Heat transfer in the finned fluidized bed tubular heat exchanger by Joon Taik Kim A thesis submitted to the Graduate Faculty in partial fulfillment of the requirements for the degree of MASTER OF SCIENCE in Chemical Engineering Montana State University © Copyright by Joon Taik Kim (1970) Abstract: Local and average heat transfer coefficients for bed -to-wall heat transfer from a fluidized bed tubular heat exchanger with extended surfaces were investigated. The fluidized bed tubular heat exchanger consisted of a 44-inch long, 5.5-inch inside diameter shell with 19, 3/4-inch diameter stainless steel tubes arranged in a 1-inch triangular pitch. Air was used as the fluidizing medium and glass spheres of 0.0185-inch average diameter were used in this study. Tubes at the four possible tube locations tube were heated electrically. 3/16-inch stainless steel wire was used as an extended surface. The stainless steel wire was wrapped around the outside of each 19 tubes in a helical sprial. Variables studied include particle concentration, gas mass velocity and twist ratio. The Results of This Study Are as Follows 1. Gradual increase in the weighted average heat transfer coefficients with respect to the number extended surface were observed. Local heat transfer coefficients decreased with the distance from the entrance of the fluidized bed. Tube locations had only a slight effect on local heat transfer coefficients. 2. The average sectional coefficients according to the particle mode heat transfer with the extended surface were higher than the coefficients calculated from the bare tube surface. 3. With local heat transfer coefficients and experimentally determined sectional particle fractions over the 11 different sections of the fluidized bed, Nusselt numbers were correlated with an equation based on a particle mode heat transfer mechanism. 4. It is concluded that particle Nusselt numbers are proportional to 0.48 of I-ε. S t a t e m e n t o_f Pevrni ns i on t o Copy In . p r e s e n t i n g t h i s requi r ement s sity, for thesis in p a r t i a l f u l f i l l m e n t of t h e f o r an a d v a n c e d d e g r e e a t Mont ana S t a t e U n i v e r ­ I agree t h a t inspection. the Li br ar y shal l make, i t f r e e l y a v a i l a b l e I f u r t h e r agree t h a t per mi s s i on f o r e x t e n ­ s i v e copyi ng of t h i s thesis f o r s c h o l a r l y p u r p o s e s may be g r a n t e d by my ma j o r p r o f e s s o r , o r , D i r e c t o r of L i b r a r i e s . p u b l i c a t i o n of t h i s in his absence, by t h e I t i s u n d e r s t o o d t h a y any c o p y i n g o r thesis for financial a l l o we d w i t h o u t my w r i t t e n permi ssion. . Date gain s h a l l n o t be FlL 27,; mo HEAT TRANSFER IN THE FINNED FLUIDIZED BED TUBULAR'HEAT EXCHANGER JOON T. KIM A t h e s i s s u b m i t t e d t o t h e Gr a d u a t e F a c u l t y i n p a r t i a l f u l f i l l m e n t of t h e r e q u i r e m e n t s f o r t h e d e g r e e of MASTER OF SCIENCE in Chemi cal Engineering Appr oved: Ch a i r ma n , Exa mi ni ng Commi t t e e MONTANA STATE UNIVERSITY Boz e ma n, Mont ana Mar ch, 1970 J o o n Ta l k Ki m, t h e a u t h o r , Seoul, Kor ea. was bor n March 1 7 , 1 945 , in He i s t h e son o f Mr. Young J a Chun. He r e c e i v e d h i s e l e m e n t a r y and s e c o n d a r y e d u c a t i o n a t Seoul , Kor e a. School i n F e b r u a r y , 1963. Yons ei University He g r a d u a t e d f r om Pai In Ma r c h, J a n u a r y , 1 96 7 t o S e p t e mb e r , 1 968, he e n r o l l e d a t conducted vari ous feasibility industries services e n g i n e e r and i n gas c o n v e r s i o n . E n g i n e e r i n g De p a r t me n t a t Mont ana S t a t e U n i v e r s i t y as a r e s e a r c h a s s i s t a n t ber From s t u d i e s on AID and OECF l oa n specializing i n Chemi cal Engineering. he wor ked w i t h t h e Medium I n d u s t r y Bank as a t e c h n i c a l He e n r o l l e d 1963, Chai Hi gh i n Seoul , K o r e a , and g r a d u a t e d F e b r u a r y , 1967 wi t h a B. S . d e g r e e i n Chemi cal granted Chang Hwa Kim and Mrs. i n Se p t e m­ 1 968 wo r k i n g t o wa r d Ma s t e r o f S c i e n c e d e g r e e . ACKNOWLEDGEMENTS I would l i k e to t hank Dr. Wi l l i am E. Ge n e t t i o f Montana S t a t e U n i v e r s i t y f o r h i s a s s i s t a n c e and e ncouragement t hr o ug h o u t t h e d u r a t i o n of t h e investigation. I wi s h t o e x p r e s s my g r a t i t u d e to Mr. Ronald D. Aa f e d t f o r h i s a s s i s t a n c e whi ch he l pe d me to c o mp l e t e my s t u d y . So Young Hahn f o r h e r h e a r t f u l research. Special I w o u l d / l i k e to thank Miss h e l p t o f i n i s h my s t u d y and t h a n k s go t o my p a r e n t s f o r t h e i r e n ­ c o u r a g e me n t t h r o u g h o u t t h e p e r i o d o f r e s e a r c h . I wi s h t o a c k n o wl e d g e t h e f i n a n c i a l support I received from t he E n g i n e e r i n g Experi ment S t a t i o n a t Montana S t a t e University. I V TABLE OF CONTENTS I• II. I n t r o d u c t i o n ...................................................... L i t e r a t u r e Su r v e y and Th e o r y ................................... 3 ................................................... 28 III. E x p e r i me n t a l Ap p a r a t u s IV. E x p e r i me n t a l P r o c e d u r e ................................ V. Calculations VI. Page -j 45 ................................................................. 40 A n a l y s i s o f D a t a .......................53 VI I . R e s u l t s and C o n c l u s i o n .................................................. 30 VIII' . L i t e r a t u r e C i t e d ................................................................. 33 ' APPENDICES App e n d i x I No me n c l a t u r e Appe ndi x I I Ev a l u a t i o n of Appe ndi x I I I ■ Appe ndi x IV App e n d i x V 86 0 and R- 93 A Typi c al Dat a S h e e t C a l i b r a t i o n Tabl es f or T h e r mo c o u p l es Compl e t e Da t a ( Ta b l e IV) 95 ' 97 . 119 V .LIST OF FIGURES Page Fi gure I . S o l i d movement and gas f l o w as v i s u a l i z e d by b u b b l i n g bed model . Figure 2 . Co r r e l a t i o n for heat t r a n s f e r c o n t a i n i n g wa l l and f l u i d i z e d b e t we e n bed 18 Fi gure 3 . C o r r e l a t i o n f o r h e a t t r a n s f e r b e t we e n i n t e r n a l v e r t i c a l t u b e s and f l u i d i z e d bed. 19 C o r r e c t i o n f a c t o r Cr f o r non a x i a l l o c a t i o n of i mmer s ed - t ubes . 20 F i g u r e 4. F i g u r e 5. 7 ICPP m u l t i p l e - t u b e d a t a compar ed wi t h ■V r e e d e n b e r g ' s c o r r e l a t i o n f o r h e a t t r a n s f e r to a s i n g l e t ube 22 F i g u r e 6. Fl ow d i a g r a m o f t h e f l u i d i z i n g a p p a r a t u s 29. Fi gure 7 . (A) (B) 31 Fi gure 8 . Tube l a y o u t : s howi ng l o c a t i o n s h e a t i n g el ernen t . F i g u r e 9. Di agr am of e l e c t r i c a l circuit. 36 Fi gu r e 10. Ex p l o d e d vi ew of t h e t u b e wal l t e mpe r a t ur e probe. 39 F i g u r e 11 . Av e r a g e N u s s e l t number s c o r r e l a t i o n without f l ui di za t i on. . 54 F i g u r e 12. Vertical profiles 56 F i g u r e 13. Local heat t r a n s f e r c o e f f i c i e n t s . 59 F i g u r e 14. Local he a t , t r a n s f e r c o e f f i c i e n t s 61 F i g u r e 15. Local heat t r a n s f e r c o e f f i c i e n t s 63 Ge n e r a l Equi pme nt Gl a s s p a r t i c l e s fluidized of bed t e m p e r a t u r e 34 vi F i g u r e 16. Local heat transfer c o e f f i c i e n t s . 64 F i g u r e 17. Local heat t r a n s f e r c o e f f i c i e n t s . 66 F i g u r e 18. Local heat t r a n s f e r c o e f f i c i e n t s . 68 F i g u r e 19. Local heat t r a n s f e r c o e f f i c i e n t s . 70 F i g u r e 20. Local heat t r a n s f e r c o e f f i c i e n t s . 71 F i g u r e 21. Av e r a g e s e c t i o n a l c o e f f i c i e n t s batch f l u i d i z a t i o n for 73 F i g u r e 22. C o r r e l a t i o n f o r a v e r a g e c o n t a c t t i me . 77 F i g u r e 23. The p r e s e n t m o d i f i e d c o r r e l a t i o n f o r s e c t i o n a l p a r t i c l e N u s s e l t n u mb e r s . 7 9' F i g u r e '24. The c o r r e l a t i o n f o r n and R. 93 F i g u r e 25. Nomograph t o c a l c u l a t e Gmf 94 vii LIST OF TABLES PageTa b l e I . E x p e r i me n t a l Pr ogr am 44 Tabl e II . D i f f e r e n c e of Local Heat T r a n s f e r C o e f f i c i e n t Bet ween D i f f e r e n t Ex t e n d e d S u r f a c e s 65 Tabl e I I I . The We i g h t e d Av e r a g e Co n t a c t Ti mes 74 Tabl e Compl e t e Dat a 119-142 IX V111 ABSTRACT Local and a v e r a g e h e a t t r a n s f e r c o e f f i c i e n t s f o r bedt o - w a l l h e a t t r a n s f e r f r om a f l u i d i z e d bed t u b u l a r h e a t e x ­ c h a n g e r wi t h e x t e n d e d s u r f a c e s wer e i n v e s t i g a t e d . "[he f l u i d i z e d bed t u b u l a r h e a t e x c h a n g e r c o n s i s t e d of a 4 4 - i n c h l o n g , 5 . 5 - i n c h i n s i d e d i a m e t e r s h e l l wi t h 19, 3/ 4 m c h d i a m e t e r s t a i n l e s s s t e e l t u b e s a r r a n g e d i n a 1- i n c h triangular pitch. Ai r was us ed as t h e f l u i d i z i n g medium and g l a s s s p h e r e s o f 0 . 0 1 8 5 - i n c h a v e r a g e d i a m e t e r wer e used in t hi s study. Tubes a t t h e f o u r p o s s i b l e t u b e l o c a t i o n s t u b e wer e heated e l e c t r i c a l l y . 3 / 1 6 - i n c h s t a i n l e s s s t e e l wi r e was us e d as an e x t e n d e d s u r f a c e . The s t a i n l e s s s t e e l wi r e was wr a ppe d a r o u n d t h e o u t s i d e o f eac h 19 t u b e s i n a h e l i c a l sprial. Variables studied include p a r t i c l e concentrati on gas mass v e l o c i t y and t w i s t r a t i o . The R e s u l t s o f Th i s Study Ar e as Fo l l o ws 1. Gr a d u a l i n c r e a s e i n t h e w e i g h t e d a v e r a g e h e a t t r a n s f e r c o e f f i c i e n t s wi t h r e s p e c t t o t h e number e x t e n d e d s u r ­ f a c e wer e o b s e r v e d . Local h e a t t r a n s f e r c o e f f i c i e n t s d e c r e a s e d wi t h t h e d i s t a n c e f r om t h e e n t r a n c e of t h e f l u i d i z e d bed. Tube l o c a t i o n s had onl y a s l i g h t e f f e c t on l o c a l h e a t t r a n s f e r c o e f f i c i e n t s . 2. The a v e r a g e s e c t i o n a l c o e f f i c i e n t s a c c o r d i n g t o t h e p a r t i c l e'-mode h e a t t r a n s f e r wi t h t h e e x t e n d e d s u r f a c e wer e h i g h e r t h a n t h e c o e f f i c i e n t s c a l c u l a t e d from t h e b a r e • t ube s u r f a c e . 3. Wi t h l o c a l h e a t t r a n s f e r c o e f f i c i e n t s and e x p e r i m e n t a l l y d e t e r m i n e d s e c t i o n a l p a r t i c l e f r a c t i o n s o v e r t h e 11 d i f f e r e n t s e c t i o n s o f t h e f l u i d i z e d be d, N u s s e l t number s wer e c o r r e l a t e d wi t h an e q u a t i o n ba s e d on a p a r t i c l e mode h e a t t r a n s f e r me c ha ni s m, 4. I t is concluded t h a t p a r t i c l e p r o p o r t i o n a l to 0 . 4 8 o f 1 - e . N u s s e l t number s a r e Introduction. The s t udy o f d e s i g n methods f o r improved f l u i d i z e d bed h e a t e x c h a n g e r s as i n d u s t r i a l he a t t r a n s f e r equi pment has become g r e a t l y i mp o r t a n t , b e c a u s e o f i t s i s o t h e r ma l a c t e r i s t i c a l o n g wi t h v a r i o u s a p p l i c a t i o n s physical in chemi cal and operations. Fluidization tional char­ i s t he phenomenon in which t he g r a v i t a ­ f o r c e a c t i n g on a dens e p a c k e t o f p a r t i c l e s is c o u n t e r a c t e d by an upward f l u i d s t r e a m, which c a u s e s t h e s e particles t o be ke pt more or l e s s in a f l o a t i n g s t a t e . The uni f orm t e mp e r a t ur e d i s t r i b u t i o n o f the f l u i d i z e d bed i s due t o t he t u r b u l e n t f l u i d - s o l i d s continuous, s us pende d mot i on and the f r e q u e n t c o n t a c t s between the h e a t i n g s u r f a c e and a new swarm o f p a r t i c l e s by t he r a p i d c i r c u l a t i o n o f t he f l u i d i z e d s t r e am. Even i f t he f undame nt al s o f f l u i d i z a t i o n were not f u l l y and c o mp l e t e l y , u n d e r s t o o d , many f l u i d i z e d - s o l i d s have a c h i e v e d commerci al success. Fluid-bed c a t a l y t i c c r a c k i n g u n i t s wi t h t he c o n v e r s i o n l e v e l exampl e. correlations processes The need f o r h e a t , mas s , of 50-60 percent i s and momentum t r a n s f e r in f l u i d i z e d beds was paramount f o r f l u i d i z e d bed t e c h n i q u e s t o be a s u c c e s s . •One o f t he n o t i c e a b l e a dv a n t a g e s o f f l u i d i z e d - b e d s to o n e - p h a s e f l o w i s hi gh r a t e s o f h e a t t r a n s f e r . It is well- -2' known t h a t h i g h e r h e a t . t r a n s f e r c o e f f i c i e n t s wi t h e x t e n d e d s u r f a c e s , however, t h i s effect can be a c h i e v e d is s ome t i mes d i s m i s s e d as a means t o i mpr ove p e r f o r ma n c e o f a h e a t e x c h a n g e r b e c a u s e o f t h e c o r r e s p o n d i n g l y h i g h e r power c o n ­ s u mp t i o n . Numer ous s t u d i e s of vari ous have been made t o f i n d out t h e e f f e c t types of extended s ur f a c e s t r a n s f e r in t u r b u l e n t t r a n s f e r e q u i p me n t . but i t is spiral wi r es on t h e r a t e f l ow f o r d i f f e r e n t Thes e r e s u l t s of heat industrial a r e i n no way g e n e r a l , at l e a s t e vi dent t h a t extended s ur f aces or t w i s t e d s t r i p s heat ha ve some e f f e c t s c r e a s i n g t he r a t e of h e at t r a n s f e r in i n d u s t r i a l like on i n ­ heat t r a n s ­ f e r e q u i p me n t f o r s i n g l e p h a s e s y s t e m s . • A number o f s t u d i e s coefficients and a v e r a g e h e a t t r a n s f e r f o r h e a t t r a n s f e r f r om an i n t e r n a l bundl e of t u b e s present on l o c a l t o a f l u i d i z e d - b e d have been made. investigation transfer rates t ube in a is a study of local The and a v e r a g e h e a t i n t h e f l u i d i z e d bed t u b u l a r h e a t e x c h a n g e r wi t h t h e e x t e n d e d s u r f a c e s . Local heat t r a n s f e r c o e f f i cents we r e me a s u r e d wi t h a movi ng t h e r mo c o u p l e p r obe i n s i d e an electrically me a s u r e l o c a l heated tube. Th i s p r o b e made i t heat t r a n s f e r c o e f f i ci en t s a tube f or vari ous gas r a t e s and p a r t i c l e p o s s i b l e to a t any p o i n t a l o n g concentrations. The r a t e o f h e a t t r a n s f e r was c o r r e l a t e d wi t h t h e a r e a o f extended s u r f a c e s . -3- ■Literature F l u i d Mechani cal Su r v e y and Theor y Appr oach o f FTu i d i zed Beds By a s s u mi n g a f u l l y free, spherical in the t h r e e - d i me n s i o n a l in t he t wo - d i me n s i o n a l approach, phases d e v e l o p e d c i r c u l a r b u b b l e and s o l i d - potential to p o s t u l a t e case, Da vi ds on useful cylindrical (3) a d o p t e d a c o n t i n urn f l o w f o r bot h t h e f l u i d and p a r t i c u l a t e t h e mot i on o f r i s i n g b u b b l e . Da vi ds on model was n o t s u f f i c i e n t l y first case, accurate, Even i f i t was t he a p p r o a c h t o t h e mo t i o n o f a r i s i n g b u b b l e i n the g a s - s o l i d f l u i d i z e d bed. Mur r ay ( 17) a d o p t e d a c o n t i n u m a p p r o a c h f o r t h e t wo- p h a s e mo t i o n o f t h e f l u i d and s o l i d s i n a f l u i d i z e d bed. Momentum and mass c o n s e r v a t i o n e q u a t i o n s wer e a p p l i e d t o obtain solutions the b e d . f o r t h e mo t i o n c a u s e d by r i s i n g b u b b l e s i n The s t a b i l i t y analysis and t h e e q u a t i o n s been d e r i v e d t o p r o v i d e a means o f c l a s s i f y i n g sys t e ms , b u t he di d n o t e v a l u a t e equation, so t h a t no q u a n t i t a t i v e Ande r s on and J a c k s o n purposes it the a c t ua l (I) the r oot s had fluidized of h i s secular r e s u l t s wer e o b t a i n e d . realized that for practical i s n e c e s s a r y t o s e e k some met hod o f s i m p l i f y i n g p r o b l e m so t h a t i t system of p a r t i a l differential J a c k s o n have us e d a f or mal mean v a r i a b l e s to t r a n s l a t e can be d e s c r i b e d by a s mal l equations. m a t h e ma t i c a l An d e r s o n and d e f i n i t i o n of l ocal t h e p o i n t Na v i e r - S t o k e s e q u a t i o n s — .4 . i o r t h e f l u i d and t h e Ne wt oni an e q u a t i o n s o f mo t i o n f o r t he p a r t i c l e s somewhat d e v o i d o f number o f t e r ms whose f or ms a r e y e t u n d e t e r mi n e d . Ac c o r d i n g , t o t h e r e ne wa l and F a i r b a n k s icles (18), model p r o p o s e d by Mi c kl e y owi ng t o t h e b u b b l e s , p a c k e t s of p a r t ­ a r e renewed c o n t i n u o u s l y be t we e n t h e b u l k o f t h e bed and t n e v i c i n i t y of the wal l . The r a t e o f , h e a t b e t we e n a no n - h o mo g e n e o u s f l u i d i z e d on t he t h e r ma l r e ne wa l transfer bed and a wa l l c o n d u c t i v i t y of t hese packets de pe nds and on t h e i r frequency. I t appears a quantity, d e t e r m i n e d more s p e c i f i c a l l y t h e r e n e wa l a c c o r d i n g t o a more c o mp l e t e r e p r e s e n u a ci on o f h y d r o d y n a m i c : p r o c e s s . solid particles is f r e q u e n c y to, t o be I f t h e swarm of assi mi l a t e d to a q u a s i - f l u i d i t is possible t o w r i t e t h e e q u a t i o n o f mo t i o n f o r t h e t wo - pha s e s y s t e m. A vol ume whi c h i s e n c o u n t e r e d h e r e i s s u f f i c i e n t l y s ma l l t o be c o n s i d e r e d as i n f i n i t e l y e nough t o c o n t a i n Ru c k e n s Le i n r e ne wa l a sufficiently s m a l l , but a l s o large l a r g e number o f p a r t i c l e s . ( 24) s u g g e s t e d t h a t a s y n t h e s i s model and t h e linearized instability b e t we e n t h e t h e o r y mi ght be . abl e t o g i v e i n f o r m a t i o n wi t h r e s p e c t t o t h e r e n e wa l quency. The e x p e r i me n t a l , r e s u l t s ( 18) show t h a t fre^. o f Mi c kl e y and F a i r b a n k s w i s i n t h e r a n g e I - 10 s e c ^ and t h a t i t does n o t de pend t o o much on t h e f l u i d i z a t i o n velocity. For -5glass spheres c omput ed t h a t o f 10 ^ me t e r d i a m e t e r R u c k e n s t e i n t h e r e ne wa l ( 24) f r e q u e n c y i s a b o u t 4 s e c ~^ and p r e d i c t e d a weak d e p e n d e n c e of w on v e l o c i t y . ■ -6- Newly P r o p o s e d Bu b b l e - b e d Model Several theoretical i n ' Heat T r a n s f e r me c ha ni s ms o f f l u i d i z e d bed model s ' h a v e been . p r o p o s e d and some of t h o s e have been b r i e f l y s u mma r i z e d by G e n e t t i (8 ) for heat t r a n s f e r in o r d e r to p r o ­ vi de a ba s i s f o r unde r s t a ndi ng c o r r e l a t i o n s presented in his Kuni i whi ch have been r e c e n t wor k. and L e v e n s p i e l (11, 12) have p r o p o s e d a model f o r t h e f l o w of gas t h r o u g h a f l u i d i z e d be d , mo d e l , o r a t h r e e - r e g i o n model the bubble-bed whi ch have vi ewed as uni - f r o ml y s i z e d b u b b l e s s u r r o u n d e d by c l o u d s and f o l l o w e d by wa ke s . A; . s ke t ch o f t h i s model shown t h a t t h i s model i s good enough t o f i t for g a s - s o l i d heat t r a n s f e r , conversion Kuni i in c a t a l y t i c I. They have the repor t ed data g a s - s o l i d mass t r a n s f e r and reactions. and L e v e n s p i e l d e n s e b u b b l i n g r egi on. . i s g i v e n in Fi g . have o n l y been c o n c e r n e d wi t h t h e Th i s r e g i o n a p p l i e s whe r e a c o n t i n u o u s e x c h a n g e o r f l o o wi n g up of s o l i d particles t r a n s fe r surface T h i s c o n c e p t has been is continuing. s o me t i me s e x p l a i n e d on t h e b a s i s ■For t h e b u b b l e p h a s e , Kuni i wi t h s e v e r a l along the heat of t h e " p a c k e f ' t h e o r y and L e v e n s p i e l ( 9). have s t a r t e d n e c e s s a r y a s s u m p t i o n s t o s i m p l i f y t h e pr obl e m f r om t h e Da v i d s o n model (4). They have t a k e n t h e b u b b l e s i z e t o be u n i f o r m t h r o u g h o u t t h e bed o r s e c t i o n o f bed and c a l l e d , it the e f f e c t i v e cr owd o f b u b b l e s bubble s i z e . The v e l o c i t y , o f r i s e of a has been r e l a t e d t o t h e v e l o c i t y o f r i s e of Bubble phase Wake Emulsion phase Fjgure I. S o l i d movement ana gas f l ow as v i s u a l i z e d by b u b b l i n g bed m o d e l . - 8a s i n g l e b u b b l e by umf + u b r " uo + 0 . 7 1 1 ( gd^) % mf U) whe r e Ujjr,. = 0. 711 ( d b ) '2. I g n o r i n g s ma l l bubbl e amount s o f s o l i d s i nsi de the r i s i n g ( me a s u r e d t o be f r om 0 . 2 % t o I % by d i f f e r e n t igators), t h e y have t a k e n t h e . b u b b l e voi d f r a c t i o n The a v e r a g e bed v o i d a g e \n bubbles invest­ Ejj = I . has been r e l a t e d t o t h e v o i d a g e and e mu l s i o n p h a s e by e f = Se fa + ( I - S ) E g = S _+■ ( I - S ) E e whe r e S = t h e vol ume f r a c t i o n By a s s u mi n g E of bubbl es = Emf , v o i d a g e s ( 2) i n t h e bed. and bed h e i g h t s have - been c o r r e l a t e d by 1- s and The b u b b l e p h a s e v a r i a b l e s d b , to give u o ■ 1- mf U jj ( 3) and 6 have been c o r r e l a t e d and u i .e. mf mf 5 1 mf mf For t he- e mu l s i o n : p h a.se ,' Kunid; and- Le v e n s p i:eIo ( 1 1 , 1 2 ) have a s s ume d t h e v o i d f r a c t i o n o f t h e wake t o be t h a t o f t h e e mu l s i o n p h a s e and have c o r r e l a t e d t h e r e l a t i v e v e l o c i t y o f upwar d p e r c o l a t i n g gas, u , and o f downward f l o wi n g s o l i d . - 9- us » the s u p e r f i c i a l u gas v e l o c i t y of minimum f l u i d i z a t i o n “ u s ( 5a) 5' The downward v e l o c i t y o f s o l i d i s g i v e n by aS u^ Us 1- 6 -ctS whe r e a = Var i abl es d ^ , Ufa vol ume o f wake, d r a g g e d up t o t h e bed b e h i n d a r i s i n g b u b b l e ( vol ume o f b u b b l e ) $, ue , and u have been c o r r e l a t e d - t o g i v e uo and um f 3 i ' 6 U b I S ( - a 6 >umf] ' E q u a t i o n 6 has been a p p r o x i m a t e d t o g i v e t he e x p r e s s i o n t h e whol e r a n g e o f f l o w s , and t h e r e s u l t i s identical 6) for to Equat i on 4 uo " ( 1 “ 6 ) u mf S uo umf S ( 7) -10Bed - t o - Wal I Heat T r a n s f e r i n G a s - S o l i d Fl u i d i z e d Beds Much work has been done on b e d - t o - w a l l r o r numer ous h e a t i n g s u r f a c e equations heat t r a n s f e r ar r angement s . Emp i r i c a l have been d e v e l o p e d t o p r e d i c t h e a t t r a n s f e r coefficients Frantz f o r h e a t t r a n s f e r f r om t h e s e s u r f a c e s . ( 7) heat t r a n s f e r has s u mma r i z e d wor k done on s u r f a c e - t o - b e d in f l u i d i z e d beds. numer ous propos ed c o r r e l a t i o n s Genet t i ( 8 ) has d i s c u s s e d and s e v e r a l heat t r a n s f e r me c ha ni s ms f o r f l u i d i z e d bed h e a t t r a n s f e r . Us u a l l y f l u i d i z e d s y s t e ms have low enough a b s o l u t e t emperatures so t h a t t h e r ma l c o u n t e d as a s i g n i f i c a n t i n many m e t a l l u r g i c a l techniques contributing applications r e c e n t l y have s t u d i e d b e d - t o - w a l l a r e s u f f i c i e n t l y hi gh S z e k e l e y and F i s h e r radiation of t he st udy of b e d - t o - wa l l the convect i ve Ho we v e r , r a d i a t i o n may be an i m p o r t a n t p a r t o f t h e heat t r a n s f e r process. on t h e b a s i s factor. o f t h e f l u i d i z e d bed the processing t emper at ur es so t h a t t h e r ma l over-all r a d i a t i o n may be s a f e l y d i s ­ ( 25) heat t r a n s f e r heat t r a n s f e r in r e g i me done by B o t t e r i 11 and e t a I (2). Whi l e none o f t h e propos ed mec hani s ms has been s u f ­ ficient to p r e d i c t heat t r a n s f e r c o e f f i c i e n t s different situations encountered, f o r many v a r i o u s me c ha ni s ms e x p l a i n i n g t h e hi gh r a t e s o f h e a t t r a n s f e r b e t we e n ■- .. -11e x c h a n g e r w a l l s and f l u i d i z e d can be c l a s s i f i e d (I) beds have been s u g g e s t e d , and as f o l l o w s : van He er de n e t a I ( 10) and Wi cke and P e t t i n g t h e f l u i d i z i n g medium ( g a s ) and t h e s o l i d s fluidized Therefore, a c t e d as a s t i r r i n g t r a n s p o r t e d mos t o f t h e h e a t , bed was v i s u a l i z e d there (32): as wel l stirred agent and t he liquid. is the s t e a dy s t a t e conduct i on t hrough t h e e mu l s i o n p h a s e . (.2) Leva e t a I ( 1 5 ) , Wal t o n (16): Dow and J a k o b (5) and L e v e n s p i e l and t h e s c o u r i n g a c t i o n of t h e s o l i d s a l o n g t h e h e a t e x c h a n g e r wal l r e duc e s t h e t h i c k n e s s l a m i n a r gas f i l m and i n c r e a s e s of t h e t he r a t e of he a t transfer. (3) , Mi c kl e y and F a i r b a n k s (18): t h e f l u i d i z e d .bed was as s umed t o be composed o f " p a c k e t s " whi ch renewed i n t e r ­ m i t t e n t l y by t h e v i o l e n t d i s t u r b a n c e of t he f l u i d i z e d bed, in t he core p o r t i o n and wher e u n s t e a d y - s t a t e d i f f u s i o n o f h e a t to newl y a r r i v e d mo b i l e e l e me n t s o c c u r r e d . ( 4) Z i e g l e r e t a I ( 34) and B o t t e r i l I and Wi l l i a ms u n s t e a d y - s t a t e c o n d u c t i o n by s i n g l e p a r t i c l e s c o n t a c t wi t h h e a t e xchange r w a l l s . been f u r t h e r mo d i f i e d by Genettf= Th i s model (2): in d i r e c t has ( 8 ) t o g i v e more c o mp l e t e p r e d i c t i o n s wi t h r e s p e c t t o e x p e r i m e n t a l da t a . - -12Th i s m o d i f i e d model The r e s u l t s facts. i s a d o p t e d i n t h e p r e s e n t wor k. o f t h i s model p r e d i c t two e s t a b l i s h e d The N u s s e l t number i s c o n d u c t i v i t y of t he s o l i d s i n d e p e n d e n t o f t he r ma l (19,34) and i s p r o p o r t i o n a l to a bout t he s q u a r e r o o t of t he p a r t i c l e f r a c t i o n , I - c (20). The r e s u l t s o f t h e model also predict a maximum N u s s e l t n u mb e r , whi ch a l s o i s an e s t a b l i s h e d fact (15),.'' -13- 1. A R a t h e r Di f f e r e n t Bed Model E x p i a n a t i on A c c o r d i nq t o t h e Bubbl e Y o s h i d a 1 K u n i i 1 and L e v e n s p i e l ( 33) have t r i e d t h e me c ha ni s ms p r o p o s e d by Mi c k l e y and F a i r b a n k s van h e e r d e n e t a I ( 10) and Wi cke and P e t t i n g a p p l i e d t h e bubbl e, model transfer. However , to p o s t u l a t e They have s t a r t e d film-penetration transfer^ this I and have and some of not we l l - k n o wn . t h e o r y f o r gas a b s o r p t i o n i n t o l i q u i d s (26). The e q u a t i o n whi ch f i l m - p e n e t r a t i o n model f o r mass and h e a t is 3 T 3 T wher e (32), t h e p r e d i c t i o n of t h e b a s i s of t h e p r o p o s e d by Toor and Ma r c h e l l o represents ( I S ) 1 and b e d - t o - w a 11 h e a t t h e wor k i s n o t c o m p l e t e , t he q u a n t i t a t i v e par amet er s are s t i l l to uni fy 3.2T ________ Pe ^p s O— < x — < Ie /e pS^ps ^ ^ - s ITif ) = eff ect ive thickness o f e mu l s i o n l a y e r . I '' A.- t h i n l a y e r o f e mu l s i o n o f t h i c k n e s s I ^ s u d d e n l y c o n ­ t a c t s t h e e x c h a n g e r wa l l and a f t e r a s h o r t t i me i t i s s u d d e n ­ l y moved away t o r e p l a c e a f r e s h e l e me n t o f e mu l s i o n fr om t h e c o r e p o r t i o n o f t h e b e d . T h e r e f o r e i t wi l l i n c l u d e t h e s t e a d y s t a t e c o n d u c t i o n o f h e a t t h r o u g h an e mu l s i o n l a y e r a t t h e wa l l and t h e u n s t e a d y s t a t e a b s o r p t i o n of h e a t by e mu l s i o n el eme-nts . -14And b o u n d a r y c o n d i t i o n s are T - Tb at t = 0 Ii X CU T = Tb at II X T = . Tw a t 0 The s o l u t i o n o f t h e above e q u a t i o n V V Tb sin nrr(l-x/l ) -------— exp ( - n 2Tr2- J - I - ) nf e n+ 1 t 2 z t- D n=I From t h e above s o l u t i o n , fer coefficient the i n s t a n t a n e o u s local ( 9) heat t r a n s ­ i s f ound t o be 1/ 2 r ke Pe ^ps ti is oo I + 2 Trt 2 "I 2 z exp(-n at n=I e " ■n Tr PO I + 2 PO -n . a t' I e The o b s e r v e d c o e f f i c i e n t o f h e a t t r a n s f e r h a ve r a ge d v a l ue of t he i n s t a n t a n e o u s W ( 10) and t h a t is i s t h e t i me coefficient, g i v e n by ht h t l - I (: t ) d t ( T l ) o whe r e I ( t ) = t h e age d i s t r i b u t i o n e l e me n t s on t h e s u r f a c e . f u n c t i o n o f e mu l s i o n I -15Two t y p e s o f age d i s t r i b u t i o n Case I . r ene wa l . r andom s u r f a c e r e n e w a l , and Case 2 . A number o f e x p r e s s i o n s transfer coefficients, the d i f f e r e n t bubbl e f l ow, uniform s u r f a c e f o r t he obser ved heat hw> have been d e r i v e d a c c o r d i n g t o criterions. The b u b b l i n g bed model st r eams. f u n c t i o n s have been c o n s i d e r e d : g i v e s a s i mp l e r e p r e s e n t a t i o n o f t h e e mu l s i o n f l o w and t h e i n t e r a c t i o n of t h e s e However , two e m p i r i c a l e x p r e s s i o n s whi ch have been r e p o r t e d by Wen and Leva ( 31) and Wender and Cooper ( 3 0 ) . are u s u a l l y recommended f o r t he d e s i g n o f t he b e d - t o - w a l l ' heat t r a n s f e r . 2. Some ^ n e r a l i z e d De s i gn Equat i ons f o r Wa l l - t o - Be d Heat Transfer B e d - t o - e x t e r i o r wa l l Wen and Leva ( 31) heat t r a n s f e r : a t t e mpt e d t o c o r r e l a t e some e a r l i e r o b s e r v a t i o n s o f s o l i d s mo t i o n i n t h e bed wi t h h e a t t r a n s f e r phenomena t h r o u g h a b o u n d a r y l a y e r . the c h i e f r e s i s t a n c e wa l l They.considered t hat t o heat e x c h a n g e bet ween a c o n t a i n i n g and a f l u i d i z e d bed i s i n t h e l a mi n a r f i l m a t t he vessel boundary. The t h i c k n e s s o f t h e f i l m i s t he v e l o c i t y of p a r t i c l e s a l o n g t h e wal l t he " s c o u r i ng act i on; ' o f t he p a r t i c l e s . o f p l o t t i n g and c r o s s p l o t t i n g , i n f l u e n c e d by p a r i m a r i l y due t o By t he usual method t h e f o l l o w i n g r e l a t i o n was -16o b t a i ned': hd k P V R whe r e n = t h e f l u i d i z a t i o n efficient R = t h e bed e x p a n s i o n r a t i o . Nomogr aphi c s o l u t i o n s g i v e n i n App e n d i x I I . ‘:Of t h e d i m e n s i o n l e s s f o r e v a l u a t i o n o f rj and R have been Wender and Cooper ( 30) made a c u r v e gr oup Y/F wi t h t h e p a r i Cl e Re ynol ds number as shown i n F i g u r e 2 wi t h f i v e d a t a s e t s included. The t e r m Y and F a r e d e f i n e d a s : ( 13) F= I + 7 . Se - 0 . 4 4 Be d - t o - ' i n t e r i o r wa l l ( 14) heat t r a n s f e r : I n t e r n a l , v e r t i c a l - t u b e h e a t t r a n s f e r was f o u n d t o be i ndependent of t ube l e n g t h , size di stribution. particle s ha pe and p a r t i c l e Wender and Cooper (30) made a s t r a i g h t l i n e p l o t o f t h e d i me n s i o n a l Z/ CR gr oup wi t h t h e p a r t i c l e Re ynol ds number as shown i n F i g u r e 3 wi t h s i x d a t a s e t s i nc l ude d f o r the i n t e r n a l The t e r m Z i s d e f i n e d a s : vertical heat t r a n s f e r s u r f a c e . -17- Z = ( 15) ( l - e ) ( C s / C g ) 0 - 80 The t e r m a l l o ws (p s / p g ) ° - 66 for non-axial t u b e l o c a t i o n and may be e v a l u a t e d f r om F i g u r e 4 whi ch o r i g i n a l l y was g i v e n by Vr e e d e n b e r g ( (28). The e q u a t i o n o f t h i s 0. 43 k[Ir*] -)(- 0. 33Cp(- -) c g pg Noe and Knudsen ( 2 2 ) f r om a v e r t i c a l tube i n a f l u i d i z e d bed. Th i s ly d i f f e r e n t 8°(^)(16) g have made a s t u d y o f h e a t t r a n s f e r tubes T h e i r d a t a was compar ed t o t h e c o r r e l a t i o n ( 30) t h e i r e xper i ment al correlation. \0.23C. } ( r 1- is: l o c a t e d in a bundl e of v e r t i c a l o f Wender and Cooper all V correlation u s i n g a v a l u e o f Cr = 2 . Al most d a t a was w i t h i n + 50 p e r c e n t o f t h e i s f a i r a g r e e me n t c o n s i d e r i n g t h e g r e a t ­ geomet r i es. I mme r s e d , horizontal-tube h e a t t r a n s f e r has been s t u d i e d by Vreedenberg ( 29) a l o n g wi t h t h e e f f e c t o f t u b e diameter, particle size, shape, and d e n s i t y , c i t y on t h e h e a t t r a n s f e r c o e f f i c i e n t , large-scale beds. and gas . v e l o ­ i n c l u d i n g d a t a on The r ecommended c o r r e l a t i o n s are: -18- 0005 °.01 0.1 R I 10 F i g u r e 2. C o r r e l a t i o n f o r h e a t t r a n s f e r bet ween c o n t a i n i n g wal l f l u i d i z e d bed. and 100 ) ------------------------------------ -- SX-? a , X -- (f * ' T x " :.;. ^ -------------- X r » A > - V i ^ -::A A ‘“ v ^ a -6 1 r a l:x » - .............. C r % , lx^p F i g u r e 3. .> x - (Z/CR)X10 s zX C o r r e l a t i o n f o r h e a t t r a n s f e r be t wee n i n t e r n a l * t u b e s and bed -20- Center of vessel DIMENSIONLESS C o r r e c t i o n f a c t o r Cr POSITION Fi gure 4 for nonaxial l o c a t i o n of i mmer sed t u b e s V2 I T V t i 0.66 (-T-M.)0 ' 3 g. 0.44 ( dt i ; pq uo ) ( ps 07) - )( - f o r Re y n o l d s number l e s s t h a n 2 , 0 0 0 , and hwdt i 420 '( c PSp ) ° - 3 kg 0. 3 ( d t i p q llo j j pg ) ( ■ 0 8) d'P- ' p"s ^ g ■) f o r Re ynol ds number g r e a t e r t h a n 2 , 5 0 0 . Petrie, F r e e b y , and Buckham ( 28) relation best f i t t i n g have p r o p o s e d t h e c o r ­ I CPP1. dat a f o r h e a t t r a n s f e r from t h e v a r i o u s non- . f i nned m u l t i p l e h o r i z o n t a l f l u i d i z e d bed h e a t e x c h a ng e r . Nu. G 14(- ( P r ) 1/ ^ tube bundl es in t he Th a t i s Dj ^)2/3 09) 3ITlf The e x p e r i m e n t a l d a t a shows a maximum d e v i a t i o n o f 64 p e r ­ c e n t f r om V r e e d e n b e r g 1s c o r r e l a t i o n , t h e dat a b e t t e r . However , t h e a g r e e me n t o f t h e p r o p o s e d d a t a wi t h V r e e d e n b e r g ' s c o r r e l a t i o n a single wh i l e E q u a t i o n 19 f i t s tube is good. f or heat t r a n s f e r to T h e i r d a t a i s shown i n F i g u r e 5 . The At omi c Ener gy Co mmi s s i o n ' s cessing plant. I daho Chemi cal Pr o- 1000 800 600 (GDtyL y V f s / l ) 0.03 F i g u r e 5. 0.10 ICPP m u l t i p l e - t u b e d a t a compar ed wi t h V r e e d e n b e r g 1s c o r r e l a t i o n . -23- 3. C o r r e l a t i o n Model , Used i n Th i s Wor k, For Wal I - t o - Be d Heat T r a n s f e r The model initially s u g g e s t e d by Z i e g l e r e t a I (34) and B o t t e r i 11 and Wi I Ltams ( 2) f u r t h e r e x t e n d e d by Ge n e t t i ( 8 ) i s mo d i f i e d in t h i s and Br aze I t on ( 34) fer coefficients present study. Ziegler, Koppel , showed t h a t t h e w a l I - t o - b e d h e a t t r a n s ­ v a r i e d wi t h s o l i d h e a t c a p a c i t y , was i n d e p e n d e n t o f s o l i d t h e r ma l conductivity, C , but Ps k . A p a r t i c l e whi c h has been i n t h e b u l k medi um i s vi ewed t o move a d j a c e n t t o t h e wa l l s u r f a c e wher e t h e p a r t i c l e s u d d e n l y b a t h e d by t h e f l u i d a d j a c e n t t o t h e wa l l wa l l t emperature. In t h e mean t i me t h e p a r t i c l e h e a t by c o n v e c t i o n f r om t h e f l u i d a t t he receives adj a ce nt to the w a l l . A f t e r s ome t i me t h e p a r t i c l e leaves t h e b u l k f l u i d i z e d medi um. The ma j o r p o r t i o n o f h e a t t r a n s f e r is several is t h e wal l a s s ume d t o o c c u r by t h i s and r e t u r n s mec hani s m. to With a s s umpt i ons t he boundary probl em d e s c r i b i n g t he t emper a t ur e p r o f i l e , T ( r , 8 ), j a c e n t t o t h e wa l l i n a p a r t i c l e wh i l e i t is solved. is ad­ The t i me a v e r a g e d h e a t f l u x i s o b t a i n e d as: (20) (H * |_ ) 2 where 8= the average contact time In o r d e r t o g e t t h e e x p r e s s i o n f o r t h e h e a t t r a n s f e r f l u x b a s e d on t h e wa l l surface surface, per u n i t area wi l l of p a r t i c l e s particle fraction, to have t o be d e r i v e d . p e r u n i t a r e a , Yp » w i l l (I - e )0' 48. at the The number be r e l a t e d t o t h e I - e , and t h e p a r t i c l e d i a me t e r . heat t r a n s f e r c o e f f i c i e n t portional t h e number o f p a r t i c l e s The has been c a l c u l a t e d t o be p r o ­ A relation o f t h e f o l l o w i n g f or m is proposed: (21 For a c o m p l e t e l y c o v e r e d s u r f a c e wi t h h e x a g o n a l Yp , and I - e packing. are ( e = 1 4/ 27 22) ( 23) Therefore K1 = I . 59 ( 24) and (25) ) By s u b s t i t u t i n g E q u a t i o n 24 and Equat i on 25 i n t o E q u a t i o n 2 1 , . we can g e t t h e f o l l o w i n g e x p r e s s i o n f o r T . 59 ( I - e ) 0. 48 Y, : ( 26) By m u l t i p l y i n g q p by Ypj we can w r i t e an e q u a t i o n f o r 1P ^ ' P t h e h e a t f l u x f r om t h e wa l l s u r f a c e : S 1Q O - O 0 - ^ k n (Tw- T h ) -(27] 9 = YpSp 6k vi The p a r t i c l e + 8 ^ p )2 N u s s e l t number i s 5 ( l - e ) 0.48 Nu ( 28) 6k 8 r.) ( 1 +- p Sc Sd P1 Wi t h t h e a i d o f d i me n s i o n a l a n a l y s i s Ge n e t t i duced t h e f o l l o w i n g . e q u a t i o n f o r 1/ 2 97 By s u b s t i t u t i n g E q u a t i o n 28, d, g" ( 8 ) has i n t r o ­ ■ (-V ) 4 / 3 as e x p r e s s e d i n Eq u a t i o n 29, the f ol l owi ng c o r r e l a t i o n number s can be o b t a i n e d : ( 29) into f or aver age Nus sel t ■“ 2 6 - 5 ( ^ n - f e ) 0 - 48 'Nu. P I + 580 Re (- )(- Most o f t h e d a t a c a l c u l a t e d wi t h t h e c o a r s e g l a s s ( 30) -J1 - P A f ) 4 / 3 ' 2 by G e n e t t i for f l u i di za t i on s p h e r e s and t h e al umi num p a r t i c l e s are w i t h i n +20 p e r c e n t of E q u a t i o n 30. Ki dd ( 14) has s t u d i e d h e a t t r a n s f e r and p r e s s u r e dr op f o r n i t r o g e n f l o wi n g i n t u b e s c o n t a i n i n g t w i s t e d t a p e s and has i n t r o d u c e d t w i s t r a t i o Y. T wi s t r a t i o Y has been d e f i n e d as t h e number o f t u b e d i a m e t e r p e r 180° t w i s t . About t h e c o n s t a n t of E q u a t i o n 28 as a r e s u l t of several a s s umpt i ons Ge n e t t i generalization ( 8 ) has r e p o r t e d 5. For E q u a t i o n 28 can be r e w r i t t e n : Ci(l-e)0' 1Nu „ = ( 31) — ( 1+ - 9 - ^ P^C^dp' -)■ 6k e The d i m e n s i o n l e s s gr oup ----- g d 2 ps s p r e l a t e d to the fol l owi ng v a r i a b l e s : 'I. v mass v e l o c i t y G 2. p a r t i c l e d i a m e t e r d^ 3. twist ratio Y 4. gas v i s c o s i t y u i n E q u a t i o n 31 can be . - 21 Wi t h t h e a i d of d i me n s i o n a l less - analysis t he f o l l o wi n g d i me n s i o n ­ g r oup can be o b t a i n e d : (-Izl-). Y. H Wi t h t h e s e g r o u p s an e q u a t i o n o f t h e f o l l o w i n g f or m f o r t h e 6 k_6" di mensi onl es s -i s o b t a i ned : gr oup - S c Sd P 6f % = P5 = Sd P2 1 ( 32) — M= C ( ■ 2 Substituting 2 ' E q u a t i o n 32 i n t o E q u a t i o n 31, the f ol l owi ng is obtained: C1 ( V e ) % 0.48 Co ( Y-I I + ( 33) \bl2 E x p e r i me n t a l The e x p e r i m e n t a l Ap p a r a t u s e q u i p me n t o f t h e p r e s e n t investigation was d e s i g n e d and a s s e mb l e d i n o r d e r t h a t : t h e s t u d y o f l o c a l and a v e r a g e h e a t t r a n s f e r c o e f f i c i e n t s fluidized c o u l d be made i n a bed t u b u l a r h e a t e x c h a n g e r wher e an e l e c t r i c a l l y h e a t e d bundl e of v e r t i c l e t u b e s wer e s y m m e t r i c a l l y p l a c e d . Some o f t h e e q u i p me n t c omp o n e n t s us e d i n t h i s wer e us e d i n a p r e v i o u s p r e s e n t study s t u d y u n d e r t a k e n by G e n e t t i The ma j o r i t e ms o f e q u i p me n t a r e a model e x c h a n g e r , an a i r b l o w e r , an e l e c t r i c a l s o u r c e , a n d . . me a s u r i n g d e v i c e s . fluidized ( 8 ). bed h e a t s y s t e m and power The me a s u r i n g d e v i c e s include m a n o m e t e r s , t h e r m o c o u p l e s and a p r e c i s i o n p o t e n t i o m e t e r . general A f l o w d i a g r a m o f t h e e q u i p me n t i s shown i n F i g u r e 6 and a p h o t o g r a p h of t h e e q u i p me n t i s shown i n F i g u r e 7 ( A) . 1. S i l e n c e r 2. Compressor 3. D r a i n 4 . S h u t off v a lv e 5.O rific e m e te r 6. Experimental t u b e 7. D i s e n g a g i n g s e c t i o n 8. D ist ri b u t i o n s e c t i o n Tem p e r a t u re probe handle T : T e m p e r a t u re p r o b e R: P r e s s u r e t a p H e a t i ng element © . r Ex h a u s t P° rf © Tubes inside t t Fi gure 6 . Flow d i a g r a m of t h e f l u i d i z i n g a p p a r a t u s . -30- T jre' E x p e r i me n t a l The e x p e r i m e n t a l vertical h e a t e x c h a n g e r col umn c o n s i s t e d o f a t ube bundl e c o n t a i n i n g The E x p e r i me n t a l shell Heat Ex c h a n g e r Column was c o n s t r u c t e d distributing section, Shel l : h e a t i n g e l e me n t s and a s h e l l . The o u t s i d e o f t h e e x p e r i m e n t a l in t h r e e s e c t i o n s , t he e xpe r i me nt a l t he c o n i c a l section, air the d i s e n ­ gaging s e c t i o n . The c o n i c a l air distributing section is a t t a c h e d at the l o we r p a r t o f t h e col umn t o e xpand t h e a i r f l o w f r om t h e p i p e d i a m e t e r t o t h e col umn d i a m e t e r . A i ron-constantan t h e r m o c o u p l e was i n s e r t e d t h r o u g h t h e wal l t o me a s u r e t h e a i r inlet The e x p e r i m e n t a l of t h i s section temperature. s e c t i o n was c o n s t r u c t e d f r om t h e 6 - i n c h OD and 4 4 - i n c h l ong c a s t a c r y l i c t u b e wi t h t h e 1/ 4 i nch t h i c k wa l l . El e v e n i r o n - c o n s t a n t a n t h e r mo c o u p l e s wer e i n s e r t e d t h r o u g h t h e wa l l shown i n F i g u r e 6 . screen shields a i r only: wa l l of t h i s e xpe r i me nt a l The t h e r m o c o u p l e s a r e p r o t e c t e d by i n o r d e r t o g i v e c o n t a c t wi t h t h e f l u i d i z i n g El e v e n p r e s s u r e t a p s a r e a l s o p l a c e d of t h i s col umn as e xpe r i me nt a l i n t he col umn as shown i n F i g u r e 6 . Th e s e pr essure taps have f i n e s c r e e n c o v e r s s o l d e r e d on t o p r e v e n t the f l u i d i z e d particles f r om r u n n i n g i n t o t h e t a p s . The d i s e n g a g i n g s e c t i o n was c o n s t r u c t e d f r om t h e 9 - i n c h -31 - (A) F i g u r e 7. (A) Ge n e r a l e q u i p me n t (B) Gl a s s p a r t i c l e s -32- OD and 1 2 - i n c h l ong c a s t a c r y l i c thick wall. t u b e wi t h t h e 1 / 4 - i nch Four h o l e s , I 1 / 2 - i n c h i n d i a m e t e r , wer e d r i l l ­ ed i n t h e wa l l o f t h e d i s e n g a g i n g s e c t i o n I 1/ 2 - i n c h e s f r om t he top to l e t the f l u i d i z i n g air escape. The s e h o l e s wer e c o v e r e d wi t h f i n e mesh s c r e e n t o p r e v e n t t h e h i g h l y f l u i d ­ ized p a r t i c l e s f r om b e i n g bl own o u t o f t h e c ol umn. One h o l e , i n c h i n d i a me t e r , , was made i n t h e t o p p l a t e whi c h i s c o v e r i n g the di sengagi ng s e c t i o n , to put t he p a r t i c l e s and t h a t h o l e was o c c a s i o n a l l y us ed i n t o t h e bed and t o bl ow o u t t h e u n ­ necessary p a r t i c l e s f r om t h e b e d . An a l u m e l - c hr ome ! c o u p l e was i n s e r t e d t h r o u g h t h e wa l l t h e r mo ­ of t he d i s e n g a g i n g s e c t i o n .to me a s u r e t h e a i r o u t l e t t e m p e r a t u r e . The Tube Bundl e wi t h t h e He a t i n g E l e m e n t s : b u n d l e i s 6 0 - i n c h l ong and c o n s i s t s less steel The t ube o f n i n e t e e n 321 s t a i n ­ t u b e s 3 / 4 - i n c h OD wi t h 0 . 0 1 2 - i nc h t h i c k a r r a n g e d in I -inch t r i a n g u l a r shown i n F i g u r e 7. pitch. The c o mp l e t e t u b e l a y o u t i s The 3 / 1 6 - i n c h s t a i n l e s s steel wi r e has been wr a ppe d a r o u n d t h e o u t s i d e o f eac h t u b e i n a h e l i c a l spiral. A f t e r e x a mi n i n g t h e e f f e c t of t h e f i r s t wi r e as an ext ended s u r f a c e , the second, the t h i r d , and t h e f o u r t h wi r e was wr a p p e d a r o u n d eac h t u b e t o s e e t h e g r a d u a l wal I - vt o - b e d h e a t t r a n s f e r . E x p e r i me n t a l Pr ogr a m. The d e t a i l s wi l l i n c r e a s e in be e x p l a i n e d i n One end of e a c h - t ube' , e x c e p t t h e >-33he a t i n g t u b e s , was f i t t e d wi t h a p l a s t i c fitting i n t o t h e l o we r t u b e s h e e t . The h e a t i n g t u b e s • (4 t u b e s as shown i n F i g u r e 8 ) a r e f i t t e d wi t h c o p p e r e l e c t r o d e s top e l e c t r o d e pl ug t o f a c i l i a t e on t h e t op and t h e b o t t o m. has a p o r c e l a i n t u b e i n s e r t e d i n i t The to prevent c o n t a c t b e t we e n t h e e l e c t r o d e and t h e al umi num t u b e h o u s i n g the l eads faciliated i n s i d e the h e a t i ng t u b e . to f i t The bot t om e l e c t r o d e is i n t o t h e l o we r t u b e s h e e t and has a 1/ 4 - i n c h h o l e t o . a c c e p t a No. 10 c o p p e r wi r e us ed as a power lead. The b o t t o m t u b e s h e e t i s made o f a p e r f o r a t e d s t e e l s h e e t wi t h a 200 mesh wi r e s c r e e n we l de d t o i t t h e movi ng p a r t i c l e s section. to prevent f r om r u n n i n g o u t f r om t h e e x p e r i me n t a l The h e a t i n g t u b e s a r e i n s u l a t e d f r om t h i s sheet wi t h r u b b e r r i n g s . The A i r BI o w e r : air Ai r was s u p p l i e d by a S u t o r b i l t 57-TP b l o we r d r i v e n by a 1 750 RPM, 7 1 / 2 HP AC i n d u c t i o n mo t o r . Two and one h a l f inch s t e e l a i r to t he e xpe r i me nt a l p i p e was used t o t r a n s p o r t t h e heat exchanger. The 2 1 / 2 - i n c h p i p e was r e d u c e d t o two i n c h e s b e f o r e e n t e r i n g t h e a i r section. intake The a i r f l o w r a t e was c o n t r o l l e d by two g a t e v a l v e s . On e , a t w o - i n c h - b y - p a s s valve, c o n t r o l l e d t h e a i r f l o wi n g t hr ough a by- pas s t o t he a t mo s p h e r e . The. ot her control -34- . Fi gure 8 . Tube l a y o u t : e l e me n t . : ' • : s howi ng l o c a t i o n s of h e a t i n g v a l v e was i n t h e 2 1 / 2 - i n c h a i r s u p p l y l i n e . was me t e r e d by a s h a r p - e d g e d o r i f i c e The a i r f l ow located i n t h e mi d d l e o f t he a i r s uppl y l i n e . The ETec t'r i c Sys t em and Power S o u r c e : A voltage t r a n s ­ f o r me r was us e d t o s u pp l y e n e r g y t o t h e wi r e wr a ppe d s t a i n ­ less steel circuit heating tubes. A di agr am of t he e l e c t r i c a l i s shown i n F i g u r e 9. The r e s i s t a n c e in the c i r c u i t was a d j u s t e d so t h a t t h e c u r r e n t was a b o u t 48 amps. The emf and c u r r e n t wer e me a s u r e d by an AC v o l t m e t e r wi t h a r a n g e o f z e r o t o 15 v o l t s z e r o t o 50 amps . and an AC ammet er wi t h a r a n g e of H e a t in g tubes Constant vo l t a g e tranform er -36- A : Ammeter V Volmeter No. 10 Copper w ire No.10 / Copper wire F i g u r e 9. Di agr am of e l e c t r i c a l circuit. -37- Me a s u r i n q De v i c e s s u r e : The U- t u b e ma nome t e r s have been us ed t o me a s u r e t h e p r e s s u r e drop a c r o s s t h e bed and an i n c l i n e d ( an a n g l e o f 30° ) U- t u b e ma nome t e r has been us e d t o me a s u r e t he p r e s s u r e dr op a c r o s s t h e s h a r p - e d g e d o r i f i c e me t e r . A c o l o r e d manometer f l u i d wi t h a d e n s i t y o f 1 . 0 0 gm/ cm3 was used . T e mp e r a t u r e : tubes The wal l t e mp e r a t u r e of t h e h e a t i n g (4 t u b e s as shown i n F i g u r e 8 ) wer e measured u s i n g c h r o me ! - a l u me l t her mocoupl e s . The t h e r mo c o u p l e . p r o b e was d e s i g n e d t o move up and. down t h e h e a t i n g t u b e . manner wa l l t u b e wal l temperatures at various posi t i ons wer e m e a s u r e d . In t h i s i n s i d e t he Two i n s u l a t e d t he r mo c o up l e s wer e r un t h r o u g h t h e p r o b e c a s i n g whi ch r ounde d t o t h e s ha pe of t he t u b e w a l l , and b o t h wer e embedded i n two c oppe r c o n t a c t . Each copper c o n t a c t was h e l d a g a i n s t t h e i n s i d e t u b e wal l wi t h a s p r i n g . The p r o b e a s s e mb l y i s shown i n F i g u r e 10. ly ment i oned, e l e v e n i r o n - c o n s t a n t a n t he r mo c o upl e s were i n s e r t e d t h r o u g h t h e wa l l of t he e x p e r i me n t a l me a s ur e t h e bed t e m p e r a t u r e s . a c h r o me l - a l u me l : col umn t o An i r o n - c o n s t a n t a n t h e r mo ­ c o u p l e was p l a c e d i n s i d e the a i r d i s t r i b u t i n g ■■ ■ .i : As p r e v i o u s ­ s e c t i o n and t h e r mo c o u p l e was p u t i n t o t h e mi d d l e of v. I .. . - I . .• v 11 ..'e r r . o . u y■ . ■ • -i r- ■■ . . . -38- the di sengagi n s e c t i o n . let and o u t l e t Bot h wer e t o me a s u r e t h e gas temperature. k e p t i n an i c e b a t h a t 3 2 ° F . Al I r e f e r e n c e j u n c t i o n s wer e The t h e r mo c o u p l e emf was r e a d u s i n g a Leeds and No r t h r o p Co. 0381600. A switching t he r moc oupl e c i r c u i t s . in­ p o t e n t i o m e t e r model s y s t e m was u s e d t o c o mp l e t e t h e -39- TOP VIEW Micarta — i Ti. d i a .X "77" i n. Spring -— in.d ia.X -r- in- 16 ^ — in.dia.X -y in - Copper contact 0 . 7 3 8 in. FRONT F i g u r e 10. VIEW Ex pl ode d vi ew of t h e t u b e wal l probe. t emper at ur e -4 .0 - Exper i mental Exper i me nt al Program and Procedure Program: The o b j e c t i v e o f t h i s to de t e r mi ne heat t r a n s f e r c o e f f i c i e n t s study is in a v e r t i c a l l y arranged U n ite d t u b e b u n d l e f o r a i r f l o wi n g t h r o u g h a fluidized steel bed a t v a r i o u s o p e r a t i n g c o n d i t i o n s . The s t a i n l e s s wi r e s wr a ppe d a r o u n d t h e o u t s i d e of each t u b e i n a helical spiral ' have been us ed t o i n c r e a s e t h e r a t e of h e a t transfer. The v a r i a b l e s transier gas; t o be c o n s i d e r e d in g a s - s o l i d f l u i d i z e d d e n s i t y , pg ; v i s c o s i t y , conductivity, density, kg ( 2) properties ps ; s p h e r i t y , city, uq ( 4) static specific heat, of t he s o l i d s : fl ow c o n d i t i o n s : and ( 5) bed h e i g h t , f e r s u r f a c e , type of f i n , Cp s ; properties o f ' C ; t h e r ma l di amet er , velocity, superficial velo- g e o me t r i c p r o p e r t i e s : and h e a t i n g t u b e l o c a t i o n . in t h i s gas v e l o c i t y , study are s t a t i c h e a t i n g t ube l o c a t i o n , and t h e e x t e n d e d s u r f a c e a r e a . He a t f l u x , t u b e wa l l t emperat ure p r o f i l e , b u l k gas t e m p e r a t u r e p r o f i l e d ; ( 3) c o n d i t i o n s t he l engt h of he at t r a n s ­ V a r i a b l e s under c o n s i d e r a t i o n bed h e i g h t s u p e r f i c i a l (I) mi ni mum f l u i d i z a t i o n ; voi d f r a c t i o n , bed d i a m e t e r , beds a r e : specific heat, a t mini mum f l u i d i z a t i o n : um f ; v o i d a Se ’ emf y; in b e d - t o - w a l I heat and v e r t i c a l have been me a s u r e d i n o r d e r t o •r 41 calculate t h e r a t e o f h e a t t r a n s f e r and t o f i n d o u t t h e e f f e c t of t he i n c r e a s i n g s u r f a c e a r e a . Ai r has been us e d as t h e f l u i d i z i n g medi um and o n l y one t u b e b u n d l e c o n f i g u r a t i o n i nch s t a i n l e s s steel has been c o n s i d e r e d . The 3/ 16- wi r e has been us ed as an e x t e n d e d s u r ­ face. Properties solid particle of S o l i d s : Onl y one t y p e and one s i z e of has been us ed i n t h i s study. Co a r s e g l a s s s p h e r e s , m a n u f a c t u r e d by 3M Company, o f 0 . 0 1 8 5 - i n c h a v e r a g e d i a m e t e r wer e u s e d . The d e n s i t y o f g l a s s p a r t i c l e s i s 3 156 I b / f t . A m i c r o p h o t o g r a p h o f t h e p a r t i c l e s ( F i g u r e ; SB) shows t h a t t h e g l a s s particles S t a t i c Bed H e i g h t s : and n i n e i n c h e s are spherical. Static bed h e i g h t s o f f i v e , have been i n v e s t i g a t e d . taken wi t hout p a r t i c l e s ■ seven Dat a wer e a l s o i n o r d e r t o compar e wi t h d a t a r e p o r t e d by Donohue ( 6) and G e n e t t i (8). Static bed h e i g h t s wer e me a s u r e d wi t h a s c a l e whi ch was on t h e e x p e r i m e n t a l h e a t e x c h a n g e r c ol umn. F l u i d Mass V e l o c i t y : was us e d i n t h i s A wi de r a n g e o f gas v e l o c i t i e s s t u d y t o d e t e r m i n e t h e most e f f e c t i v e v e l o c i t y and t o f i n d t h e e f f e c t i v e n e s s o f e x t e n d e d s u r f a c e s as a f u n c t i o n o f gas f l o w r a t e s . He a t i n g Tube L o c a t i o n : Since v e r t i c a l l y ar r anged •,/ .'“ 4 2 f i n n e d t ube l a y o u t i s s y mme t r i c a l as i t i s shown i n F i g u r e 8 o n l y f o u r h e a t i n g t u b e l o c a t i o n s wer e needed t o i n v e s t i g a t e all p o s s i b l e h e a t i n g t ube l o c a t i o n s . t r a n s f e r has been s t u d i e d a t a l l for various static The r a t e o f h e a t f our d i f f e r e n t bed h e i g h t s , g a s velocities locations and t he i n c r e a s i n g ammount o f e x t e n d e d s u r f a c e ( wr a ppe d s t a i n l e s s steel wires). The h e a t i n g t u b e l o c a t i o n s F i g u r e 8, and w i l l tion be r e f e r r e d b y - n u mb e r . i s number ed o n e ; the l o c a t i o n a r e shown in The c e n t e r l o c a ­ h a l f t h e d i s t a n c e from t h e c e n t e r i s number ed two and t h e two o u t e r l o c a t i o n s are number ed t h r e e and f o u r . The h e a t i n g t u b e wa l l eleven p o s i t i o n s were I 1 / 2 . 27 1 / 2 , a l o n g t h e t ub e . 3 1/2, 31 1 / 2 , t u b e t e m p e r a t u r e was me a s u r e d a t 7 1/2, 11 1 / 2 , For a l l f uns t h e l o c a t i o n s 15 1 / 2 , 19 1 / 2 , 23 1 / 2 , 35 1/ 2 and 39 1 / 2 i n c h e s f r om t h e bot t om wer e us e d t o g e t t h e n e c e s s a r y d a t a t o o b t a i n t h e t e m p e r ­ a t u r e p r o f i l e along the t u b e . The s e e l e v e n p o s i t i o n s a r e c o r r e s p o n d i n g p o s i t i o n s o f t h e t h e r mo c o u p l e s whi ch wer e i n s e r t e d t h r o u g h t h e wal l of t he e x p e r i me n t a l col umn t o me a s u r e . t h e . t e m p e r a t u r e s of t h e bed. lir e Type o f FJ_n: The 3 / 1 6 - i n c h s t a i n l e s s , s t e e l ■has been us e d as an e x t e n d e d s u r f a c e . The s t a i n l e s s wi r e steel wi r e has been wr a ppe d a r o u n d t h e o u t s i d e o f e a c h 19 t u b e s r 43r in a h e l i c a l spiral . A f t e r e x a mi n i n g t h e f i r s t the second, the t h i r d , wi r e as an e x t e n d e d s u r f a c e , and t h e f o u r t h wi r e was wr apped around each t ube to see t he gr adual transfer wal I - to-bed heat i n c r e a s e wi t h t h e i n c r e a s i n g amount o f e x t e n d e d surface. For t h e f i r s t w i r e , t he rate of he a t t r a n s f e r wer e me a s u r e d f o r d i f f e r e n t s t a t i c velocities at all different bed h e i g h t s and gas h e a t i n g t ube l o c a t i o n s . same pr oc e dur e was us e d f o r t h e s e c o n d , t h e t h i r d , f o u r t h wi r e. and t h e The f o l l o w i n g c h a r t shows t h e c o mp l e t e pr ogr a m o f t h i s various s t a t i c The study at d i f f e r e n t bed h e i g h t s , heating l ocati ons gas v e l o c i t i e s i ng amount o f e x t e n d e d s u r f a c e . for and t h e i n c r e a s ­ -44- Ta b l e I No . o f FBH No. of Wi re SBH 5" SBH 7" SBH 9" Wl w2 I w3 w4 wl w2 w3 w4 2 i Wl w2 w3 3 w4 wl w2 w3 4 w4 wI = one e x t e n d e d s u r f a c e w3 = t h r e e e x t e n d e d s u r f a c e s w2 - two e x t e n d e d s u r f a c e s w4 = f o u r e x t e n d e d s u r f a c e s SBH = s t a t i c bed h e i g h t FBH = f l u i d i z e d 1 = slightly 2 = fairly 3 . = we l l bed h e i g h t fluidized fluidized fluidized 4 = highly f l u i d i z e d ( a b o v e minimum f l u i d i z a t i o n ) ••-41Ex p e r i m e n t a l The f o l l o w i n g r o u t i n e pr ocedur e is f ol l owed bef or e maki ng eac h e x p e r i m e n t a l 1. Procedure run: The d e s i r e d amount o f g l a s s in t he e xpe r i me nt a l and t h e c o n t r o l f l ow r a t e . c o l u mn ’. gate valves particles is placed The a i r b l o we r i s t u r n e d o n 3 i s a d j u s t e d t o g i v e t he d e s i r e d The d e s i r e d f l u i d i z e d bed h e i g h t is obtained by a d j u s t i n g t h e c o r r e c t o p e n i n g s f o r t h e s e two c o n t r o l valves. The v a l v e s a r e t i g h t e n e d t o m a i n t a i n t h e c o n s t a n t fl ow r a t e d u r i n g t he e x p e r i me n t a l 2. The power s u p p l y i s in the e l e c t r i c wi l l circuit period. t u r n e d on. The r e s i s t a n c e i s a d j u s t e d so t h a t t h e c u r r e n t be a b o u t - 4 6 - 5 0 a mpe r es and t h e v o l t a g e a b o u t 7 . 8 - 8 .6 v o l t s . 3. A t hermos f l a s k i s f i l l e d wi t h c r u s h e d i c e and wat er . The t h e r mo c o u p l e r e f e r e n c e j u n c t i o n s is pl aced in t h e f l a s k t o g i v e a r e f e r e n c e t e m p e r a t u r e o f 32° F. 4. ternal The p o t e n t i o m e t e r i s b a l a n c e d a g a i n s t an i n standard c e l l . 5. to t h e i r 6. t u b e wa l l The t u b e wa l l initial p r o b e t h e r mo c o u p l e s have been s e t positions. When s t e a d y s t a t e has been o b s e r v e d i n regard to t e m p e r a t u r e e mf s , t h e r e c o r d i n g o f d a t a i s begun -46The i o i l owi ng p r o c e d u r e has been used i n r e c o r d i n g t h e necessary data: 1. The v o l t a g e and c u r r e n t f r om t h e power s u p p l y a r e me a s u r e d wi t h an AC v o l t m e t e r and an AC a mme t e r . s u r e dr op a c r o s s t h e m e t e r i n g o r i f i c e The p r e s ­ i s me a s u r e d wi t h a w a t e r ma n o me t e r . 2. The t u b e wa l l wi t h a p o t e n t i o m e t e r . p r o b e t h e r mo c o u p l e emf i s me a s u r e d The probe i s t h e n p l a c e d i n t h e s e c o n d p o s i t i o n and t h e p r o b e i s a l l o we d t o a t t a i n state. The same pr oc e dur e i s c o n t i n u e d u n t i l positions 3. Whi l e, t h e p r o b e i s comi ng t o s t e a d y s t a t e gas t e m p e r a t u r e s , bet ween t h e r e ma i n i n g dat a are m e a s u r e d . The gas i n l e t t e mp e r a t u r e , gas o u t l e t t e mp e r a t u r e , 11 b u l k and bed p r e s s u r e drops a r e r e c o r d e d a t 11 t i me i n t e r v a l s 4. 11 p r obe have been m e a s u r e d . p r o b e emf me as ur e me nt s , e qua l all steady d u r i n g t he course of t he r un. The power s u p p l y v o l t a g e and c u r r e n t a r e c he c ke d a g a i n and a v e r a g e d . ■ The o r i f i c e p r e s s u r e dr op i s a l s o c h e c k e d a t t h e end o f t h e r u n . After all t h e data a r e r e c or de d f o r one r u n , t h e e q u i p ­ ment i s t u r n e d o f f , a not he r fun. or t he p r o c e d u r e i s r e p e a t e d a gai n f o r In t h i s m a n n e r , d a t a a r e t a k e n f o r t h e different static bed h e i g h t s , gas f l o w r a t e s , and an i n - ... ■ in ­ c r e a s i n g . amount o f e x t e n d e d s u r f a c e a r e a a t d i f f e r e n t h e a t ­ i ng t u b e l o c a t i o n s . App e n d i x I I I . A typical d a t a s h e e t can be f ound in C a l c u l a t i ons Ihe basi c c a l c u l a t i o n s calculations f r om t h e r mo c o u p l e e m f ' s , d i f f e r e n c e s-s h e a t f l u x , we i ght e d l oc a l transfer a r e gas f l ow r a t e , t e m p e r a t u r e local local heat t r a n s f e r c o e f f i c i e n t s , heat t r a n s f e r c o e f f i c i e n t s , coefficient, above c a l c u l a t e d t emper at ur e and s e c t i o n aver age heat pressure dr ops . d a t a bed s e c t i o n v o i d f r a c t i o n s s e c t i o n average heat t r a n s f e r c o e f f i c i e n t s From t h e and bed have been c a l c u l ­ ated . Al I c a l c u l a t i o n s have been p e r f o r me d wi t h t h e a i d of SDS SIGMA 5/ 7 and HEWLETT-PACKARD 2116B d i g i t a l Sof t war es are l i s t e d us e d a r e B a s i c , Fortran IV and APL. c o mp u t e r s . Al I of t h e s e i n Appe ndi x IV. Co mp u t a t i o n s Us i ng Re a d i n g s : The key emf v a l u e s whi ch b r a c k e t t h e t e m p e r a t u r e range me a s u r e d f o r t h e l o c a l t emperat ure are 1. 52, i ng a f i f t h - o r d e r t h e good f i t results t u b e wa l l 1.98, p o l y n o mi a l 2.45, t e m p e r a t u r e and gas o u t l e t 2.89, 3.36, Pa s s through t hese si x poi nt s gives over t he t e mpe r a t ur e r a n g e . The c a l c u l a t e d have been c ompa r e d with' c a l i b r a t i o n t h e r mo c o u p l e c h r o m e ! - a Iumel and 3 . 8 1 . tables for t h e r m o c o u p l e s i n Appe ndi x V. The key v a l u e s whi c h b r a c k e t t h e t e m p e r a t u r e r a n g e me a s u r e d .•-49- f o r the l ocal bul k f l u i d i z e d bed t e m p e r a t u r e and gas i n l e t t e mp e r a t u r e .ar e 1. 65 , 1. 79 , I . 94, 2.52. 2.23, 2.38, and The f or m o f t h e La g r a n g i an f o r mu l a g i v e n by a s i x t h - o r d e r p o l y n o mi a l t h r o u g h t h e s e 7 p o i n t s g i v e s t h e good f i t over t he t e mpe r a t ur e range. The c a l c u l a t e d r e s u l t s been c ompa r ed wi t h c a l i b r a t i o n t he r moc oupl e s i n App e n d i x V. p o l a t i o n f o r mu l a intervals, tables have for iron-constantan Si nce t he L a g r a n g e ' s i s a p p l i c a b l e f o r e i t h e r e qual the i n t e r p o l a t e d t o any g i v e n E( x) functional inter­ or unequal value corr espondi ng i s g i v e n by T. The b u l k f l u i d i z e d f o r t h e 11 t u b e wa l l ical 2.08, bed t e m p e r a t u r e s a r e c a l c u l a t e d probe p o s i t i o n s met hod d e s c r i b e d a b o v e , a c c o r d i n g t o t h e nume r ­ and t h e n t h e l o c a l t emper at ur e d i f f e r e n c e . i s c a l c u l a t e d f r om t h e f o l l o w i n g e q u a t i o n : AT I oc V ( 34) Tb The h e a t f l u x was c a l c u l a t e d dissipated in t he h e a t i n g e l e me n t . by d e t e r m i n i n g t h e power The p r o d u c t o f t h e me a s u r e d c u r r e n t and v o l t a g e d r o p g i v e s t h e power d i s s i p a t e d i n t h e h e a t i n g e l e me n t and t h e c o n n e c t i n g l e a d s . p r e s s i o n us e d f o r t h e h e a t f l u x t h e e l e c t r i c a l the l eads under c o n s i d e r a t i o n 0.87(1 V - The e x ­ r e s i s t a n c e of is: 0.03122 r ) (35). .-50- The l o c a l heat t r a n s f e r c o e f f i c i e n t i s c a l c u l a t e d f r om the f ol l owi ng e q u at i on: ( 36) h I oc = 9 / ATl o c The e q u a t i o n us e d t o c a l c u l a t e f er c o e f f i c i e n t the aver age heat t r a n s - i s as f o l l o w s : hOV ( 37) - V A T av whe r e AT. Th i s i n t e g r a l ATl o c dZ has been n u m e r i c a l l y e v a l u a t e d u s i n g a l e a s t - s q u a r e p o l y n o mi a l fit o f d e g r e e n. The p r e s s u r e dr op a c r o s s the sharp-edged o r i f i c e me a s u r e d wi t h a ma n o me t e r i n c l i n e d a t 30° . b a l a n c e o f t h e two col umns is The p r e s s u r e i n t h e i n c l i n e d U- t u b e manomet e r gives ipOHfice = i h ( PL- P g ) s i n (38) whe r e Ah = t h e r e a d i n g o f manomet e r i n f e e t . The a c t u a l gas f l o w r a t e G i s c a l c u l a t e d f r om t h e s h a r p - edged o r i f i c e c a l i b r a t i o n . The g e n e r a l i z e d e q u a t i o n t o calculate t h e mass f l o w r a t e t hr ough; a c o n s t a n t - a r e a d i f ­ ferential t y p e o f f l u i d me t e r i s r 5.1 - A = KAmY[2%gT( P ^ - P g ) ] ! / 2 w + actual mass f l ow Am = t h e c r o s s Pgl ( 39) sectional a r e a o f a f l ow m e t e r , f t 3 = gas d e n s i t y u p s t r e a m l o c a t i o n , I b fflZ f t and f o r a c o m p r e s s i b l e f l u i d t h e e x p a n s i o n f a c t o r , 2 Y, is' us ed and i s g i v e n by I - ( 0. 41 4 P-i - P? + 0 . 3 5 3 )YP I ( 40) whe r e 3 = t h e r a t i o o f t h e d i a m e t e r s T = Cp/ Cv Kr e t z s c h me r ( 26) has shown t h a t K _ " C c i - eV (41 ) Z2 whe r e C = c o e f f i c i e n t o f d i s c h a r g e , However , di mensi onl ess. t h e e q u a t i o n whi ch has been used t o ' c a l c u l a t e t he gas f l o w r a t e f r om t h e p r e s s u r e d r o p a c r o s s a c o n c e n t r i c , sharp-edged o r i f i c e is ( 42) 1/ 2 3600K YA. [ZScAPorificePST] N whe r e G mass f l o w r a t e , I b fflZhr f t 2 Ao : c r o s s s e c t i o n a l a r e a of o r i f i c e o p e n i n g , f t ' 2 Ah : c r o s s s e c t i o n a l a r e a of h e a t e x c h a n g e r , f t 9 c : 3 2 . 1 7 4 l b f f t / l b ffls e c 2 The - p r e s s u r e dr op a c r o s s ferent positions me t e r f l u i d bed o v e r 11 d i f ­ a r e me a s u r e d wi t h ma nome t e r s u s i n g a mano­ having a s p e c i f i c i ng e q u a t i o n g i v e s t h i s APfa = -*j— the f l u i d i z e d g r a v i t y of 1. 00. The f o l l o w ­ p r e s s u r e drop: Ah ( p b - p g ) ( 43) whe r e Ah = t h e ma nome t e r r e a d i n g i n f t . C o m p u t a t i ons From t h e C a l c u l a t e d D a t a : The v o i d f r a c t i o n s , positions, e , a r e c a l c u l a t e d f o r eac h of 11 wher e p r e s s u r e taps are l o c a t e d , of t h e h e a t e x ­ c h a n g e r f r om t h e me a s u r e d v a l u e s o f bed s e c t i o n p r e s s u r e drops. The f o l l o w i n g e q u a t i o n i s a good a p p r o x i m a t i o n f o r batch f l u i d i z a t i o n : 1-e APb g C ( 44) Lg Ap The mini mum f l u i d i z a t i o n mass v e l o c i t y i s c a l c u l a t e d using the f ol l owi ng equat i on (21): 0 . 0 0 1 2 5 Dp2 ( p s - p q) ° - 9 pq 1 - 1 g • mf = U ( 45) •? 5"3 A n a l y s i s : o f Dat a Av e r a g e N u s s e l t Numbers C o r r e l a t i o n Wi t h o u t F l u i d i z a t i o n Dat a wer e t a k e n w i t h o u t f l u i d i z a t i o n resulting t o compar e t h e a v e r a g e N u s s e l t number s wi t h the. f o l l o w i n g c o r ­ relation: — kg = Cn D °* 6 ( de-G- ) 0 , 6 P r 1 Oe v P z ( 46) whe r e Dg = t h e e q u i v a l e n t d i a m e t e r i n i n c h e s ba s ed on f o u r t i me s t h e h y d r a u l i c r a d i u s . The t e r m (— ^ ^ 3 ) was c a l c u l a t e d f r om t h e 9 d a t a wi t h P '= 7 . 0 5 i n a l l c a s e s . Thi s d i m e n s i o n l e s s p r o r ' dt G d u c t i s p l o t t e d v e r s u s t h e d i me n s i o n a l t er m Dg— p— i n F i g ­ u r e Tl . The c o r r e l a t i o n of G e n e t t i i n F i g u r e Tl . ( 8) is also represented The c o r r e l a t i o n o f Ge n e t t i p e r c e n t o f Do n o h u e ' s c o r r e l a t i o n ( 8) i s w i t h i n +25 (6). C a l c u l a t e d N u s s e l t number s u s i n g e q u a t i o n 46 a r e a l l h i g h e r t h a n t h o s e c a l c u l a t e d f r om Ge n e t t i Th i s ( 8) and Donohue ( 6) i s wha t woul d be e x p e c t e d s i n c e e x t e n d e d s u r f a c e a r e a for heat t r a n s f e r is a v a i l a b l e . Genetti' s results f o r a b a r e b u n d l e wi t h 3 / 4 - i n c h t u b e s . Vertical The s o l i d l i n e shows F l u i d i z e d Bed T e mp e r a t u r e P r o f i l e s Wi t h t h e a i d o f 11 t h e r m o c o u p l e s p r o t r u d i n g f r om t h e Genett i ( 6"shel l , 3 / 4 " t u b e s ) ( Nu )( Pr) -54- IOOO Fi gure 1 1 . 1500 2 000 4000 5000 6000 Ave r a ge N u s s e l t number s c o r r e l a t i o n wi t h f l u i d i z a t i o n . 7000 8000 9000 .r.55- o u t e r wa l l of v e r t i c a l wer e d e t e r m i n e d . Static i n c h e s wer e e x a mi n e d . f o r we l l c o l u mn , fluidized f l u i d i z e d bed t e m p e r a t u r e s bed h e i g h t o f s e v e n i n c h e s and n i n e Vertical b u l k gas t e m p e r a t u r e p r o f i l e s beds a r e shown i n F i g u r e 12. shown mass v e l o c i t i e s a r e a p p r o x i m a t e l y same. For t h e u s e s Two d i f f e r e n t amount of e x t e n d e d s u r f a c e s wer e c o mp a r e d . F i g u r e 12 (A) and (B) a r e s t a t i c i n c h e s and n i n e tended s u r f a c e . bed h e i g h t s o f s e v e n and n i n e i n c h e s , Al I p r o f i l e s t emperat ure p r o f i l e ; effect was a p p r o x i m a t e l y 31 i n c h e s , Local but wi t h f o u r t i me s show a u n i f o r ml y h o we v e r , f o r g r e a t e r e x ­ i s more n o t i c e a b l e . bed h e i g h t o f s e v e n i n c h e s t h e f l u i d i z a t i o n ization ex­ F i g u r e 12 (C) and (D) a r e a l s o f o r s t a t i c t ended s u r f a c e area t h i s static of s e ven i n c h e s r e s p e c t i v e l y and f o r t h e f i r s t the ext ended s u r f a c e a r e a . distributed bed h e i g h t s For height and f o r ni n e i n c h e s t h e f l u i d ­ h e i g h t s wer e a r o u n d 3 8 - 4 2 i n c h e s . He a t Tr a n s f e r C o e f f i c i e n t s , f o r Bat ch F l u i d i z a t i o n Local heat t r a n s f e r c o e f f i c i e n t s t h e p r o b e number f r om t h e e x p e r i e mnt al c o n s t a n t gas mass v e l o c i t y . heat t r a n s f e r c o e f f i c i e n t s t u b e e n t r a n c e of a The we i g h t e d a v e r a g e l o c a l of f o u r d i f f e r e n t t ube l o c a t i o n s have been c a l c u l a t e d f o r each r u n . Tocalheat transfer are p l o t t e d versus coefficients Thi s w e i g h t e d a v e r a g e o f one e x t e n d e d s u r f a c e ■ -56- 88 RUN 7WIK3 Ui si 87 = g 86 t- 85 ~ ....^ G - 1, 320 E 4 8 12 16 20 DI STANCE FROM ENTRANCE, INCHES (B) 106 ,o 16 20 24 28 32 36 40 DI STANCE FROM ENTRANCE, KiCHES "I 103 UJ io m C 3 cj f- 102 ^ O d UrLJ ° Ti- i m tfl S I- ui 100 I •o— V' a ----- 1------- 1------Z -----" ^ 4 28 2?. ° DISTANCE ' f r om ENTRANCE, INCHES •c O L u . I DISTANCE Figure 12. 1 ° •• © G =1,230 RUN 7W4H3 3o 40 T 102 — r r~- i Ui t/) D O-----*s — <5 S i o i os Ul o- 100 - RUN 9W4H3 TEI I -O---- o- -45- G = l , 254 I FROM Vertical 28 32 ENTRANCE, INCHES fluidized 36 bed t emperat ure p r o f i l e s 457- are c ompa r ed t o t h e a v e r a g e l o c a l heat t r a n s f e r c o e f f i c i e n t s o f two s t h r e e and f o u r e x t e n d e d s u r f a c e s t o o b s e r v e t he e f f e c t o f t h e i n c r e a s i n g amount o f t h e e x t e n d e d s u r f a c e . Wi r e .1 i n d i c a t e s one e x t e n d e d s u r f a c e . one more a d d e d , t h e r e f o r e , two e x t e n d e d s u r f a c e s A p p r o x i m a t e l y t h e same s t a t i c bed h e i g h t s , Wi r e 2 i n d i c a t e s bed h e i g h t , and so on. fluidized and gas mass v e l o c i t i e s wer e us ed t o a s s u r e t h e same c o n d i t i o n s f or four d i f f e r e n t extended sur f ace areas considered. F i g u r e 13 shows l o c a l the s l i g h t l y ization) of f i v e heat t r a n s f e r c o e f f i c i e n t s for (just a l i t t l e fluidized bed. b i t above t h e mini mum f l u i d ­ The d a t a a r e f o r s t a t i c i n c h e s and mass v e l o c i t i e s For t h e s e mass v e l o c i t i e s o f 526 and 481 l b ^ / h r f t 2 . p a r t i c l e s wer e f l u i d i z e d t o t he h e i g h t s o f a p p r o x i m a t e l y e i g h t and n i n e i n c h e s . these heights heat t r a n s f e r c o e f f i c i e n t s . Since the f l u i d i z e d one, bed h e i g h t s wer e a r o u n d e i g h t and t h e we i g h t e d a v e r a g e c o e f f i c i e n t s probe. t wo, Profiles Above t h e amount o f e x t e n d e d s u r f a c e had no s i g n i ­ f i c a n t e f f e c t on l o c a l ni ne i n c h e s , bed h e i g h t pr obe, t h r e e , f o r pr obe and p r o b e f o u r have been compar ed o f Wi r e I and Wi r e 2 show t h a t t h e c o e f f i c i e n t s Wi r e 2 a r e s l i g h t l y h i g h e r t h a n Wi r e I . Profiles of of Wi r e 3 and Wi r e 4 a l s o show t h a t t h e c o e f f i c i e n t s . o f Wi r e 4 a r e slightly h i g h e r t h a n Wi r e 3 and bot h a r e r e l a t i v e l y higher . than t he c o e f f i c i e n t s of Wi r e I and Wi r e 2. a r e l o we r i n t h e s e c a s e s velocities, Coefficients t h a n f o r r u n s a t h i g h e r mass and a r a p i d dr op i n h e a t t r a n s f e r c o e f f i c i e n t s i s o b s e r v e d a t t h e p o s i t i o n above p r o b e 4. The h i g h l y f l u i d i z e d i s shown i n F i g u r e 14. 1442, all bed o f f i v e 1 4 58, 1 410, and 1360 l b ^ h r f t 2 r e s p e c t i v e l y . The o v e r ­ s e c t i o n was 44 i n c h e s , and i n t h i s of r u n s p a r t i c l e s wer e f l u i d i z e d a p p r o x i m a t e l y 33 and 38 i n c h e s . f luidized condition for s t a t i c investigation. i nches The d a t a a r e f o r mass v e l o c i t i e s o f l e n g t h of t he t e s t series bed f o r s t a t i c Gr a dua l to.the h e i g h t s of The s e a r e t h e mos t h i g h l y bed o f f i v e increase inches in t h i s i n t h e we i g h t e d a v e r a g e c o e f f i c i e n t s wi t h r e s p e c t t o t h e number of. e x t e n d e d s u r f a c e is observed. Compar i ng t h e h e a t t r a n s f e r c o e f f i c i e n t s , l o c a l heat t r a n s f e r c o e f f i c i e n t s t han the o t h e r . fficients o f Wi r e 4 a r e r e ma r k a b l y h i g h e r For Wi r e I , Wi r e 2, and Wi r e o t h e c o e ­ are s l i g h t l y i n c r e a s i n g wi t h t h e number of w i r e s . In t h e l o we r p a r t o f t h e f l u i d i z e d in l ocal heat t r a n s f e r c o e f f i c i e n t s Wi r e 2 , and Wi r e 3. bed s i g n i f i c a n t i s o b s e r v e d f o r Wi re I , In t h e h i g h e r s e c t i o n of t h e F i g u r e t h e amount o f i n c r e a s e on l o c a l heat transfer c o e f f i c i e n t s o f Wi r e 4 compar e t o Wi r e 3 was 29- 38 B t u / h r f t decr ease in l ocal increase 0F. Gr a dual h e a t t r a n s f e r c o e f f i c i e n t s wi t h d i s t a n c e -59- TRANSFER COEFFICIENT, SBH 5 INS. VV 3 LOCAL HEAT @ Probe N um ber F i g u r e 73. Local From Entrance heat t r a n s f e r coefficients. is observed. particle and i t In t h e l o we r p a r t o f t h e f l u i d i z e d concentration profiles (27). i s g r e a t e r than the hi ghe r s e c t i o n . causes the hi gher heat t r a n s f e r r a t e . bed h e i g h t o f f i v e inches a r e o f Type I , For r e l a t i v e l y served t h a t local local For s t a t i c heat t r a n s f e r c o e f f i c i e n t as d e s c r i b e d by Toomy and J o h n s t o n e l ow s t a t i c bed h e i g h t heat t r a n s f e r p r o f i l e s Th i s a g r e e s wi t h G e n e t t i that bed t h e ( 8 ). heat t r a n s f e r c o e f f i c i e n t Genet t i it has been o b ­ a r e o f Type I . has a l s o profiles investigated f o r s t a t i c , bed h e i g h t o f f o u r i n c h e s wer e of Type I e x c e p t f o r t h e c o e ­ fficient profile The we l l inches fluidized 2. bed f o r s t a t i c i s shown i n F i g u r e 15. o f 1 335, cities at tube l o c a t i o n bed h e i g h t o f s e v e n The d a t a a r e f o r mass v e l o c i t i e s 1 238 , and 1 235 l b ^ / h r f t ^ . For t h e s e mass v e l o ­ p a r t i c l e s wer e f l u i d i z e d t o t h e h e i g h t s o f a r o u n d 30 inches. Gr a dua l increase i n t h e we i g h t e d a v e r a g e c o e f f i c i e n t s wi t h r e s p e c t t o t h e number o f i n c r e a s e d e x t e n d e d s u r f a c e observed. In t h e l o we r p a r t o f t h e f l u i d i z e d particle concentrations a r e hi gh of l o c a l h e a t t r a n s f e r c o e f f i c i e n t s wi t h t h e probe 3 l ocal heat t r a n s f e r c o e f f i c i e n t s t he i n c r e a s e increasing For i n s t a n c e , in f o r Wi r e I , Wi r e 2, Wi r e 3 and Wi r e 4 wer e 3 6. 43 , 3 9 . 2 2 , - 4 0 . 4 3 , respectively. bed wher e ( I - e = 0 . 1^ 0 . 3) amount o f e x t e n d e d s u r f a c e was o b s e r v a b l e . is and 4 5 . 2 3 The same t e n d e n c y was o b s e r v e d up t i l l p r obe 8,. -61 - LOCAL HEAT TRANSFER C O EFFCI ENT, BTU/Hr. F t^ 0F SBH 5 INS. W4 Probe F i g u r e 14. Number Local From Entrance heat t r a n s f e r c o e f f i c i e n t s . - 162- For Wi r e I and Wi r e 2 p r o f i l e s Johnstone ( 27) c o n c l u d e d t h a t prevailed in al l runs a r e o f Type I . Toomey and i n t h e s t u d y c u r v e s of Type I i n whi ch t h e d i m e n s i o n l e s s gr oup dpLf / Ay was g r e a t e r t h a n 0 . 0 0 8 . Ho we v e r , t h e p r o f i l e s of Wi r e 3 and Wi r e 4 a r e of Type 11 wh i l e t h e v a l u e o f t he di mensi onl ess g r oup d pLf / Ay i s 0 . 0 0 9 1 . The g e n e r a l f l ow p a t t e r n w i t h i n t h e s y s t e m a p p a r e n t l y d e t e r m i n e s t h e s ha pe of t he c u r v e . dpl ^/ Aj Wi t h t h i s i n mi nd t h e d i m e n s i o n l e s s gr oup i s t oo s i mp l e r e p r e s e n t a t i o n t o d e t e r m i n e t h e shape of c u r v e . For G = 1490, fluidized the e n t i r e for s t a t i c shows t h e s e r u n s . e xpe r i me nt a l col umn was bed h e i g h t o f s e v e n i n c h e s . Particularly, local, he at t r a n s f e r c o e f f i c i e n t s p a r t o f t h e bed was o b s e r v e d . significant F i g u r e 16 increase in f o r Wi re 4 i n t h e de ns e At p r obe 4 h e a t t r a n s f e r c o e f f i c i e n t s , seem somewhat i n c o n s i s t e n t s i n c e t h e ma g n i t u d e of i n c r e a s e in the c o e f f i c i e n t s f o r Wi re 2 and Wi r e 3 i s s u p p o s e d t o be l a r g e r t h a n Wi r e I , c e n t s o f t h o s e a r e l o we r t h a n Wi r e I . and y e t t h e c o e f f i * Heat t r a n s f e r p r o f i l e s f o r t h e s e r u n s a r e o f Type I . F i g u r e 17, F i g u r e 18 and F i g u r e 19 a r e o f s t a t i c h e i g h t of ni ne i nc h e s . Ob s e r v a b l e i n c r e a s e in l ocal bed heat t r a n s f e r c o e f f i c i e n t wi t h r e s p e c t t o t h e e x t e n d e d s u r f a c e - 63 - LOCAL HEAT TRANSFER COEFFICIENT, BTU/ Hr. Ft SBH 7 INS. A W2 Probe Figure 15, Local Number heat t r a n s f e r From E n t r a n c e coefficients. "6 4- 1,490 LOCAL HEAT transfer COEFFICIENT, B T U / H r . F t 2 C r S B H 7 I MS . w 3 Probe Figure 16 Local heat Number From E n t r a n c e transfer coefficients. ■- 6 5 - a r e a was o b s e r v e d . For s t a t i c bed h e i g h t o f n i n e i n c h e s t h e d i f f e r e n c e o f t h e c o e f f i c i e n t bet ween Wi r e I , Wi re 2 , Wi r e 3 and Wi r e 4 wer e r e ma r k a b l y l a r g e c ompar ed t o s t a t i c bed h e i g h t o f f i v e and s e v e n i n c h e s . Tabl e II D i f f e r e n c e o f Local Hea.t T r a n s f e r C o e f f i c i e n t Bet ween D i f f e r e n t Ex t e n d e d S u r f a c e Ext e n d e d Surface Local Wi r e I Wi r e 2 Wi r e 3 Wi r e 4 He at T r a n s f e r C o e f f i c i e n t Bt u / h r f t 2 °F Pr obe 2 Pr obe 3 Pr obe 4 Pr obe 5 37.69 40. 16 36.34 40. 03 2 9. 33 36.87 1 8 . 54 21. 14 62.45 66. 91 67. 45 6 2 . 34 59. 81 81.13 77.58. 76.98 T a b l e 11 shows t h e d i f f e r e n c e of h e a t t r a n s f e r c o e f f i ­ c i e n t b e t we e n d i f f e r e n t e x t e n d e d s u r f a c e f o r mass v e l o c i t i e s o f 745 and 886 I b ^ / h r f t ^ . are.fluidized Local particular r un p a r t i c l e s t o h e i g h t s of a p p r o x i m a t e l y 18 t o 21 i n c h e s . heat t r a n s f e r c o e f f i c i e n t s we r e hi gh w h i l e i n t h e d e n s e p a r t o f ..the f l u i d i z e d profiles For t h i s bed I - e was a r o u n d 0 / 3 . o f Wi r e I and Wi r e 2 a r e o f . T y p e I . The -66- SBH 9 INS Q W3 PROBE NUMBER FROM ENTRANCE F i g u r e 17. Local heat t r a n s f e r coefficients. -:r:;&7T In F i g u r e 18 p a r t i c l e s wer e f l u i d i z e d t o 29 i n c h e s . the p r o f i l e s I f we c o n s i d e r up t o probe 8 i n t h e s e r uns all di me ns i onl es s a r e o f Type 1 1 wh i l e t h e v a l u e o f t h e g r oup d p Lf / AT i s we l l ma t e l y 0 . 1 0 8 ) . The p r o f i l e s 17 a r e a l s o o f Type I I . increases t o h e i g h t s o f 24 over 0. 008 (approxi­ o f Wi r e 3 and Wi r e 4 i n F i g u r e Genet t i ( 8 ) has i n d i c a t e d t h a t i n t h e ma g n i t u d e o f t h e g r o u p , Dt 2/ L f Sfa, a p p e a r to i n c r e a s e t he t e n de nc y toward Type II p r o f i l e s . For s t a t i c bed h e i g h t o f n i n e i n c h e s and i n F i g u r e 19 t h e gr oup 2 Dt /' Lf Sb 15 ^ b o u t 0 . 0 0 2 5 . T h i s a g r e e s wi t h G e n e t t i ( 8 ) s i n c e t he p e r c e n t a g e o f Type I p r o f i l e s was 20 p e r c e n t , when t he v a l u e o f t h e goup Dt 2/ L f Sb i s 0 . 0 3 0 6 . In F i g u r e 19 t h e d i f f e r e n c e o f l o c a l coefficients between W i r e . I , Wi r e 2 , Wi re 3 , and Wi re 4 are e v i d e n t l y c o mp a r a b l e a t each p r o b e . local heat t r a n s f e r c o e f f i c i e n t s R e l a t i v e l y l ow c o e f f i c i e n t s The h i g h l y f l u i d i z e d inches 1665, 1693, Wi r e 4 l o c a l Wi r e 3. Gr adual d e c r e a s e in wi t h d i s t a n c e i s o bs e r v e d . f o r Wi r e I a r e o b s e r v e d . bed f o r s t a t i c i s shown i n F i g u r e 20. e xpe r i me nt a l heat transfer bed h e i g h t o f n i ne The e n t i r e s e c t i o n o f t he col umn was f l u i d i z e d . Mass v e l o c i t i e s 1637 and 1506 I b ^ / h r f t 2 wer e e x a mi n e d . heat t r a n s f e r c o e f f i c i e n t s of For a r e l o we r t h a n Ho we v e r , t h e u n i f o r m t e m p e r a t u r e d i f f e r e n c e from -68- HEAT TRANSFER COEFFICIENT, BTU/Hr. Ft . SBH 9 INS. W2 LOCAL A Probe N um ber F i g u r e 18. Local From Entrance heat t r a n s f e r c o e f f i c i e n t s . r.6?probe I t o probe 6 ( l o c a l heat t r a n s f e r c o e f f i c i e n t s a r o u n d 35 B t u / h r f t 2 °F) wer e o b s e r v e d . local Gr adual h e a t t r a n s f e r c o e f f i c i e n t s wi t h d i s t a n c e are decr eas e in is also observed. F i g u r e 20 and F i g u r e 21 a r e t y p i c a l w e l l - f l u i d i z e d bed. Vertical i n t h e c a s e of t h e f l u i d i z e d gas t e mp e r a t ur e s a r e u n i f o r m and t he t e mpe r a t ur e d i f f e r e n c e bet weeh t he' , fluidized bed and t h e h e a t i n g wa l l t h r o u g h o u t t h e bed a r e g r a d u a l l y i n c r e a s i n g w i t h t h e s ma l l magni t ude. With t h e i n c r e a s e d amount o f e x t e nd e d s u r f a c e s t h i s e f f e c t was pa r t icularly fficients noticeable. T h e r e f o r e , local heat t r a n s f e r c o e ­ wer e i n c r e a s i n g g r a d u a l l y wi t h t h e i n c r e a s e d a- amount o f e x t e n d e d s u r f a c e s . The Dependency, on Tube L o c a t i o n s No s i g n i f i c a n t d e p e n d e n c y on t u b e l o c a t i o n has been observed. However, mass v e l o c i t i e s , i n l ow s t a t i c wa l l bed h e i g h t and i n low t e mp e r a t u r e s vary s l i g h t l y t o t u b e . , wi t h no c o n s i s t e n t t r e n d . h e i g h t s and a t hi gh mass v e l o c i t i e s i n wa l l f r om t u b e At hi gh s t a t i c bed negligible difference t e mp e r a t ur e s bet ween d i f f e r e n t t u b e l o c a t i o n s , has been n o t i c e d . ■ -70- LOCAL HEAT TRANSFER COEFFICIENT, BT U / H r . F t ? 0 F SBH 9 INS. $ W3 10 Probe Figure 19. Number Local From neat it Entrance transfer coefficients. -71 - SBH 9 INS. O I 2 3 4 5 Probe N u m b e r Figure 20. Local heat . i** 6 From 7 8 9 10 11 Entrance transfer coefficients. r72. Av e r a g e S e c t i o n a l C o e f f i c i e n t s Genet t i ' s C o r r e l a t i o n f o r Bat ch F l u i d i z a t i o n E q u a t i o n 30, t h e c o r r e l a t i o n f o r a v e r a g e N u s s e l t n u mb e r s , static i s shown i n F i g u r e 21. The c a l c u l a t e d d a t a f o r bed h e i g h t o f n i n e i n c h e s u s i n g Eq u a t i o n 30 a r e a l s o shown i n F i g u r e 2 1 . Wi t h e x p e r i m e n t a l I y d e t e r m i n e d s e c t i o n a l fractions and l o c a l ferent sections coefficients heat t r a n s f e r c o e f f i c i e n t s of t he f l u i d i z e d f o r .Wire I , particle o v e r 11 d i f ­ bed a v e r a g e s e c t i o n a l Wi r e 2, Wi r e 3, and Wi r e 4 a r e c o mp a r e d . None o f t h e d a t a c a l c u l a t e d u s i n g E q u a t i o n 30 i s bel ow G e n e t t i ' s d a t a . sectional area Not i ceabl e increase in average c o e f f i c i e n t s wi t h r e s p e c t to e xt e nde d s u r f a c e is not iced. The l e a s t s quare f i t s of t h e d a t a f o r e a c h e x t e n d e d s u r f a c e show t h a t t h e e x p o n e n t f o r I - e r a n g e f r om 0 . 4 6 t o 0 . 5 2 . One o f t h e v a r i a b l e s heat t r a n s f e r i s ge o me t r i c p r o p e r t i e s on a v e r a g e s e c t i o n a l Th i s v a r i a b l e t o be c o n s i d e r e d i n b e d - t o - w a l I coefficients of e x t e n d e d s u r f a c e s h o u l d be d e t e r m i n e d . s h o u l d a l s o c o r r e l a t e wi t h t h e e x p r e s s i o n of average sect i onal coefficients . 040 <X>t-40 (0<3) GD. coefficie 4€Z3Za Ave r a ge s e c t i o n a l GO F i g u r e 21. -7 3- 5 2 2 5 0 0 4 - 0 % .0£74-._ The Mo d i f i e d C o r r e l a t i on Ac c o r d i n g t o The S e c t i o n a l Coefficients E q u a t i o n 31 has been us e d t o c a l c u l a t e t imes, 0: average contact ' ' 0 Wi t h l o c a l sectional ( 47) N u s s e l t number s and e x p e r i m e n t a l I y d e t e r mi n e d particle fractions of t he f l u i d i z e d bed, o v e r t h e 11 d i f f e r e n t s e c t i o n s average p a r t i c l e c o n t a c t times, 6, wer e c omput e d and t h e we i g h t e d a v e r a g e s o f e a c h r un have been c a l c u l a t e d wi t h C^ = 1 0 . Tabl e I I I The We i ght e d Av e r a g e C o n t a c t Ti mes Amount of Ex t e n d e d S u r f a c e s UD Ii >- wI , CXl Il ' > - w2 . Y= I 2 w3 , Y= I 8 . w4 , • Y-I Y 0 , sec 0.83333 0. 9 1 6 6 7 0.587 0.483 '0.94444 0.95833 0.395 0.376 75 ■ C a l c u l a t e d we i g h t e d a v e r a g e c o n t a c t t i me s of s t a t i c heights bed s e v e n i n c h e s and n i n e i n c h e s a r e shown i n Ta b l e I I I . As e x p e c t e d wi t h t h e i n c r e a s i n g amount o f e x t e n d e d s u r f a c e s t h e a v e r a g e c o n t a c t t i me s wer e d e c r e a s e d . of b e d - o f - wa 11 h e a t t r a n s f e r If the process i s v i s ua-l-i zed as t h e p e n e t r a t i o n o f t h e b o u n d a r y l a y e r by q u a s i - f l u i d (particles g a s ) eddies f r om t h e b u l k o f t h e s t r e a m and t h e s c o u r i n g a c t i o n of t h e fluidized particles, Woul d be e x p e c t e d to a v e r a g e c o n t a c t t i me . of h e a t t r a n s f e r . then obviously the exert influence the most turbulence intensity on t h e Th a t woul d be a l s o t r u e on t h e r a t e The amount o f e x t e n d e d s u r f a c e s , in o t h e r wor ds t u r b u l e n c e p r o m o t e r s , have been i n c r e a s e d f r om Y-I t h e v a l u e ----- y— o f 0. 8 3 3 3 t o 0. 91 667 , 0 . 9 4 4 4 4 and t o 0 . 9 5 8 3 3 . Particularly t h e s i z e o f e d d i e s whi ch woul d be e x p e c t e d . t o have some e f f e c t on t h e N u s s e l t number woul d e x e r t some influence i n t h e a v e r a g e c o n t a c t t i me . Be c a u s e t h e amount o f b o u n d a r y l a y e r d i s r u p t i o n and e n e r g y d i s s i p a t i o n wi t h t h e i n c r e a s e amount o f e x t e n d e d s u r f a c e s pr omot e r s ) are proport ional (or t u r b u l e n t t o t h e eddy s i z e . C a l c u l a t e d c o n t a c t t i me s a v e r a g e d 0 . 5 5 5 s e c o n d s for s t a t i c bed h e i g h t of 5 i n c h e s . i n t h e r a n g e r e p o r t e d by G e n e t t i Thes e v a l u e s a r e a l l ( 8 ) and Z i e g l e r e t a I ( 3 4 ) . ■To o b t a i n a c o r r e l a t i o n f o r t h e c o n t a c t t i m e s , -76- Q . ■ ' 6k 0 t h e d i m e n s i o n l e s s - q u a n t i t i e s ——9--- wer e c a l c u l a t e d . scales The s e q u a n t i t i e s i n F i g u r e 22. Y-I Y and a r e p l o t t e d on l o g a r i t h m The f o l l o w i n g c o r r e l a t i o n represents the d a t a : P s c S dP1 Y-I Y 6 . 8 5 6 Re. -R •By s u b s t i t u t i n g 6 3 as e x p r e s s e d x- 0 .8 -) ( 48) i n E q u a t i o n 48 i n t o E q u a t i o n 31 ,' t h e f o l l o w i n g c o r r e l a t i o n f o r p a r t i c l e N u s s e l t number s can be o b t a i n e d wi t h = 10: NUp =_______ IO cH I - e ) 0 - 48 ( 49) 6.856 ( I z l - ) - 0 .8 whe r e <f> = s p h e r i t y , 2 t h e r a t i o o f t h e s u r f a c e a r e a of the p a r t i c l e ^ to t he s u r f a c e a r e a of a s phe r e o f same a v e r a g e d i a m e t e r . ' Y = number o f t u b e d i a m e t e r p e r 180° t w i s t . Mi c r o s c o p i c e n l a r g e m e n t s o f p a r t i c l e s [ F i g u r e 7 ( B) ] shows t h a t the gl ass study are s p h e r i c a l , particles and 9 - I was u s e d . data, us ed i n t h i s E q u a t i o n 49 as wel l a r e shown i n F i g u r e 23. Static as t h e e x p e r i me n t a l bed h e i g h t s o f f i v e . -77 - O © + X = 6 . 8 5 6 Re S S P Fi g ur e 22. 0.8333 0.9167 0.9444 0.9583 O © C o r r e l a t i o n f o r a ve r age c o n t a c t t i me. s e v e n , and n i n e i n c h e s are r e p r e s e n t e d i n t h e d a t a shown i n F i g u r e 23. The v a l u e s Y o f 6 , 1 2 , - 1 8 , and 24 have been represented i n t h e d a t a shown i n F i g u r e 23. c o r r e l a t i o n accor di ng to the s e c t i o n a l The mo d i f i e d coefficients has been s t u d i e d o v e r 11 d i f f e r e n t p o i n t s a l o n g t h e f l u i d i z e d bed wi t h d i f f e r e n t mass v e l o c i t i e s . ( a b o u t 95 p e r c e n t ) in t h i s Most o f t h e d a t a a r e w i t h i n +25 p e r c e n t o f E q u a t i o n 49 study. The e x p o n e n t 0 . 4 8 f o r I - e c i t e d by G e n e t t i r ef e r enc e to ot her present investigators investigation. ( 8 ) wi t h ( 18,. 2 0 )' a g r e e s wi t h t h e B a c k - c a l c u l a t e d we i g h t e d a v e r a g e c o n t a c t t i me s c o r r e l a t e wi t h t h e p r e s e n t m o d i f i e d d i m e n s i o n ­ less g r o u p s and a r e i n a g r e e me n t wi t h t h e p r e v i o u s c a l c u l a ­ tions. 9 8 9 S 8 ’9 8 1.25 F i g u r e 23. 2 3 4 5 6 7 8 9 10 1 Humb^r6 s e n t m° d i f 1 e d c o r r e l a t i o n f o r s e c t i o n a l 2 3 p a r t i c l e Nus s e l t -80- R e s u l t s and Co n c l u s i o n Local and a v e r a g e he-at t r a n s f e r c o e f f i c i e n t s b e d - t o - w a 11 h e a t t r a n s f e r f r om a f l u i d i z e d for bed t u b u l a r h e a t e x c h a n g e r wi t h e x t e n d e d s u r f a c e s wer e i n v e s t i g a t e d . was us e d as t h e f l u i d i z i n g medi um and c o a r s e g l a s s wer e f l u i d i z e d in t he e x p e r i me n t a l He a t t r a n s f e r c o e f f i c i e n t s Ai r particles h e a t e x c h a n g e r col umn. f o r a i r f l o wi n g t hrough t h e h e a t e x c h a n g e r w i t h o u t f l u i d i z a t i o n wer e a l s o i n v e s t i g a t e d . Av e r a g e N u s s e l t Numbers w i t h o u t F l u i d i z a t i o n The a v e r a g e h e a t t r a n s f e r c o e f f i c i e n t s f o r a i r alone have been c ompar ed wi t h t h o s e c a l c u l a t e d f r om an a c c e p t e d correlation f or m ( 6 , 8 ) : it is concluded t h a t c o e f f i c i e n t s wer e o b t a i n e d i n t h i s s u r f a c e area f or heat t r a n s f e r F l u i d i z e d Bed Ther mal fluidized very s ma l l . tributed Local st udy s i nc e extended is avai l a bl e. Gr adi ent s From me a s u r e me n t s of v e r t i c a l profiles, higher bed t h e r ma l fluidized bed t e m p e r a t u r e g r a d i e n t s a r e shown t o be Al I p r o f i l e s wer e s howi ng u n i f o r m l y d i s ­ t emperat ure p r o f i l e s . He a t T r a n s f e r C o e f f i c i e n t s Gr a dua l coefficients increase i n t h e we i g h t e d a v e r a g e h e a t t r a n s f e r wi t h r e s p e c t t o t h e number of e x t e n d e d s u r f a c e “ ' " '8 -1 - is observed t hr oughout the runs. coefficients heat t r a n s f e r a r e o b s e r v e d t o d e c r e a s e wi t h t h e d i s t a n c e f r om t he e n t r a n c e of t he f l u i d i z e d coefficients Local bed. Local heat t r a n s f e r v a r i e d s l i g h t l y wi t h d i f f e r e n t t ube l o c a t i o n s . Av e r a g e S e c t i o n a l Coefficients The a v e r a g e . s e c t i o n a l coefficients have been compar ed wi t h t h e d a t a c a l c u l a t e d f r om an e s t a b l i s h e d c o r r e l a t i o n None o f t h e d a t a of t h i s s t u d y i s bel ow G e n e t t i ' s d a t a f o r bare t u b e s . As e x p e c t e d , ( 8 ). an i n c r e a s e i n a v e r a g e s e c t i o n a l c o e f f i c i e n t s . wi t h r e s p e c t t o e x t e n d e d s u r f a c e a r e a i s o b ­ tained. I t i s f ound t h a t t h e e x p o n e n t f o r 1 - e r a n g e f r om .0.46 t o 0 . 5 2 . The Mo d i f i e d C o r r e l a t i on Ac c o r d i n g t o t h e S e c t i onal Coefficients Wi t h l o c a l heat t r a n s f e r c o e f f i c i e n t s d e t e r mi n e d s e c t i o n a l ferent sections particle f r a c t i o n s o v e r t h e 11 d i f ­ of t he f l u i d i z e d c o r r e l a t e d wi t h E q u a t i o n b e d , N u s s e l t number s a r e 49. 10 tj) ( I - e ) Nu 0.48 ( 49) 6.856 1+ i :i I and e x p e r i m e n t a l Iy ReP -82- Several conclusions 1. ratio, Particle Y, can be drawn f r om t h i s correlation; N u s s e l t number s a r e d e p e n d e n t on t w i s t Th i s a l s o i mp l i e s t h a t p a r t i c l e N u s s e l t number i s d e p e n d e n t upon e x t e n d e d s u r f a c e a r e a . 2. P a r t i c l e N u s s e l t number s a r e p r o p o r t i o n a l t o ( I - c ) 0 *48 3. P a r t i c l e N u s s e l t number s have weak d e p e n d e n c y on gas mass v e l o c i t i e s . Most o f t h e d a t a a c c o r d i n g t o t h e mo d i f i e d c o r r e l a t i o n this in i n v e s t i g a t i o n a r e w i t h i n +25 p e r c e n t o f E q u a t i o n 49. -83- L i t e r a t u r e Ci t ed I. An d e r s o n , T . B. and J a c k s o n , 6 , 527 ( 1 9 6 9 ) . 2. B o t t e r i l I , J.. S . M. and W i l l i a m s , Chem. E n g r s . , 41, 21 7 ( 1 963 ) . 3. Da v i d s o n , (1961 ) . 4. Da v i d s o n , J . F . , H a r r i s o n , D. , " F l u i d i z e d P a r t i c l e s , " Ca mbr i dge U n i v e r s i t y P r e s s , New York ( 1 9 6 3 ) . 5. Dow, W. M. and J a k o b , M. , Chem. Eng . P r o g . , (1951). 6. Donohue , D. A. , I n d . Eng . Chem. , ± 1 > 2499 ( 1 9 4 9 ) . 'I. J.F., Trans. Roy, Inst. I n d . Eng. Chem. Fund J . R. , T r a n s . Inst. Chem. E n g r s . , 1 9 , F r a n t z F . J . , I . Chem. Eng. . , 6_9, 1 61 ( S e p t , I I . I b i d . , page 89 ( Oc t . I , I 962) I I I . I b i d . , page 103 ( Oc t . 29 , 1 96 2 ) . P h . D. T h e s i s , 230 47., 537 1 7, 1 962) 8. G e n e t t i , W. E. , University. 1 968 , Or egon S t a t e 9. G e l ' p e r i n, N. I . , A i n s h t e i n , V. G. and K o r o t y a n s k a y a , L . A. , I n t . Chem. E n g . , I , I 37 ( 1 96 9 ) . 11. Ku n i i , D. and L e v e n s p i e l , O. , 7, 446 ( 1 9 6 8 ) . . 12. Ku n i i , D. and L e v e n s p i e l , O. , I n d . Eng. Chem. P r o c e s s De s i gn and De v e l o p me n t , _7 , 481 ( 1 9 6 8 ) . . 13. Kret zschmer , F., Forshung. , pa g e s 9 3 - 9 5 . 14. Ki d.d, G. J . , J r . , 15. Leva , M. , We i n s t r a u b , M. and Gr ummer , M. , Chem. Eng P r o g . , 45, 563 ( 1 9 4 9 ) . I n d . En g . Chem. F u n d . , V o l . 4, Ma r c h - Ap r i I , OO OY van H e e r d e n , C . , Nobel , P . and van K r e v e l en , D. W. , Chem. En g . S c i . , I , 51 ( 1 9 5 1 ) . CO 10. A. I . Ch. E. J ; , 4, 581 (1 9 6 9 ) . -84- 16. L e v e n s p i e l , 0. and Wa l t o n , J . S . , Chem. Eng. Pr og. Symp. S e r . , No. 9, V o l . 50, " He at T r a n s f e r - R e s e a r c h S t u d i e s f o r 1 9 5 4 , " A. L. Ch-. E . , pgs . 1 - 1 3 . 17. Mu r r a y , 18. Mi c k l e y , H. S. and F a i r b a n k s , I , 374 ( 1 9 5 5 ) . 19. McAdams, W. H. , " He a t T r a n s m i s s i o n , " Y o r k , M c G r a w - H i l l , 1954, page 299. 20. Mi c k l e y , H. S. and T r i l l i n g , 41, 1135 ( 1 9 4 9 ) . 21 . M i l l e r , C. 0. I 220 ( 1 951 ). 22. Noe, A. R. and Kn u d s e n , J . G. , Chem. Eng . Pr og. ■ Symp. S e r . , V o l . 64, No. 82, " He a t T r a n s f e r , " A. I ., Ch'. E . , 1968, 2 0 2 - 2 1 1 . 23. P e t r i e , J . C. , F r e e b y , W. A. and J . A. , Chem.. Eng. Pr og . , Erl, 45 ( 1 9 6 8 ) . 24. R u c k e n s t e i n , E . , P r o c e e d i n g s o f t h e T h i r d I n t e r n a t i onal He a t T r a n s f e r C o n f e r e n c e , P a p e r s 113 -151 , Vol . IV, page 298- 301 ( 1 9 6 6 ) . 25. S z e k e l y , J . and F i s h e r , 833 ( 1 9 6 9 ) . Chem. Eng . Sci . , 24, 26. Toor , H. L. and Mar chel I o , J . M. , A. 4, 97, ( 1 9 5 8 ) . I . Ch . E . J • S 27. Toome y, R. D. and J o h n s t o n e , H. F . , Chem; Eng. Pr og. Symp. S e r . , V o l . 49, No. 5, " He a t T r a n s f e r , " A. I . E. , 1953, pa ge s 5 1 - 6 3 . J.D., J. F l u i d Me c h . , 2J_, 465 ( 1 9 6 5 ) . D . F . , A. C. A. , 3rd, Ch . E . J . , ed., I n d . Eng. New Chem. , K . , I n d . En g . Chem. , 43^ and Logwi nuk, A. R. J . , 28. V r e e d e n b e r t , H. A. , J . Appl . Chem. , 29. V r e e d e n b e r g , H. A. , Chem. 30. We n d e r , L . and C o o p e r , G. T . , A. 15 ( 1 9 5 8 ) . Eng. I. Sci., 2_, 526 ( 1 95 2 ) . 1J_, 274 (I 960) . I . Ch. E . J . , £, Ch . -85- ■31. Wen5 C. Y. and Leva, M. , A. (1956). F. , I . Ch. E. J . , 2, 482 32. Wi c ke 5 E. and p e t t i n g , 301 (1.954. Chemi e- I ngr . Tech. , 26 — 33. Y o s h i d a 5 K. , K u n i i 5 D. and Levenspi e l , 0 . , Heat Mass T r a n s f e r , 1_2 , 529 ( 1 9 6 9 ) . 34. Z i e g l e r , E. N. , Ko pp e l 5 L. B. and B r a z e ! t o n , W. T I n d . Eng. Chem. Fund. , 3_, 224 (1 96 4 ) . In t . J Appendix I Nomenclature Symbol Definition A v e r y s ma l l c o n s t a n t f o r E q u a t i o n 18 A1 Di me ns i ons Di me n s i o n l e s s A To t a l s u r f a c e a r e a o f p a r t i c l e s i n t h e bed ft2 Ah Crossectional changer ft2 Am C r o s s - s e c t i o n a r e a o f a f l o w me t e r ft2 Ao Cross-sectional opening ft2 ; a • b B1 C. cO cI C2 Cg Sg Cps CR Cs D1 a r e a of o r i f i c e ■Sur f ace a r e a o f p a r t i c l e / u n i t l e n g t h o f bed - AP AT a r e a of he a t e x ­ ' S u r f a c e a r e a of e n t i r e bed coefficient solid ft2 /ft ft2 f o r E q u a t i o n 32 Di me n s i o n ! e s s C o e f f i c i e n t f o r E q u a t i o n 32 Di me n s i o n l e s s Di me n s i o n l e s s A c o n s t a n t whi ch i n c r e a s e s wi t h p a r t i c l e s i z e f o r E q u a t i o n 18 C o e f f i c i e n t of d i s c h a r g e Const ant Di me n s i o n l e s s Const ant Di me n s i o n l e s s Di me n s i o n l e s s Const ant S p e c i f i c h e a t o f gas Specific constant Specific constant h e a t o f gas a t pressure h e a t of s o l i d a t pressure C o r r e c t i o n f o r n o n - a x i al tube l o c a t i o n , f o r case of i n t e r n a l heat t r a n s f e r surface S p e c i f i c h e a t of s o l i d Ou t e r d i a m e t e r of a x i a l cylinder Di me n s i o n l e s s Bt u Z l b m0 F B t u / 1 b m°F B t u / l b m°F D i me n s i o n l e s s Bu t Z l b m0F ' ft - .8 7 - a Z- Da i me t e r o f f l u i d i z e d d b E f f e c t i v e d i a me t e r of bubbl e P a r t i c l e di amet er ft . Tube d i a m e t e r ft d P- d P bed ft ft dt i ' Ou t e r d i a m e t e r o f h o r i z o n t a l tube i mmer s ed emf E l e c t r o m o t i v e f o r c e p r o d u c e d by t h e t h e r mo c o u p l e F Term d e f i n e d g A c c e l e r a t i o n due t o g r a v i t y Di me n s i o n l e s s ft/hr2 9C Gravitational l b Hf t i n E q u a t i o n 14 Const ant ft mi I i vol t s I b .cs e c 2 G S . Gas mass v e l o c i t y I bm/ h r f t 2 Mass v e l o c i t y o f f l u i d i z a t i o n o f a bed Ib^/hr f t 2 • ^nif C a l c u l a t e d mi nimum f l u i d i z i n g gas /■ ' I bm/ hr f t 2 mass v e l o c i t y h Heat t r a n s f e r c o e f f i c i e n t Btu/hr ft°F hav Av e r a g e h e a t t r a n s f e r c o e f f i c i e n t Btu/hr ft °F ^loc Local B t u / f t 2oF ht T i me - a v e r a g e d h e a t t r a n s f e r coefficient B t u Z f t 2oF ht i Local i n s t a n t a n e o u s h e a t transfer coefficient B t u Z f t 2oF hW He a t t r a n s f e r c o e f f i c i e n t b e t we e n bed and s u r f a c e B t u Z f t 2oF Ah Manomet er , r e a d i n g s ’ I(t) I heat t r a n s f e r c o e f f i c i e n t ■ I •! ft I • . Age d i s t r i b u t i o n f u n c t i o n of e mu l s i o n e l e me n t s on t h e surface C u r r e n t f l o wi n g t h r o u g h t h e h e a t i n g e l e me n t g Di me n s i o n l e s s . ' ■ Amperes • ‘ ■ I I I '! ■T -88 K Kr e t z c h me r c o e f f i c i e n t k Ther mal k. E f f e c t i v e t h e r ma l c o n d u c t ­ i v i t y of e mu l s i o n l a y e r Ther mal c o n d u c t i v i t y o f gas B t u / f t h r 0F Ther mal B u t / f t h r 0F L L conductivity c o n d u c t i v i t y of s o l i d Effective thickness I ayer Bed h e i g h t o f e mu l s i o n Mean h e i g h t o f f l u i d i z e d Le ngt h o f h e a t t r a n s f e r ' mf bed Btu/hr f t °F Bt u/ f t ° f ft ft ft surface ft He i g h t o f bed a t mini mum f l u i d ­ izing conditions Bed s e t t l e d h e i g h t ft Term d e f i n e d i n E q u a t i o n 20 up Particle N u s s l e t number ua v Av e r a g e p a r t i c l e h a v V kg ' Di me n s i o n l e s s D i me n s i o n l e s s hW N u s s l e t n u mb e r , Di me n s i o n l e s s Pressure I b^/ f x I Ups t r e a m p r e s s u r e Ib^/ft2 2 Downs t r eam p r e s s u r e Ib^/ft2 O r i f i c e p r e s s u r e dr op lbf / f t 2 Prandtl Di me n s i o n l e s s AP number C ^ p / kg Heat f l u x f r om h e a t t r a n s f e r surface • Btu/hr f t 2 *1 Ra t e o f h e a t l o s s f r om f l u i d i z e d bed Bt u/ hr R- Bed e x p a n s i o n r a t i o D i me n s i o n l e s s .89- qP : Re Cd But/hr f t 2 Re y n o l d s number Di mens i on! Particle Di mens i on! T e mp e r a t u r e l CD T . C 'r Re y n o l d s n u mb e r , D G/y P Ra d i a l d i s t a n c e f r om t h e c e n t e r o f t h e bed TV I n l e t and o u t l e t t e m p e r a t u r e respectively T2 ft °F °F Bed t e m p e r a t u r e 0F Av e r a g e t e m p e r a t u r e o f gas a t any l e v e l i n bed 0F e mp e r a t u r e o f b u b b l e g a s , and of Tg b 5 Tge T e mu l s i o n gas 0F Tb " He at t r a n s f e r t o a p a r t i c l e near the heat t r a n s f e r sur f a ce Tg Tgi • Tgo T S TW I n l e t gas t e m p e r a t u r e 0F Initial 0F gas t e m p e r a t u r e . Solid t emperat ure 0F Wal l °F t emperat ure "b'"br Ri s i n g v e l o c i t y of a bubbl e in a b u b b l i n g bed and v e l o c i t y o f bubbl ewi t h r e s p e c t t o e mu l s i o n a head o f i t ft/hr ue Upward gas v e l o c i t y w i t h i n e mu l s i o n phase f t / hr ■ uf uITlf % us V - umf / e mf ' S u p e r f i c i a l gas v e l o c i t y a t mi ni mum f l u i d i z a t i o n c o n d i t i o n s S u p e r f i c i a l gas v e l o c i t y . ( ba s e d on empt y t u b e ) Downward v e l o c i t y o f s o l i d s i n . e mu l s i o n p h a s e Vo l t a g e dr op a c r o s s t h e h e a t i n g e l e me n t ft/hr f t / hr ft/hr ft/hr volts - -9 0- V Vf W wg ' Vg Vo l u me t r i c f l o w r a t e f t J/hr V e l o c i t y o f gas ft/hr Ac t u a l mass f l ow r a t e Gas f l o w r a t e 1V ws Superficial v e l o c i t y o f gas X Fi l m t h i c k n e s s o r d i s t a n c e from t he heat exchange s u r f a c e t i me s s p e c i f i c ft/hr wC Gas f l o w r a t e o f gas Y Ex p a n s i o n f a c t o r Y Y Term d e f i n e d i n E q u a t i o n 13 T wi s t r a t i o ; t h e number of t u b e d i a m e t e r p e r 180° t w i s t Z Term d e f i n e d i n E q u a t i o n 15 hr heat ft BTU °F hr D i me n s i o n l e s s Di me n s i o n l e s s D i me n s i o n l e s s Di me n s i o n l e s s ;--91 - Vol ui net r i c F r a c t i o n o f S o l i d s Definition Symbol ' Volume o f e mu l s i o n t r a n s p o r t e d upwar ds b e h i n g a b u b b l e pe r v o l ume o f a b u b b l e ’ Ra t i o of t he o r i f i c e d i a me t e r ■ to t he pi pe di amet e r Vo l u m e t r i c f r a c t i o n of s o l i d s 'a Y Number of p a r t i c l e s surface area . YP per uni t - Di mens i ons Di me n s i o n l e s s D i me n s i o n l e s s Di me ns i onl ess 0 parti c l e s / f t Voi d f r a c t i o n Voi d f r a c t i o n of e mu l s i o n pha s e Di me n s i o n ! e s s Av e r a g e Voi d f r a c t i o n i n t h e f l u i d i z e d bed Voi d f r a c t i o n of s t a t i c bed Di me n s i o n l e s s Voi d f r a c t i o n o f bed a t minimum f l u i d i z a t i o n conditions- Di me n s i o n l e s s £mf V n F l u i d i z a t i o n e f f i c i e n c y , or D i me n s i o n l e s s 0 0 ■ V TS tV t S C o n t a c t t i me Av e r a g e c o n t a c t t i me hr hr 8 E0 e ef £m Bed d e n s i t y Pb ■ pe - ' Ap p a r e n t d e n s i t y o f e mu l s i o n D i me n s i o n l e s s D i me n s i o n l e s s p I b mZf t 3 Gas d e n s i t y 1V f t S I b mZ f t 3 Gas d e n s i t y o f u p s t r e a m l o c a t i o n I b mZ f t 3 p gi . pS V - Particle density Viscosity Gas v i s c o s i t y yg I b mZ f t 3 I b raZ f t hr . l b m/ f t hr -9v 2’' Ki n e ma t i c v i s c o s i t y f . t 2/ hr Sphericity. D i me n s i o n l e s s Rat i o of t he p a r t i c l e s ur f ace, a r e a t o t he a r e a of a s p h e r i c a l p a r t i c l e of t h e same d i a m e t e r Di me n s i o n l e s s Vol ume f r a c t i o n o f b u b b l e s f l u i d i z e d bed D i me n s i o n l e s s in Appe ndi x 11 E v a l u a t i o n o f p and R -E6- Paruiclo Diameter, inch 0.012 £ Fi gure 24. t- The c o r r e l a t i o n f or g and R. -94- NOTIl - L i f t fcrricht] s c o l t of CC rrtsponJs to G„< (Ib/ftfhr) 0 f (inch) Ia ft (or right) scaio of Grnf 3 0 0 0 - o IOOOOO U r (C-P) 0 .0 3 5 : 0 .0 3 (Ps-PfrIPFtIi/0* O.C5 0.03 20— 800 •500 ■: 0.02 | 0.02 j o o 5 J-200 0 01 -too 0005 0.01 0 003 L 0.002 .O O flj F i g u r e 25. Nomograph t o c a l c u l a t e . Appe ndi x I I I A typical data sheet -95Sampl e Raw Dat a S h e e t Run: 9H3W3 J u n e 2, Time S t a r t e d : Ti me F i n i s h e d : 1 969 1 0 : 2 5 A. M. 2. 45 P.M. Number of Exended S u r f a c e s : 3 S t a t i c Bed H e i g h t : 9 inches F l u i d i z e d Bed H e i g h t : 38 i n c h e s Vo l t me t e r Readi ngs : 7.5 v o l t s , 7. 7 v o l t s Ammet er R e a d i n g s : 50 amps 51 amps Manomet er ( I ) r e a d i n g : (22 3 / 8 rV 22 1/ 4 i n c h ) (21 3 / 8 % 21 1 / 4 i n c h ) ( f o r a i r f l o w r a t e ) Tube Wal l Pr obe I Pr obe 2 Pr obe 3 Pr obe 4 Pr ove 5 Pr obe Th e r mo c o u p l e s emf by mv Locati on I Location 2 Location 3 Locati on 4 2.380 2.458 2. 549 2. 319 2. 197 2. 273 2. 332 2. 077 1. 975 2 . 01.8 2. 018 . 853 1. 791 1. 815 I .7 97 . 740 1. 671 1. 695 1. 637 . 587 1. 570 • I . 587 1.588 I . 549 1. 559 I . 575 Pr obe 8 . I . 543 Pr obe 9 . I . 551 I . 541 1. 5 5 7 I . 568 I . 569 I . 559 I . 575 1. 557 Pr obe 10 I . 571 Pr obe 11 I . 598 I . 566 1. 574 I . 563 I . 542 I . 542 Pr obe 6 Pr obe 7 . 552 I . 557 • ■ I '96r. Bul k Bed Th e r mo c o u p l e s emf by mv Section I Section 2 Section 3 Section 4 Section 5 Section 6 I . 815 I . 838 I . 837 I . 834 I . 825 Section■ 7 ■r.. 825 8 9 I . 804 I . 809 I . 807 I . 815 Section Section S e c t i o n 10 S e c t i on I I I . 825 Manomet er (2) ' Readi ng, Inches Manomet er I Ah Manomet er 2 Ah 3. 25 3. 00 Manomet er Manomet er 3 4 Ah Ah 2 . 25 2 . 00 Manomet er 5 Manomet er 6 Ah Ah I . 25 •o. 75 • Manomet er Manomet er 7 Ah 8 . Ah 0 . 50 0 . 125 Manomet er 9 Ah Manomet er 10 Manomet er I I ' Ah ■ Ah 0 . 00 0 . 00 4. 00 Ii Appe ndi x IV C a l i b r a t i o n T a b l e s f o r Ther mocoupl I 2 3^ Th e r mo c o u p l es 4 5 6 7 8 9 0F 0 60 0 . 618 0 . 640 0 . 662 0 . 684 0 . 706 0 . 729 0. 751 0. 774 0. 096 0. 818 70 0 . 840 I . 064 0 . 862 I . 086 I . 311 0 . 884 I . I 09 I . 334 0 . 906 I . 131 I . 357 0 . 929 0 . 951 I . 176 I . 403 0. 974 I . I 99 0. 996 0. 221 I . 01 9 I . 041 I . 426 I . 448 I . 244 I . 471 I . 266 I ., I 93 I . 538 I ., 561 I . 607 I .,653 I ., 882 I ., 676 I .,699 I ., 837 I . 630 I . 859 I .,905 I ., 928 I . 722 I ., 951 80 90 I . I 54 I . 380 100 I . 289 I . 516 I 10 I . 745 I . 768 I ..791 I . 583 I . 814 120 I . 974 I .. 997 2 . 020 2 . 043 2 ., 066 2 . 088 2..111 2.,134 2., I 57 2.J 80 I 30 140 I 50 2 . 203 2 ,. 433 2 . 663 2 .. 225 2 . 455 2 ,. 685 2 . 248 2 ,. 478 2 ,. 708 2 . 270 2 ,. 500 2 ,. 730 2 . 293 2 ,. 523 2 . 753 2 . 316 2..340 2..363 2.,409 I 60 2 . 892 3 . I 22 2 ,. 91 5 2 . 937 2 . 960 2 . 982 2 . 546 2 . 776 3. 006 2..569 2 .799 3,. 029 2,.593 2 . 822 3,. 052 2.. 386 2,. 61 6 2,. 846 3 . 076 3 . 145 3 . I 69 3 . 262 3 . 285 3 . 309 3 . 378 3. 469 3 . 492 3 . 515 3 . 538 3 .562 3 . 585 3 . 818 3 . 608 3 . 841 3 . 402 3 . 632 3 .21 5 3 . 447 3. 239 3 . 355 3 . 192 3 . 424 2,.869 3,. 099 3,. 332 3 . 655 3 . 883 3 . 678 3 .91 I 3. 701 3 . 934 3 . 725 3 . 958 3 . 748 3 .981 3 .771 4 . 004 3 . 795 170 I 80 I 90 200 3 . 865 2..639 4 . 028 “Z6“ Chr omel - Al ume l I r o n C o n s t a n t a n T h e r mo c o u p l es I 2^ 3 0F O 60 0 ,. 785 0 ,. 813 O. 842 0 ,. 871 0 . 900 0 ,. 929 O. 957 0 . 986 I ,. 01 5 I . 044 70 I ,. 073 I . 361 I ,. 101 I ,. I 59 I ,. 447 I ,. 188 I . 476 I . 736 2 ,. 026 I . 765 2 . 055 I . 217 I . 505 I ,. 794 I ,. 246 I ,. 533 I ,. 823 I . 274 I . 389 I . 678 I ,. 968 I . 30 I . 418 I . 797 1997 I ,. 332 I ,. 620 I ,. 910 2 ,. 084 2 ,. 113 I . 562 I . 852 2 . 143 I ,. 303 I .591 I ,. 881 2 . 259 2 . 289 2 . 318 2 . 347 2 . 376 2 . 405 2 . 435 80 90 100 I ,. 939 2 . 230 5 6 7 8 9 2 . 1722 2 ,. 201 2 . 464 2 ,. 493 -98- no I . 649 4 Appendix V' Compl e t e Dat a (Table IV) -99- FBH RUN NOBWl Hl G= =527 IN 9 lbm / h r f t ? . 18.228 1— 6 h |yc, Btu/ hr ft2 °F I 0.0 0.79 2 0.0 1.12 3 4 0.0 I .29 0.0 I .87 0.0 2.27 0.0 2.69 7 8 0.0 3.90 0.0 6.65 9 0.0 21.49 10 0. 1 34.23 11 0.375 34.10 Probe no. 5 6 Btu / hr ft2 , “ =267 RUN MO. hOV " 9 . 0 FBH llW H r f t - , 5 WI H2 G - - 1 009 B t u / hr f r °F IN 16 Rep —24 g i —e h |oc , B t u / Hr f t 2 o F I 0.0 3.05 2 0.0 3.29 3 4 0.0 3.49 0.0 3.78 5 0.0 4.51 6 0.0 6.20 7 0.0 11.09 8 0.00625 22.34 0. 1 38.37 10 0.225 39.24 11 0.325 45.65 Pr obe no. 9 Q = 333 Dt u/ hr f t 2 , Hq v - 1 6 . 4 B t u / Hr ft 2 °F RUN NO- 5W1H3 G — 1 2 54 Probe no. IN 5 Rep - 4 3 . 3 7 5 h |0(_, Bfu/ hr ff2 I— E I 0.0 2.89 2 0.0 3.24 3 4 0.0 3.46 0.0 4.44 3 6 0.0 6.18 0.0625 8.71 7 0.0125 18.11 8 0.05 23.13 9 0.15 28.74 10 0.25 30.35 11 0.225 33.70 Q = 301 btu/hrft2 , RUN NO. 5W1H4 1 443 G == Pr obe no. 14.3 Hqv = FDH lbm/ | i r ft2. I—E B t u / hr ft2 °n IN 3 8 Rep = 4 9 . 9 1 2 h |oc, BtuZhrft2 o F 0.0 4.33 2 0.0 5.14 3 4 0.0 6.18 0.0 7.42 3 0.0125 1 0 . 1 2 6 0.025 14.87 7 0.0375 18.96 8 0.075 25.21 9 0.15 0.275 Q = 316 B t u / hr f t 2 , OJ OD 11 29.59 OO 0 . 2 'd- 10 rx> I rx> ' rtit^ lbm / hr f t , h a v — 1 6 . 3 g t u / hr f t 2 o F -101 - FBH RUN N0. 5W2 G — 527 Probe no. ' I b m / h r f t 2 , 0.0 2 0.0 5 0.0 4 0.0 5 6 0.0 7 8 0.0 0.0 9 0.0 neP ^ 18 . 2 2 8 I'i |o , Btu/ hr ft2 °F I—E I IN 8 0.69 0.86 1. 11 I . 58 2.29 0.0 2.77 3.86 5.76 10 0.075 ii 0.375 Q = 280 RUN NO. G= Btu/ hr 5W2H2 I 009 2.125 , FBH Ibm/ hr I—6 Pr obe no. 39.28 ___ 3 9 , 7 8 _ BvuZhrf f2 o F hov — 9*5 IN Rep = 14 34.9 h Ioc , Bt u/ hr ft* 0F 0.0 2.60 2 0.0 2.83 3 4 0.0 3.12 0.0 3.48 5 0.0 5.86 6 0.0 7.63 7 0.0 11.28 8 0.0 25.01 9 0. 1 38.85 10 0.225 41 . 2 3 11 0.325 Q = 294 Bt u / hr ft^ , C\ LT I h Qv = I 6 • I B t u / hr f t ^ °F -102- RUN I—€ IN 25 Rcp = 4 3 . 9 9 7 Btu/ hr h I 0.0 3.45 2 0.0 3.77 3 4 0.0 4.84 0.0 6.22 3 0.0 9.53 6 0.025 14.78 7 8 0.05 20.62 0.0875 26.48 9 0.125 38.38 H O Probe no. ' FBH i b m / h r f t 2. 2 H3 9 7 o ij — \ c I 6 0.2 38.67 11 0.275 45.16 Q— 285 Btu/hrft2 , I—e P robe no. I 0.0 2 0.0 3 4 0.0 5 0.125 6 0.025 7 0.0375 8 0.0875 9 0.125 10 0.175 11 0.275 Q= 1 8 • 6 B t u / hr fI2 c T- hc v " F BH lbm / h r ( t 2 RUN NO. 5W2H4 G = 1455 I IN Rep = , B t u / h r ft ' , 33 50.43 h Iqc z Bt u/ hr ft2 °F 4.66 5.55 7.33 0.0 281 °F 9.73 12.25 17.47 19.51 22.83 27.61 30.05 J 4.33 = 1 7 . i B t u / h r f t 2 °F run NO. 5W3H1 G — 481 Probe no. : ' FBH IN 9 Bep= 16. 637 ,bm / hrfl , h | o , Btu/ hr f f2 °F 1— 6 I 0.0 2 0.0 3 4- 0.0 2.08 0.0 2.76 5 0.0 3.55 6 0.0 4.25 7 8 0.0 5.70 0.0 9.77 9 0.0125 I . 02 I . 93 32.60 io 0.125 41 . 71 ii 0.35 32.11 Q = 261 Bt u/ hr ft2 , RUN N O . 5W3H2 G == 1 009 P robe no. h QV = = 1 1 - 6 FBH Ibm/ h r ft7- , I—G B t u / hr ft2 °F IN 16 Bep — 3 4 . 9 h | o c , B t u / hr ft 2 °F I 0.0 3.56 2 0.0 3.98 3 4 0.0 4.20 0.0 4.69 5 0.0 5.80 6 0.0 8.54 7 0.0 18.08 8 0.025 26.98 9 0.075 41.21 10 0.325 40.71 11 0.30 35.68 Q — = 276 Q B t u / hr f t 2 , hav = 17 B tu Z h r tt2oF -104- RUN NO. G — 5W3H3 1273 FEH lbm / h r f t / I—6 Rep= I 0.0 4.35 2 0.0 4.86 2 0.0 5.70 l.\. 0.0 7.42 5 0.00625 10.61 6 0.01875 16.38 7 0.025 20.44 8 0.075 24.93 9 0.125 31.16 0.175 34.27 11 0.25 34.55 Q= 276 RUN NO. B t u / hr ft2 . IN 38 Rep = 4 8 . 7 7 lbm, / h r f t 2 , I —G P r o b e no. h Ioc , Btu/hr U2 o F I 0.0 9.18 2 0.00625 9.62 5 4 0.0125 10.18 0.025 I 2.2 7 5 0.025 15.26 6 0.0125 19.19 7 0.0375 22.48 8 0.0875 24.37 9 0. 1 29.16 10 0.175 31 . 8 4 ii 0.25 20.95 Q = 269 G tu/hrft2 , 9 7 1 7 . 3 B t u / h r ft2 °F hav = FBH 5W3H4 G= 1 4 1 0 _9 Io ^z B t u / h r f t 2 °F O h 43 H P r o b e no. 25 |M ha v = I 9 . 2 B t u / h r ft2oF -105- RUN NO- 5W4H1 G — 481 h |o ( , I—€ P r o b e no. IN 9 • Rep= 1 6 . 6 3 7 FBH lbm / h r f t 2, B t u / h r f t 2 °F I 0.0 I .78 2 0.0 2.10 5 4- 0.0 2.46 0.0 3.04 5 0.0 3.38 G 0.0 4.04 7 0.0 5.51 8 0.0 9.42 9 0.00625 33.43 10 0. 1 41.17 ■ 11 0 .4 37.49 Q = 236 B tu/ Urft2 , = I2 FEH bm/ h r i i 2, RUN NO. 5W4H2 G = 1 032 P r o b e no. hav I—G h B t u / hr IN Rep = I oc , 16 35.661 B t u / hr f t2 ° r I 0.0 3.58 2 0.0 4.02 5 0.0 4.40 4- 0.0 5.27 5 6 0.0 6.20 0.0 8.82 7 0.0625 17.16 8 0.0375 25.63 9 0. 1 33.47 10 0.2 30.99 11 0.3 24.91 Q = 232 B t u / hr f t 2 , ha v = ft2 cT 1 4 . 7 B t u / h r ftZoF -106- RUN NO. G= Probe no. : • 5W4H3 1217 _ FBH Ibm Z l l r f l ' IN 24 Rep = 42.06 h |o c , Btu/ hr ft2 0F 1— € I 0.0 4.31 2 0.0 4.86 3 4 0.0 5.63 0.0 7.36 5 6 0.0 10.19 0.0125 15.40 7 0.025 21 .91 8 0.0625 35.65 9 0. 1 46.00 io 0.3 48.63 ii 0.25 38.47 Q=T 240 Btu/ h r (t2 , RUN NO. 5W4H4 G =- 1 3 6 0 21,3 t h B t u / hr ft2 °F I N38 Rep- ^y FBH l l ' m/ br f i— e Pr obe no. Ha v = Ioc , Bt u/ hr f (2 °F I 0.0 7.16 2 0.0 8.42 3 4 0.00625 10.37 0.0125 12.72 5 0.0125 16.25 6 0.025 20.12 7 0.05 23.79 8 0.0625 30.43 9 0. 1 37.04 10 0.15 38.99 11 0.25 39.00 Q= 2 54 Bt u / hr f t 2 , ha v = 041 21 . 9 Bt u/ hr f t 2 °F -107- RUN Probe no. : ' FDH IN I 2 lbInZhrft , Rup = 2 3 . 5 2 1 NO; h | o , B t u / hr ft2 °F I— € I 0.0 I .67 2 0.0 I .49 3 4 0.0 I . 52 0.0 2. 11 5 6 0.0 2.79 0.0 3.70 7 0.0 6.34 8 0.0 17.67 9 0.5 33.89 io 0.35 42.01 ii 0.375 47.74 Q = 276 Btu/ hr ft2 , BtuZhrft2 o F CxJ CsJ CO Il 2 ZK 7W1H2 RUN NO. G = 1 097 hav = = 1 3 . 4 FBH IbmZ h r f t 7- I—G h|oc , Btu/ hr ft2 °F I 0.0 2.94 2 0.0 3.21 3 4 0.0 3.53 0.0 4.91 5 0.0 7.56 6 0.0 14.96 7 0.025 30.94 8 0.125 40.16 9 0.25 41.12 10 0.25 40.46 11 0.275 46.91 Probe no. Q = 292 B t u / hr f t 2 , Hq v = 21 . I B t u / h r H 2 o F -1087WI HS G = 1325 RUN FBH NO. R ep= 4 5 .855 h | o c , B t u / h r f t 2 °F 1— 6 P r o b e no. 31 in Ibm / h r f t 2 , I 0.0 3.84 2 0.0 4.77 5 0.0 6.12 lV 0.0 7 . 57 2 6 0.025 13.34 0.05 21 . 7 2 7 8 0.125 33.27 0.175 32.29 9 0.2 36.43 10 0.2 37.10 11 0.275 44.49 Q= run 310 B l u / hr ft2 , 7W1H4 G - — 1490 NO. 21.6 FBH ltW h r ft7-, I—6 P r o b e no. hav = B t u / hr ft'- IN 40 R e p = s i . 538 h |oc , B t u / hr f t 2 °F I 0.0 6.54 2 0.00635 8.25 3 4 0.00635 9.85 0.0125 11.30 5 0.0375 14.55 6 0.05 21 . 63 7 0.05 32.54 8 0.125 37.72 0.125 43.52 10 0.175 43.91 11 0.225 58.40 9 Q = # @) Btu/hrft2 , °F h Qv = 2 5 . 6 B tuZ hrft2oF -109- FBH RUM NO. 7W2H1 G = 68 0 —€ h Io f , B i u / h r f t 2 °F I 0.0 2.43 2 0.0 2.63 3 0.0 2.99 4 0.0 3.52 5 6 0.0 4.47 0.0 6.04 7 0.0 10.42 8 0.0 28.94 9 0.0875 58.58 O I—I ' lbm A ' ft , I P r o b e no. 12 S fp = 23.521 in 0.3 60.50 11 0.375 70.98 Q = 352 RUN NO. G= P r o b e no. B t u / hr f t 2 , 7 W2 H2 I 097 21.1 Iia v - FBH IbmZ h r f t 2-, B i V h r ft2 °F IN 19 R = P = 37.91 HIoc / B t u / h r f t - ° F i —e I 0.0 2.90 2 0.0 3.25 3 4 0.0 3.60 0.0 4.35 3 0.0 . 5.63 6 0.0 8.49 0.0625 20.81 0.075 30.99 0.25 33.62 10 0.25 34.03 11 0.325 36.07 7 8 9 Q — 294 B tu /h r ft2 , h Qv = 1 g 2 B t u / h r ftZoF RUN NO. G= 7 W2 H3 1325 FDH Ib m / h ’ fl , 1— 6 Probe no. IN Rep h | o c 27 45.865 , B t u / h r f t 2 °F I 0.0 3.59 2 0.0 4.17 3 4 0.0 5.36 0.0 7.65 5 6 0.0 13.20 0.025 21.28 7 8 0.075 30.29 0.125 34.19 9 10 0.175 39.22 0.225 36.57 ii 0.275 42.28 Q= run 285 B t u / h r f t 7- 7 VJ2 H4 . G -= 1 49 0 I 2I. 4 Iio v = FBH IbmZ h r f t 2 , n o P r o b e no. , — 6 B t u / hr ft2 c F IN 38 Rep = J 1 5 3 8 ^loc7 *ir f I 0.0 4.58 2 0.0 5.54 0.00625 8.56 3 4 0.025 12. 01 0.0375 16.56 6 0.05 26.12 7 0.0625 32.52 8 0.175 33.06 0.2 35.64 10 0.245 36.15 ii 0.275 39.53 5 9 q = Q = 281 Bt u / hr f t 2 , H q v :=r 2 2 . 7 Btu/hrft^°F -111- FBH ' km Z hr f t ' RUN NO. 7W3H1 G = 680 Probu no. in I5 R- p —2 3 . 5 2 1 h | oc , Btu/ hr ft2 0F i—e I 0.0 2.75 2 0.0 3.15 5 4 0.0 3.52 0.0 4.17 5 0.0 4.98 6 0.0 7.23 7 8 0.0 13.83 0.0 44.11 9 0.0625 47.65 0.175 45.55 0.3 37.11 10 ■ 11 Q =255 Bt u/ hr ft7', 7W3H2 RUN NO. G- = I 009 Ha v = 18,9 FBH IbmZhr ft2, Bt u Zh r f l 2 o F IN 22 R e p = 24 g i —e h |o£ , Bt u/ hr ft2 °F I 0.0 3.85 2 0.0 4.34 5 0.0 5. 11 4 0.0 6.65 5 0.0 10.76 6 0.0 20.72 7 0.025 36.53 8 0. 1 45.33 9 0.225 43.75 10 0.225 43.66 11 0.35 34.09 Pr obe no. Q — 259 B v u / hr f t 2 , ha v — 2 3 . 2 G t u / h r f t Z F RUN NO. G= P r o b e no. ' 7 W3 H3 1 238 I— | f\j FBH ! b m / h r f l 2, € 31 42.821 Rep = h |oc , B t u / h r f t 2 °F I 0.0 4.88 2 0.0 5.88 3 4 5 0.0 7.83 0.00625 11.05 0.025 15.65 6 0.0375 23.76 7 0.075 35.12 8 0.15 37.61 9 0.2 40.43 0.25 36.77 0.35 36.99 10 11 O = 268 B t u / hr ft2 , 7W3H4 RUN NO. G = - 1 49 0 P r o b e no. 23 3 hc v — " IN 41 Rcp= 51 _ 533 FBH lbm Zhr ftz , 1— 6 h B f u / h r ft2 °F Ioc , Bt u/ Itr f t 2 °F 0.0 10.38 0.125 12.62 5 4 5 0.025 14.35 0.05 17.38 0.05 20.61 6 0.075 26.15 0.1 32.05 0.1 34.01 0.15 37.62 1 2 7 8 9 10 11 Q =27 I 0.15 ' 0.225 Bt u / hr f t 2 , 36.37 40.16 ba v = 2 5 . 5 B t u / h r ft Z°F -113RUN 7W4H1 G=745 Probe no. ' F BH NO. in lbm' Z hr f t ' I5 fieP ^ s . 769 i—e h |o ( , Btu/ h r ft^ °F I 0.0 2.96 2 0.0 3.31 5 4 0.0 3.85 0.0 4.54 5 0.0 5.94 6 0.0 8.96 7 8 0.0 20.31 0.025 54.88 9 0.2 62.02. 10 0.3 52.86 11 0.4 58.34 Q = 234 RUN Bfo/ hr ft' , 7W4H2 1054 FBH NO. G r= lbm/ h r f t 2-, I—e P ro b e no. Hciv — 2 4 . 5 Biu/ hr r l ? ° F 8N 22 Rep = hIoc' 36.422 B f u Z h r f t 2- 0 F I 0.0 3.95 2 0.0 4.66 3 4 0.0 5.53 0.0 6.88 5 0.0 10.70 6 0.0125 21 . 41 7 0.0375 37.30 8 0.15 50.53 9 0.25 55.22 10 0.3 46.47 11 0.3 38.57 Q= 230 , B t u / h r ft ^, Hq v = . R ' u / h r f t ?-°F 25.16 RUN NO- 7W4H3 G = i^3b Re ' IN 31 P 42.717 h | oc, R f u / h r f t 2 o F I— 6 Probe no. ' FKH Ibmz / h r ft ' I 0.0 5.03 2 0.0 6 .3 7 3 0.0 8 .33 L\- 0.00625 13.52 5 0.0125 17.10 6 0.05 26.33 7 0. 1 39.20 8 0.125 40.37 9 0.2 45.23 IO 0.2 38.92 11 0.3 36.75 Q= 249 Bt u/ hr ft2 , RUN NO. 7 W4 H4 G := ' 4 9 0 25.4 — FBH IbmZ h r f R S I—G Pr obe no. hav B t u / hr ft2 °F IN 44 Rep =S i . 538 h Ioc , Bf u / hr f 2 0.0 14.90 3 4- 0.0 15.96 0.00625 18.96 5 0.0125 21 . 57 6 0.05 7 0.1 32.89 8 0.125 36.31 9 0.2 47.12 10 0.2 60.56 11 0.3 61.19 q — 246 B t u / hr f t ^ , OJ 12.80 OJ 0.0 r^. I °F hQ v— 3 0 . 9Btu/lir F RUN NO. G = ■ 9W1H1 745 h I o c , Bt u/ hr ft2 °F I— € Probe no. • FDH IN 21 Ibm A r f t 2z R e p = 2 5 . 7 6 9 I 0.0 2.41 2 0.0 2.70 3 4 0.0 3.02 0.0 3.61 5 0.0 4.61 6 0.0 6.99 7 0.00625 18.54 8 0.15 29.33 9 0.3 36.34 10 0.3 37.69 11 0.375 4 7 . 20 Efu/ Urfi1 , Q = 271 9W1H2 G = = 745 IN 29 FEH RUN NO. Ibm/ hr ft2-, I —6 Pr obe no. 1 6 . 7 Bt u / h r f r ° F hav — Rep = 3 4 . 9 hI q c , Bt u/ hr ft2 °F I 0.0 3.48 2 0.0 4.35 3 4 0.0 5.52 0.0 8.53 5 0.025 14.406 6 0.05 2 4 . 094 7 0.125 36.119 8 0.175 31 9 0.2 37.21 10 0.3 36.91 Ii 0.325 47.58 Q = 292 Bt u / hr ft ^ , hav — . 99 22.5 Btu/hr f t 2' ° F RUN NCk _9W1H3 G — 745 Probe no. : PB" »M ! b m/ h r f t , Rep- 42 50.431 h |oe , Btu/ hr ft2 °F 1— 6 I 0.0 8.98 2 0.025 9.87 3 4 0.025 11.53 0.05 12.79 3 0.05 15.23 6 0. 1 17.54 7 0. 1 18.89 8 0.15 21 . 92 9 0.2 23.95 0.25 26.96 0.35 34.43 io ii hav = 1 8 . 1 Bl u/ hr ft2 , Q =279 9W1H4 RUN NO. G — 887 FBH IbrnZ h r t f S IN 48 Rep = 5 7 . 6 2 5 h I—6 Pr obe no. B t u / hr ft2 c F Ioc , Bt u/ hr ft2 °F I 0.0 11.09 2 0.025 13.34 3 4 0.025 13.29 0.0375 14.58 3 0.05 16.28 6 0. 1 19-85 7 0.125 21 . 4 9 8 0.15 21 . 8 0 9 0.175 28.23 10 0.175 35.57 ii 0.25 47.16 Q = 297 B t u / hr ft , h (JV= 2 I . 5 Bt u / h r f t 2 °F RUN NOG= 9 W2 HI 1009 FBH |N I 7 A r f t 7z Rep = 2 5 . 7 6 9 h I o c , B t u / hr f t 2 °F I— 6 Probe no. I 0.0 3.50 2 0.0 4.37 5 0.0 4.82 4 0.0 5.88 5 0.0 7.23 6 0.0 12.39 7 0.0 21.14 8 0.0625 36.67 9 0.225 40.03 10 ■ ii 0.325 40.16 0.375 43.91 289 hr f t 2 . B tu/ 9W2H2 RUN NO. G — 1 054 hov = 1 9 . 5 FBfi IbmZ h r f t 2, IN 24 Rep - 36.42 , Btu/ hr ft2 °F I—€ Pr obe no. B t u / hr ft2 0 F I 0.0 4.95 2 0.0 6.03 5 0.0 6.90 4 0.0 10.57 5 0.0 14.74 6 0.0125 24.68 7 42.73 8 0.1 0 .2 9 0.325 39.53 10 0.325 40.66 11 0.45 34.33 Q= 294 Bt u / h r ft2 , 45.37 hQV= 24 . 7Btu/ hr ft2 °F -USRUN N O- G Probe no. ' 9W2H3 1 0 09 38 ifsj pbh lbm / h r f t 2 , Rep = 50.43 h |o(Z B t u / hr ft2 °F I— € I 0.0 6.11 2 0.0 8.71 5 0.0125 12.35 4 0.0375 17.43 5 0.0625 21 . 59 6 0.1 31 . 95 7 0.15 32.49 8 0.15 31 . 47 9 0.225 32.03 1 0 0.225 33.18 i i 0.35 36.67 Q = 291 Bt u/ Iirft2 , 9W2H4 G — 1054 RUN NO. Huv — 2 4 . 2 FDH, Ibm, / hr fU, B t u / hr ft7 cF IN 47 Rep = 5 7 . 6 2 i — e h ^ , Bt u/ hr ft 7- °F I 0.0 15.75 2 0.0375 18.34 0.05 20.43 0.075 21 . 0 6 0.07 5 23.54 0.075 27.96 0.075 28.07 I .0 29.87 0.125 34.94 0.175 38.67 0.25 48.32 P robe no. 3 4 5 6 7 8 9 1 0 1 1 Q =355 B t u / hr f t 2 , h OV " 2 7 . 6 BtuA r f t 2 0F RUN NO 9W4H1 I 666 FBH ,m 2 I lbH1A rft , Rep = 30.68 i—e h B t u / hr ft- °F I 0.0 3.77 2 0.0 4.50 3 4 0.0 5.36 0.0 7.07 3 6 0.0 13.06 0.0125 28.97 Probe no. 7 8 0.05 76.98 0.225 77.58 9 0.25 81.13 10 0.25 66.91 11 0.35 66.19 Q — 244 RU N Bt u/ hr A > 9W4H2 G — I 694 MO. P robe no. btiV— 3 9 . 2 FBH IbmZhr ft2 , I — e h Bt u / h r IN 27 Rep = 3 6 . 4 2 2 Ioc , B t u / hr f t 2 °F 1 0.0 4.78 2 0.0 5.31 0.0 7.90 3 4- 5 6 7 8 9 10 11 Q = 246 0.00625 12.73 0.0125 21 . 66 0.05 36.15 0.125 46.49 0.225 43.45 0.25 45.07 0.35 38.82 0.35 34.95 B t u / hr ft^ , °F ha v = 2 7 . 5 B t u / h r f t ? °F RU N NO. G 9W4H3 1638 Probe no. • ' IN 38 FBH lbm / hrft2. i—e 43.375 llIoc' BfU//*,r ff2 0 f I 0 .0 2 0.00625 3 4 0.0125 5 6 0.05 7 0.075 8 0.175 9 0.25 10 0.25 11 0.3 0.025 0.075 Q — 246 Bt u/ hr ft “ , RUN NO. G = I 506 IbmZlir ft2-, I—6 Pr obe n o . hav — 3 1 . 6 DiuZhr ft7 °t. IN 47 Rep - 5 2 . 0 5 6 H , B t u / hr ft7-°F Ioc I 0 .0 15.19 2 0.0375 17.97 3 4- 0.05 20.42 0.0625 24.61 5 0.1 27.23 6 0.1 34.97 7 0.1 36.15 8 0.175 35.65 9 0.2 36.17 10 0.3 36.62 11 0.25 35.75 q _ 249 Btu/hrft2 , ^q v — 3 0 . 4 Ct u/ hr ft2 F MONTANA STATE UNIVERSITY LIBRARIES N378 K562 cop. 2 Kim, Joon Taik Heat tr a n s fe r in the fin n ed f lu id iz e d bed tubular h a t exchanger NAMK AN O A O D w K Sg