Writing a Lab Report for Chem 113 Rachel Chupik and Jason Denny General Information • Have a title page – Name, date, section, experiment • • • • • Use size 12 font in a standard font type Make heading clearly visible TYPE everything Must be your original work ASK your TA questions when in doubt The Abstract (0.9) • Three main components – Chemical principles – Experiment synopsis – Success criteria !!! Third person, passive voice !!! This experiment will test and exercise the principles of acidbase titration and determination of equivalence, as well as exercises on the determination of the pKa of a weak acid. Through the use of the known reactivity of a base (NaOH), an acid of unknown reactivity and measured mass will be reacted to determine equivalence, and equivalent weight, and by recording changes in pH, these data can be used to determine the pKa. Success will be determined by comparing the resulting pKa with the table of pKa values listed at the back of the text with a reasonable result being within 10% of any listed value. Experimental (2) • • • • • • Balanced chemical equations Mathematical equations Reagent table Materials list Diagram Procedure Equations (0.8) • Chemical equations • Mathematical equations – Typed – Balanced – Include phases – Typed – One equation for each type of calculation performed • Example from Exp 17: • Example: Mg (s) + 1/2 O2 (g) MgO (s) % 𝑀𝑀 = % RSD = 𝑚𝑚𝑚𝑚 𝑀𝑀 𝑚𝑚𝑚𝑚 𝑀𝑀𝑀 𝑆𝑆 𝑎𝑎𝑎 x 100 x 100 Reagent Table (0.3) • Include any chemical reactant you used • Make table with at least the name, formula and molar mass • Write diatomics as diatomics • List molecular weight to at least 2 decimal places Symbol H2SO4 NaOH C20H14O4 Common Name Sulfuric acid Sodium hydroxide Phenolphthalein Molecular Weight (g.mol-1) 98.079 39.9969 318.33 Materials List (0.3) and Diagram (0.2) • Materials List – All equipment and glassware used in the experiment – NO chemicals • Diagram – Computer generated or copied from online source – Referenced Procedure (0.4) • Simple, concise, stepwise outline of what YOU did • Example: !!! Third person, past tense, passive voice !!! – 1. A 0.2567 gram portion of the unknown acid was weighed and added to the beaker, along with 50 mL of water and 1 drop of phenophthalein. – 2. Standardized sodium hydroxide (NaOH) was titrated into the solution, the changes in pH were recorded, more data points were recorded, smaller volumes were added, as the rate of change increased. Results/Data Tables (2) • N3….No Naked Numbers – Always include units • Make the table visually appealing – Make sure a word is not split over two lines • Include raw data and calculated numbers Emission Color Scale Reading Wavelength (nm) Energy (J) Energy Level Purple 180 350 1.2 5 Blue 170 450 1.5 4 Green 160 550 1.8 3 Yellow 150 650 1.9 2 Calculations (1.5) • BAD example – 43/7=6.1 • AWESOME example • Include units throughout and highlight final answer – Again make it visually appealing Graph (0.5) Helium Spectrum: Scale Reading vs. Wavelength 8 7 y = 1.1429x - 0.3333 R² = 0.9796 Scale Reading 6 5 4 3 2 1 0 0 1 2 3 4 Wavelength (nm) 5 6 7 Discussion • There is not a minimum length but it should not exceed 2 pages • MUST have three sections – Chemical concept (1) – Experimental observations (1) – Results (1) – Understanding of material (1) Conclusions • MUST include 3 things and only needs to be a single paragraph – Results (0.3) – Statistics (% error) (0.5) • Compare to literature value if possible – Sources of error (0.2) • Human error doesn’t count