Email: Phone: Cell: Fax: cetin@clarkson.edu (315) 268-6514 (315) 276-8051 (315) 268-6695 Photo-Acoustics Research Laboratory Photo-Acoustics Research Laboratory Dept. of Mechanical and Aero. Engineering Clarkson University Potsdam, New York 13699-5725 Microspheres in Acoustic Fields: Rolling Moment Resistance and Work-of-Adhesion Measurements Çetin Çetinkaya 1 Dept. of Mechanical and Aeronautical Engineering, Clarkson University – February 7, 2007 Photo-Acoustics Research Laboratory M. D. M. Peri and C. Cetinkaya, Applied Physics Letters, Vol. 86, 2005. Microspheres in Acoustic Fields: Rolling Moment Resistance and Work-of-Adhesion 2 Dept. of Mechanical and Aeronautical Engineering, Clarkson University – February 7, 2007 Substrate Transducer Laser Spot 21.4 mm PSL Photo-Acoustics Research Laboratory Excitation Pulse Coupling Gel Interferometer Head Output Signal Laser Spot Laser Spot Vibrational Motion of Particles in Acoustic Fields 3 Dept. of Mechanical and Aeronautical Engineering, Clarkson University – February 7, 2007 β 1 r3 2 δ 3 2 − β 2α r3 4 δ 3 4 M = 6πW A ( D / 2) 2 θ • Measured work of adhesion: 18.4 mJ/m2 • Measured rocking frequency: 64.1 kHz • Rocking frequency (calculated): 72.4 kHz • Axial resonance frequency: 1.83 MHz • Work of adhesion (literature): 23.5 mJ/m2 • PSL on Si substrate M. D. Murthy Peri and C. Cetinkaya, Journal of Colloid and Interface Science, Vol. 288, 2005. M. D. Murthy Peri and C. Cetinkaya, Philosophical Magazine A, Vol.Research 85, No. Laboratory 13, 2005. Photo-Acoustics FA = Axial Vibration vs. Rocking Motion 4 Dept. of Mechanical and Aeronautical Engineering, Clarkson University – February 7, 2007 Displacement(nm) Dept. of Mechanical and Aeronautical Engineering, Clarkson University – February 7, 2007 0 50 100 150 200 T im e ( µ s e c ) P 1 75kH z 400V 250 300 350 400 -6 0 50 52 1 2 3 4 5 x 10 54 56 58 60 62 64 66 68 70 72 74 76 Photo-Acoustics Research Laboratory 78 80 82 84 M u ltip lic a t io n F a c t o r (4 .3 3 )-P 1 7 5 k H z 4 0 0 V F re q (k H z ) M. D. Murthy Peri and C. Cetinkaya, under review for publication in Applied Physics Letters. -6 -4 -2 0 2 4 6 6 7 8 86 88 90 92 94 96 98 100 W a fe r P a rtic le 5 • Further Research: Shifts of resonance frequencies indicate nonlinearity and/or dissipation (capillary effect) • Measured work of adhesion: 26.16 mJ/m2 • Measured rocking frequency: 76.5 kHz • Measured rocking amplitude: θmax~ 0.06 deg • The rocking frequency is calculated as 72.4 kHz • Air-coupled excitation at 75kHz Air-Coupled Excitation of Rocking Motion (amplitude) Photo-Acoustics Research Laboratory W. Ding, A. Howard, M.D. Peri and C. Cetinkaya, under review for publication in Philosophical Magazine . 6 • Detachment force is much larger than rolling force; • Particle has to be glued to a cantilever; • Adhesion measurement based on detachment is difficult; Contact Experiments: Rolling Moment Resistance Dept. of Mechanical and Aeronautical Engineering, Clarkson University – February 7, 2007 Work-of-adhesion of PSL particles on silicon substrates are measured in a noncontact manner; Acoustic excitation of PSL particle has been demonstrated; A contact method work-of-adhesion measurement method that does not require any size information prior to testing has been developed and presented; Critical rolling distances are reported. Reference papers are listed in this document for further examination. • • • • Photo-Acoustics Research Laboratory Experimental evidence on existence of rolling resistance moment in a non-contact way, for the first time, has been presented; • Conclusions and Remarks 7 Dept. of Mechanical and Aeronautical Engineering, Clarkson University – February 7, 2007