compared to conventional complete spray programs. In both reduced spray trials, no differences in mean adult numbers and larvae of D. suzukii were detected between treatments. Mean counts immediately after sprays (i.e., 3±12 d after treatment) were also similar in complete and alternate row sprays. Both reduced spray strategies had significantly more Stethorus spp.; additionally, alternate row sprays had significantly more Psyllobora spp. No difference in fruit knockdown by complete or border spray was observed. These reduced pesticide strategies are additional tools to consider in D. suzukii IPM programs that reduce amount of spray area, application time, and input costs while conserving natural enemies. Keywords: Border spray, alternate row middle spray, blueberry, raspberry, natural enemies, fruit knockdown Introduction Drosophila suzukii (Matsumura) (Diptera: Drosophilidae) is an invasive pest of small and stone fruits in the Americas and Europe (Walsh et al., 2011; Cini et al., 2012; Deprá et al., 2014). Female flies cause direct damage by ovipositing into susceptible ripe fruit (Lee et al., 2011b). Eggs develop into larvae that feed on fruit flesh, rendering fruit unmarketable. To prevent fruit loss and to meet zero to low tolerance infestation levels set by packing plants, growers currently apply broad-spectrum insecticides multiple times during the harvest season (Bruck et al., 2011). They are faced with several challenges such as knocking mature fruits off of plants, managing insecticide pre-harvest and restricted entry intervals (PHI and REI), impacting natural enemies (Roubos et al., 2014a) and risking possible secondary pest outbreaks, all of which increase production costs. 58 Reduced insecticide strategies such as spraying alternate row middles versus every row middles (complete sprays) and border sprays are possible tools to curtail these challenges (VanEe et al., 2000; Roubos et al., 2014b). The alternate row middle method, henceforth alternate row, involves skipping an alley so that only one side of each plant row is treated (Lewis & Hickey, 1964). During the next application, the spray equipment travels down these skipped alleys and treats the previously non-sprayed side of the rows so that, after two applications, both sides of each planting row are treated. This reduced spray strategy uses the same rate and volume as complete sprays (i.e., same active ingredient coverage on the entire field delivered at two separate applications). Complete sprays refer to full coverage of the crop field (i.e., both sides of each plant row treated). Alternate row sprays have been used on mobile insect pests such as plum curculio in peaches (McVay et al., 1994; Lan et al., 2003). Furthermore, at least 72% of all apple growers in Pennsylvania used alternate row sprays to manage an array of pests, with fruit damage only reported from the apple budmoth (Platynota idaeusalis W.) (Hull et al., 1983). The advantages of spraying alternate rows include an approximately 50% reduction of input costs such as fuel, labor, tractor wear, and amount of insecticides; reduced environmental impact; and conservation of natural enemies. In apples treated with alternate row sprays, the phytophagous mite predator, Stethorus punctum L. (Coleoptera: Coccinelidae) was conserved (Asquith & Colburn, 1971), and in citrus, biological control of scales was enhanced (DeBach et al., 1955; Ripper, 1956). A possible disadvantage of alternate row sprays compared to every row sprays is an increased risk of pest attack by leaving one side of each plant row untreated at each application. In border sprays (DeBach & Bartlett, 1951), pesticide is applied to crop plants in the field border at the same rate and volume as complete field sprays, while leaving the center of the field untreated. Border sprays are typically effective against pests migrating into the field from field margins (Lafleur & Hill, 1987; Ferguson et al., 2000) and against µedge oriented¶ colonizers (Reardon & Spurgeon, 2003). Border sprays have been used to manage apple maggot, codling moth (Trimble & Solymar, 1997; Trimble & Vickers, 2000), and plum curculio (Chouinard et al., 1992; Vincent et al., 1997) in apple orchards, 59 alfalfa weevil in alfalfa (Roberts et al., 1987), and strawberry bud weevil in strawberries (Kovach et al., 1999). Systemic insecticides have been applied to potato borders for Colorado potato beetle (Blom et al., 2002) and an attract and kill applied to cucumber borders for melon fly management (Prokopy et al., 2003). Possible advantages of border sprays include reduced fruit knockdown within the field, reduction of insecticide inputs, fewer environmental impacts, and conservation of natural enemies (Trimble & Solymar, 1997). A disadvantage includes a greater risk of leaving the center of a treatment plot vulnerable to pest attack. We hypothesize that reduced spray strategies of alternate row and border sprays will be as effective as complete field applications at managing the highly mobile D. suzukii (Mitsui et al., 2010) and will conserve natural enemies. Mobility of D. suzukii was tested by a preliminary mark-release-recapture study using fluorescent dusts that showed D. suzukii moved approximately 67±87 m in 36 h (J.C. Lee, unpublished). Field margins with non-FURSKRVWVVXFKDVµ+LPDOD\D¶EODFNEHUU\Rubus armeniacus F.) may also provide refuge for overwintering adults and a source for invasion of the cultivated raspberry fields when ripe (Klick et al., 2014a). Our objectives were to determine whether reduced spray strategies in western Oregon berry crops would manage D. suzukii and have less impact on non-target arthropods. Materials and methods We tested the more conservative reduced spray strategy, alternate row sprays, in a highly preferred crop, raspberry (Lee et al., 2011b; Burrack et al., 2013; Bellamy et al., 2013; Atallah et al., 2014), and the less conservative strategy, border sprays, in a less preferred crop, blueberry (Bellamy et al., 2013). Alternate row spray trials in raspberry. Experimental sites and design. A total of four commercial red raspberry (Rubus idaeus L.) sites, using conventional management practices, were selected during 2011±2013 harvest seasons (4±6 wk per season) in the Willamette Valley, Oregon. Each site was arranged in a randomized complete block design. In 2011, a ~36 ha raspberry farm was selected in Albany, Oregon, henceforth Farm A, containing three blocks with selectively assigned plots that were each treated with alternate row or complete sprays. These three experimental units were selectively 60 DVVLJQHGEHFDXVHRIDSDUDOOHOVWXG\7KHILUVWWZREORFNVZHUHµ&DVFDGH%RXQW\¶ raspberry with treatment plots immediately next to each other. The third block was µ0HHNHU¶UDVpberry with treatment plots spatially separated by ~200 m. Each treatment SORWLQEORFNRQHZDVaKDRIµ&DVFDGH%RXQW\¶DQGKDGWKUHHDGXOWD. suzukii monitoring traps and two yellow sticky traps. The treatment plots in the other smaller blocks were 4±5 ha and each had two adult D. suzukii monitoring traps and one yellow sticky trap. Traps within each plot were along a single transect and spaced 30±50 m apart. ,QDaKDµ6DDQLFK¶UDVSEHUU\IDUPLQ-HIIHUVRQ2UHJRQKHQFHIRUWK)DUP%KDG three blocks with randomly assigned treatment plots. Trap numbers were the same across blocks in 2012 and 2013 trials. Each plot was ~8 ha with eight adult D. suzukii monitoring traps divided along two transects. In 2013, two of the blocks from Farm B were selected, omitting one of the low-yielding blocks; and two additional raspberry IDUPVZHUHVHOHFWHG2QHRIWKHVHIDUPVZDVDVPDOOKDEORFNRIµ&KHPDLQXV¶ raspberry grown under conventional management for U-Pick, henceforth Farm C, which was ~200 m west of FDUP%7KHRWKHUVLWHZDVDµ0HHNHU¶UDVSEHUU\IDUPKHQFHIRUWK Farm D, in Talbot, Oregon, with two blocks. Each block was ~10 ha. Farms A and D were overhead irrigated and Farms B and C were drip irrigated. All 2012 and 2013 sites had the same number of adult D. suzukii monitoring traps per plot (eight along two transects) spaced 10±80 m (dependent on plot size). Monitoring D. suzukii and non-target arthropods. All D. suzukii adults were monitored with a clear 10-hole trap (Lee et al., 2012) baited with ~150 ml apple cider vinegar (5% acidity, Fred Meyer Apple Cider Vinegar, Kroger Co., Cincinnati, OH) and a drop of unscented dish soap to break the surface tension and facilitate drowning. Apple cider vinegar was refreshed weekly and traps serviced twice per week by recording the total number of male and female D. suzukii adults caught per trap. Fifty fruit of marketable quality were collected twice per week during the harvest season throughout the canopy within a 3 m distance from each adult trap. Fruit samples were brought back to the laboratory and evaluated for larval presence using the salt extraction method. Fruits were lightly crushed in a sealable plastic bag to reveal flesh, soaked for 15 min in a 10 brix salt 61 solution (273 g salt per 3.8 liter water), and number of larvae was recorded (Dreves, 2014). In 2011, non-target arthropods (i.e., natural enemies and common pests) were monitored during the harvest season at Farm A using yellow sticky cards (Pherocon® AM No-Bait Traps, Trécé Inc., Adair, OK) placed halfway between the adult D. suzukii monitoring traps and replaced weekly. Ten leaflets of different size and age were collected weekly throughout the canopy within 10 m of each yellow sticky trap and brought back to the laboratory for examination of mites and aphids. In 2012 and 2013, additional non-target arthropod sampling methods were incorporated into the studies to increase diversity and abundance of organisms captured compared to 2011. Non-target arthropod sampling was conducted 7 d post-harvest using yellow sticky cards, leaf collections, sweep net, vacuum, and beat sheet. Eight non-target arthropod collections per plot were made in the vicinity of adult D. suzukii monitoring traps. Yellow sticky cards, as previously described, were in the field for 7 d. Leaves were collected for mites and aphids, as previously described. Twenty 180° sweeps with a ~40 cm diameter net were taken by walking ~15 m down the row middle while continuously sweeping from the plant row on the right down across the row middle to the plant row on the left. Sampling with vacuum (Shred-N-Vac, ES-2000, Echo Inc., Lake Zurich, IL) was performed by walking 10 m down a row middle while sampling throughout the top, center, and bottom canopy on the right side and switching to the left side for another 10 m. Contents from sweeps and vacuums were collected and each sealed in large sealable plastic bags and brought to the laboratory along with yellow sticky cards and leaves, arthropods identified to at least family level (except spiders and microhymenoptera), and numbers recorded. For beat sheet sampling, a cloth sheet was placed on the bottom row support cables (~0.5 m above ground) near an adult D. suzukii monitoring trap and vigorously shaking the top row support cables (within the top canopy of the plant row) 50 times. Arthropods were immediately identified on the beat sheet and recorded. The various collection methods did not overlap in the same areas (i.e., arthropods were collected from a previously nonsampled area). 62 Border spray trial in blueberry. Experimental site and design. $aKDµ/LEHUW\¶ blueberry (Vaccinium corymbosum L.) site in Albany, Oregon, managed using conventional practices, was selected during 2012 and 2013. The site was arranged in a randomized complete block design with three replications in the harvest seasons (7±9 wk). Each block had a randomly assigned border spray and complete spray plot (2.8 ± 5.3 ha). Blocks 1 and 2 were drip irrigated and block 3 was overhead irrigated. In 2013, the grower installed weed mat and trellis in blocks 1 and 2. Eight monitoring traps of adult D. suzukii, as previously described, were used per plot with four placed in the crop border (~5 m into the field, on each side of a plot) and four in the crop interior (40±60 m into the field from the border trap). Monitoring D. suzukii, non-target arthropods, and fruit knockdown. Adult and larval D. suzukii were monitored by trapping and larval extraction methods, respectively, twice per week, as previously described. Non-target arthropods were collected as previously described (yellow sticky cards, leaf collections, sweep net, and vacuum). Beat sheet sampling was not used out of concern for excessive fruit knockdown. Plants near the east and west adult D. suzukii monitoring traps, representing the crop border and interior of each plot, were selected to quantify fruit knockdown from each spray strategy. Within 24 h prior to application (border and complete sprays), fruit that dropped naturally or from hand-harvest was cleared from thHDUHDXQGHUQHDWKWKHVHOHFWHGSODQW¶VFDQRS\DQG within 24 h after spray applications, fruit knocked down by sprayers was collected, weighed (g), and recorded. Insecticide applications. Growers or crop consultants made all pesticide decisions and applications at the raspberry and blueberry sites based on biweekly reports of D. suzukii adult and larval counts in the field. In the alternate row spray trial in raspberry, a typical pre-harvest spray targeting orange tortix (Argyrotaenia franciscana W.) and obliquebanded leafroller (Choristoneura rosaceana H.) (both Lepidoptera: Torticidae) was applied to every row (i.e., complete spray) with insecticides also effective against D. suzukii (Bruck et al., 2011). Table 4.1 shows insecticides, rates, cultivars, and mean number of complete and reduced spray applications per treatment plot at each site. Mean number of sprays per treatment plot versus total sprays was displayed in Table 4.1 63 because of differences in application numbers between blocks. Raspberry growers made 1 ± 2 insecticide sprays specifically targeting D. suzukii. Complete and alternate row sprays were made with a Trellis Boom in 2011 (Farm A), Pul Blast in 2012 (Farm B), and Pak BlaVW)DUP'DQG3XO%ODVW)DUPV%DQG&LQDOOIURP5HDU¶V Manufacturing Company, Eugene, Oregon). Border spray applications in blueberry were made with a cannon sprayer (J-1000, Jacto Inc., Pompea, Brazil) traveling around the perimeter of the crop and spraying pesticides up to 30 m into the field. Complete spray applications were made with an overthe-URZ7UHOOLV%RRP5HDU¶V0DQXIDFWXULQJ&RPSDQ\(XJHQH2UHJRQVSUD\HUWKDW treated two entire plant rows per pass in 2012 and a track-elevated sprayer (TR4 Tracker, GK Machine Inc., Donald, Oregon) that treated four entire plant rows per pass in 2013. All insecticide applications (Table 4.1) targeted D. suzukii with the exception of neonicotinoid applications to control an aphid outbreak in 2012. Economic analysis. An economic impact scenario of the reduced spray strategies was estimated on a 4.05 ha plot with two insecticide sprays compared to the complete application method (Table 4.2). Insecticide cost, machine time, sprayer cost, fruit loss from knockdown in the 2012 border spray trial, and money saved were included in the analysis. Table calculations for alternate row, border, and complete sprays were based on berry economics (Julian et al., 2011). The analyses included: 1) estimated cost of insecticide material to treat 4.05 ha twice. Insecticide savings are 50% in alternate row and 70% in border applications based on area sprayed by each method; 2) the machine time to treat 4.05 ha with an airblast sprayer based on travel speed of 4.8 km h-1 and 0.74 ha treated per hour and the time to treat the same area at 10.9 ha per hour for border sprays with a cannon sprayer traveling at the same speed. Hectare per hour is the product of tractor speed (4.8 km h-1), row width (3 m), and efficiency (50%) over a conversion factor of 8.25 (C.F. Seavert, personal communication). Efficiency is the actual time spent spraying, excluding filling the tank, traveling to field, adjusting nozzles, and associated activities; 3) airblast sprayer (alternate row and cover sprays) and cannon sprayer (border spray) costs to treat 4.05 ha for labor, variable machine cost such as repairs and maintenance, and fixed machine cost including depreciating interest and insurance. The 64 airblast and cannon sprayers were a 757 L unit and 398 L units with power-take-off, respectively; 4) fruit knockdown loss in complete spray is based on the difference in fruit knockdown between border and complete sprays of 41.9 kg ha-1 and blueberry value of $3.30 kg-1 (average fresh and processed value) in 2012; 5) money saved is the difference in sprayer and insecticide cost between treatments. Analysis in the border spray trial includes savings from decreased fruit knockdown. Data analysis. All statistical analyses were made in R (R Core Team, 2013) using RStudio (RStudio, 2012) with Į = 0.05. Cochran-Mantel-Haenszel chi-squared test for count data was used to determine if sums of each gender were in excess in 2 × 2 tables for each block (Ramsey & Schafer, 2002))LVKHU¶V([DFW7HVWIRUFRXQWGDWDZDVXVHG for small sample sizes (Ramsey & Schafer, 2002). The linear mixed effects model fit by restricted maximum likelihood (REML) to determine differences between treatments of mean adults and larvae across the entire season (collection date and traps) were used for the alternate row spray trials. In the model, treatments were fixed effects and blocks were random effects. As only 1±2 treatment sprays were made, a separate analysis was performed using the same model but only with mean counts between 3±12 d after sprays to assess efficacy within the insecticide residual period (Bruck et al., 2011). Henceforth, this will be referred to as µAfter Spray¶. The border spray trial was a completely randomized block design in a two factorial experiment. There were two levels each within treatment (border and complete sprays) and trap position (border and interior traps). Linear mixed effects model fit by REML was used to detect differences in mean adults captured across the harvest season with treatment and trap position as fixed effects and treatment plots nested within blocks as random effects (larval counts were either zero or too low to permit analysis). A drop in deviance test was performed to fit the most appropriate model (Ramsey & Schafer, 2002). The model with the lowest Akaike information criterion (AIC) and non-significant difference between other models was deemed most appropriate using ANOVA. When the full model was most appropriate, linear combinations of coefficients were used to answer treatment and trap position questions. All P-values are reported with 95% confidence intervals (CI) and Bonferroni adjusted when two comparisons were made (Į = 0.025). 65 Natural log-transformation was used when normality or equal variance assumptions were not met. Log10 (x + 1)-transformation was used to transform 0, when present in the dataset. Estimates and confidence intervals were back-transformed, in the case of transformed data, and presented in tables along with the original means and standard errors. Individual non-target arthropods collected 7 d post-harvest in 2012 and 2013 were averaged across collection types (sweep, vacuum, beat sheet, yellow sticky cards, and leaf) and all traps within a treatment plot, to assess the overall impact of treatments. For example, anthocorids from all collection methods and trap captures within a treatment plot were combined and expressed as mean number per plot during post-harvest. This was done to detect plot level population changes, regardless of collection method, and to boost otherwise low counts. Only sufficiently large counts of non-target arthropods were included in the analysis. If the mean number of a non-target arthropod was less than 1.0 per treatment plot, the arthropod was not included in the analysis because counts were deemed too low to draw any firm conclusions. In alternate row trials, non-target arthropods were averaged across collection type (i.e., mean arthropod per treatment plot) and statistically analyzed as previously described for D. suzukii adults and larvae. In border spray trials, post-harvest non-target arthropods were averaged across collection type and trap positions (border and interior) (i.e., mean arthropod per trap position within a treatment plot) and statistically analyzed as previously described for D. suzukii adults. Fruit knockdown collected after insecticide applications in the border spray trials were averaged across collection periods and for each trap position (i.e., fruit knockdown per trap position within a treatment plot) and analyzed as previously described for D. suzukii and non-target arthropods. Results Alternate row spray trials in raspberry. Adults and larvae of D. suzukii. Adult D. suzukii were not separated by gender based on Ȥ2 test. No significant differences in mean adult and larval counts throughout the harvest season or during the After Spray period (3± 12 d after treatment application) were detected between alternate row and complete spray 66 treatments from 2011 to 2013 at four cultivated raspberry farms in the Willamette Valley, Oregon (Table 4.3). Non-target arthropods: natural enemies and common pests. In 2011, we observed 0.73 times as many Stethorus spp. individuals captured in alternate row spray, compared to complete spray (P-value = 0.003, CI = 0.57, 0.90). In 2013, alternate row sprayed plots had approximately four times more Stethorus spp. counts than complete sprayed plots (Pvalue = 0.01, CI = 1.72, 8.33) and about twice as many Psyllobora spp. (Coleoptera: Coccinelidae) counts (P-value = 0.033, CI = 1.08, 2.86) compared to counts found in complete spray plots (Table 4.4). Predatory mites (Mesostigmata: Phytoseiidae) were numerically higher in alternate row spray in 2012 and 2013 (Table 4.4). No significant differences between alternate row and complete spray were found in the following natural enemies (Table 4.4): microhymenoptera (Hymenoptera: Parasitic Apocrita - suborder), predatory thrips (Thysanoptera: Aeolothripidae), spiders (Araneae), rove beetles (Coleoptera: Staphylinidae), lacewings (Neuroptera: Chrysopidae and Hemerobiidae), and anthocorids (Hemiptera: Anthocoridae); and in the following common pests (Table 4.5): cucumber beetle (Coleoptera: Chrysomelidae), boxelder bug (Hemiptera: Rhopalidae), and pest mites (Acari: Tetranychidae). Border spray trial in blueberry. Adults and larvae of D. suzukii. In 2012, gender was not separated based on Ȥ2 test; however, gender was evaluated separately in 2013 because the odds in favor of an excess of females were 0.75 times greater in border spray plots (Pvalue = 0.026, CI = 0.59, 0.96). No significant differences in mean adult counts were detected between border and complete spray treatments during the 2012 and 2013 harvest VHDVRQVRIDFXOWLYDWHGµ/LEHUW\¶EOXHEHUU\IDUPLQthe Willamette Valley, Oregon (Table 4.6). In 2012, the effect of trap position on trap counts varied with treatment. Adults captured in complete spray plots were estimated to be 68% lower in interiors compared to borders (P-value = 0.017, CI = 0.12, 0.88) (Table 4.7). At last collection of the 2012 harvest season, two larvae were found in fruit collected from the border (n = 50) and two larvae from the interior (n = 50) of one of the border spray plots. At the end of the 2013 harvest season, one larva was found in fruit collected from the border (n = 50) and five 67 larvae from the interior of border spray plots (n = 200). A single larva was found in fruit collected from the interior (n = 50) of a complete spray plot. Non-target arthropods: natural enemies and common pests. In 2013, natural enemies captured in border spray plots were estimated to have about four times more Stethorus spp. than in complete spray plots (P-value = 0.045, CI = 1.04, 14.29) (Table 4.6). Since trap position varied with treatment, there were marginally fewer Stethorus spp. in complete spray interiors than borders (P-value = 0.081, CI = 0.15, 1.48) (Table 4.7). Although there was no effect of treatment on microhymenoptera (Table 4.6), trap position varied with treatment. In 2012, complete spray plots had an estimated 51% fewer microhymenoptera in the interior than in the border (P-value = <0.001, CI = 0.38, 0.64) (Table 4.7). In 2013, interiors were estimated to have 48% fewer microhymenoptera than borders (P-value = <0.001, CI = 0.42, 0.64) (Table 4.7). No significant differences between border and complete spray were found in the following natural enemies: predatory thrips, lacewings, and predatory coccinelids (Coleoptera: Coccinelidae); and in the following common pests: cucumber beetles (Table 4.6). Fruit knockdown. There was marginal evidence of more fruit knockdown in complete spray compared to border spray treated plots in 2012 (P-value = 0.082, CI = -0.33, 19.07). A mean weight of 16.4 g (±6.5 SE) of blueberries was knocked down in complete spray plots and only 5.1 g (±2.5 SE) in border spray plots. In 2013, only 1.2 g (±0.3 SE) and 1.5 g (±0.3 SE) were knocked down in complete and border spray plots, respectively. Discussion This study demonstrated that alternate row and border sprays provided control of D. suzukii similar to complete spray applications and prevented yield loss, thereby showing that reduced spray application strategies are important management tools for this pest. Reduced spray treatments resulted in higher numbers of natural enemies and lowered input costs. The hypothesis of minimizing D. suzukii populations with reduced sprays was supported because of likely D. suzukii mobility within field and movement from field margins into the cultivated crop (Mitsui et al., 2006; Klick et al., 2014a). No differences in adult and larval counts were detected in the alternate row trials in raspberry. We suspect within-field movement is high and flies from untreated rows move to treated crop 68 rows. Fly movement from field margins into blueberries most likely was reduced with the use of border sprays in the low-pressure D. suzukii year of 2012. The integration of complete sprays may be necessary in a high-pressure D. suzukii year, as in 2013. It is possible more females were trapped in 2013 border spray plots because they are more resilient to insecticides than males (Bruck et al., 2011). The lack of rain enabled longer residual activity of insecticides (Van Timmeren & Isaacs, 2013), which would be important in fields receiving lower insecticide inputs (i.e., reduced spray strategies). The effect on D. suzukii adults and larvae during the residual period of the insecticides (i.e., After Spray) was similar in complete and alternate row spray plots. Mean D. suzukii counts from After Sprays (3±12 d after treatment application) more accurately depict treatment effect rather than mean counts from the entire harvest season. Only 1±2 insecticide treatment applications specifically targeting D. suzukii were made during the harvest season, and residual activities of the insecticides (e.g., malathion, zeta-cypermethrin) persist for 10±14 d at best (Bruck et al., 2011). The After Spray analysis of D. suzukii adults and larvae was not performed in the border spray trial because of frequent treatment applications (approximately every 7 d). An unexpected outcome of this research was the effect of trap position in complete spray blueberries. In 2012, traps in borders (~5 m into the field) of complete spray plots had significantly higher D. suzukii and microhymenoptera counts than traps placed in interiors (40±60 m into the field). In addition, higher D. suzukii counts in the borders occurred less than 5 d after applications, whereas interior traps had 0 to very low counts (data not shown). This suggests that placing monitoring traps in borders may not be an accurate indicator of a plot-wide effect from a complete spray. Insects in border areas of complete spray plots may have less insecticide exposure than insects in interior areas. Although border traps do not necessarily estimate plot-wide adult D. suzukii populations accurately, they are still valuable indicators of early pest presence and level of pressure. It is unclear why fly captures in trap positions were similar in border spray plots. Perhaps the cannon sprayer (i.e., border spray) provided better penetration and coverage into border plant canopies than the vertical boom sprayers (i.e., complete spray) improving insecticide exposure to D. suzukii. Another possibility is that complete spray plots were 69 exposed to higher D. suzukii pressure than border-spray plots. Indeed, block 3, which was overhead irrigated, had an outlier trap in the complete spray plot with consistently high counts throughout the harvest seasons. To reduce crop risk, the alternate row spray interval can be shortened (Lewis & Hickey, 1972); and border sprays can be integrated with complete sprays to overcome higher pest pressure (estimated using degree day models and monitoring traps) or to µclean up¶ a field (Vincent et al., 1999; Trimble & Vickers, 2000). Level of insecticide residual activity may also influence crop risk, which varies between production regions, as risk is influenced by weather. For example, western Oregon likely has longer insecticide residual activity (Bruck et al., 2011) than North Carolina because of lower humidity and less rainfall in the summer (Burrack et al., 2013). Other factors possibly impacting insecticide efficacy include the method of irrigation, inactive ingredients such as additives, stickers, spreaders, and ultraviolet light breakdown (Van Timmeren & Isaacs, 2013). Overhead irrigation is suspected of reducing spray residuals and creating a more ideal habitat of higher humidity and moisture for D. suzukii (Tochen et al., 2014a), thus increasing risk. The reduced spray strategies lowered the effect on natural enemies. The conservation of a phytophagous mite predator, Stethorus spp., in alternate row sprays was consistent with previous work in apple orchards (Lewis & Hickey, 1972). This is the first report of conserving Psyllobora spp. by using alternate row sprays in raspberries and Stethorus spp. conservation in border-sprayed blueberries. Despite conservation of Stethorus spp. no differences were detected in pest mite densities (Acari: Tetranychidae), which are secondary pests of raspberry (Bounfour & Tanigoshi, 2001). We did not detect differences in pest densities from one section of the field to another, unlike in other studies (Vincent et al., 1997; Trimble & Vickers, 2000). Trimble and Vickers (2000) reported that oblique-banded leafroller (OBLR) damage levels were greater in the field center in one of the years of applying border spray treatments in an apple orchard. OBLR is a major contamination pest of raspberry and managed with a preharvest spray applied to both sides of each plant row, as was done in this study. Two blocks in 2012 were treated with neonicotinoid for a secondary pest outbreak of aphids 70 (Hemiptera: Aphididae), which was not effective on D. suzukii adults in direct-spray laboratory bioassays (Bruck et al., 2011), but has shown efficacy against adult and immature stages in semi-field and field trials (Van Timmeren & Isaacs, 2013) and curatively for post-infested fruit (Wise et al., 2014). Honeydew from aphids can reduce fruit quality (Oatman & Platner, 1972). A single neonicotinoid application for aphid control to the entire border spray plot late in the 2013 season (Table 4.1) was made after D. suzukii larvae were detected. Larval densities did not change and remained very low after treatment. More microhymenoptera were found in borders of complete spray plots in 2012 and in borders of both treatment plots in 2013, suggesting possible movement from surrounding field margins into the crop. If natural enemies migrate into the field from field margins (Longley et al., 1997), then border sprays may also affect them. Van Driesche et al. (1998) reported that leafminer parasitism in apple orchards was only higher in 2nd generation parasitoids but not in succeeding generations that were border sprayed (Van Driesche et al., 1998), suggesting there may be a lag effect of border sprays on natural enemy populations. Poor predation of cottony cushion scale occurred in California citrus by predacious Vedalia beetle (Coleoptera: Coccinelidae) when DDT was treated in two rows surrounding treatment plots (four trees) when compared to untreated control (DeBach & Bartlett, 1951), as the beetles were also affected by the border sprays. Another study revealed that parasitism of apple maggot was unaffected by border spray treatments when compared to complete sprays, regardless of plot size (Van Driesche et al., 1998). Border sprays seem to thus affect natural enemies differently and are perhaps dependent on the mobility of the organism. It is important that monitoring occur not just in field borders, but also in interiors, to assess natural enemies, pest pressure, and treatment efficacy on the entire plot. Blueberry fruit knockdown and loss seem highly dependent on sprayer type and cultural plant management practices including trellising and pruning, row width, plant size, and cultivar architecture characteristics such as having a compact growth habit. In 2012, an over-the-row Trellis Boom sprayer was attached to a tractor, rows were untrellised, and plants were four years oOGDQGRQH\HDUIURPPDWXULW\µ/LEHUW\¶ 71 blueberries are notoriously difficult to prune as they produce long shoots that grow into the row middle by harvest, increasing the likelihood of drop. Hand-pickers and deer likely confounded fruit knockdown data, as only marginal differences were detected. In 2013, the grower upgraded to a track-elevated sprayer and trellised the rows, which greatly reduced fruit knockdown in complete spray plots. Plots were treated immediately after fruit was picked to reduce fruit knockdown by the sprayer. The effect of the cannon sprayer on fruit knockdown appeared minimal, and there was no position effect detected in treated borders compared to untreated interiors of border spray plots. Based on the findings presented, reduced spray strategies may be implemented in low-risk and low-pressure situations and perhaps integrated with other non-insecticide pest management tools (Edson et al., 1998; Atanassov et al., 2003). The appropriate plot size for border spray treatments using a cannon sprayer is between 2 and 5 hectares. Extensive monitoring at least twice per week is important to understand the dynamics and effects of the reduced spray treatments on adult and larval D. suzukii populations (Kleiber et al., 2014). Further work is needed to assess the seasonal and long-term impacts of reduced sprays on non-target arthropods, rather than just post-harvest effects. Pest pressure from D. suzukii varies during the season (Van Timmeren & Isaacs, 2013), with low populations in winter (Dalton et al., 2011), and the highest populations from mid-VXPPHUWRIDOOLQPRVWUHJLRQV,QWKHERUGHUVSUD\WULDOWHQµ/LEHUW\¶ blueberries in containers placed along the field margin of each block as untreated controls did not serve as a good indicator of D. suzukii pressure due to low trap counts. Crop risk is greater in reduced spray strategies compared to complete spray strategies because approximately 50±70% of the crop is untreated at each application. Manipulating temporal and spatial factors that affect D. suzukii populations may reduce this risk. Knowledge of high-density and low-density D. suzukii areas (Klick et al., 2014a) and crop ripening phenology (Lee et al., 2011b) could facilitate integration of reduced spray strategies into a D. suzukii management program, such as reduced spray applications in low fly density areas onto fruit that ripen in early summer when populations are still low. Acknowledgements 72 We acknowledge Adam Cave, Austin Cuenca, Evan Dishion, Kelly Donahue, Christina Fieland, Amanda Lake, Jesse Mindolovich, Danielle Selleck, Scott Shane, Bev Thomas, Amelia Thornhill, Oscar Vargas, and Jeff Wong for assistance in the laboratory and field. Thanks to the cooperating raspberry and blueberry growers to permit these trials in the busy harvest season. Thanks to Jacto Inc. for donating the J-1000 cannon sprayer for the trial period. Helpful discussions with Leonard Coop, Joe DeFrancesco, Joe Kleiber, Danielle Lightle, Clark Seavert, and Megan Woltz were greatly appreciated. Oregon State University Statistical Consulting helped with the experimental design, and Hannah Tavalire provided statistical analysis advice. We greatly appreciated early draft reviews by Daniel Dalton and Amy Dreves. Funding was provided by Oregon State University Agricultural Research Foundation, Oregon Blueberry Commission, WSARE, USDA SCRI Grant 2010-51181-21167, and USDA CRIS 5358-22000-037-00D. Mention of proprietary or brand names are necessary to report factually on available data; however, the USDA neither guarantees nor warrants the standard of the product, and the use of the name by USDA implies no approval to the exclusion of others that also may be suitable. This article is in the public domain and not copyrightable. It may be freely reprinted with customary crediting of source. 73 Table 4.1 Insecticide applications in the alternate row trials (Farms A-D) of raspberry and border spray trials (Farm E) of blueberry during pre-harvest (p) and harvest (h) seasons. The rate (kg AI ha-1 and liter ha-1), number of plots per cultivar, mean number of complete sprays (C) per complete spray plot, and mean number of sprays per reduced spray plot (alternate row = AR, border spray = B). Note: complete sprays were applied in pre-harvest to AR plots and integrated during the 2013 season in B plots. For example, at raspberry Farm A, 0.03 kg zeta-cypermethrin was mixed in 748 liters of water ha-1 and DSSOLHGRQFHDV&WRWZRµ&DVFDGH%RXQW\¶DQGRQHµ0HHNHU¶&DQG$5SORWVLQSUHharvest 2011. 74 Table 4.1 Farm Year a Insecticide trade name Mustang Max Active ingredient Kg AI ha-1 liter ha-1 (AI) # plots per cultivara Mean complete sprays Mean sprays per reduced (C) per C plotb spray (AR or B) plotb zeta-cypermethrin 0.03 748.32 2 CB, 1 M 1p 1 p-C malathion 2.24 748.32 2 CB, 1 M 1.3 h 1.3 h-AR A 2011 A 2011 Malathion Aquamul 8 B 2012 Mustang Max zeta-cypermethrin 0.03 701.55 3S 1 p, 1 h 1 p-AR, 1 h-AR B 2012 Delegate WG spinetoram 0.10 701.55 3S 1h 1 h-C B 2013 Delegate WG spinetoram 0.10 701.55 2S 1 p, 1 h 1 p-C, 1 h-AR B 2013 Mustang Max zeta-cypermethrin 0.03 701.55 2S 1h 1 h-AR C 2013 Brigade bifentrhin 0.11 748.32 1 CH 1p 1 p-C C 2013 Mustang Max zeta-cypermethrin 0.03 748.32 1 CH 1h 1 h-AR D 2013 Tundra EC bifenthrin 0.11 561.24 2M 1p 1 p-C D 2013 Mustang Max zeta-cypermethrin 0.03 561.24 2M 1h 1 h-AR E 2012 Lannate methomyl 1.01 701.55 3L 1h 1 h-B E 2012 Mustang Max zeta-cypermethrin 0.03 701.55 3L 1.7 h 1.7 h-B E 2012 Imidan 70W phosmet 1.12 701.55 3L 1h 1 h-B E 2012 Admire Pro imidacloprid 0.70 701.55 3L 0.6 h 0.6 h-C E 2013 Mustang Max zeta-cypermethrin 0.03 701.55 3L 1 p, 2.7 h 1 p-B, 2.3 h-B, 0.7 h-C E 2013 Danitol fenpropathrin 0.34 701.55 3L 2h 1.3 h-B, 0.6 h-C E 2013 Malathion 8 Aquamul malathion 1.40 701.55 3L 0.3 h 1 p-B, 1 h-B, 0.3 h-C E 2013 imidacloprid 0.70 701.55 3L - 0.3 h-C Admire Pro &XOWLYDUVLQFOXGH&% µ&DVFDGH%RXQW\¶UDVSEHUU\0 µ0HHNHU¶UDVSEHUU\6 µ6DDQLFK¶UDVSEHUU\&+ µ&KHPDLQXV¶UDVSEHUU\/ µ/LEHUW\¶ blueberry b Means shown because of differences in number of sprays between blocks; p = pre-harvest period, h = harvest season; Treatments: C = Complete spray, AR = Alternate row spray, B = Border spray 75 Table 4.2 Economic costs associated with alternate row and border spraying compared to the complete spray method on 4.05 ha. Insecticide Machine Sprayer Fruit knockdown Money costb ($) timec (hr) costd ($) losse ($) savedf ($) Alt. row 500.00 2.75 163.26 - 705.20 Complete 1,000.00 5.49 368.46 - - 300.00 0.46 94.86 - 1601.60 1,000.00 5.49 368.90 628.00 - Treatmenta Border Complete a Table calculations for alternate row, border, and complete sprays based on berry economics.(Julian et al., 2011) b Estimated cost of insecticide material to treat 4.05 ha twice. Savings are 50% in alternate row and 70% in border applications based on area sprayed by each method c Machine time to treat 4.05 ha with an airblast sprayer based on travel speed of 4.8 km h1 and 0.74 ha treated per hour and the time to treat the same area at 10.9 ha per hour for border sprays with a cannon sprayer traveling at the same speed. Hectare per hour is the product of tractor speed (4.8 km h-1), row width (3 m), and efficiency (50%) over a conversion factor of 8.25 (C.F. Seavert, personal communication). Efficiency is the actual time spent spraying d Airblast sprayer (alternate row and complete spray) and cannon sprayer (border spray) costs to treat 4.05 ha for labor, variable machine cost (repairs and maintenance) and fixed machine cost (depreciating interest and insurance). The airblast and cannon sprayers were a 757 liter unit and 398 liter unit with power-take-off (PTO), respectively e Based on difference in fruit knockdown between border and complete sprays of 41.9 kg ha-1 and blueberry value of $3.30 kg-1 (average 2012 fresh and processed value) in 2012 f Money saved is the difference in sprayer and insecticide cost between treatments (border spray trial includes fruit knockdown savings) 76 Table 4.3 Comparison of mean (±SE) D. suzukii adults and larvae in alternate row and complete spray plots throughout the harvest season and during the After Spray period (3 ± 12 d after treatment application) in 2011, 2012, and 2013 in raspberry. Complete spray treatment was used as reference group. Estimates represent multiplicative increase in median counts in the alternate row spray treatment. Treatment Adults Larvae 2011 2012 2013 2011 2012 2013 Alt. rowa 0.6±0.4ab 0.3±0.1a 0.8±0.1a 1.3±0.7a 0.1±0.04a 0.8±0.3a Complete 0.8±0.2a 0.3±0.1a 1.2±0.2a 0.6±0.2a 0.1±0.05a 1.0±0.3a Transformation Log (ln) Log (ln) Log (ln) Log (ln) Log (ln) Log (ln) 2 2 4 2 2 4 0.440 1.172 0.367 2.053 1.379 1.223 Harvest df Estimate CI P-value 0.04, 5.26 0.16, 8.33 0.11, 1.75 0.289 0.762 0.353 0.01,333.33 0.11, 1.72 0.69, 2.17 0.610 0.638 0.389 After Spray Alt. row 0.10±0.06a 0.07±0.04a 0.30±0.07a 0.15±0.11a 0.06±0.05a 0.12±0.04a Complete 0.52±0.22a 0.12±0.06a 0.27±0.07a 0.00±0.00a 0.06±0.05a 0.14±0.06a Transformation Log10(x+1) Log10(x+1) Log10(x+1) Log10(x+1) Log10(x+1) Log10(x+1) df Estimate CI P-value a 2 2 4 2 2 4 7.368 9.640 10.097 11.400 10.000 9.845 3.47, 15.64 8.27, 11.23 8.60, 12.45 0.223 0.410 0.633 7.94, 16.37 8.13, 12.30 8.65, 11.21 0.259 1.000 0.755 Original mean and SE are shown with back-transformed estimates and confidence intervals (CI) (Į = 0.05). b Same lower-case letters within a column are not significantly different (Į = 0.05) based on linear-mixed effects model. 77 Table 4.4 Comparison of mean (±SE) natural enemies in alternate row and complete spray plots 7 d post-harvest in 2011, 2012, and 2013 in raspberry. Complete spray treatment was used as reference group. Estimates represent multiplicative increase in median counts in the alternate row spray treatment, in the case of log-transformed data. Microhymenoptera Treatment 2011 2012 Pred. mite Stethorus 2013 2011 2012 2013 2012 2013 Pred. thrips 2012 2013 Spider Rove 2012 2013 2012 Psyllobora Lacewing Anthocorid 2013 2013 2013 Alt. rowa 15.6±1.7ab 30.8±3.2a 36.5±4.7a 1.2±0.3a 6.7±3.8a 1.7±0.6a 2.3±0.5a 3.3±0.6a 9.0±3.2a 6.1±1.1a 1.6±0.3a 1.0±0.2a 0.6±0.2a 1.9±0.3a 0.7±0.1a 0.9±0.2a Complete 17.4±2.9a 23.7±3.4a 41.2±6.3a 0.5±0.2b 5.1±2.6a 0.4±0.1b 1.8±0.6a 2.8±0.6a 13.6±2.8a 8.8±1.8a 1.3±0.4a 1.0±0.2a 1.8±0.8a 1.2±0.2b 1.1±0.2a 1.0±0.3a Log (ln) Log (ln) Transformation Log (ln) Log (ln) Log (ln) df Estimate CI P-value a - - Log (ln) Log (ln) - Log (ln) Log (ln) Log (ln) Log (ln) 2 2 4 2 2 4 2 4 Log (ln) Log (ln) 2 4 2 4 2 4 4 4 1.006 1.291 0.962 0.731 1.583 3.831 1.175 1.422 0.460 0.880 0.835 0.075 0.750 1.748 0.696 0.944 0.41, 2.41 0.66, 2.50 0.58, 1.58 0.57, 0.90 -6.08, 2.91 1.72, 8.33 0.22, 6.25 0.65,3.13 0.07, 3.13 0.35,2.22 0.35, 4.00 -0.28, 0.43 0.04, 12.5 1.08, 2.86 0.35, 1.39 0.23, 3.85 0.979 0.242 0.93 0.003 0.919 0.01 0.719 0.276 0.222 0.73 0.59 0.591 0.707 0.033 0.224 0.916 Original mean and SE, are shown with, in the case of log-transformed data, back-transformed estimates and confidence intervals (CI) (Į = 0.05). Samples were combined in all collection methods (sweep, vacuum, beat sheet, yellow sticky cards, and leaf) to assess plot level differences b Different letters within a column are significantly different (Į = 0.05) based on linear-mixed effects model 78 Table 4.5 Comparison of mean (±SE) common pests found in alternate row and complete spray plots 7 d post-harvest in 2011, 2012, and 2013 in raspberry. Complete spray treatment was used as reference group. Estimates represent multiplicative increase in median counts in the alternate row spray treatment. Treatment Pest mites Boxelder bug Cucumber beetle 2012 2013 2012 2013 Alt. rowa 328.8±180.9a 47.6±23.2a 1.3±0.3a 3.8±0.6a Complete 301.8±185.0a 57.48±25.4a 2.1±0.8a 4.5±0.6a Transformation df Estimate CI P-value a Log (ln) Log (ln) Log10(x+1) Log (ln) 2 4 2 4 1.412 0.267 9.747 0.827 0.27, 7.14 0.02, 4.00 1.04, 91.03 0.47, 1.47 0.465 0.248 0.965 0.408 Original mean and SE are shown with back-transformed estimates and confidence intervals (CI) (Į = 0.05). Samples were combined in all collection methods (sweep, vacuum, beat sheet, yellow sticky cards, and leaf) to assess plot level differences b Same lower-case letters within a column are not significantly different (Į = 0.05) based on linear-mixed effects model 79 Table 4.6 Comparison of mean (±SE) D. suzukii adults throughout the harvest season and natural enemies and common pests 7 d post-KDUYHVWLQDQGLQERUGHUDQGFRPSOHWHVSUD\SORWVLQµ/LEHUW\¶EOXHEHUU\&RPSOHWHVSUD\WUHDWPHQW was used as reference group. Estimates represent multiplicative increase in median counts in the border spray treatment. Treatment Natural enemies Drosophila suzukii Adults Malesa 2012 Females 2013 Microhymenoptera Stethorus Pred. thrips Common pest Lacewing Pred. coccinelid Cucumber beetle 2012 2013 2013 2012 2012 2013 2012 2013 Borderb 0.4±0.1ac 0.6±0.1a 1.0±0.1a 15.2±2.9a 12.6±1.6a 6.0±1.0a 3.5±0.6a 1.2±0.3a 1.4±0.4a 3.0±0.5a 8.5±1.4a Complete 0.5±0.1a 0.7±0.2a 0.7±0.1a 18.5±3.1a 10.9±1.9a 3.1±0.5b 3.0±0.5a 0.3±0.2a 0.7±0.3a 2.5±0.6a 5.9±1.2a Full Reduced Reduced Full Reduced Full Reduced Reduced Reduced Reduced Reduced Log (ln) Log (ln) Log (ln) Log (ln) Log (ln) Log(ln) Log (ln) Log10(x+1) Log10(x+1) Log (ln) Log (ln) Model Transformation df Estimate CI P-value a 4 2 2 4 2 4 2 2 2 2 2 1.689 1.490 1.739 0.631 1.202 3.831 1.166 14.872 13.061 1.244 1.610 2.97, 74.47 4.66, 36.57 0.27, 5.56 0.73, 3.57 0.400 0.381 0.601 0.124 0.51, 5.56 0.14, 16.67 0.28, 11.11 0.32, 1.27 0.291 0.545 0.327 0.139 0.85, 1.70 0.151 1.04, 14.29 0.31, 4.35 0.045 0.665 Gender were analyzed separately based on Ȥ2 tests in 2013 Original mean and SE are shown with back-transformed estimates and confidence intervals (CI) (Į = 0.05). Natural enemy and common pest samples were combined in all collection methods (sweep, vacuum, yellow sticky cards, and leaf) to assess plot level differences c Different letters within a column are significantly different (Į = 0.05) based on linear-mixed effects model b 80 Table 4.7 Comparison of mean (±SE) D. suzukii adults throughout the harvest season and natural enemies 7 d post-harvest in 2012 and 2013 collected from border (~5 m into the field) and interior (40±60 m into the field) trap positions of border and complete spray SORWVLQµ/LEHUW\¶EOXHEHUU\7KHUHGuced model applied in 2013 microhymenoptera did not permit treatment separation. Border trap was used as reference group. Estimates represent multiplicative increase in median counts in the interior traps. Trap position Natural enemies Drosophila suzukii Adults Microhymenoptera 2012 2012 Stethorus 2013 Border Complete Border Complete 2013 Border Complete Border trapa 0.4±0.1ab 0.7±0.2a 15.9±3.9a 25.3±5.3a 15.3±2.0a 4.8±1.1a 4.3±0.8a Interior trap 0.4±0.1a 0.2±0.1b 14.5±4.4a 11.6±2.0b 8.2±1.1b 7.2±1.6a 2.0±0.4a Model Full Full Full Full Reduced Full Full Transformation Log (ln) Log (ln) Log (ln) Log (ln) Log (ln) Log (ln) Log (ln) df Estimate CI P-value 4 4 4 4 5 4 4 1.172 0.319 0.874 0.494 0.522 1.775 0.465 0.42, 3.24 0.12, 0.88 0.67, 1.14 0.38, 0.64 0.42, 0.64 0.56, 5.64 0.15, 1.48 0.615 0.017 0.147 a 0.0007 0.0005 0.157 0.081 Original mean and SE are shown with back-transformed estimates and confidence intervals (CI) that were Bonferroni adjusted for two comparisons (Į = 0.025). Natural enemy samples were combined in all collection methods (sweep, vacuum, yellow sticky cards, and leaf) to assess plot level differences b Different letters within a column are significantly different (Į = 0.05) based on linearmixed effects model 80 81 CHAPTER 5 Marking Drosophila suzukii with rubidium or 15N Jimmy Klick, Wei Q. Yang, Denny J. Bruck Journal of Economic Entomology 10001 Derekwood Lane, Suite 100 Lanham, MD 20706 USA Manuscript accepted 81 82 Abstract Drosophila suzukii has caused significant economic damage to berry and stone fruit production regions. Markers that are systemic in plants and easily transferred to track organisms are needed to trace D. suzukii exploitation of host resources and trophic interactions. High and low concentrations of the trace element, rubidium (Rb), and the stable isotope, 15N, were tested to mark D. suzukii larvae feeding on fruits of enriched strawberry plants grown in containers under greenhouse conditions. Fly marker content and proportion of flies marked 1, 7, and 14 d after emergence from enriched fruits and fly dry mass were analyzed. Nearly 100% of the flies analyzed 14 d after emerging from 15N enriched plants were marked, whereas only 30±75% and 0±3% were marked 14 d after emerging from high and low Rb concentration plants, respectively. Rapid Rb decay, strong 15N persistence, and the economics of using these markers in the field to elucidate D. suzukii pest ecology are discussed. Keywords: Rubidium, 15N, insect marking, strawberry, Drosophilidae, spotted wing drosophila Introduction Drosophila suzukii Matsumura (Diptera: Drosophilidae) larvae feed on the interior of ripening berry and stone fruits, causing significant economic losses in production regions of Europe and the Americas (Walsh et al., 2011; Cini et al., 2012; Deprá et al., 2014). Insect marking tools can be used to understand movement and dispersal of pests and trophic interactions (Hagler & Jackson, 2001), which may lead to improved integrated pest management (IPM) (Dorn et al., 1999; Jeger, 1999; Carriere et al., 2006; Klick et al., 2014a, 2015). An ideal marker for field experiments is inexpensive, environmentally friendly, easily applied, acquired and persistent, and clearly identifiable (Hagler & Jackson, 2001). Protein marking is one such tool and has been successfully used to mark D. suzukii in the laboratory (Klick et al., 2014b) and resident flies in a mark-capture study in the field (Klick et al., 2014a). Traceable proteins cannot be incorporated into plants. Systemic marking tools are required to determine what plant hosts are being utilized by resident flies in nature and to understand particular aspects of pest ecology. The trace element, rubidium (Rb), and the stable isotope, 15N, have been successfully used to mark 83 resident arthropods that have fed on enriched hosts in the field (Stimmann, 1974; Nowatzki et al., 2003; Tillman et al., 2007; Hood-Nowotny & Knols, 2007). Natural background levels of Rb and 15N are low. Small insects absorb the non-toxic mark from the environment (Berry et al., 1972; Steffan et al., 2001). Our objective was to compare the suitability of rubidium and 15N to help determine trophic interactions and sink-source relationships in complex and simple landscapes. We address this by determining 1) the persistence of these markers and percentage marked in adult D. suzukii that emerge from marked fruits of treated strawberry plants and 2) the effect of these markers on fly mass (as an indicator of fitness). Materials and methods Marking D. suzukii. On 25 May 2012, twenty-five strawberry (Fragaria x ananassa µ7RWHP¶SODQWV with green fruits were transplanted from the field (Oregon State University Botany Farm, Corvallis, Oregon) to 4.1 liter containers (21.6 cm × 17.1 cm, Anderson Die & Manufacturing, Portland, Oregon), arranged in a randomized block design, and grown under greenhouse conditions (16L: 8D photoperiod at 13±24 °C). To prevent feral D. suzukii from infesting fruits, fine-mesh netting (No-See-Um, Eastex Products, Holbrook, MA) bags were sealed over each plant before fruit turned color. The soil of each plant was drenched with a 250 ml solution five times over a 2 wk period (approximately every 3 d) with one of the following treatments: deionized water (control), 210 ppm N from 15N enriched NH4NO3 (5 atom%, Isotec Inc., Miamisburg, OH), 500, and 5,000 ppm RbCl (99.8% trace metals basis, Sigma-Aldrich, St. Louis, MO). Treatments were replicated four times. The water treatment was replicated eight times to provide a set of controls (n = 4) in Rb and 15N analysis. Henceforth, treatments will be referred to as control, 15N, 500, and 5,000 ppm Rb. On 18 June, when ripe fruit was present, each plant was moved from the greenhouse into a transparent cage (22 × 22 × 27 cm) topped with fine-mesh netting. Five mature (3± 15 d old) laboratory-reared D. suzukii adults (as described in Bruck et al., 2011) of each gender were added to each cage and placed in an incubator room at 22 °C, 35% RH, and 16L: 8D photoperiod in a randomized block design. Flies were removed after 70 h of exposure. All leaves were removed and fine-grain white sand (0.15 mm, Unimin, New 84 Canaan, CT) added to the soil surface to facilitate detection of emerged D. suzukii. The first emergence of adults occurred 7 d after the start of fly exposure; 8-17 d after start of exposure, a mean of 27 (± 9 SD) adult flies per plant (N = 20) emerged and were collected in respective treatment tubes (32-121BF, Genesee Scientific, San Diego, CA) with 2 cm3 of Drosophila cornmeal diet (Drosophila Stock Center, San Diego, CA) 0DUNRZ2¶*UDG\ZKLFKZDVUHIUHVKHGHYHU\G$mean subset of 18 (± 10 SD) adult flies were harvested from each replicate at 1, 7, and 14 d post-emergence, killed by freezing, and stored individually in 1.5 ml microcentrifuge tubes at -80 °C. Each sample was dried at 60 °C for 48 h and weighed on a microscale (C-35, Orion Cahn®, Thermo Electron Corporation, Waltham, MA) prior to mark analysis. Analysis of Rb-marked D. suzukii. Each fly sample was digested in 6 ml of concentrated HNO3 using a microwave (Multiwave 3000, Anton Paar) for 40 min (20 min microwave and 20 min cool down) at 140±190 °C and 20 bar pressure. Water (18.2 M-Ohm) was used to quantitatively transfer to conical centrifuge tubes with a final volume of 50 ml and HNO3 concentration of 15% (vol/vol). Rb measurements were made by Inductively Coupled Plasma Mass Spectrometry (ICP-MS) using a Thermo Scientific X-Series II. Instrument drift was monitored and corrected with an indium (In) internal standard added to every solution to yield a final concentration of 1 ppb In. For the samples, 3 ml aliquots of digested sample were pipetted into 14 ml tubes spiked with In and diluted to 5 ml with 1% (vol/vol) HNO3. Rb standards were diluted from a commercial standard (Sigma-Aldrich, St. Louis, MO) to make a working range of 0.02 to 20 ppb Rb. The standards also contained 1 ppb In and 5% HNO3. The higher acid concentration in the standards was necessary for proper uptake and washout of Rb (Rb in a pure solution of 1% HNO3 had delayed uptake and washout). Any suppression from the higher acid concentration was corrected by the In internal standard. Apple leaves (SRM 1515, National Institute of Standards and Technology) containing a known amount of Rb were analyzed to verify the analytical accuracy. Fourteen apple leaf samples were analyzed. Rb recovery was very good and ranged from 91-115%. Results from the ICPMS for the fly samples were measured as SSW5EDQGFDOFXODWHGWRȝJ5ESHUJUDPRID. suzukii. 85 Analysis of 15N-marked D. suzukii. Individually-dried whole flies were encased in 8 × 5 mm tin capsules (D1006, Elemental Microanalysis Ltd, Okehampton UK) and processed by the Oregon State University Stable Isotope Research Unit using an elemental analyzer and Isotope Ratio Mass Spectrometer. Data Analysis. Statistical analyses were made in R v3.0.3 (R Core Team, 2013) with an Į level of 0.05, or a Bonferroni-adjusted Į level of 0.006 and 0.017 for analyses involving nine (Rb marker content) and three (Rb effect on fly dry mass) comparisons, respectively (Ramsey & Schafer, 2002). Linear mixed effects models fit by restricted maximum likelihood were used to estimate differences between treatments in marker content and dry mass within each gender (Crawley, 2013). Analyses were performed separately for each gender because persistence and mark content varied in male and female flies. The marker content model included treatment by date and treatment by age as fixed effect and fly tube nested within date and nested within container as random effect. Age was included as interaction because the effect of treatment on marker content was expected to change with age. Response variables were natural-log transformed if assumptions of normality and equal variance were not met. The effect of treatment varied by age and by date; therefore, vectors of linear combinations of model coefficients were created to estimate differences in means between treatments. Estimates and confidence intervals were back-transformed, where applicable, and reported with non-transformed means and standard deviations. An individual fly sample was scored as marked if the marker value exceeded the mean value of the control flies plus three times the standard deviation of controls (Stimmann, 1974). Cochran-Mantel-Haenszel chi-squared tests were used to determine if marked: non-marked flies exceeded null expected ratios while accounting for emergence date (Ramsey & Schafer, 2002). The dry mass model included treatment by date of emergence as fixed effect with fly age as covariate and fly tube nested within date of emergence as random effect. Age was included as a covariate to account for the variance due to age. A drop in deviance test was performed to fit the most appropriate model (Ramsey & Schafer, 2002). 86 Results Both marker types were detected in flies that emerged from fruits of enriched strawberry plants. Rb content in emerged flies decreased rapidly, whereas 15N remained persistent and detectable in nearly all flies for the entire trial period (14 d) (Tables 5.1 and 5.2). All (38) 1 d old flies that emerged from fruits with 500 and 5,000 ppm Rb were considered marked and had more Rb than controls (Tables 5.1 and 5.2). Only flies from the high concentration (5,000 ppm Rb) had more Rb and a greater marked: non-marked ratio than controls throughout the entire trial period (14 d) (Tables 5.1 and 5.2). The percentage of females marked with Rb 14 d after emerging from the high concentration fruits was 75% or 2.5 times that of males from the same treatment (Table 5.1). Detailed statistical outputs of treatment comparisons are presented in Table 5.2. All flies (except 1 out of 124) analyzed for 15N were considered marked after emergence from enriched fruits at all time periods tested (Table 5.1). Female and male flies that emerged from fruits treated with 15N were estimated to have 7 (P-value < 0.0001, CI = 1.06, 1.08) and 8% (P-value < 0.0001, CI = 1.07, 1.09) more 15N atom% per D. suzukii than controls, respectively, regardless of age. Since no control and nearly 100% of 15N flies were considered marked at all time periods, no statistical comparisons were possible (i.e., the odds ratio could not be calculated) (Table 5.1). The treatments had no effect on female and male dry mass. Discussion The 15N mark was highly persistent in flies that emerged from enriched plants, but Rb rapidly decayed with time in flies from the low concentration and slightly less so in flies from the high concentration treatments. In other studies, rapid loss of Rb occurred 2±4 d after lygus and western corn rootworm stopped feeding on enriched plants (Fleischer et al., 1986; Nowatzki et al., 2003), but persisted for up to 27 d in Medfly (Van Steenwyk et al., 1992). Food source may affect Rb decay as the rate of Rb loss correlated with KCl in food of Drosophila spp. and Megaselia scalaris (Fairbanks & Burch, 1968). Furthermore, KCl is physiologically similar to the RbCl used in this study and was abundant in excretions of insects (Ramsay, 1953). 87 Similar to our findings, all treated aphids that fed on 15N enriched oat plants remained marked 10±16 d after transfer to non-enriched oats (Nienstedt & Poehling, 2000). Several factors may explain why 15N was persistent in flies: nitrogen is retained from food as proteins to make tissue and muscle in immature arthropods (Speight et al., 2009), nitrogen can be resorbed (Mira, 2000), and insects typically retain signatures of larval foods as adults (Hood-Nowotny & Knols, 2007). The markers tested at given concentrations did not affect fly dry mass. However, similar Rb concentrations tested in other studies have been shown to have adverse effects on insects. High concentrations of Rb (6,000 ppm to diet) affected development, fecundity and longevity of tufted apple bud moth (Knight et al., 1989), and concentrations above 5,000 ppm reduced survivorship in blueberry leaftier (Polavarapu et al., 1992). D. suzukii had a similar amount of Rb as Medfly (Van Steenwyk et al., 1992). Spra\LQJRULQMHFWLQJȝJ5EPORQFRIIHHIUXLWUHVXOWHGLQ0HGIOLHVZLWK± ȝJ5EJZKLFKGLGQRWKDYHDQ\DGYHUVHELRORJLFDOHIIHFWV$GYHUVHHIIHFWVRI15N have not been reported. Costs of D. suzukii analysis for Rb and 15N were seven and eight-fold higher, respectively, than egg protein marking (Klick et al., 2014a,b). However, 15N and Rb may be used to answer other research questions, such as the origin of a fly and trophic interactions, but may be limited in scale by the high costs. Field marking material costs may be offset if the rate of decay of 15N is shown to be much slower than egg protein. Rb was less favorable than 15N as a marker because of shorter persistence and the risk of negative effects on insect biology. Future work should determine the role of other host material on marker effect and the persistence of 15N in D. suzukii. The 15N mark successfully labeled D. suzukii via enriched plants and was highly persistent without any known adverse biological effects; hence, providing a tool for tracing pest exploitation of host resources and other trophic interactions. Acknowledgements We acknowledge Molly Albrecht, Kelly Donahue, Amanda Lake, and Scott Shane for technical assistance. Thanks to Jadwiga Giebultowicz, George Hoffman, Joe Kleiber, Gail Langellotto, Jana Lee, and Bob Van Steenwyk for helpful discussions; and Amy 88 Dreves for reviewing an early draft of this manuscript. We are grateful to Suean Ott and Carolyn Scagel for digesting Rb samples and Andy Ungerer and the Oregon State University (OSU) W.M. Keck Collaboratory for ICP-MS assistance. We appreciate the help of David Myrold and the OSU Stable Isotope Research Unit for 15N analysis. Thanks to Hannah Tavalire for statistical consultation and manuscript review. Funding was provided by the Agricultural Research Foundation, USDA SCRI Grant 2010-5118121167, and USDA CRIS 5358-22000-037-00D. 89 Table 5.1 Mean ȝJ5EJD. suzukii (Rb marking) and 15N atom% D. suzukii (15N marking) (± SD), ratio of marked: nonmarked, and percent marked (%) in female and male D. suzukii 1, 7, and 14 d after emergence from fruits of strawberry plants enriched with Rb or 15N. Mean marker content (± SD)a Treatment 1 No. d after emergence 7 Rb marking Female Control 15.31 ± 10.96b 14.27 ± 5.21b 500 ppm Rb 167.23 ± 123.90a 13.70 ± 13.02a 5,000 ppm Rb 608.66 ± 126.37a 66.96 ± 44.94a Male Control 14.41 ± 5.23c 17.06 ± 5.55b 500 ppm Rb 136.76 ± 55.13b 19.79 ± 13.92b 5,000 ppm Rb 1,080.64 ± 998.35a 178.63 ± 393.87a Marked: non-markedb Percent marked (%) 14 No. d after emergence 1 7 14 No. d after emergence 1 7 14 8.56 ± 9.16b 14.65 ± 9.03b 75.83 ± 49.99a 1: 8b 0:22 b 1: 25b 11: 0a 1:22 b 1: 31b 7: 0a 5:2 a 21: 7a 11 100 100 0 4 71 4 3 75 8.04 ± 7.83b 15.38 ± 8.60b 32.24 ± 17.85a 0: 7b 0:13 b 0: 30b 12: 0a 1:12 a 0: 20b 8: 0a 7:4 a 13: 31a 0 100 100 0 8 64 0 0 30 15 N marking Female Control 15 N 0.37 ± 0.0008b 0.40 ± 0.0144a 0.37 ± 0.0007b 0.39 ± 0.0109a 0.37 ± 0.0007b 0.39 ± 0.0089a 0: 7 10: 1 0: 30 20: 0 0: 26 28: 0 0 91 0 100 0 100 Male Control 15 N 0.37 ± 0.0005b 0.41± 0.0032a 0.37 ± 0.0006b 0.40 ± 0.0095a 0.37 ± 0.0006b 0.40 ± 0.0107a 0: 5 6: 0 0: 19 28: 0 0: 20 31: 0 0 100 0 100 0 100 a Different letters within the same gender of a marker and same column are significantly different using linear mixed effects model. Statistical output is presented in Table 5.2 b Different letters within the same gender of a marker and same column are significantly different based on Cochran-MantelHaenszel chi-squared test. Since no flies were considered marked in the control and nearly 100% marked in the 15N treatment, no statistical comparisons were possible (i.e., the odds ratio could not be calculated) 90 Table 5.2 Output of statistical comparisons for Rb marker content and ratio of marked: non-marked 1, 7, and 14 d after emergence from fruits of strawberry plants enriched with Rb. Estimates represent a multiplicative increase in median marker content in the 500 or 5,000 ppm Rb treatments. Treatment comparison 1 d after emergence dfa Estimate Rb marker content Female 7 d after emergence 14 d after emergence 95% CI P Estimate 95% CI P Estimate 95% CI P 0.0006* 2.40 0.82-7.03 0.0230NS b 500 - control 37 15.08 3.02-75.27 <0.0001** 8.43 1.60-44.51 5,000 - control 37 72.07 13.09-396.74 <0.0001** 10.64 2.22-51.12 0.0001* 10.01 3.66-27.34 <0.0001** 5,000 - 500 37 4.78 0.89-25.62 0.0100NS 1.26 0.27-5.94 0.6629NS 4.17 1.39-12.54 0.0005* 500 - control 36 8.47 1.73-41.36 0.0004* 3.03 0.25-36.67 0.2025NS 1.09 0.12-9.52 0.9201NS 5,000 - control 36 149.15 27.34-813.58 <0.0001** 46.45 4.00-539.96 <0.0001** 29.53 2.86-305.30 0.0002* 5,000 - 500 36 17.62 3.04-102.20 <0.0001** 15.33 1.22-192.25 27.38 2.67-280.70 0.0002* Male Rb marked: non-markedc Female Ȥ2 0.0033* Ȥ2 Ȥ2 500 - control 1 11.67 0.0006* 0.83 0.3613NS 0.30 0.5827NS 5,000 - control 1 8.13 0.0044* 9.16 0.0025* 19.59 <0.0001** 5,000 - 500 1 Na Na 7.51 0.0062* 21.30 <0.0001** Male 500 - control 1 12.35 0.0004* 0.88 0.3496NS Na Na 5,000 - control 1 8.77 0.0031* 6.34 0.0118* 8.21 0.0042* 5,000 - 500 1 Na Na 3.40 0.0654NS 5.63 0.0177* Back-transformed estimates and confidence intervals (CI); NS, non-significant; *, P-value < 0.006; **, P-value < 0.0001 a One less df in males because males were missing from one of the emergence dates b Linear mixed effects model with a Bonferroni-adjusted Į level of 0.006 for nine comparisons c Cochran-Mantel-Haenszel chi-squared test with an Į level of 0.05 91 CHAPTER 6 Conclusion Jimmy Klick 92 Spotted wing drosophila, Drosophila suzukii (Diptera: Drosophilidae), is a global threat to small and stone fruits production. The lack of biological control, large monocultures, high production standards, global trade of fruits, expansive host range, and pest biology and ecology created the perfect storm for D. suzukii to establish as a global pest. Insecticides, applied as complete cover sprays are currently the primary technique used for protecting susceptible fruit from infestation (Beers et al., 2011; Bruck et al., 2011; Van Timmeren & Isaacs, 2013). However, environmental and non-target concerns, high potential of developing insecticide resistance, and IPM are driving research towards developing sustainable management tools. Drosophila suzukii pressure is dependent on the population density exerted on a crop and typically varies temporally (i.e., by year or time of season) and spatially (i.e., local or regional). Understanding factors that influence fly pressure facilitates risk assessment. Some of these factors include weather, landscape, crop, and microclimate. For example in the Willamette Valley of Oregon, a mild winter (more spring survivors), a landscape abundant with crop and non-crop D. suzukii hosts (increased oviposition, refuge, and food sites throughout the season), a crop that ripens late in the season when populations are highest, soft fruit (easier to oviposit), and a field that is overhead irrigated (high humidity) is a high-risk scenario. In contrast, a cold winter (fewer spring survivors), a landscape abundant with non-hosts (fewer resource sites throughout the season), an early ripening crop when populations are still recovering from winter, firm fruit (more challenging to oviposit), and a drip irrigated field (low humidity) is a low-risk scenario. Proactive growers could further reduce risk by making conditions unfavorable for D. suzukii and implementing additional management tools such as sanitation, physical barriers (e.g., netting), pruning to open canopy, timely harvesting, and post-harvest cold storage. These methods along with enhancement, protection, and implementation of biological control and other management tactics (e.g., attract-and-kill, bait sprays) are currently under development and will play an increasing role in achieving the long-term goal of reducing insecticides by providing growers holistic management strategies for D. suzukii. The ideal D. suzukii management program involves multiple tools across the entire year. Although little published literature currently exists on alternative 93 management practices, a possible IPM scenario in Oregon throughout the year may look like this: suspected overwintering sites could be the focus of spring mass trapping, localized bait sprays, or attract-and-kill efforts followed by the use of physical barriers or border sprays that intercept D. suzukii before moving into a crop. During the harvest season, alternate row sprays, frequent harvests, drip irrigation, maintaining an open canopy, and utilizing sanitation practices to minimize breeding sites could be practiced to lower the risk by manipulating the environment to be less conducive to D. suzukii. Improved monitoring efforts with the use of an effective and selective lure and trap design paired with a predictive model (estimating activity and events), along with seasonal sampling of larvae for assessing damage are vital to understand risk, measure treatment effect, and for detection throughout the year. Post-harvest methods of cold storage and irradiation may prevent larval development in infested fruit and treatment of unpicked or dropped fruit (e.g., kaolin clay protective film on fruit or fruit crushing) may reduce oviposition and fly densities. Research is underway around the globe to develop these future strategies and will greatly improve pest knowledge and management. The work herein showed that a landscape with alternate hosts in non-crop areas is part of a high-risk scenario because higher fly densities were reported in those non-crop areas. Protein marking flies in this mark-capture study showed that flies move from adjacent non-crop areas into the crop. Although low numbers of marked individuals were recovered and it is not clear if flies visited or originated from the non-crop areas, conclusions of movement from non-crop to crop were supported by fly density data from other researchers. To address the latter shortcoming, 15N marking tools that are systemic in plants showed high persistence in flies reared from enriched strawberries in a greenhouse and could be used to determine origin of a fly in the field and help understand additional pest ecology questions. Reduced spray strategies, such as border and alternate row sprays, may be more easily implementable in low-risk scenarios. As long as adult and larval D. suzukii populations are monitored extensively (e.g., twice per week, one trap per hectare, bait replaced weekly), growers could possibly adapt the reduced insecticide application strategies to lower insecticide inputs and conserve natural enemy fauna, which are the 94 overarching goals in IPM programs. Further efforts are needed to evaluate reduce spray methods across a wider spectrum (e.g., variable spatial and temporal scales, different crops and pest pressure) before widespread implementation can be recommended. These methods could be the first step in D. suzukii management on the long path towards reducing insecticides and impact on natural enemies. There is still little understanding on D. suzukii movement and exploitation of non-crop hosts. Early ripening non-crop hosts may have a larger impact on population densities, especially if the phenology between non-crop and crop hosts is similar. 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