©GOES 746 . - ·- ,. --,,"" ' ,··.·;; I., , . ·_ . :.·~ .' _,,_, __ _, ..,--~----- -··---~, t!fj!lffu~ ·Expiration Date:Januatv·3l, 2016 . · --- - "~"-,--_, .. :,_~:~·_:-:"<~~ .. ~- '., ;.~ ·:·h,- i ' cl. ~ . Cover5: 2/1/2015 - 1131/2016 Director~ Laboratory Services Division y{\(,'h'M- ~~'.>~ - -- -- Certifi~ation Officer LITHO IN U.S.A. This certificate remains the property o(the North Dakota State. Department.or" Health and may be recalled, for cause, at any time, by theDepilriilienL''R:e00griition~ofan ouf:of-statefaboratory's certification or accreditation from another state c~rtlfica~iqn qr-acpredi¥!tfon-progdun by the North Dakota State Department of Health is neither an endorsement. of.the. results reported l:Jy.the"laboratory nor a guarantee of the validity or accuracy of the results reported by the'labmai9b'------~· ·' Date oflssue: May 26; 2015 . -,.__ . _·,,.__ C~ffificatiop Nillnber: R-205 •' :· .·=\-·; _-·,_1~- Eurofins LancasterLabOtatortes.,I~c. -2425 Ne~iiolland Pike - Lancaster, PA ·.·.·...·. -~'.' <by : •• . . .· . < . . ·State of Pennsylvania IDepamnent ofEnvironinental Protection · . . -, ·. •.,..: iJ'.[6'.i: < ·.. . . . ., All Clean Water Act, Resource Cons~ati©n·aii'.c!R~~overy Act; Sii:feDrinking Water Act chemical parameters by the methods on the'accoriipanymg list of certified parameters for this laboratory . The North Dakota State Departrtierit ofHealth re<;ognizes the certification or accreditation of -· NORTH DAKOTA STA:'f~DEP'ARTMENT OF HEALTH RECOGNITION OF CEifTJ:F'ICATION OR.ACCREDITATION Certified Parameters for Eurofins Lancaster Laboratories, Inc. 2425 New Holland Pike, Lancaster, PA Issued by North Dakota Department ofHealth Laboratory Services Division - Chemistry May26,2015 Certification Period: February OJ, 2015 through January 31, 2016 Lab Certification No: R-205 Based on Certificate No: 014-001 From the State ofPennsylvania Department ofEnvironmental Protection Program Clean Water Act Thursday, May 28, 2015 Parameter Method Color Acidity Alkalinity Hardness (Calcium) Conductivity Residue-total Residue-filterable Non-filterable Residue (Total Suspended Solids) Setlleable Solids Chromium (Hexavalent) Cyanide Amenable to Chlorination Manual distillation for Fluoride Fluoride Manual distillation for Ammonia Ammonia asN Ammonia as N Digestion for Phosphorous Orthophosphate Orthophosphate Phosphorus (Total) Sulfide Sulfide Silica (Dissolved) Biochemical Oxygen Demand (BOD) Carbonaceous Biochemical Oxygen Demand (CBOD) Total Organic Carbon (TOC) Surfactants (MBAS) Cyanide (Total) Residue-Volatile 1,2,3,4,6,7,8,9-0ctachlorodibenzofuran (OCDF) 1,2,3,4,6,7,8,9-0ctachlorodibenzo-p-dioxin (OCDD) 1,2,3,4,6,7,8-Heptachlorodibenzofuran (HpCDF) 2120 B-2001 2310 B-1997 2320 B-1997 2340 C-1997 2510 B-1997 2540 B-1997 2540 C-1997 2540 D-1997 2540 F-1997 3500 Cr B-2009 4500-CW G-1999 4500-F-B-1997 4500-F- C-1997 4500-NH3 B-1997 4500-NH3 C-1997 4500-NH3 D-1997 4500-P B-1999 4500-P E-1999 4500-P F-1999 4500-P F-1999 4500-S(2-) D-2000 4500-S(2-) F-2000 4500-Si02 C-1997 5210 B-2001 5210 B-2001 5310 C-2000 5540 C-2000 ASTM D7511-09 EPA 160.4 EPA 1613B EPA 1613B EPA 1613B Source # Status 91 6 6 6 6 6 6 6 6 107 91 6 6 6 6 6 91 91 91 91 91 91 107 91 91 91 91 109 70 74 74 74 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Cerf1fied Certified Certified Page 1 o/26 Program Clean Water Act Parameter Method 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (HpCDD) 1,2,3,4,7,8,9-Heptachlorodibenzofuran (HpCDF) 1,2,3,4, 7 ,8-Hexachlorodibenzofuran (HxCDF) 1,2,3,4, 7,8-Hexachlorodibenzo-p-dioxin (HxCDD) 1,2,3,6, 7 ,8-Hexachlorodibenzofuran (HxCDF) 1,2,3,6,7 ,8-Hexachlorodibenzo-p-dioxin (HxCDD) 1,2,3,7,8,9-Hexachlorodibenzofuran (HxCDF) 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin (HxCDD) 1,2,3,7,8-Pentachlorodibenzofuran (PeCDF) 1,2,3,7,8-Pentachlorodibenzo-p-dioxin (PeCDD) 2,3,4,6,7,8-Hexachlorodibenzofuran (HxCDF) 2,3,4,7,8-Pentachlorodibenzofuran (PeCDF) 2,3, 7,8-Tetrachlorodibenzofuran (TCDF) 2,3, 7 ,8-Tetrachlorodibenzo-p-dloxin (TCDD) EPA 16138 EPA 16138 EPA 16138 EPA 16138 EPA 16138 EPA 16138 EPA 16138 EPA 16138 EPA 16138 EPA 16138 EPA 16138 EPA 16138 EPA 16138 EPA 16138 EPA 1631 E EPA 1664 A EPA 1664 B EPA 1666A EPA 1666A EPA 1666A EPA 1666A EPA 1666A EPA1666A EPA 1666A EPA1666A EPA 1666A EPA 1666A EPA1666A EPA1666A EPA1666A EPA 1666A EPA 1666A EPA 1671 A EPA 1671 A EPA 1671 A EPA 1671 A EPA 1671 A EPA 1671 A EPA 1671 A EPA 1671 A EPA180.1 EPA200.7 EPA 200.7 EPA200.7 EPA200.7 EPA200.7 EPA 200.7 EPA200.7 EPA200.7 Mercury Oil and Grease Oil and Grease 4-methyl 2-pentanone (MIBK) Diisopropyl Ether Ethyl Acetate lsobutyraldehyde lsopropyl acetate lsopropyl alcohol Methyl formate n-Amyl acetate n-Amyl alcohol n-Butyl acetate n-Heptane n-Hexane Tert-Butyl alcohol Tetrahydrofuran Xylenes (Total) 2-Methoxyethanol Acetonitrile Diethylamine Dimethyl sulfoxide Ethanol Methanol n-Propanol Triethylamlne Turbidity Aluminum Antimony Arsenic Barium Beryllium Boron Cadmium Calcium Thursday, May 28, 2015 Source # Status 74 74 74 74 74 74 74 74 74 74 74 74 74 74 80 72 111 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 70 2 2 2 2 2 2 2 2 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Page2o/26 Program Clean Water Act Parameter Method Chromium Cobalt Copper Iron Lead Magnesium EPA 200.7 EPA200.7 EPA 200.7 EPA200.7 EPA 200.7 EPA200.7 EPA200.7 EPA200.7 EPA 200.7 EPA 200.7 EPA200.7 EPA200.7 EPA200.7 EPA200.7 EPA200.7 EPA 200.7 EPA200.7 EPA 200.7 EPA200.8 EPA200.8 EPA 200.8 EPA200.8 EPA200.8 EPA200.8 EPA200.8 EPA200.8 EPA200.8 EPA200.8 EPA200.8 EPA200.8 EPA 200.8 EPA200.8 EPA 200.8 EPA200.8 EPA200.8 EPA 200.8 EPA200.8 EPA200.8 EPA200.8 EPA200.8 EPA200.8 EPA200.8 EPA 200.8 EPA200.8 EPA 245.1 EPA 300.0 EPA300.0 EPA300.0 EPA 300.0 Manganese Molybdenum Nickel Potassium Selenium Silver Sodium Thallium Tin Titanium Vanadium Zinc Aluminum Antimony Arsenic Barium Beryllium Boron Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Molybdenum Nickel Potassium Selenium Silver Sodium Thallium Tin Titanium Vanadium Zinc Mercury Bromide Chloride Fluoride Nitrate as N Thursday, May 28, 2015 Source # Status 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 70 9 9 9 9 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Page3 o/26 Program Clean Water Act Parameter Method Nitrite as N Sulfate Cyanide (Total) Ammonia as N Total Kjeldahl Nitrogen (TKN) Nitrate + Nitrite as N Nitrate as N Nitrite as N Phosphorus (Total) Chemical Oxygen Demand (COD) Phenolics (Total) 1,2-Dichlorobenzene 1,2-Dichloroethane 4-methyl 2-pentanone (MIBK) EPA300.0 EPA300.0 EPA 335.4 EPA 350.1 EPA 351.2 EPA 353.2 EPA353.2 EPA 353.2 EPA 365.1 EPA 410.4 EPA420.4 EPA 524.2 EPA524.2 EPA524.2 EPA524.2 EPA524.2 EPA 524.2 EPA524.2 EPA524.2 EPA524.2 EPA602 EPA602 EPA602 EPA608 EPA608 EPA608 EPA608 EPA608 EPA608 EPA608 EPA608 EPA608 EPA608 EPA608 EPA608 EPA608 EPA608 EPA608 EPA608 EPA608 EPA 608 EPA 608 EPA608 EPA608 EPA608 EPA608 EPA608 EPA608 EPA622 Benzene Chlorobenzene Chloroform Methylene chloride Tetrahydrofuran Toluene Benzene Ethylbenzene Toluene 4,4'-DDD 4,4'-DDE 4,4'-DDT Aldrin alpha-BHC Aroclor 1016 Aroclor 1221 Aroclor 1232 Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260 beta-BHC Chlordane (Technical) delta-BHC Dieldrin Endosulfan I Endosulfan II Endosulfan Sulfate Endrin Endrin Aldehyde gamma-BHC (Lindane) Heptachlor Heptachlor Epoxide Toxaphene Azinphos-methyl Thursday, May 18, 1015 Source # Status 9 9 9 70 70 70 70 70 70 70 9 120 120 120 120 120 120 120 120 120 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 92 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Page4 o/16 Program Clean Water Act Parameter Bolstar (Sulprofos) Chlorpyrifos Demeton-0 Demeton-S Diazinon Dichlorovos Disulfoton Ethoprop Fensulfothion Fenthion Merphos Methyl parathion Mevinphos Naled Phorate Stirofos 1, 1, 1-Trichloroethane 1, 1,2,2-Tetrachloroethane 1, 1,2-Trichloroethane 1, 1-Dichloroethane 1, 1-Dichloroethene 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dlchloropropane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2-Chloroethyl vinyl ether Acrolein Acry/onitrile Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane Cls-1,3-Dichloropropene Dibromochloromethane Ethyl benzene Methylene chloride Tetrachloroethene Toluene Trans-1,2-Dichloroethene Trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride (chloroethene) Tlrursday, May 18, 1015 Method EPA622 EPA622 EPA622 EPA622 EPA622 EPA622 EPA622 EPA622 EPA 622 EPA622 EPA 622 EPA622 EPA622 EPA622 EPA622 EPA622 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 Source # Status 92 92 92 92 92 92 92 92 92 92 92 92 92 92 92 92 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Page5of16 Program Clean Water Act Thursday, May 18, 1015 Parameter Method 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methyl-4,6-dinitrophenol 2-Nitrophenol 3,3'-Dichlorobenzidine 4-Bromophenyl Phenyl Ether 4-Chloro-3-methylphenol 4-Chlorophenyl Phenyl Ether 4-Nitrophenol Acenaphthene Acenaphthylene Anthracene Benzidine Benzo(a)anthracene Benzo(a)pyrene Benzo(b)Huoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl Butyl Phthalate bis(2-chloroethoxy)methane bis(2-Chloroethyl)ether bis(2-Ethylhexyl)phthalate Chrysene Dibenzo(a,h)anthracene Diethyl phthalate Dimethyl phthalate Di-n-butyl phthalate Di-n-octyl phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane lndeno(1,2,3-cd)pyrene lsophorone Naphthalene Nitrobenzene N·Nitrosodimethylamine EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA 625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 Source # Status 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Page6o/16 Program Clean Water Act Parameter Method N-nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrena Cyanide (Available) Cyanide (Free) EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 OIA-1677-09 OIA-1677-09 65 65 65 65 65 65 113 113 Certified Certified Certified Certified Certified Certified Certified Certified SW6461010 SW6461311 SW6461312 SW6466010B SW646 60108 SW6466010B SW6466010B SW6466010B SW646 60108 SW646 60108 SW6466010B SW6466010B SW6466010B SW8466010B SW8466010B SW8466010B SW846 60108 SW846 60108 SW646 60108 SW846 60108 SW646 60108 SW646 60108 SW8466010B SW8466010B SW846 60108 SW846 60108 SW846 60108 SW646 60108 SW6466010B SW646 60108 SW6466010B SW846 60108 SW8466010C SW846 6010C SW8466010C SW846 6010C SW846 6010C SW8466010C SW6466010C 64 61 62 64 64 64 64 64 64 64 64 64 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 64 64 84 84 84 96 96 96 96 96 96 96 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Source # Status Resource Conservation and Recovery Act lgnitability Toxicity Characteristic Leaching Procedure (TCLP) Synthetic Precipitation Leaching Procedure (SPLP) Aluminum Antimony Arsenic Barium Beryllium Boron Cadmium Calcium Chromium Cobalt Copper Iron Lead Lithium Magnesium Manganese Molybdenum Nickel Potassium Selenium Silica Silver Sodium Strontium Thallium Tin Titanium Vanadium Zinc Aluminum Antimony Arsenic Barium Beryllium Boron Cadmium Thursday, May 18, 1015 Page 7of16 Program Parameter Resource Conservation and Recovery Act .. Thursday, May 18, 1015 Calcium Chromium Cobalt Copper Iron Lead Lithium Magnesium Manganese Molybdenum Nickel Potassium Selenium Silica Sliver Sodium Strontium Thallium Tin Titanium Vanadium Zinc Aluminum Antimony Arsenic Barium Beryllium Boron Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Molybdenum Nickel Potassium Selenium Silver Sodium Strontium Thallium Tin Titanium Vanadium Zinc Method SW846 6010C SW846 6010C SW846 6010C SW8466010C SW8466010C SW8466010C SW8466010C SW8466010C SW8466010C SW8466010C SW8466010C SW8466010C SW846 6010C SW8466010C SW8466010C SW8466010C SW8466010C SW8466010C SW8466010C SW846 6010C SW846 6010C SW846 6010C SW8466020A SW8466020A SW8466020A SW8466020A SW8466020A SW8466020A SW8466020A SW8466020A SW8466020A SW8466020A SW8466020A SW8466020A SW8466020A SW8466020A SW8466020A SW846 6020A SW846 6020A SW846 6020A SW846 6020A SW846 6020A SW8466020A SW8466020A SW8466020A SW8466020A SW8466020A SW8466020A SW8466020A Source # Status 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Page8of16 Program Parameter Resource Conservation and Recovery Act • • Thursday, May 28, 2015 Perchlorate Chromium (Hexavalent) Chromium (Hexavalent) Mercury Mercury 1,2-Dibromo-3-Chloropropane (D8CP) 1,2-Dibromoethane Diesel Range Organics Ethanol Ethylene Glycol Gasoline Range Organics lsobutyl Alcohol lsopropyl alcohol Methanol n-butyl alcohol n-Propanol Total Petroleum Hydrocarbons Diesel Range Organics Ethanol Ethylene Glycol Gasoline Range Organics lsobutyl Alcohol lsopropyl alcohol Methanol n-butyl alcohol n-Propanol Total Petroleum Hydrocarbons Benzene Ethylbenzene lsopropylbenzene m-Xylene Naphthalene a-xylene p-Xylene Toluene Xylenes (Total) 4,4'-DDD 4,4'-DDE 4,4'-DDT Aldrin alpha-8HC alpha-chlordane beta-8HC Chlordane (Technical) delta-8HC Dieldrin Endosulfan I Endosulfan II Endosulfan Sulfate Method SW8466850 SW846 7196A SW846 7199 SW8467470 SW846 7471 SW846 8011 SW846 8011 SW84680158 SW846 80158 SW84680158 SW84680158 SW84680158 SW84680158 SW84680158 SW84680158 SW84680158 SW846 80158 SW846 8015C SW846 8015C SW846 8015C SW846 8015C SW846 8015C SW846 8015C SW846 8015C SW846 8015C SW846 8015C SW846 8015C SW846 80218 SW846 80218 SW846 80218 SW846 80218 SW846 80218 SW846 80218 SW8468021B SW8468021B SW8468021B SW8468081A SW8468081A SW8468081A SW846 8081A SW8468081A SW846 8081A SW846 8081A SW846 8081A SW846 8081A SW846 8081A SW846 8081A SW846 8081A SW846 8081A Source # Status 96 81 84 69 69 81 81 84 84 84 84 84 84 84 84 84 84 96 96 96 96 96 96 96 96 96 96 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Page9o/26 Program Parameter Resource Conservation and Recovery Act Endrin Endrin Aldehyde Endrin Ketone gamma-8HC (Lindane) gamma-chlordane Heplachlor Heptachlor Epoxide Melhoxychlor Mirex Toxaphene 4,4'-DDD 4,4'-DDE 4,4'-DDT Aldrin alpha-8HC alpha-chlordane bela-8HC Chlordane (Technical) delta-8HC Dieldrin Endosulfan l Endosulfan It Endosulfan Sulfate Endrin Endrin Aldehyde Endrin Ketone gamma-8HC (Lindane) gamma-chlordane Heptachlor Heptachlor Epoxide Methoxychlor Mirex Toxaphene Aroclor 1016 Aroclor 1221 Aroclor 1232 Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260 Atrazine Azinphos-methyl (Gulhion) 8olslar (Sulprofos) Carbophenothlon Chlorfenvinphos Coumaphos Demeton-0 Demeton-S Diazinon Thursday, May 28, 2015 Method SW846 8081A SW846 8081A SW846 8081A SW846 8081A SW846 8081A SW846 8081A SW846 8081A SW846 8081A SW846 8081A SW846 8081A SW846 80818 SW846 80818 SW846 80818 SW846 80818 SW846 80818 SW846 80818 SW846 80818 SW846 80818 SW846 80818 SW846 80818 SW846 80818 SW846 80818 SW846 80818 SW846 80818 SW846 80818 SW846 80818 SW846 80818 SW846 80818 SW846 80818 SW846 80818 SW846 80818 SW846 80818 SW846 80818 SW846 8082A SW846 8082A SW846 8082A SW846 8082A SW846 8082A SW846 8082A SW8468082A SW846 8141A SW846 8141A SW8468141A SW846 8141A SW846 8141A SW846 8141A SW846 8141A SW846 8141A SW846 8141A Source # Status 84 84 84 84 84 84 84 84 84 84 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 82 82 82 82 82 82 82 82 82 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Page JOo/26 Program Parameter Resource Conservation and Recovery Act Dichlorovos DisuJfoton EPN Eth ion Ethoprop Famphur Fensulfothion Fenthion Malathion Merphos Methyl parathion Mevinphos Naled Parathion, methyl Ph orate Ronne I Simazine Stirofos Tokuthion Trichloronate Atraz!ne Azinphos-methyl 8olstar (Sulprofos) Carbophenothion Chlorpyrifos Coumaphos Demeton-0 Demeton-S Diazinon Dichlorovos (DDVP) Disulfoton EPN Ethion Ethoprop Ethyl parathion Famphur Fensulfothion Fenthion Malathion Merphos Methyl parathion Mevinphos Na led Phorate Ronnel Simazine Stirofos Tokuthion Trichloronate Tflurstlay, May 28, 1015 Method SW846 8141A SW846 8141A SW846 8141A SW846 8141A SW846 8141A SW846 8141A SW8468141A SW846 8141A SW846 8141A SW846 8141A SW846 8141A SW846 8141A SW846 8141A SW846 8141A SW846 8141A SW846 8141A SW846 8141A SW846 8141A SW846 8141A SW846 8141A SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 SW846 81418 Source # Status 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Page 11 o/26 Program Parameter Method Source # Sta/us Resource Conservation and Recovery Act 2,4,5-T 2,4,5-TP (Silvex) 2,4-D 2,4-06 Dalapon Dicamba Dlchloroprop Dinoseb MCPA MCPP Pentachlorophenol Picloram 1, 1, 1,2-Tetrachloroethane 1, 1, 1-Trichloroethane 1, 1,2,2-Tetrachloroethane 1, 1,2-Trichloroethane 1, 1-Dichloroethane 1, 1-Dichloroethene 1, 1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane (D6CP) 1,2-Dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 1,4-Dloxane 2,2-Dichloropropane 2-6utanone (MEK) 2-Chloroethyl vinyl elher 2-Chlorotoluene 2-hexanone 2-Nitropropane 4-Chlorotoluene 4-methyl 2-pentanone (Ml6K) Acetone Acetonitrile Acrolein Acrylonitrile Benzene Benzyl Chloride Bromobenzene Bromochloromethane Thur.rday, May 28, 2015 SW846 8151A SW846 8151A SW846 8151A SW8468151A SW846 8151A SW846 8151A SW846 8151A SW846 8151A SW846 8151A SW846 8151A SW846 8151A SW846 8151A SW846 82606 SW846 82606 SW846 82606 SW846 82608 SW846 82606 SW846 82606 SW846 82606 SW846 82606 SW846 82606 SW846 82606 SW846 82606 SW846 82606 SW846 82606 SW84682606 SW84682606 SW84682606 SW84682606 SW84682606 SW84682606 SW84682606 SW84682608 SW846 82606 SW846 82608 SW846 82606 SW846 82606 SW846 82608 SW846 82606 SW846 82606 SW846 82606 SW846 82606 SW846 82606 SW846 82606 SW846 82606 SW846 82606 SW846 82606 SW84682606 SW84682606 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Page 12of26 Program Parameter Method Source # Status Resource Conservation and Recovery Act Bromodlchloromethane Bromofonn Bromomethane Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane Chloroprene Cis-1,2-Dichloroethene Cis-1,3-Dichloropropene Crotonaldehyde Dibromochloromethane Dibromomethane DichlorodiRuoromethane Diethyl Ether Epichlorohydrin Ethanol Ethyl Acetate Ethyl Methacrylate Ethylbenzene Ethylene Oxide Hexachlorobutadiene Hexachloroethane lodomethane lsobutyl Alcohol lsopropyl alcohol /sopropylbenzene m+p-Xylene Methacrylonitrile Methyl methacrylate Methyl tert butyl ether Methylene chloride Naphthalene n-butyl alcohol n-Butylbenzene n-Propylamine N-Propylbenzene a-xylene Pentachloroethane p-lsopropyltoluene Propionilrile sec-Butyl benzene Styrene Tert-Butyl alcohol Tert-Butylbenzene Tetrachloroethene Toluene Thursday, May 28, 2015 SW846 8260B SW846 8260B SW846 8260B SW8468260B SW8468260B SW8468260B SW8468260B SW846 8260B SW846 8260B SW846 8260B SW846 8260B SW846 8260B SW8468260B SW8468260B SW8468260B SW8468260B SW8468260B SW846 8260B SW846 8260B SW846 8260B SW846 8260B SW846 8260B SW846 8260B SW8468260B SW8468260B SW8468260B SW8468260B SW846 8260B SW846 8260B SW846 8260B SW846 8260B SW846 8260B SW8468260B SW8468260B SW8468260B SW8468260B SW846 8260B SW846 8260B SW846 8260B SW846 8260B SW846 8260B SW846 8260B SW8468260B SW8468260B SW8468260B SW846 8260B SW846 8260B SW846 8260B SW846 8260B 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Page 130/26 Program Parameter Resource Conservation and Recovery Act trans-1,2-Dlchloroethylene trans-1,3-Dichloropropylene trans-1,4-Dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl Acetate Vinyl chloride (chloroethene) Xylenes (Total) 1, 1, 1,2-Tetrachloroethane 1, 1, 1-Trichloroethane 1, 1,2,2-Tetrachloroethane 1, 1,2-Trichloroethane 1, 1-Dichloroethane 1, 1-Dichloroethene 1, 1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimelhylbenzene 1,2-Dibromo-3-Chloropropane (D8CP) 1,2-Dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-0ichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 1,4-Dioxane 2,2-Dichloropropane 2-butanone 2-Chloroethyl vinyl ether 2-Chlorotoluene 2-hexanone 2-Nitropropane 4-Chlorotoluene 4-methyt 2-pentanone (Ml8K) Acetone Acetonitrile Acrolein Acrylonitrile Benzene Benzyl Chloride Bromobenzene Bromochloromethane Bromod!chloromethane Bromoform Bromomethane Carbon Disulfide Thursday, May 18, 1015 Method SW846 82608 SW846 82608 SW846 82608 SW846 82608 SW846 82608 SW846 82608 SW846 82608 SW84682608 SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW846 8260C SW846 8260C SW846 8260C SW846 8260C SW846 8260C SW846 8260C SW846 8260C SW846 8260C SW846 8260C SW846 8260C SW846 8260C SW846 8260C SW8468260C SW846 8260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW846 8260C SW846 8260C SW846 8260C SW846 8260C Source # Status 84 84 84 84 84 84 84 84 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified PageUo/26 Program Parameter Method Source # Status Resource Conservation and Recovery Act Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane Chloroprene Cis-1,2-Dichloroethene Cis-1,3-Dlchloropropene Crotonaldehyde Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl Ether Epichlorohydrin Ethanol Ethyl Acetate Ethyl Methacrylate Ethylbenzene Ethylene Oxide Hexachlorobutadiene Hexachloroethane lodomethane lsobutyl Alcohol lsopropyl alcohol lsopropylbenzene Methacrylonitrile Methyl methacrylate Methyl tert butyl ether Methylene chloride M-P xylene Naphthalene n-butyl alcohol n-Butylbenzene n-Propylamine N-Propylbenzene a-xylene Pentachloroethane p-lsopropyltoluene Propionitrile sec-Butylbenzene Styrene Tert-Butyl alcohol Tert-Butylbenzene Tetrachloroethene Toluene Trans-1,2-Dichloroethene Trans-1,3-Dichloropropene trans-1,4-Dichloro-2-butene Trichloroethane Thursday, May 28, 2015 SW846 8260C SW846 8260C SW846 8260C SW846 8260C SW846 8260C SW846 8260C SW846 8260C SW846 8260C SW846 8260C SW846 8260C SW8468260C SW8468260C SW846 8260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW8468260C SW846 8260C SW8468260C SW8468260C SW846 8260C 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 101 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Page 15 o/26 Program Parameter Resource Conservation and Recovery Act Trichlorofluoromethane .. Vinyl Acetate Vinyl chloride (chloroethene) Xylenes (Total) 1,2,4,5-Tetrachlorobenzene 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,2-Dinitrobenzene 1,2-Diphenylhydrazine 1,3,5-Trinitrobenzene 1,3-Dichlorobenzene 1,3-Dinitrobenzene 1,4-Dichlorobenzene 1,4-Dinitrobenzene 1,4-Naphthoquinone 1,4-Phenytenediamine 1-Chloronaphthalene 1-Naphthylamine 2, 2'-oxybis( 1-Chlo ropropa ne) 2,3,4,6-Tetrachlorophenol 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dichlorophenol 2,6-Dinitrotoluene 2-Acetylaminofluorene 2-Chloronaphthalene 2-Chlorophenol 2-Methyl-4,6-dinitrophenol 2-Methylnaphthalene 2-Methylphenol (o-Cresol) 2-Naphthylamine 2-Nitroaniline 2-Nilrophenol 2-Picoline 3,3'-Dichlorobenzidine 3,3'-Dimethoxybenzidine 3,3'-Dimethylbenzidine 3+4 Methylphenol 3-Methylcholanthrene 3-Nitroaniline 4,4'-Methylenebis (2-chloroaniline) 4-Aminobiphenyl 4-Bromophenyl Phenyl Ether 4-Chloro-3-methylphenol 4-Chloroaniline Thursday, May 28, 2015 Method SW8468260C SW8468260C SW8468260C SW8468260C SW8468270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW8468270C SW8468270C SW8468270C SW8468270C SW8468270C SW8468270C SW8468270C SW8468270C SW8468270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW8468270C SW8468270C SW8468270C SW8468270C SW8468270C SW8468270C SW8468270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW8468270C SW8468270C SW8468270C Source # Status 101 101 101 101 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Pagel6of26 Program Parameter Resource Conservation and Recovery Act 4-Chlorophenyl Phenyl Ether 4-Nitroaniline 4-Nitrophenol 4-Nitroqulnoline-1-oxide 5-Nitro-o-toluidine 7, 12-Dimethylbenz(a)anthracene Acenaphthene Acenaphthylene Acetophenone alpha,alpha-Dimethylphenethylamine Aniline Anthracene Ara mite Benzenethiol Benzidine Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g, h, i)peryle ne Benzo(k)fluoranthene Benzoic Acid Benzyl Alcohol bis(2-chloroethoxy)methane bis(2-Chloroethyl)ether bis(2-Elhylhexyl)phthalate Butyl benzyl phthalate Chlorobenzilate Chrysene Diallate Dibenzo(a,h)anthracene Dibenzo(a,j)acrid ine Dibenzofuran Diethyl phthalate Dimethoate Dimethyl phthalate Dimethylaminoazobenzene Di-n-butyl phthalate Di-n-octyl phthalate Dinoseb Diphenylamine Disulfoton Ethyl methane sulfonate Famphur Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Thursday, May 28, 2015 Method SW8468270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW8468270C SW8468270C SW8468270C SW8468270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW8468270C SW8468270C SW8468270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW8468270C SW8468270C SW8468270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW8468270C SW8468270C SW8468270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW8468270C SW8468270C SW8468270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW8468270C SW8468270C SW8468270C SW846 8270C SW846 8270C SW846 8270C Source # Status 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Page 17o/26 Program Parameter Resource Conservation and Recovery Act Hexachloropropene lndeno(1,2,3-cd)pyrene lsodrin lsophorone lsosafrole Kepone Methapyrilene Methyl methanesulfonate Methyl parathion Naphthalene Nitrobenzene n-Nitrosodiethylamine N-Nllrosodimethylamine N-Nitroso-di-n-butylamine N-nitroso-di-n-propylamine N-Nitrosodiphenylamine N-Nitrosomethylethylamine n-Nitrosomorpholine N-Nitrosopiperidine N-Nitrosopyrrolidine o,o,o-Triethyl Phosphorothioate o-Toluidine Parathion, ethyl Pentachlorobenzene Pentachloronitrobenzene Pentachlorophenol Phenacetin Phenanthrene Phenol Phorate Phthalic Anhydride Pronamide Pyrene Pyridine Safrole Sulfotepp Thionazine 1,2,4,5-Tetrachlorobenzene 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,2-Dinitrobenzene 1,2-0iphenylhydrazlne 1,3,5-Trinitrobenzene 1,3-Dichlorobenzene 1,3-Dinilrobenzene 1,4-Dichlorobenzene 1,4-Dinilrobenzene 1,4-Naphthoquinone 1,4-Phenylenediamine Tflursday, May 18, 2015 Method SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW8468270C SW8468270C SW8468270C SW8468270C SW8468270C SW8468270C SW8468270C SW8468270C SW8468270C SW8468270C SW8468270C SW8468270C SW8468270C SW8468270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 8270C SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW84682700 SW84682700 SW84682700 SW84682700 SW84682700 SW84682700 SW84682700 Source # Status 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 96 96 96 96 96 96 96 96 96 96 96 96 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Page 18 o/26 Program Parameter Resource Conservation and Recovery Act 1-Chloronaphthalene 1-Naphthylamine 2 ,2'-oxybis (1-Ch loropropane) 2,3,4,6-Tetrachlorophenol 2 ,4, 5-Trich lorop he no I 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-0imethylphenol 2,4-Dinilrophenol 2,4-Dinitrotoluene 2,6-Dichlorophenol 2,6-Dinitrotoluene 2-Acetylaminofluorene 2-Chloronaphthalene 2-Chlorophenol 2-Methyl-4,6-dinitrophenol 2-Methylnaphthalene 2-Methylphenol {o-Cresol) 2-Naphthylamine 2-Nitroaniline 2-Nitrophenol 2-Picoline 3&4-Methylphenol 3,3'-Dichlorobenzidine 3,3'-Dimethoxybenzidine 3,3'-0imethylbenzidine 3-Melhylcholanthrene 3-Nitroaniline 4,4'-Methylenebis (2-chloroaniline) 4-Aminobiphenyl 4-Bromophenyl Phenyl Ether 4-Chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl Phenyl Ether 4-Nitroaniline 4-Nitrophenol 4-Nitroquinoline-1-oxide 5-Nitro-o-toluidine 7, 12-Dimethylbenz(a)anthracene Acenaphthene Acenaphthylene Acetophenone alpha,alpha-Oimethylphenethylamine Aniline Anthracene Aramite Benzenethiol Benzidine Benzo(a)anthracene Thursday, May 28, 2015 Method SW84682700 SW84682700 SW84682700 SW84682700 SW84682700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW84682700 SW84682700 SW84682700 SW84682700 SW84682700 SW84682700 SW84682700 SW84682700 SW84682700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW84682700 SW84682700 SW84682700 SW84682700 SW84682700 SW84682700 SW84682700 SW84682700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW84682700 SW84682700 SW84682700 SW84682700 SW84682700 SW84682700 SW84682700 SW84682700 SW846 82700 SW846 82700 Source # Status 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Page 19of26 Program Parameter Metltod Source # Status Resource Conservation and Recovery Act Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,l)perylene Benzo(k)fluoranthene BenzolcAcid Benzyl Alwhol Benzyl Butyl Phthalate bis(2-chloroethoxy)methane bis(2-Chloroethyl)ether bis(2-Ethylhexyl)phthalate Chlorobenzilate Chrysene Diallate Dibenzo(a,h)anthracene Dibenzo(a,j)acrid ine Dibenzofuran Diethyl phthalate Dimethoate Dimethyl phthalate Dimethylaminoazobenzene Di-n-butyl phthalate Di-n-octyl phthalate Dinoseb Diphanylamine Disulfoton Ethyl methane sulfonate Famphur Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Hexachloropropene lndeno(1,2,3-cd)pyrene lsodrin lsophorone lsosafrole Kepone Methapyrilene Methyl methanesulfonate Methyl parathion Naphthalene Nitrobenzene n-Nitrosodiethylamine N-Nitrosodimethylamine N-Nitroso-di-n-butylamine N-nitroso-di-n-propylamine N-Nitrosodiphenylamine Thursday, May 18, 1015 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 SW846 82700 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified PagelOo/26 Program Parameter Resource Conservation and Recovery Act N-Nitrosomethylethylamine n-Nitrosomorpholine N-Nitrosopiperidlne N-Nitrosopyrrolidine o,o,o-Triethyl Phosphorothioate o-Toluidine Parathion, ethyl Pentachlorobenzene Pentachloronitrobenzene Pentachlorophenol Phenacetin Phenanthrene Phenol Ph orate Phthalic Anhydride Pronamide Pyrene Pyridine Safrole Sulfotepp Thionazine 1,2,3,4,6, 7,8,9-0ctachlorodibenzofuran (OCDF) 1,2,3,4,6, 7,8,9-0ctachlorodibenzo-p-dioxin (OCDD) 1,2,3,4,6, 7,8-Heptachlorodibenzofuran (HpCDF) 1,2,3,4,6, 7 ,8-Heptachlorodibenzo-p-dioxin (HpCDD) 1,2,3,4,7,8,9-Heptachlorodibenzofuran (HpCDF) 1,2,3,4,7,8-Hexachlorodibenzofuran (HxCDF) 1,2,3,4,7,8-Hexachlorodibenzo-p-dloxin (HxCDD) 1,2,3,6,7,8-Hexachtorodibenzofuran (HxCDF) 1,2,3,6,7,8-Hexachtorodibenzo-p-dioxin (HxCDD) 1,2,3, 7,8,9-Hexachlorodibenzofuran (HxCDF) 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin (HxCDD) 1,2,3,7,8-Pentachlorodibenzofuran (PeCDF) 1,2,3, 7,8-Pentachlorodibenzo-p-dioxin (Pe COD) 2,3,4,6, 7 ,8-Hexachlorodibenzofuran (HxCDF) 2,3,4, 7,8-Pentachlorodibenzofuran (PeCDF) 2, 3, 7,8-Tetrachlorodibenzofuran (TCDF) 2,3, 7 ,8-Tetrachtorodibenzo-p-dioxin (TCDD) Total Heptachlorodibenzofuran (HpCDF) Total Heptachlorodibenzo-p-dioxin (HpCDD) Total Hexachlorodibenzofuran (HxCDF) Total Hexachtorodibenzo-p-dioxin (HxCDD) Total Pentachlorodibenzofuran (PeCDF) Total Pentachlorodibenzo-p-dioxin (PeCDD) 2,5-Dimethylbenzaldehyde Acetatdehyde Benzaldehyde Butanal Crotonaldehyde Thu,.day, May 28, 2015 Method SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468270D SW8468290 SW846 8290 SW8468290 SW8468290 SW846 8290 SW846 8290 SW846 8290 SW846 8290 SW846 8290 SW846 8290 SW846 8290 SW846 8290 SW846 8290 SW846 8290 SW846 8290 SW846 8290 SW846 8290 SW846 8290 SW846 8290 SW846 8290 SW846 8290 SW846 8290 SW846 8290 SW846 8315A SW846 8315A SW846 8315A SW846 8315A SW846 8315A Source # Status 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 84 84 84 84 84 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Page21 o/26 Program Parameter Resource Conservation and Recovery Act Formaldehyde Hexanal lsovaleraldehyde m-Tolualdehyde o-Tolualdehyde Pentanal Propanal p-Tolualdehyde .. Aldicarb Aldicarb sulfone Carbary! Carbofuran Methiocarb Methomyl Oxamyl ..• Thu,..day, May 18, 1015 Propoxur 1,3,5-Trinitrobenzene 1,3-Dinitrobenzene 2,4,6-Trinitrotoluene 2,4-Dlnltrotoluene 2,6-Dinitrotoluene 2-Amino-4,6-Dinitrotoluene 2-Nitrotoluene 3-Nitrotoluene 4-Amino-2,6-Dinitrotoluene 4-Nitrotoluene Hexahydro-1,3,5-trinitro-1,3,5-triazine (ROX) Methyl-2,4,6-trinitrophenylnitramine (Tetryl) Nitrobenzene Octahydro-1,3,5, 7-tetranitro-1,3,5, 7-tetrazocine (HMX) 1,3,5-Trinitrobenzene 1,3-Dinitrobenzene 2,4,6-Trinitrotoluene 2,4-Dinitrotoluene 2,6-Dlnitrotoluene 2-Amino-4,6-Dinitrotoluene 2-Nitrotoluene 3-Nitrotoluene 4-Amino-2,6-Dinitrotoluene 4-Nitrotoluene Hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX) Methyl-2,4,6-trinitrophenylnitramine (Tetryl) Nitrobenzene Octahydro-1,3,5, 7-tetranitro-1,3,5, 7-tetrazocine (HMX) Cyanide (Total) pH pH Conductivity Conductivity Metltod SW8468315A SW8468315A SW8468315A SW8468315A SW8468315A SW8468315A SW8468315A SW8468315A SW8468318 SW8468318 SW8468318 SW8468318 SW8468318 SW8468318 SW8468318 SW846 8318 SW846 8330 SW846 8330 SW846 8330 SW846 8330 SW846 8330 SW846 8330 SW846 8330 SW846 8330 SW846 8330 SW846 8330 SW846 8330 SW846 8330 SW846 8330 SW846 8330 SW846 8330A SW8468330A SW8468330A SW8468330A SW8468330A SW8468330A SW8468330A SW8468330A SW8468330A SW8468330A SW8468330A SW8468330A SW8468330A SW8468330A SW846 9012 SW846 9040 SW846 9045 SW846 9050 SW846 9050A Source # Status 84 84 84 84 84 84 84 84 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 96 96 96 96 96 96 96 96 96 96 96 96 96 96 69 69 69 69 84 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Page11of16 Program Parameter Resource Conservation and Recovery Act Bromide Chloride Fluoride • Nitrate as N Nitrite as N Sulfate Total Organic Carbon (TOC) Phenolics (Total) Diesel Range Organics Method Source # Status SW8469056 SW8469056 SW8469056 SW8469056 SW8469056 SW846 9056 SW846 9060 SW846 9066 Wl(95) ORO 82 82 82 82 82 82 69 69 119 Certified Certified Certified Certified Certified Certified Certified Certified Certified 203 2130 B 2320 B 2340 2510 B 2540C 4500-F- C 4500-P E 4500-Si02 C 5310C 5540C EPA 1613 EPA 180.1 EPA 200.7 EPA200.7 EPA 200.7 EPA200.7 EPA 200.7 EPA200.7 EPA200.7 EPA200.7 EPA200.7 EPA200.7 EPA200.7 EPA200.7 EPA 200.7 EPA200.7 EPA200.8 EPA 200.8 EPA 200.8 EPA 200.8 EPA200.8 EPA 200.8 EPA200.8 EPA200.8 EPA200.8 EPA200.8 EPA200.8 1 1 1 1 1 1 1 1 107 1 1 29 9 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Safe Drinking Water Act Manual distillation for Fluoride Turbidity Alkalinity Hardness (Total) Conductivity Filterable Residue (Total Dissolved Solids) Fluoride Orthophosphate as P Silica Total Organic Carbon (TOC) Surfactants (MBAS) Dioxin (2,3,7,8-tetrachloro-p-dioxin) Turbidity Aluminum Barium Beryllium Cadmium Calcium Chromium Copper Iron Magnesium Manganese Nickel Silver Sodium Zinc Antimony Arsenic Barium Beryllium Cadmium Chromium Copper Lead Manganese Nickel Selenium Thursday, May 28, 2015 c Page23o/26 Program Safe Drinking Water Act Parameter Method Thallium EPA200.8 EPA200.8 EPA 245.1 EPA300.0 EPA300.0 EPA300.0 EPA 300.0 EPA300.0 EPA 300.0 EPA335.4 EPA353.2 EPA353.2 EPA353.2 EPA504.1 EPA 504.1 EPA 507 EPA507 EPA 507 EPA508 EPA 508 EPA 508 EPA508 EPA508 EPA508 EPA508 EPA508 EPA508 EPA 508 EPA 515.1 EPA 515.1 EPA 515.1 EPA 515.1 EPA 515.1 EPA 515.1 EPA524.2 EPA524.2 EPA524.2 EPA 524.2 EPA524.2 EPA524.2 EPA524.2 EPA524.2 EPA 524.2 EPA 524.2 EPA 524.2 EPA524.2 EPA 524.2 EPA524.2 EPA524.2 Zinc Mercury Bromide Chloride Fluoride Nitrate as N Nitrite as N Sulfate Cyanide Nitrate + Nitrite as N Nitrate as N Nitrite as N 1,2-Dibromo-3-Chloropropane (DBCP} 1,2-Dibromoethane Alachlor Atrazine Simazine Chlordane (Technical) Endrin Heptachlor Heptachlor Epoxide Hexachlorobenzene Hexachlorocyclopentadiene Lindane Melhoxychlor PCBs as Aroclors (screen) Toxaphene 2,4,5-TP (Silvex} 2,4-D Dalapon Dinoseb Pentachlorophenol Picloram 1, 1, 1-Trichloroethane 1, 1,2-Trichloroethane 1, 1-Dichloroethene 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,4-Dichlorobenzene Benzene Bromodichloromethane Bromoform Carbon Tetrachloride Chlorobenzene Cis-1,2-Dichloroethene Dibromochloromethane Thursday, May 18, 1015 Source # Status 2 2 2 9 9 9 9 9 9 9 9 9 9 28 28 28 28 28 28 28 28 28 28 28 28 28 28 28 25 25 25 25 25 25 28 28 28 28 28 28 28 28 28 28 28 28 28 28 28 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Page14of16 Program Safe Drinking Water Act Th11rsday, May 18, 1015 Parameter Method Ethylbenzene Methylene chloride Styrene Tetrachloroethene Toluene Total Trihalomethanes Trans-1,2-Dichloroethene Vinyl chloride (chloroathana) Xylenes [Total) Alachlor Atrazine Benzo(a)pyrene bis(2-athylhaxyl)adipata bls(2-Ethylhexyl)phthalate Endrin gamma-BHC (Lindane) Heptachlor Heptachlor Epoxide Hexachlorobenzene Hexachlorocyclopentadiene Melhoxychlor Slmazlne Carbofuran Oxamyl (Vydate) EPA524.2 EPA524.2 EPA524.2 EPA524.2 EPA 524.2 EPA524.2 EPA 524.2 EPA524.2 EPA 524.2 EPA525.2 EPA525.2 EPA525.2 EPA525.2 EPA525.2 EPA525.2 EPA525.2 EPA525.2 EPA525.2 EPA525.2 EPA525.2 EPA 525.2 EPA 525.2 EPA531.1 EPA531.1 Source # Status 28 28 28 28 28 28 28 28 28 28 28 28 28 28 28 28 28 28 28 28 28 28 28 28 Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Page25of16 Program Parameter Method Source # Status Symbol Reference Limited to RCRA Water Samples Only Limited to RCRA Solid Samples Only Source Reference 1 No Source Listed 2 "Methods for the Determination of Metals in Environmental Samples - Supplement I", EPN600/R-94/111, May 1994 6 9 25 Standard Methods for the Examination of Water and Wastewater, 20th edition (1998), American Public Health Association "Methods for the Determination of Inorganic Substances in Environmental Samples", EPA/600/R-93-100, August 1993 Methods for the Determination of Organic Compounds in Drinking Water, EPN600/4-88-039, December 1966, Revised July 1991 28 Methods for the Determination of Organic Compounds in Drinking Water- Supplement Ill, EPN600/R-95-131, August 1995 29 "Tetra-through Octa-Chlorinated Dioxins and Furans by Isotope-Dilution HRGC/HRMS", EPN621-8-94-005, October 1994 65 40 CFR Part 136, Appendix A 69 Test Methods for Evaluating Solid Waste Physical Chemical Methods (SW646) Third Edition, EPA-SW-646-03-038, EPA Office of Solid Waste and Emergency Response 70 "Methods for Chemical Analysis of Water and Wastes" Environmental Protection Agency, EPA-600/4-79-020, revised March 1983 and 1979 where applicable 72 USEPA Office of Water, EPA-821-R-98-002, P899-121949, February 1999 Method 16138, National Technical Information Services, stock number PB95-104774 74 80 USEPA Method 1631, Revision E, "Mercury in Water by Oxidation., Purge and Trap, and Cold Vapor Atomic Fluorescence Spectrometry," September 2002, Office of Water, U.S. Environmental Protection Agency (EPA-621-R-02-024). 61 Test Methods for Evalualing Solid Waste Physical Chemical Melhods (SW846) Third Edition, as amended by Update I, July 1992, EPA 62 Test Methods for Evaluating Solid Waste Physical Chemical Methods (SW646) Third Edition, as amended by Update II, September 1994, 64 Test Methods for Evaluating Solid Waste Physical Chemical Methods (SW646) Third Edition, as amended by Update Ill, December 1996, Office of Solid Waste and Emergency Response EPA Office of Solid Waste and Emergency Response EPA Office of Solid Waste and Emergency Response 91 92 Standard Methods for the Examination of Water and Wastewater, 21st Edition (2005), American Public Health Association Methods for the Determination of Nonconventional Pesticides in Municipal and Industrial Wastewater- Volume I - EPA-821-R-93-010-A August 1993, Revision 1 96 Test Methods for Evaluating Solid Waste Physical Chemical Methods (SW646) Third Edition, as amended by Final Update IV, February 101 www.epa.gov/sw-646 (SW-646 On-Line: New Methods) 107 109 111 113 119 120 Standard Methods for the Examination of Water and Wastewater, 22nd Edition, American Public Health Association Annual Book of ASTM Standards, Vol 11.02, ASTM International, any year containing the cited version of the method. www.epa.gov/waterscience/methods/ Method OIA-1677-09, Available Cyanide by Ligand Exchange and Flow Injection Analysis (FIA). 2010. 01 Analytical Wisconsin DNR Modified DRO Method, Wisconsin DNR September 1995 40 CFR Part 136.3 Table 1F - List of Approved Methods for Pharmaceutical Pollutants 2007, EPA Office of Solid Waste and Emergency Response Thursday, May 28, 2015 Page26o/26