DECAY AND PERMEAMILITY TESTS CU SHEET MATERIALS USED AS SOIL COVERS IN EASEMENTLIESS MUSES May 1955 C raILV No. 2007 UNITED STATESLDEPARTMENT OF AGRICULTURE LOREST SERVICE FOREST PRODUCTS LABORATORY Madison 5, Wisconsin In Cooperation with the University of Wisconsin • DECAY AND PERMEABILITY TESTS OF SHEET MATERIALS USED AS SOIL COVERS IN BASEMENTLESS HOUSES By C.'S. MOSES, Pathologist 1 2 Forest Service Forest Products Laboratory,-,-U. S. Department of Agriculture Summary Eleven samples of sheet materials used or proposed for use as soil covers in basementless houses were tested for decay resistance. Only asbestosfibered specimens were free from fungus attack,but on the basis of the test and experience, asphalt roll roofings of other fibers and in weights of 45 pounds and over were also judged adequate to serve as soil covers. The water vapor transmission of artificially and naturally infected samples of roll roofing was tested by conventional and simplified techniques.' No important increases in permeance were found to result from fungus attack. Introduction The use of 55-pound roll roofing on the soil under basementless houses has been recommended as one means of keeping wood subfloor structures Maintained at Madison, Wis., in cooperation with the University of Wisconsin. 2 -Part of the research on this project was performed under the Housing Research Program of the Office of the Administrator, Housing and Home Finance Agency. • Report No. 2007 -1- Agriculture-Madison • too dry to decay.2 In this use, the roll roofing acts as a vapor barrier, preventing soil moisture in the form of water vapor from invading the crawl space where it can condense on and be absorbed by the wood. Wood with a moisture content of 20 percent or less will not decay. Other materials have also been proposed and used as soil covers, and records areavailable concerning their efficiency over a 5-year period.1 Roll roofing and other sheet materials used as soil covers necessarily undergo severe exposure to attack of fungi and other micro-organisms during service. Any resultant loss of strength might be detrimental to the use of this material, especially if it were to be crawled over consistently or subjected to forces tending to dislodge it. Of even greater importance is the knowledge of whether such fungus attack might increase its permeability to water vapor. However, while a water vapor transmission of 1 perm or less has been suggested for vapor barriers apparently no standard for the permeance of soil covers has been proposed.1 The trials reported herein are attempts to compare some properties of sheet materials as measured by accelerated laboratory tests. These experiments were intended to supplement the information continuing to be supplied by the service tests. Some of the research repor t ed here has been used as the basis of an article in "Housing Research"- but is included in brief form in order to bring together all work in this field. It should be noted that these data apply only to sheet materials used as soil covers and that no attempt has been made to interpret the results of using such materials as membranes under slab-on-ground construction. 'Diller, Jesse D. Reduction of decay hazard in basementless houses on wet sites. Forest Pathology Special Release No. 30. 1950. Diller, Jesse D. Soil cover reduces decay hazard of basementless -houses. Forest Pathology Special Release No. 38. 1953. 2Britton, Ralph R., and Robert C. Reichel. Water vapor transmission of building materials using four different testing methods. HUFA Tech. Bull. No. 12: 13-15. 1950. 6 -Russell, William A. Durability of moisture-resistant membrane materials in contact with the ground. H&BTA Housing Research No. 4: 23-28. 1952. Report No. 2007 -2- • • I. Resistance to Fungus Attack Method of Obtaining Data A total of 11 samples of soil cover materials were tested for fungus resistance by a modified soil-block method./ From 3 to 10 replicates of each sample were exposed to various fungi for a period of 3 months in individual containers incubated at 80° F. and 70 percent relative humidity. Deterioration due to fungus attack was measured by the loss in weight, but for a number of roll roofing samples the loss in tensile strength also was measured. Specimens used for the tensile tests were 4 by 1/2 inch with the fiber direction parallel to the long dimension while the remainder were 4-1/2 inches in diameter. The latter size was selected so as to compare with those used in the permeability test described later. Loss in weight was computed from equilibrium weights of the specimens placed, before and after exposure to the test fungi, in rooms adjusted for constant temperature and relative humidity (one test was at 73° F. and 50 percent relative humidity, the other at 80° F. and 65 percent relative humidity). The tensile values were determined on a Schopper Tensile Tester according to TAPPI standard method T 404 M 47. In all cases, values were adjusted according to reference specimens exposed in uninoculated containers. Results and Conclusions The results of the tests of soil cover materials are given in table 1. All fibers except the asbestos were subject to deterioration by fungi. While the weight losses of the roll roofing samples were relatively low because of the small proportion of fiber in them, the strength losses were considerable. However, there were no great differences in this respect between roofings of various weights. Since experience with 45and 55-pound asphalt roll roofing has been favorable, it would appear that these and roofings containing asbestos fibers were sufficiently resistant to fungi to serve as soil covers. The weight losses for the asphalt laminate-specimens were high, and in most cases the paper faces of the sheets were completely disintegrated. The tarred felt sample was resistant to some fungi but not to all; it 'Duncan, Catherine G. Soil-block and agar-block techniques for evaluation of oil-type wood preservatives: creosote, copper naphthenate and pentachiorophenol. Forest Pathology Special Release No. 37. 1953. • Report No. 2007 -3- • also tended to become brittle after fungus exposure and probably would be easily punctured and torn if used as a soil cover. Permeability to Water Vapor of II. Artificially Infected Specimens The data in this section were the basis of the article in Housing Research that was previously mentioned.6 Method of Obtaining Data Three replicate specimens of six types of roll roofing 4-1/2 inches in diameter were testd for permeance at the National Bureau of Standards by the dry method.– These specimens, together with their aluminum holders, then were exposed to the action , of 3 decay fungi in pure culture according to a modified soil-block technique for a period of 3 months. They were returned to the Bureau of Standards and tested for permeance again. The original permeance value of these specimens, their weight loss due to fungus exposure, and permeance value after this exposure are shown in table 2. Results and Conclusions No important changes in permeance occurred as a result of exposure to fungus attack although measurable weight losses were incurred by some specimens, and the fungi were observed to grow through a number of them (table 2). Except for the 15-pound asphalt saturated felt which was too badly deteriorated for permeance tests to be made, all the samples would appear to have adequate durability and vapor barrier efficiency for soil covers. III. Permeability to Water Vapor of Naturally Infected Specimens Permeance tests were made on 2 samples of 45-pound roll roofing that had been used as a soil cover for 2 years and thus exposed to the -The tests of water-vapor permeance were carried out under the direction of E. R. Oglio. Report No. 2007 -4- • • deterioration induced by natural infection and handling. Samples of new roll roofing were tested for comparison. Method of Obtaining Data The used specimens of soil cover were of two sorts -- those that showed evidence of fungus infection , in the form of mycelial mats (fig. 1) and those that appeared noninfected in a visual examination. The. defects in the specimens included both the deterioration due to fungus infection and that caused' by handling and crawling on the roll roofing while it was installed and used as a soil cover. Such obvious defects as tears and cracks were eliminated but the specimens tested had undergone considerable rubbing, flexing, and a slight amount of pitting from contact wItth the soil. The new specimens were selected from a roll of roofing which had been kept at room temperature. The test was run in an incubator maintained at 95° F. and 90 percent relative humidity. There was no provision for mechanically circulating the air. The test dishes used to hold the specimens were the bottom parts of 95 millimeter (3-3/4 inches in diameter) Petri plates having ground edges. These plates allowed the specimens an exposed• area of 9.95 square inches or 0.00641 square meter. All tests were by the dry method, and the desiccant used was anhydrous calcium chloride, about 23 grams to a dish. A scale accurate to 0.05 gram was used to obtain successive weights of the units. Three kinds of sealers were used. The edges of the roofing specimens were given two coats of aluminum varnish; The samples were fastened and sealed to the Petri plates with a coating of a solvent-base, synthetic rubber cement,and then melted wax (a mixture of amorphous and paraffin wax prepared for the purpose) was run around the outside of the plate at the junction of the specimen. The units (fig. 2) were placed in the incubator with the specimen down so that the calcium chloride was in direct contact with the roll roofing. Wood sticker strips 1/2 inch thick, placed outside the test area, elevated the units above the wire shelves of the incubator so that passage of air over the sample was not restricted. Each unit was kept in the same relative position during the test. The units were weighed at intervals of a few days until it became apparent that gain in weight would be slow. The intervals were then lengthened and observations continued for about 6 months. The permeability of the specimens was calculated from the constant rate of weight change. This was conveniently found by-plotting successive weights against time and using the data where at least three of these 111 Report No. 2007 -5- • points lay on a straight line. Water vapor transmission in grams per 24 hours per square meter was calculated according to the method of the • American Society for Testing Materials Committee on Water Vapor Transmission, dated January 1, 1951. W.V.T. = ELX_01 txa where is the gain in grams, t is the time in hours during which gain was noted, and a is the exposed area of the specimen in square meters. Water vapor transmission may also be expressed in grains per hour per square foot, which is grams per 24 hours per square meter multiplied by the factor 0.0597. When the water vapor transmission in grains per hour per square foot is adjusted to 1 inch of mercury vapor pressure differential, the result is given in perms.a This is done by dividing the values in grains per hour per square foot by the vapor pressure difference in inches of mercury during the test; in this case the calculated pressure was 1.49 inches of mercury. Results and Conclusions The results of the permeability tests are given in table 3. The values obtained suggest that any handling of the roll roofing material tends to produce an increase in permeance and that the presence of obvious decay definitely causes an increase. However, since all water vapor transmission was below the limit of 1 perm these differences are of little practical importance. The soil cover from which these samples were taken had given complete protection against condensation moisture in the crawl spaces of 2 test houses for 2 seasons. Whether the infection can proceed to a stage where permeance is significantly affected seems doubtful in view of the reports of vapor barrier efficiency after 9 years of service. There was no easy way to evaluate the sensitivity and efficiency of the simplified water vapor transmission test used in this experiment. When uniform conditions of temperature and humidity were maintained in the incubator, plots of successive weights occurred along a straight line reasonably well; average variation in rate of weight change in a given test ranged from 0.0006 to 0.008 gram per day. One of the test units failed because of a faulty seal. Thus, it appears that this technique in conjunction with an ordinary laboratory incubator was sufficiently precise to reveal important differences in the water vapor transmission of such low permeability material as roll roofing. 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Z M 8,178 F • • Figure 2.--The unit used for the water vapor permeability test showing the Petri plate test dish, the calcium chloride within used as the desiccant, outer portion of the roll roofing specimen, the edge seal of aluminum varnish, and the wax sealer. Z M 89251 F •